CN106690411A - Butter-flavor cellulose acetate tow and application thereof in fine cigarettes - Google Patents

Butter-flavor cellulose acetate tow and application thereof in fine cigarettes Download PDF

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Publication number
CN106690411A
CN106690411A CN201611127542.0A CN201611127542A CN106690411A CN 106690411 A CN106690411 A CN 106690411A CN 201611127542 A CN201611127542 A CN 201611127542A CN 106690411 A CN106690411 A CN 106690411A
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CN
China
Prior art keywords
diacetate fiber
cream fragrance
essence
parts
tow
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611127542.0A
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Chinese (zh)
Inventor
高明奇
顾亮
李明哲
张展
董艳娟
冯晓民
纪朋
杨金初
田海英
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Henan Industrial Co Ltd
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China Tobacco Henan Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Henan Industrial Co Ltd filed Critical China Tobacco Henan Industrial Co Ltd
Priority to CN201611127542.0A priority Critical patent/CN106690411A/en
Publication of CN106690411A publication Critical patent/CN106690411A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02Manufacture of tobacco smoke filters
    • A24D3/0204Preliminary operations before the filter rod forming process, e.g. crimping, blooming
    • A24D3/0212Applying additives to filter materials
    • A24D3/022Applying additives to filter materials with liquid additives, e.g. application of plasticisers
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/08Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
    • A24D3/10Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0003Compounds of unspecified constitution defined by the chemical reaction for their preparation
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • C11B9/0015Aliphatic compounds containing oxygen as the only heteroatom
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0042Essential oils; Perfumes compounds containing condensed hydrocarbon rings
    • C11B9/0046Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
    • C11B9/0049Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0061Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F11/00Chemical after-treatment of artificial filaments or the like during manufacture
    • D01F11/02Chemical after-treatment of artificial filaments or the like during manufacture of cellulose, cellulose derivatives, or proteins

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Materials Engineering (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The invention belongs to the technical field of production of filter sticks of fine cigarettes, and particularly relates to a butter-flavor cellulose acetate tow and application thereof in fine cigarettes. The cross section of the cellulose acetate tow is in a Y shape; according to the specification requirements of the tow, the single denier is 6.0 den-11.0 den, and the total denier is 15000 den-17000 den. In the preparation of the butter-flavor cellulose acetate tow, before a tow enters a crimping machine after being ejected out of a spinneret, the tow is oiled through an oiling agent system with butter-flavor essence added, wherein the mass ratio of the butter-flavor essence added in the oiling agent system is not smaller than 0 but not larger than 5%. The smoking effect of fine cigarettes can be specifically and significantly improved by changing the aroma enhancing way, the improving effect is obvious, and thus the tow has high application value and great application and popularization significance for the design, development, production and selling of new fine cigarettes.

