CN107569399A - A kind of mascara with the effect of dense eyelashes and preparation method thereof - Google Patents

A kind of mascara with the effect of dense eyelashes and preparation method thereof Download PDF

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Publication number
CN107569399A
CN107569399A CN201710980244.4A CN201710980244A CN107569399A CN 107569399 A CN107569399 A CN 107569399A CN 201710980244 A CN201710980244 A CN 201710980244A CN 107569399 A CN107569399 A CN 107569399A
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eyelashes
mascara
carbon black
effect
phases
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不公告发明人
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Foshan Charming Biotechnology Co Ltd
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Foshan Charming Biotechnology Co Ltd
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Priority to CN201710980244.4A priority Critical patent/CN107569399A/en
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Abstract

The present invention discloses a kind of mascara with the effect of dense eyelashes, including following components:Babassu vegetable wax, beeswax, stearic acid, stearine, the stearic acid esters of PEG 100, three isostearic acid polyglycerol esters, the smooth isostearate of sorb, water, butanediol, triethanolamine, xanthans, carbon black, glycine betaine, styrene, polyethylene, the aqueous solution of myristoyl pentapeptide 17 1 ‰ etc..The present invention compounds the aqueous solution of myristoyl pentapeptide 17 1 ‰ and epipremnum aureum extract, Semen Canavaliae extract, can Synergistic, activate Eyelash follicle keratoprotein gene, so as to promote eyelashes to grow, increase eyelashes root thickness, dense, plentiful eyelashes.

Description

A kind of mascara with the effect of dense eyelashes and preparation method thereof
Technical field
The present invention relates to cosmetic field, and in particular to a kind of mascara with the effect of dense eyelashes and preparation method thereof.
Background technology
By mascara coated on eyelashes so that eyelashes towering-up is to protrude eye.The method of prominent eye is included eyelash Hair uses basic eyelashes one by one(Eyelash-by-eyelash basis) on method and mascara is fully transferred to To increase the method for the dense degree of eyelashes around eyelashes.Eyelashes are also made to be started to curl up from root visually to make long eyelashes, And make eyelashes veritably elongated using long fiber, so that eyes look very big method.Therefore, mascara, which has, increases Add the dense degree of eyelashes, make crimping eyelash and make three major functions of long eyelashes, in addition, also have intensification eyelashes, so as to Make the method for eyes look deep.These methods are provided to protrude eye.
Chinese patent CN104666190A discloses a kind of water-resistance mascara for having and increasing effect and preparation method thereof, Raw material components and its percentage by weight % are formulated as follows:Silk Powder 3-5;Stearic acid 3-9;Palm wax 3-9;Triethanolamine 0.5-3; Glycerine 5-1.0;Petroleum ether 45-55;Beeswax 20-30;Wool grease 2-6;Natural black pigment 4-9;Vitamin E 0.2-2;Firmly Resin acid aluminium 2-4;Preservative 0.1-0.3.Surplus is deionized water.The invention has the water-resistance mascara for increasing effect, its Advantage is that eyelashes can be made after use to increase 1-1.5mm, and there is fine long paper to stick up, dense natural effect, transient rise eye god Adopt, and there is good waterproof effect, be not afraid of dizzy dye.But the mascara causes it to brush to eyelash due to film forming agent is not used Hair aftershaping effect is slow, easily pollutes eyelashes and causes user uncomfortable, simultaneously because Silk Powder fiber is difficult to adhere to eyelashes, leads Consumer is caused to have to repeatedly brush the mascara on eyelashes so that enough fibers deposition reaches required cosmetic result.
The content of the invention
A kind of the present invention is intended to provide mascara with the effect of dense eyelashes.Eyelash follicle keratoprotein base can be activated Cause, promote eyelashes growth, increase eyelashes root thickness, dense, plentiful eyelashes.
