CN107557155A - Fragrant line Eight Immortals fruity essence and its application in a kind of ramuscule filter stick - Google Patents

Fragrant line Eight Immortals fruity essence and its application in a kind of ramuscule filter stick Download PDF

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Publication number
CN107557155A
CN107557155A CN201710846578.2A CN201710846578A CN107557155A CN 107557155 A CN107557155 A CN 107557155A CN 201710846578 A CN201710846578 A CN 201710846578A CN 107557155 A CN107557155 A CN 107557155A
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China
Prior art keywords
immortals
ramuscule
fragrant line
fruity essence
built
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Pending
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CN201710846578.2A
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Chinese (zh)
Inventor
高明奇
顾亮
李明哲
纪朋
冯晓民
鲁平
王宁
田海英
张展
杨金初
刘文博
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China Tobacco Henan Industrial Co Ltd
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China Tobacco Henan Industrial Co Ltd
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Priority to CN201710846578.2A priority Critical patent/CN107557155A/en
Publication of CN107557155A publication Critical patent/CN107557155A/en
Pending legal-status Critical Current

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Abstract

The invention belongs to ramuscule cigarette filter rod production technical field, and in particular to fragrant line Eight Immortals fruity essence and its patent application of application in a kind of ramuscule filter stick.It is calculated in mass percent, it is composed of the following components:5.0 ~ 10.0% orange oil, 1.0 ~ 2.0% menthol, 0.5 ~ 1.0% citral, 0.5 ~ 1.0% Poria cocos extract, 0.2 ~ 0.5% borneol, 0.05 ~ 0.1% linalool, 0.5 ~ 1.0% succinic acid, 84.4 ~ 92.25% Glycerin, mixed triester with caprylic acid capric acid;The Poria cocos extract is the extractive with organic solvent of Poria cocos.The application coordinates the improvement of ramuscule cigarette filter rod structure while fragrant line is with Eight Immortals fruity essence in providing a kind of ramuscule cigarette with peat-reek, can preferably improve the effect of sucking of ramuscule cigarette, and improvement effect is obvious, has preferable practical value.