Description

A kind of cream fragrance diacetate fiber and its application in ramuscule cigarette
Technical field
The invention belongs to ramuscule cigarette filter rod production technical field, and in particular to a kind of cream fragrance diacetate fiber and its The patent application of the application in ramuscule cigarette.
Background technology
In recent years, due to ramuscule cigarette low burnt low evil, fashion appeal in itself the advantages of, ramuscule cigarette shows good Growth momentum, domestic Cigarette Industrial Enterprise is constantly releasing new ramuscule Cigarettesize, diversified to meet smoking population Suck demand.
Ramuscule cigarette is not that simple in physical significance attenuates thick branch cigarette, itself main reason is that, will be common While the circumference of thick branch cigarette is reduced, fall cone and bag ash etc. of the resistance to suction of ramuscule cigarette, hardness, burning can all change, Thus the Research idea of traditional circumference cigarette has been not suitable for the development of ramuscule cigarette.
It is the innate advantage of ramuscule cigarette that volume is short and pithy, but because diameter is significantly less than regular-size cigarette, thus resistance to suction Greatly, light, full aroma degree deficiency of smoke etc. is as the common problem for hindering the development of ramuscule cigarette.Therefore, Cigarette Industrial Enterprise is accumulated Explore using online filter tip punching ventilation, change strand specification, reduce many technology hands such as filter stick pressure drop, optimization tobacco structure in pole Section cracks this technical barrier.
It is main to use the forms such as fragrant line, particle, capsule but above-mentioned several in prior art thinking around ramuscule cigarette flavouring The problems such as planting short ramuscule cigarette flavouring mode generally existing fragrance release uneven, resting period and flue gas inaccurate coordination.Thus It is necessary to be improved above-mentioned more traditional flavouring mode, so as to further improve the uniformity of flavouring, stability and association Tonality.
The content of the invention
Present invention aim at a kind of new diacetate fiber with cream fragrance is provided, the tow is specifically used for thin Branch cigarette is used as ramuscule filter stick application, so as to improve the flavouring effect of ramuscule cigarette to a certain extent.
Details are as follows for the technical scheme that the application is taken.
A kind of cream fragrance diacetate fiber, the cross sectional shape of its diacetate fiber is Y types, and strand specification requirement is:Single-strand is 6.0den ~ 11.0den, total denier is 15000den ~ 17000den;
The mentality of designing of the diacetate fiber is:Single-strand high, low total denier;Overall performance is required:Moisture content is(6.0±1.6)%, Oil content is(0. 70~1.50)%, fracture strength >=18.0N/Ktex, residual acetone content≤0.30%, titanium dioxide contains Measure and be(0.40±0.20)%;
It is added to have creamy before tow enters crimping machine from after spinning nozzle ejection when preparing the cream fragrance diacetate fiber The Spin Finish System of taste essence oils;The mass ratio that wherein cream fragrance essence is added in Spin Finish System is not less than 0, but does not surpass Cross 5%;Preferable amount is 0.5 ~ 2%, more preferably 1%;
The cream fragrance essence is flavor oil, and in terms of mass fraction, concrete composition is as follows:
Vanillic aldehyde 0.1- ~ 0.3 part, 1.5 ~ 4.0 parts of ethyl butyrate, 0.5 ~ 2.0 part of diacetyl, 0.1 ~ 0.4 part of amyl butyrate, 1.0 ~ 3.0 parts of methylcoumarin, 60 ~ 100 parts of corn oil, 5.0 ~ 15.0 parts of butyric acid;
Optimization formula is constituted:
0.15 part of vanillic aldehyde, 2.5 parts of ethyl butyrate, 0.75 part of diacetyl, 0.35 part of amyl butyrate, methylcoumarin 2.0 Part, 85 parts of corn oil, 9.5 parts of butyric acid.
The preparation method of the cream fragrance diacetate fiber, its main preparation process is:
First, secondary cellulose acetate sheets are dissolved in acetone soln, while secondary cellulose acetate sheets are dissolved, by filter aid and delustering agent (TiO2) add solution, then carry out multi-stage compression filtration treatment to solution, the colloid and solid in removal spinning solution are miscellaneous Matter;
Secondly, filtering rear slurry enters spinning equipment, after the spinneret orifice of Y type shaped apertures, forms Y type cross sectional shape monofilament lines The silk of density, the proportioning for carrying out different pore size hole count further according to design requirement carries out spinning;During spinning, the silk of Y type cross sectional shapes Beam is after the smaller spinneret orifice spinneret of via hole diameter obtained in spinning, meanwhile, the spinneret hole number on spinneret is than normal ramuscule filter stick Tow spinneret is more;
Finally, tow enters from after spinning nozzle ejection and is added with the Spin Finish System of butter essence and oils, subsequently into crimping machine, most After enter back into drying machine, heating evaporation falls the acetone and moisture of remnants, forms finally dried tow, is then passed through pendulum wire, beats The diacetate fiber finished product with cream fragrance is prepared into after bag.
Application of the cream fragrance diacetate fiber in ramuscule cigarette, for preparing ramuscule filter bar for cigarette.
Using the ramuscule filter bar for cigarette prepared by the cream fragrance diacetate fiber, its specification is:Length is 120mm, The a length of 16.90mm of circumference, pressure drop is 2800Pa ~ 4500Pa.