To achieve the above object, the present invention uses following technical scheme:
A kind of mascara with the effect of dense eyelashes, include the component of following mass percent:
Babassu vegetable wax 1-5%
Beeswax 3-8%
Stearic acid 1-5%
Stearine 1-3%
PEG-100 stearic acid esters 0.1-1%
Three isostearic acid polyglycerol ester 0.1-2%
The smooth isostearate 0.1-1% of sorb
Water surplus
Butanediol 3-8%
Triethanolamine 1-2%
Xanthans 0.05-0.15%
Carbon black 3-8%
Glycine betaine 1-3%
Styrene 5-30%
Polyethylene 0.1-3%
The aqueous solution 0.1-10% of myristoyl pentapeptide -17 1 ‰.
Preferably, in addition to 0.1-5% epipremnum aureum extract and 0.1-5% Semen Canavaliae extract.Wherein, the epipremnum aureum extraction The preparation method of thing is:By epipremnum aureum drying and crushing, it is small that 3-4 times of the section shepherd's purse seed oil immersion bubble 5-8 of deep-sea two is added into epipremnum aureum powder When after be concentrated under reduced pressure;The preparation method of the Semen Canavaliae extract is:Sword bean is shelled sun cured grind into powder, Filtered after the petroleum ether that 5-7 times of quality is added in sword bean powder is stirred into extraction 1-3 hours under ultrasonication, filtrate is subtracted Pressure is concentrated to give Semen Canavaliae extract.
Epipremnum aureum (scientific name:Epipremnum aureum), belong to Araeceae kylin leaf platymiscium, large-scale evergreen liana is raw It is longer than torrid areas, for normal climbing growth on the rock and trunk of rainforest, its prehensile is strong, and aerial root is flourishing, can be planted with water planting. Epipremnum aureum is evergreen all the year round and can absorb toxic gas, but the juice of epipremnum aureum is poisonous, encounter skin can cause it is red itch, eating by mistake can also make Into throat pain, epipremnum aureum is saved shepherd's purse seed oil soak extraction by the present invention with deep-sea two, and the extract of preparation not but not causes skin It is red to itch, and the development of eyelashes top layer hair follicle can be promoted, Eyelash follicle is deeply moistened, promotes Eyelash follicle activity.
Sword bean is a kind of annual plant, and belongs to pulse family.Because its beans shell looks like chaffcutter, thus it one As be referred to as sword bean.It is typically in the rivers region and south cultivation of South Korea south and China.Its root and shell also serves as medicine. Known sword bean include vitamin A and C,
Hydrolase urase, hemagglutinin and canavanine.B1, B2 and Nicotinic Acid Content contained by it be up to 3 times of common soybeans, 5 times and 4 times.With epipremnum aureum extract compounding can nutrition Glycerin, for eyelashes grow good nutrient environment function is provided.
Preferably, in addition to 0.01-0.05% essence and 0.3-0.6% preservative, wherein, the preservative is that tea is more Phenol.Tea Polyphenols is the general name of Polyphenols of Tea, including flavanol compound, anthocyanin class, flavonoids, flavonols and phenolic acid Class etc., there is antiseptic effect.
Preferably, the styrene is scattered in advance that wherein pre-dispersed liquid is by acrylic acid esters co-polymer, water, bay Alcohol polyethers -21 forms, and styrene, acrylic acid esters co-polymer, water, the mass ratio of laureth -21 are(1-10):(1- 10):(1-10):(1-10).
Preferably, the carbon black is surface-treated that described surface treatment method is:By hydrogenperoxide steam generator and charcoal It is black with 10:1-5:1 ratio is added in container, is reacted at room temperature 1-5h, is filtered after completion of the reaction, carbon black is cleaned with deionized water, Until the pH value of washing lotion is constant;Carbon black is dried into 1-10h at 100-120 DEG C.
The present invention also provides a kind of preparation method of the mascara with the effect of dense eyelashes, comprises the following steps:
1)A, B phase are mixed respectively in advance, and is heated separately to 80-85 DEG C, and the A phases are babassu vegetable wax, beeswax, tristearin The mixing of acid, stearine, PEG-100 stearic acids ester, three isostearic acid polyglycerol esters, the smooth isostearate of sorb, institute State the mixing that B phases are water, butanediol, triethanolamine, xanthans, carbon black, glycine betaine;
2)A is added in B phases, opens 3000rpm homogeneous 3-5 minutes;Insulated and stirred 20 minutes;
3)50 DEG C are cooled to, C phases is added, stirs, the C phases are styrene, polyethylene, myristoyl pentapeptide -17 1 ‰ The aqueous solution, epipremnum aureum extract, Semen Canavaliae extract, essence, preservative.