Description

Fragrant line Eight Immortals fruity essence and its application in a kind of ramuscule filter stick
Technical field
The invention belongs to ramuscule cigarette filter rod production technical field, and in particular to fragrant line is with Eight Immortals fruit in a kind of ramuscule filter stick Essence and its patent application of application.
Background technology
With the continuous improvement of people's living standards, the cigarette kind on cigarette market is also increasingly abundanter, also it is consumption Person provides more choices, and ramuscule cigarette is exactly typical case therein.From the point of view of effective sale effect, ramuscule cigarette is unique with it Glamour conquered increasing consumer.
From the point of view of cigarette quality, the tar content of ramuscule cigarette is more general than regular-size cigarette low, and suction taste is also thin, thus comparison operators The demand of particular consumer is closed, the urban woman for being particularly subject to follow the fashion, graceful, fashion is lived consumes the especially blue or green of family Look at.And as the fast development of low-coke tar cigarette, advantage of the ramuscule cigarette in terms of " tar reduction is protected fragrant " just seem especially noticeable.
Due to occupying the relatively small number of innate advantage of cigarette small volume, releasing content of coke tar, ramuscule cigarette also goes out simultaneously The problems such as smoke is light, fragrance is insufficient is showed, thus it is promoted the crowd of being applicable and certain limitation be present.Therefore, existing cigarette Manufacturing enterprise is also cracking this technical barrier by reducing many technological means such as filter stick pressure drop, optimization tobacco structure.
In terms of the ramuscule cigarette flavouring, in prior art thinking, mainly using the forms such as perfume particles, essence capsule come Supplement or increase cigarette fragrance, but this release of several ramuscule cigarette flavouring mode generally existing fragrance is uneven, the resting period is short, The defects of with flue gas inaccurate coordination, so that improving fragrance effect is not obvious enough.Thus pole is necessary in existing flavouring mode On the basis of, comprehensive means are further improved etc. by composition, flavouring mode, further to improve the uniformity of flavouring, steady Qualitative and harmony.
The content of the invention
Present invention aims at providing, a kind of Eight Immortals fruity for being directed to fragrant line in ramuscule filter stick is smart, while coordinates ramuscule to filter The improvement of rod configuration aspects, while abundant ramuscule cigarette type, further improve the flavouring effect of ramuscule cigarette.
Details are as follows for the technical scheme that the application is taken.
Fragrant line Eight Immortals fruity essence, is calculated in mass percent in a kind of ramuscule filter stick, composed of the following components:
5.0 ~ 10.0% orange oil, 1.0 ~ 2.0% menthol,
0.5 ~ 1.0% citral, 0.5 ~ 1.0% Poria cocos extract, 0.2 ~ 0.5% borneol, 0.05 ~ 0.1% linalool,
0.5 ~ 1.0% succinic acid, 84.4 ~ 92.25% Glycerin, mixed triester with caprylic acid capric acid;
The Poria cocos extract is the extractive with organic solvent of Poria cocos, and specific is, for example, the ethanol extract of Poria cocos.
Fragrant line Eight Immortals fruity essence, specific formula are, for example, in the ramuscule filter stick:8.0% orange oil, 1.6% peppermint Brain, 0.8% citral, 0.7% Poria cocos extract, 0.25% borneol, 0.08% linalool, 0.8% succinic acid, 87.77% Glycerin, mixed triester with caprylic acid capric acid.
Application of the fragrant line with Eight Immortals fruity essence in cigarette in the ramuscule filter stick, for fragrant line in ramuscule cigarette filter rod.
A kind of ramuscule composite filter of the fragrant line of built-in Eight Immortals fruity essence, the composite filter outer wrap has forming paper, interior Portion is combined by common vinegar fibre filter rod segments and the fragrant line vinegar fibre filter rod segments of built-in Eight Immortals fruity essence, wherein built-in Eight Immortals fruity essence is fragrant Line vinegar fibre filter rod segments are close to pipe tobacco section;
Common vinegar fibre filter rod segments and the fragrant line vinegar fibre filter rod segments of built-in Eight Immortals fruity essence, the cross sectional shape of diacetate fiber used is Y types, Strand specification requires:Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den;
The length ratio of common vinegar fibre filter rod segments and the fragrant line vinegar fibre filter rod segments of built-in Eight Immortals fruity essence, can be according to resistance to suction or flavouring need Ask and be adjusted, length ratio is, for example, specifically 1:1;
The fragrant line vinegar fibre filter rod segments of the built-in Eight Immortals fruity essence, its middle part are built-in with fragrant line, and fragrant line is adsorbed with Eight Immortals fruity essence;Its Preparation process is prepared by prior art, is specially:Before fragrant line enters filter-stick forming device after being come out from line roller, by equipped with one The flavoring system for determining concentration Eight Immortals fruity essence applies essence;
The The concrete specification of the composite filter, it is, for example,:Length is 120mm, a length of 16.90mm of circumference, pressure drop be 2600Pa ~ 4200Pa。
The essence applied amount of the ramuscule perfume (or spice) line filter stick list branch filter stick is 10mg ~ 30mg.
Utilize ramuscule cigarette prepared by the ramuscule composite filter of the fragrant line of the built-in Eight Immortals fruity essence.