The present invention innovatively dissolves in the characteristic of vinegar fibre Spin Finish System using oily cream fragrance essence, as vinegar Fiber tow finish additive, has prepared the diacetate fiber with cream fragrance.Preliminary Applications show that the diacetate fiber is used for After ramuscule cigarette, the uniformity of essence applying and the stability of release are not only increased, also improve fragrance and product sensory matter The harmony of amount.By the butter essence for being applied is obtained by being extracted in natural cream, therefore these aroma substances are entering After cigarette smoke, " roasting sweet " note of cigarette can be more highlighted, lift the fragrance richness and plumpness of ramuscule cigarette, and then Improve its sucking quality and sense organ comfort level.
Compared with existing perfuming technology, main advantages of the present invention have:
(1) it is with low cost:Cream fragrance essence low production cost, its raw materials for production cream is easy to get, wide material sources, thus by its Originated as spices, extract simple, it is with low cost;
(2) technique is easy:Preparation process is simple of the present invention, without making significantly adjustment to current production technology and equipment, without Large-scale instrument and equipment and expensive reagent, it is simple to operate, it is easy to control;
(3) safety and sanitation:Raw and auxiliary material of the present invention is widely used in food processing field, in the absence of toxic reagent Residue problem, thus it is safe and reliable.
In general, the application specific can suck effect by flavouring mode, the change of flavouring approach to ramuscule cigarette Significantly improved, and improvement effect is substantially, the design, exploitation and production and sales thus for new ramuscule cigarette have preferable Application value and popularization and application meaning.
Brief description of the drawings
Fig. 1 is creamy taste diacetate fiber technological process of production intention in the present invention.
Specific embodiment
Explanation is further explained to the present invention with reference to embodiment.Before specific embodiment is introduced, first to following The preparation process of diacetate fiber described in embodiment is briefly discussed below.
The main preparation process of the diacetate fiber of prior art is as described below:
First, secondary cellulose acetate sheets are dissolved in acetone soln, while secondary cellulose acetate sheets are dissolved, by filter aid and delustering agent (TiO2) add solution, then carry out multi-stage compression filtration treatment to solution, the colloid and solid in removal spinning solution are miscellaneous Matter;
Secondly, filtering rear slurry enters spinning equipment, after the spinneret orifice of Y type shaped apertures, forms Y type cross sectional shape monofilament lines The silk of density, the proportioning for carrying out different pore size hole count further according to design requirement carries out spinning;During spinning, the silk of Y type cross sectional shapes Beam is after the smaller spinneret orifice spinneret of via hole diameter obtained in spinning, meanwhile, the spinneret hole number on spinneret is than normal ramuscule filter stick Tow spinneret is more;
Finally, tow oils from after spinning nozzle ejection into the Spin Finish System for being added with butter essence(As shown in figure 1, two acetic acid Tow band 1 along figure the direction of arrow through path(Arrow prime direction)Afterwards, into Spin Finish System 2, arrow in figure is then pressed again Head direction enters subsequent processing), subsequently into crimping machine, drying machine finally being entered back into, heating evaporation falls the acetone and water of remnants Point, finally dried tow is formed, it is prepared into the diacetate fiber finished product with cream fragrance after being then passed through pendulum wire, packing.
It should be noted that be:
Material in following embodiments used by cream fragrance essence:Vanillic aldehyde, ethyl butyrate, diacetyl, amyl butyrate, methyl are fragrant Legumin, corn oil, butyric acid are Shanghai Huabao Biotechnology Co., Ltd.'s Products;
The production of diacetate fiber is prepared and carried out by China Tobacco Henan Industrial Co., Ltd's tow suppliers, and filter stick presses existing skill It is prepared by art production.
Embodiment 1
The cream fragrance diacetate fiber that the present embodiment is provided, the cross sectional shape of its diacetate fiber is Y types, and strand specification is:It is single Denier is 8.0den, and total denier is 15000den;
It is added to have creamy before tow enters crimping machine from after spinning nozzle ejection when preparing the cream fragrance diacetate fiber The Spin Finish System of taste essence oils;The mass ratio that wherein cream fragrance essence is added in Spin Finish System is 0.5%;
The cream fragrance essence is flavor oil, and concrete composition is as follows:
0.15 part of vanillic aldehyde, 2.5 parts of ethyl butyrate, 0.75 part of diacetyl, 0.35 part of amyl butyrate, methylcoumarin 2.0 Part, 85 parts of corn oil, 9.5 parts of butyric acid.
Using the very thin branch filter bar for cigarette of vinegar prepared by the cream fragrance diacetate fiber, its specification is that length is 120mm, a length of 16.90mm of circumference, pressure drop is 3200Pa.
Ramuscule cigarette sample is prepared by prior art with this ramuscule filter stick.
Using the diacetate fiber without cream fragrance essence, corresponding filter stick and prepared ramuscule cigarette as control, Smoked panel test through specialty after personnel tentatively smoke panel test, after the diacetate fiber using cream fragrance, " creamy " is prominent, excitant reduction, miscellaneous Gas is reduced, and flue gas sophistication is improved, and pleasant impression improves.
Embodiment 2
The cream fragrance diacetate fiber that the present embodiment is provided, its specification and preparation process only adjust Spin Finish System with embodiment 1 The adding proportion of middle cream fragrance essence is 1.0%.
Ramuscule filter bar for cigarette is prepared using the cream fragrance diacetate fiber, and ramuscule cigarette is prepared with the formula of embodiment 1 Sample.