The present invention has advantageous effect in that relative to prior art:
The aqueous solution of myristoyl pentapeptide -17 1 ‰ that the present invention adds, have the function that to promote eyelashes growth.Epipremnum aureum extract, Semen Canavaliae extract brings eyelashes and grows most basic nutritional ingredient, and deep layer nourishes eyelashes, prevents eyelashes from breaking because withered, promotes Absorption of the Eyelash follicle to nutritional ingredient, it can synergistically increase eyelashes quantity, improve eyelashes gloss, thickness and length.Especially The aqueous solution of myristoyl pentapeptide -17 1 ‰ and epipremnum aureum extract, Semen Canavaliae extract compound, can Synergistic, activate eyelashes Hair follicle keratoprotein gene, so as to promote eyelashes to grow, increase eyelashes root thickness, dense, plentiful eyelashes.The styrene of the present invention By scattered and carbon black in advance after surface treatment, have more preferably dispersed, it is easier to makeup, and dressing is natural.
Embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below Detailed description.Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Base Embodiment in the present invention, those of ordinary skill in the art are resulting on the premise of creative work is not made to be owned Other embodiment, belong to the scope that the present invention is protected.
Embodiment 1
A kind of mascara with the effect of dense eyelashes, include the component of following mass percent:
Babassu vegetable wax 2.5%, beeswax 5%, stearic acid 2.5%, stearine 1.5%, PEG-100 stearic acids ester 0.5%, The smooth isostearate 0.5% of three isostearic acid polyglycerol esters 1%, sorb, butanediol 5%, triethanolamine 1.25%, xanthans 0.1%, Carbon black 5%, glycine betaine 2%, styrene 15%, polyethylene 1.5%, the aqueous solution 5% of myristoyl pentapeptide -17 1 ‰, epipremnum aureum extract 2.5%th, Semen Canavaliae extract 2.5%, essence 0.03%, Tea Polyphenols 0.4%, water surplus.
The preparation method of above-mentioned mascara, comprises the following steps:
1)Mix A, B phase respectively in advance, and be heated separately to 83 DEG C, the A phases be babassu vegetable wax, beeswax, stearic acid, The mixing of stearine, PEG-100 stearic acids ester, three isostearic acid polyglycerol esters, the smooth isostearate of sorb, the B Xiang Weishui, butanediol, triethanolamine, xanthans, carbon black, glycine betaine mixing, wherein carbon black are by surface treatment, processing method For:By hydrogenperoxide steam generator and carbon black with 7:1 ratio is added in container, is reacted at room temperature 3h, is filtered after completion of the reaction, spend from Sub- water cleans carbon black, until the pH value of washing lotion is constant;Carbon black is dried into 5h at 110 DEG C;
2)A is added in B phases, opens 3000rpm homogeneous 4 minutes;Insulated and stirred 20 minutes;
3)50 DEG C are cooled to, C phases is added, stirs, the C phases are styrene, polyethylene, myristoyl pentapeptide -17 1 ‰ The mixing of the aqueous solution, epipremnum aureum extract, Semen Canavaliae extract, essence, Tea Polyphenols, wherein, mass ratio is used as 5:5:5:5 benzene second Alkene, acrylic acid esters co-polymer, water, laureth -21 disperse styrene in advance.
Embodiment 2
A kind of mascara with the effect of dense eyelashes, include the component of following mass percent:
Babassu vegetable wax 1%, beeswax 3%, stearic acid 1%, stearine 1%, PEG-100 stearic acids ester 1%, three different tristearin The smooth isostearate 1% of sour polyglycerol ester 2%, sorb, butanediol 3%, triethanolamine 1%, xanthans 0.05%, carbon black 3%, glycine betaine 1%th, styrene 30%, polyethylene 3%, the aqueous solution 0.1% of myristoyl pentapeptide -17 1 ‰, epipremnum aureum extract 5%, Semen Canavaliae extract 0.1%th, essence 0.01%, Tea Polyphenols 0.3%, water surplus.