The present invention prepares a kind of Eight Immortals fruity flavor with peat-reek first by autonomous Design composition, As the flavouring additive in ramuscule perfume (or spice) line filter stick, the ramuscule composite filter with Eight Immortals fruit flavor has been prepared.Eight Celestial fruit has relieving cough and reducing sputum effect, especially helpful to having sore throat, including having a sore throat, coughing caused by the flu of pure, And smoking causes larynx to be done, laryngalgia symptom, Eight Immortals fruit remission effect is all good.Therefore, the application is while abundant essence type, Health-care effect with certain reduction tobacco epidemic.
Preliminary Applications show, after the ramuscule perfume (or spice) line composite filter is used for ramuscule cigarette, not only increase the equal of essence application Even property and the stability of release, also improve the harmony of fragrance and product sensory quality.By the Eight Immortals fruity essence applied Allocate and obtain for natural materials, therefore these aroma substances can be highlighted more " the roasting sweet tea " of cigarette after cigarette smoke is entered Note, lifts the fragrance richness and plumpness of ramuscule cigarette, and then improves its sucking quality and sense organ comfort level.
Compared with existing perfuming technology, main advantages of the present invention have:
(1) simple process:Preparation technology of the present invention is simple, without making notable adjustment to current production technology and equipment, without Large-scale instrument and equipment and expensive reagent, it is simple to operate, it is easily controllable;
(2) safety and sanitation:Raw and auxiliary material of the present invention is widely used in food processing field, in the absence of toxic reagent Residue problem, thus securely and reliably;
(3)Release is stable:Built-in fragrant line composite filter form of the present invention, the same of fragrant line is directly contacted avoiding oral cavity When, help to slow down the loss of fragrance.
In general, the application in a kind of ramuscule cigarette with peat-reek is provided fragrant line with smart same of Eight Immortals fruity When, coordinate the improvement of ramuscule cigarette filter rod structure, can preferably improve the effect of sucking of ramuscule cigarette, and improvement effect is obvious, With preferable practical value, while abundant cigarette product type, design, exploitation and production for new ramuscule cigarette Sale has preferable Demonstration And Extension application value.
Brief description of the drawings
Fig. 1 is the ramuscule composite filter structural representation of the fragrant line of built-in Eight Immortals fruity essence provided by the present invention;
Fig. 2 is ramuscule cigarette structure schematic diagram prepared by the ramuscule composite filter of the fragrant line of Eight Immortals fruity essence built in utilization.
Embodiment
Explanation is further explained to the application with reference to embodiment., it is necessary to illustrate before specific embodiment is introduced , orange oil, citral, Poria cocos ethanol extract employed in following embodiments(Poria cocos extract), menthol, pungent capric acid it is sweet The materials such as grease are Shanghai Huabao Biotechnology Co., Ltd.'s Products;Fragrant line, ramuscule filter stick etc. are also given birth to by prior art Production is carried out.
Embodiment 1
The present embodiment provides fragrant line Eight Immortals fruity essence in ramuscule filter stick, is calculated in mass percent, composed of the following components:
5.0% orange oil, 1.0% menthol, 0.5% citral, 0.5% Poria cocos extract, 0.2% borneol, 0.05% Linalool, 0.5% succinic acid, 92.25% Glycerin, mixed triester with caprylic acid capric acid.
By prior art, the ramuscule composite filter of the fragrant line of Eight Immortals fruity essence, as shown in Figure 1, 2, prepared multiple built in preparation Filter stick 3 is closed, outer wrap has forming paper, internal by common vinegar fibre filter rod segments 2 and the fragrant line vinegar fibre filter rod segments 1 of built-in Eight Immortals fruity essence It is combined, wherein the fragrant line vinegar fibre filter rod segments 1 of built-in Eight Immortals fruity essence are close to pipe tobacco section 4;
Common vinegar fibre filter rod segments 2, the cross sectional shape of diacetate fiber used is Y types, and strand specification requirement is:6.0Y/17000 (den/den);
The fragrant line vinegar fibre filter rod segments 2 of built-in Eight Immortals fruity essence, the cross sectional shape of diacetate fiber used is Y types, and strand specification requirement is: 8.0Y/15000(den/den);
The length ratio of common vinegar fibre filter rod segments and the fragrant line vinegar fibre filter rod segments of built-in Eight Immortals fruity essence, is 1:1;The composite filter The concrete specification be:Length is 120mm, a length of 16.90mm of circumference(In Fig. 2, during actual use, filter length 30mm(Scheme 1+2 part-structures length in 2)).
When preparing the ramuscule composite filter of the fragrant line of the built-in Eight Immortals fruity essence, carried out by existing filter stick production technology, it is first First pass through filter-stick forming device and will be applied with the fragrant line of Eight Immortals fruity essence and insert filter stick center fragrant line filter stick is made, then pass through filter again Rod compounding machine and common vinegar fibre filter stick formation are ramuscule perfume (or spice) line binary compound filter candle(The ramuscule for stating the fragrant line of built-in Eight Immortals fruity essence is answered Close filter stick).After shaping, measurement result shows, fragrant line is 20mg or so with Eight Immortals fruity essence applied amount in every composite filter(I.e. The dosage of the long filter sticks of 120mm is 20mg).