The preparation method of above-mentioned mascara, comprises the following steps:
1)Mix A, B phase respectively in advance, and be heated separately to 80 DEG C, the A phases be babassu vegetable wax, beeswax, stearic acid, The mixing of stearine, PEG-100 stearic acids ester, three isostearic acid polyglycerol esters, the smooth isostearate of sorb, the B Xiang Weishui, butanediol, triethanolamine, xanthans, carbon black, glycine betaine mixing, wherein carbon black are by surface treatment, processing method For:By hydrogenperoxide steam generator and carbon black with 10:1 ratio is added in container, is reacted at room temperature 1h, is filtered, spend after completion of the reaction Ionized water cleans carbon black, until the pH value of washing lotion is constant;Carbon black is dried into 1h at 120 DEG C;
2)A is added in B phases, opens 3000rpm homogeneous 3 minutes;Insulated and stirred 20 minutes;
3)50 DEG C are cooled to, C phases is added, stirs, the C phases are styrene, polyethylene, myristoyl pentapeptide -17 1 ‰ The mixing of the aqueous solution, epipremnum aureum extract, Semen Canavaliae extract, essence, Tea Polyphenols, wherein, mass ratio is used as 1:10:1:10 benzene Ethene, acrylic acid esters co-polymer, water, laureth -21 disperse styrene in advance.
Embodiment 3
A kind of mascara with the effect of dense eyelashes, include the component of following mass percent:
Babassu vegetable wax 5%, beeswax 8%, stearic acid 5%, stearine 3%, PEG-100 stearic acids ester 0.1%, three are different hard The smooth isostearate 0.1% of resin acid polyglycerol ester 0.1%, sorb, butanediol 8%, triethanolamine 2%, xanthans 0.15%, carbon black 8%, Glycine betaine 3%, styrene 5%, polyethylene 0.1%, the aqueous solution 10% of myristoyl pentapeptide -17 1 ‰, epipremnum aureum extract 0.1%, sword bean Extract 5%, essence 0.05%, Tea Polyphenols 0.6%, water surplus.
The preparation method of above-mentioned mascara, comprises the following steps:
1)Mix A, B phase respectively in advance, and be heated separately to 85 DEG C, the A phases be babassu vegetable wax, beeswax, stearic acid, The mixing of stearine, PEG-100 stearic acids ester, three isostearic acid polyglycerol esters, the smooth isostearate of sorb, the B Xiang Weishui, butanediol, triethanolamine, xanthans, carbon black, glycine betaine mixing, wherein carbon black are by surface treatment, processing method For:By hydrogenperoxide steam generator and carbon black with 5:1 ratio is added in container, is reacted at room temperature 5h, is filtered after completion of the reaction, spend from Sub- water cleans carbon black, until the pH value of washing lotion is constant;Carbon black is dried into 10h at 100 DEG C;
2)A is added in B phases, opens 3000rpm homogeneous 5 minutes;Insulated and stirred 20 minutes;
3)50 DEG C are cooled to, C phases is added, stirs, the C phases are styrene, polyethylene, myristoyl pentapeptide -17 1 ‰ The mixing of the aqueous solution, epipremnum aureum extract, Semen Canavaliae extract, essence, Tea Polyphenols, wherein, mass ratio is used as 10:1:10:1 benzene Ethene, acrylic acid esters co-polymer, water, laureth -21 disperse styrene in advance.
Embodiment 4
A kind of mascara with the effect of dense eyelashes, include the component of following mass percent:
Babassu vegetable wax 2%, beeswax 7%, stearic acid 2%, stearine 1.5%, PEG-100 stearic acids ester 0.7%, three are different The smooth isostearate 0.9% of polyglycerol stearate 0.4%, sorb, butanediol 4%, triethanolamine 1.4%, xanthans 0.08%, charcoal Black 7%, glycine betaine 2.5%, styrene 25%, polyethylene 1.5%, the aqueous solution 8% of myristoyl pentapeptide -17 1 ‰, epipremnum aureum extract 2.5%th, Semen Canavaliae extract 1.5%, essence 0.04%, Tea Polyphenols 0.5%, water surplus.
The preparation method of above-mentioned mascara, comprises the following steps:
1)Mix A, B phase respectively in advance, and be heated separately to 84 DEG C, the A phases be babassu vegetable wax, beeswax, stearic acid, The mixing of stearine, PEG-100 stearic acids ester, three isostearic acid polyglycerol esters, the smooth isostearate of sorb, the B Xiang Weishui, butanediol, triethanolamine, xanthans, carbon black, glycine betaine mixing, wherein carbon black are by surface treatment, processing method For:By hydrogenperoxide steam generator and carbon black with 6:1 ratio is added in container, is reacted at room temperature 4h, is filtered after completion of the reaction, spend from Sub- water cleans carbon black, until the pH value of washing lotion is constant;Carbon black is dried into 8h at 110 DEG C;
2)A is added in B phases, opens 3000rpm homogeneous 3 minutes;Insulated and stirred 20 minutes;
3)50 DEG C are cooled to, C phases is added, stirs, the C phases are styrene, polyethylene, myristoyl pentapeptide -17 1 ‰ The mixing of the aqueous solution, epipremnum aureum extract, Semen Canavaliae extract, essence, Tea Polyphenols, wherein, mass ratio is used as 2:5:3:7 benzene second Alkene, acrylic acid esters co-polymer, water, laureth -21 disperse styrene in advance.
Comparative example 1
The difference of comparative example 1 and embodiment 1 is comparative example 1 not comprising the aqueous solution of myristoyl pentapeptide -17 1 ‰.
Comparative example 2
The difference of comparative example 2 and embodiment 1 in comparative example 2 carbon black without surface treatment.
Comparative example 3
The difference of comparative example 3 and embodiment 1 is comparative example 3 not comprising epipremnum aureum extract.
Comparative example 4
The difference of comparative example 4 and embodiment 1 is comparative example 4 not comprising Semen Canavaliae extract.
To embodiment 1-4 and comparative example 1-4 product, it is divided into 8 groups of experiments, every group is chosen volunteer 20, age respectively Between -30 years old 20 years old, the problem of ciliation is rare, smear corresponding product twice in eyelashes root daily, continue 56 days, respectively To using front and rear 28 days, the length of 56 days eyelashes, thickness, quantity, etc. evaluate.
28 days before and after embodiment 1-4 and comparative example 1-4 uses, 56 days using effects are respectively as shown in table 1, table 2.
The embodiment of table 1 and comparative example use the eyelashes growth result after 28 days
Detection project Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4
Eyelash length Increase by 15.4% Increase by 12.2% Increase by 10.5% Increase by 11.3% Increase by 5.0% Increase by 9.3% Increase by 6.5% Increase by 6.0%
Eyelashes thickness Increase by 8.3% Increase by 7.4% Increase by 6.7% Increase by 6.5% Increase by 2.3% Increase by 4.0% Increase by 3.8% Increase by 3.5%
Eyelashes quantity Increase by 15.6% Increase by 12.4% Increase by 11.7% Increase by 12.6% Increase by 5.4% Increase by 7.6% Increase by 6.2% Increase by 6.4%
The embodiment of table 2 and comparative example use the eyelashes growth result after 56 days
Detection project Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4
Eyelash length Increase by 25.4% Increase by 22.2% Increase by 20.5% Increase by 21.3% Increase by 15.0% Increase by 18.3% Increase by 16.5% Increase by 16.0%
Eyelashes thickness Increase by 9.3% Increase by 8.4% Increase by 7.8% Increase by 7.5% Increase by 3.5% Increase by 5.0% Increase by 4.7% Increase by 4.8%
Eyelashes quantity Increase by 35.6% Increase by 32.4% Increase by 31.7% Increase by 32.6% Increase by 7.4% Increase by 9.6% Increase by 8.2% Increase by 8.4%
According to upper table data, it is apparent that mascara provided by the invention has activation Eyelash follicle keratoprotein gene, Promote absorption of the Eyelash follicle to nutritional ingredient, have in increase eyelashes quantity, improvement eyelashes gloss, thickness and length etc. Significant effect.