It is ramuscule by the ramuscule composite filter of the fragrant line of the built-in Eight Immortals fruity essence and tobacco sample cigarette by prior art Cigarette sample sets blank control sample as test sample(Blank perfume (or spice) line is added at filter stick same position)As control Sample, evaluation is detected and is aspirated respectively to test sample and control sample by 7 professional sensory evaluation personnel.Specific flue gas inspection knot Fruit and specific suction evaluate score value referring to form hereinafter.
Suction evaluation result shows that after it with the addition of Eight Immortals fruity essence, " Eight Immortals fruit " fragrance of cigarette sample is obvious, flue gas Fragrance it is rich have certain lifting, have back a sweet tea sense, excitant is reduced, and miscellaneous gas is reduced, and flue gas sophistication improves, and pleasant impression has changed It is kind.
Embodiment 2
The present embodiment provides fragrant line Eight Immortals fruity essence in ramuscule filter stick, is calculated in mass percent, composed of the following components:
8.0% orange oil, 1.6% menthol, 0.8% citral, 0.7% Poria cocos extract, 0.25% borneol, 0.08% Linalool, 0.8% succinic acid, 87.77% Glycerin, mixed triester with caprylic acid capric acid.
With the filter stick specification of embodiment 1, the ramuscule composite filter of the fragrant line of Eight Immortals fruity essence built in preparation.After shaping, measure As a result show, fragrant line is 20mg or so with Eight Immortals fruity essence applied amount in every composite filter.
The ramuscule composite filter of the fragrant line of the built-in Eight Immortals fruity essence is made with tobacco sample cigarette for ramuscule cigarette sample For test sample, suction evaluation is carried out.
Suction evaluation result shows, after it with the addition of Eight Immortals fruity essence, " Eight Immortals fruity " obvious, cigarette of cigarette sample Gas fragrance is rich to be dramatically increased, and is had and is significantly returned sweet tea sense, and excitant significantly reduces, and miscellaneous gas is reduced, and flue gas sophistication significantly carries Height, pleasant impression are obviously improved.
Embodiment 3
The present embodiment provides fragrant line Eight Immortals fruity essence in ramuscule filter stick, is calculated in mass percent, composed of the following components:
10.0% orange oil, 2.0% menthol, 1.0% citral, 1.0% Poria cocos extract, 0.5% borneol, 0.1% Linalool, 1.0% succinic acid, 84.4% Glycerin, mixed triester with caprylic acid capric acid.
With the filter stick specification of embodiment 1, the ramuscule composite filter of the fragrant line of Eight Immortals fruity essence built in preparation.After shaping, measure As a result show, fragrant line is 20mg or so with Eight Immortals fruity essence applied amount in every composite filter.
The ramuscule composite filter of the fragrant line of the built-in Eight Immortals fruity essence is made with tobacco sample cigarette for ramuscule cigarette sample For test sample, suction evaluation is carried out.
Suction evaluation result shows, after it with the addition of Eight Immortals fruity essence, " Eight Immortals fruity " fairly obvious, cigarette of cigarette sample Gas fragrance harmony is reduced, and excitant increase, miscellaneous gas is reduced, and flue gas inaccurate coordination and has uncomfortable sweet sense, pleasant impression Not as normal cigarette(Compared with control sample cigarette).
Composite filter prepared by different embodiments is detected, further according to《The cigarette of GB/T 19609-2004 is used Conventional analysis determines TPM and tar with smoking machine》Method measure cigarette mainstream flue gas in TPM, tar, nicotine Detected with indexs such as moisture, concrete outcome is as shown in the table.
Table 1, the testing result of the ramuscule composite filter of the fragrant line of built-in Eight Immortals fruity essence prepared by different embodiments:
Table 2, the physical index and main flume testing result of kinds of cigarettes sample:
It is can be seen that from the above-mentioned data of table 1 compared with normal diacetate fiber filter stick, place the filter stick physical index of Eight Immortals fruity line Without significant difference.As can be seen from Table 2, compared with the normal cigarette of reference examples, the main flume of Eight Immortals fruity coil of wire cigarette without Significant change, the key index tar and nicotine for influenceing cigarette sense organ do not have significant changes.
Table 3, kinds of cigarettes sample sensory quality assessment result:
As can be seen from Table 3, it can obtain cigarette sensory quality by using the fragrant line composite filter of Eight Immortals fruity essence Significantly improve, its sensory evaluation scores highest can improve 1.62 points, and fragrance significantly improves, and pleasant impression improves, excitant and miscellaneous gas also have compared with It is big to reduce.
To sum up, by targetedly designing the fragrant line filter stick composition of specific fragrance, after being applied to cigarette, energy Odor characteristic during smoking property of cigarette is enough obviously improved, impression is sucked in abundant and raising, simultaneously because the present invention uses special construction Fragrant line filter stick, conventional fragrant line filter stick can be avoided quickly to be lost in, while safety and sanitation.Therefore the application highlights cigarette as one kind " Eight Immortals fruit " note, the new Eight Immortals fruity ramuscule perfume (or spice) line composite filter for improving sucking quality, in industry have and definitely push away Wide application value.