The foregoing is only a preferred embodiment of the present invention, not makees any formal limitation to the present invention;It is all The those of ordinary skill of the industry can be described in by specification and described above and swimmingly implement the present invention;It is but all familiar Professional and technical personnel without departing from the scope of the present invention, makes using disclosed above technology contents A little variation, modification and evolution equivalent variations, be the present invention equivalent embodiment;Meanwhile all realities according to the present invention Variation, modification and evolution of any equivalent variations that matter technology is made to above example etc., still fall within the technology of the present invention Within the protection domain of scheme.

Claims (6)

1. a kind of mascara with the effect of dense eyelashes, it is characterised in that include the component of following mass percent:
Babassu vegetable wax 1-5%
Beeswax 3-8%
Stearic acid 1-5%
Stearine 1-3%
PEG-100 stearic acid esters 0.1-1%
Three isostearic acid polyglycerol ester 0.1-2%
The smooth isostearate 0.1-1% of sorb
Butanediol 3-8%
Triethanolamine 1-2%
Xanthans 0.05-0.15%
Carbon black 3-8%
Glycine betaine 1-3%
Styrene 5-30%
Polyethylene 0.1-3%
The aqueous solution 0.1-10% of myristoyl pentapeptide -17 1 ‰
Water surplus.
2. a kind of mascara with the effect of dense eyelashes according to claim 1, it is characterised in that also including 0.1-5% Epipremnum aureum extract and 0.1-5% Semen Canavaliae extract.
3. a kind of mascara with the effect of dense eyelashes according to claim 1, it is characterised in that also including 0.01- 0.05% essence and 0.3-0.6% preservative, wherein, the preservative is Tea Polyphenols.
4. a kind of mascara with the effect of dense eyelashes according to claim 1, it is characterised in that the styrene is Scattered in advance, wherein pre-dispersed liquid is made up of acrylic acid esters co-polymer, water, laureth -21, styrene, acrylic acid Lipin polymer, water, the mass ratio of laureth -21 are(1-10):(1-10):(1-10):(1-10).
5. a kind of mascara with the effect of dense eyelashes according to claim 1, it is characterised in that the carbon black is table What face treated, described surface treatment method is:By hydrogenperoxide steam generator and carbon black with 10:1-5:1 ratio adds container In, 1-5h is reacted at room temperature, filters after completion of the reaction, carbon black is cleaned with deionized water, until the pH value of washing lotion is constant;Carbon black is existed 1-10h is dried at 100-120 DEG C.
6. a kind of method for preparing a kind of mascara with the effect of dense eyelashes as described in claim any one of 1-5, its It is characterised by, comprises the following steps:
1)A, B phase are mixed respectively in advance, and is heated separately to 80-85 DEG C, and the A phases are babassu vegetable wax, beeswax, tristearin The mixing of acid, stearine, PEG-100 stearic acids ester, three isostearic acid polyglycerol esters, the smooth isostearate of sorb, institute State the mixing that B phases are water, butanediol, triethanolamine, xanthans, carbon black, glycine betaine;
2)A is added in B phases, opens 3000rpm homogeneous 3-5 minutes;Insulated and stirred 20 minutes;
3)50 DEG C are cooled to, C phases is added, stirs, the C phases are styrene, polyethylene, myristoyl pentapeptide -17 1 ‰ The aqueous solution, epipremnum aureum extract, Semen Canavaliae extract, essence, preservative.
CN201710980244.4A 2017-10-19 2017-10-19 A kind of mascara with the effect of dense eyelashes and preparation method thereof Withdrawn CN107569399A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109512744A (en) * 2018-12-29 2019-03-26 广州博科健康科技集团有限公司 A kind of eyelashes growth-promoting media and preparation method thereof
CN109833260A (en) * 2019-03-06 2019-06-04 广州碧婷化妆品有限公司 A kind of eyelashes nourishing liquid preparing process

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109512744A (en) * 2018-12-29 2019-03-26 广州博科健康科技集团有限公司 A kind of eyelashes growth-promoting media and preparation method thereof
CN109512744B (en) * 2018-12-29 2021-08-24 广州博科健康科技集团有限公司 Eyelash growth liquid and preparation method thereof
CN109833260A (en) * 2019-03-06 2019-06-04 广州碧婷化妆品有限公司 A kind of eyelashes nourishing liquid preparing process

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