Claims (5)

1. fragrant line Eight Immortals fruity essence in a kind of ramuscule filter stick, it is characterised in that be calculated in mass percent, by following components group Into:
5.0 ~ 10.0% orange oil, 1.0 ~ 2.0% menthol,
0.5 ~ 1.0% citral, 0.5 ~ 1.0% Poria cocos extract, 0.2 ~ 0.5% borneol, 0.05 ~ 0.1% linalool,
0.5 ~ 1.0% succinic acid, 84.4 ~ 92.25% Glycerin, mixed triester with caprylic acid capric acid;
The Poria cocos extract is the extractive with organic solvent of Poria cocos.
2. the fragrant line Eight Immortals fruity essence in ramuscule filter stick as claimed in claim 1, it is characterised in that specific formula is:8.0% Orange oil, 1.6% menthol, 0.8% citral, 0.7% Poria cocos extract, 0.25% borneol, 0.08% fragrant camphor tree Alcohol, 0.8% succinic acid, 87.77% Glycerin, mixed triester with caprylic acid capric acid;
Or it is:
5.0% orange oil, 1.0% menthol, 0.5% citral, 0.5% Poria cocos extract, 0.2% borneol, 0.05% Linalool, 0.5% succinic acid, 92.25% Glycerin, mixed triester with caprylic acid capric acid;
Or it is:
10.0% orange oil, 2.0% menthol, 1.0% citral, 1.0% Poria cocos extract, 0.5% borneol, 0.1% Linalool, 1.0% succinic acid, 84.4% Glycerin, mixed triester with caprylic acid capric acid.
3. application of the fragrant line with Eight Immortals fruity essence in cigarette, its feature exist in the ramuscule filter stick of claim 1 or 2 In for fragrant line in ramuscule cigarette filter rod.
4. the ramuscule composite filter of the fragrant line of a kind of built-in Eight Immortals fruity essence, it is characterised in that the composite filter outer wrap has Forming paper, it is internal to be combined by common vinegar fibre filter rod segments and the fragrant line vinegar fibre filter rod segments of built-in Eight Immortals fruity essence, wherein built-in eight The fragrant line vinegar fibre filter rod segments of celestial fruity essence are close to pipe tobacco section;
Common vinegar fibre filter rod segments and the fragrant line vinegar fibre filter rod segments of built-in Eight Immortals fruity essence, the cross sectional shape of diacetate fiber used is Y types, Strand specification requires:Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den;
The length ratio of common vinegar fibre filter rod segments and the fragrant line vinegar fibre filter rod segments of built-in Eight Immortals fruity essence, specially 1:1;
The fragrant line vinegar fibre filter rod segments of the built-in Eight Immortals fruity essence, its middle part are built-in with fragrant line, and fragrant line is adsorbed with Eight Immortals fruity essence.
5. utilize ramuscule cigarette, its feature prepared by the ramuscule composite filter of the fragrant line of built-in Eight Immortals fruity essence described in claim 4 It is, the essence applied amount of single branch filter stick is 10mg ~ 30mg.
CN201710846578.2A 2017-09-19 2017-09-19 Fragrant line Eight Immortals fruity essence and its application in a kind of ramuscule filter stick Pending CN107557155A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102655771A (en) * 2009-11-23 2012-09-05 菲利普莫里斯生产公司 Novel filter segment comprising a substrate loaded with a smoke-modifying agent
CN103054186A (en) * 2012-12-27 2013-04-24 广东中烟工业有限责任公司 Chinese medicinal composite particle filter stick and preparation method thereof
CN107034017A (en) * 2017-04-27 2017-08-11 河南中烟工业有限责任公司 A kind of cigarette quick-fried pearl savory essence of dried orange peel and its application in cigarette

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102655771A (en) * 2009-11-23 2012-09-05 菲利普莫里斯生产公司 Novel filter segment comprising a substrate loaded with a smoke-modifying agent
CN103054186A (en) * 2012-12-27 2013-04-24 广东中烟工业有限责任公司 Chinese medicinal composite particle filter stick and preparation method thereof
CN107034017A (en) * 2017-04-27 2017-08-11 河南中烟工业有限责任公司 A kind of cigarette quick-fried pearl savory essence of dried orange peel and its application in cigarette

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Application publication date: 20180109