Control sample with the ramuscule cigarette in embodiment 1 is contrasted, and is smoked panel test through specialty after personnel tentatively smoke panel test, using milk After the diacetate fiber of salted cake fried in sesame oil taste, " creamy " of ramuscule cigarette than more prominent, excitant is significantly reduced, and miscellaneous gas is significantly reduced, cigarette Gas sophistication is significantly improved, and pleasant impression improves.
Embodiment 3
The cream fragrance diacetate fiber that the present embodiment is provided, its specification and preparation process only adjust Spin Finish System with embodiment 1 The adding proportion of middle cream fragrance essence is 2.0%.
Ramuscule filter bar for cigarette is prepared using the cream fragrance diacetate fiber, and ramuscule cigarette is prepared with the formula of embodiment 1 Sample.
It should be noted that because essence consumption is less, it is difficult to more accurate quantification, substantially consumption is:With Spin Finish System The adding proportion of middle essence be 1.0% as a example by, after conversion, per kilogram tow consumes about 100mg essence;Essence in Spin Finish System Adding proportion be 0.5% when, per kilogram tow consumes about 50mg essence;The adding proportion of essence is 2.0% in Spin Finish System When, per kilogram tow consumes about 200mg essence.
Control sample with the ramuscule cigarette in embodiment 1 is contrasted, and is smoked panel test through specialty after personnel tentatively smoke panel test, using milk After the diacetate fiber of salted cake fried in sesame oil taste, " creamy " of ramuscule cigarette is very prominent, and excitant increase, miscellaneous gas is reduced, and flue gas has and makes us Uncomfortable sweet sense, pleasant impression is not as the normal cigarette of control sample.
According to YCT 169-2009《The measure of pipe tobacco physicochemical property》Method detection tow sample, according to GB/T 22838—2009《The measure of cigarette and filter stick physical property》Method detection filter stick physical property, according to GB/T 19609- 2004《Cigarette conventional analysis determines TPM and tar with smoking machine》Method determine total grain phase in cigarette mainstream flue gas Thing, tar, nicotine and moisture, physical and chemical index, filter stick sample to the diacetate fiber sample in above-described embodiment and reference examples Physical index, the physical and chemical index of ramuscule cigarette sample and aesthetic quality are detected and have been evaluated that concrete outcome is as follows.
Table 1 is to diacetate fiber sample detection result:
,
As can be seen from Table 1, compared with normal diacetate fiber, the diacetate fiber physical and chemical index of butter essence is added without notable Difference, only total oil index is somewhat raised, but the key index such as crimp energy not to diacetate fiber and disconnected power is impacted.
Filter stick sample detection result in the different embodiments of table 2:
,
As can be seen from Table 2, compared with normal diacetate fiber filter stick, the diacetate fiber filter stick physics and chemistry for adding butter essence refers to Mark shows that the filter stick index that addition butter essence will not be to being molded in diacetate fiber is impacted without significant difference.
The kinds of cigarettes sample physical index of table 3 and main flume testing result:
,
As can be seen from Table 3, compared with normal diacetate fiber filter stick ramuscule cigarette, the diacetate fiber filter of butter essence is added The physical and chemical index of rod ramuscule cigarette shows that addition butter essence will not be to be molded filter stick in diacetate fiber without significant difference Filter efficiency is adversely affected.
The kinds of cigarettes sample sensory quality assessment result of table 4:
,
As can be seen from Table 4, the organoleptic quality of ramuscule cigarette can be made by using cream fragrance diacetate fiber ramuscule filter stick Significantly improve, its sensory evaluation scores highest can improve 1.56 points, and cigarette flavor is significantly improved, pleasant impression improves, excitant and miscellaneous Gas also has larger reduction, but the cream spices in cream fragrance diacetate fiber applies ratio will be adjusted according to actual conditions.
To sum up, by preparing a kind of creamy taste diacetate fiber and being molded ramuscule cigarette, will not be to diacetate fiber and filter stick Physical and chemical index is impacted, while the problems such as fragrance that can significantly improve the presence of ramuscule cigarette is rich poor.Therefore it is of the invention Ramuscule cigarette " cream " note, improvement sucking quality are highlighted as one kind, improve the new with creamy taste of sense organ comfort level Cigarette diacetate fiber is worth in whole industry popularization and application.

Claims (7)

1. a kind of cream fragrance diacetate fiber, it is characterised in that the cross sectional shape of diacetate fiber is Y types, strand specification requirement is: Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den;
Diacetate fiber performance requirement is:Moisture content is(6.0±1.6)%, oil content is(0. 70~1.50)%, fracture strength >= 18.0N/Ktex, residual acetone content≤0.30%, content of titanium dioxide is(0.40±0.20)%;
It is added to have creamy before tow enters crimping machine from after spinning nozzle ejection in cream fragrance diacetate fiber preparation process The Spin Finish System of taste essence oils;The mass ratio that wherein cream fragrance essence is added in Spin Finish System is not less than 0, but does not surpass Cross 5%.
2. cream fragrance diacetate fiber as claimed in claim 1, it is characterised in that cream fragrance essence is added in Spin Finish System Mass ratio be 0.5 ~ 2%.
3. cream fragrance diacetate fiber as claimed in claim 2, it is characterised in that cream fragrance essence is added in Spin Finish System Mass ratio be 1%.
4. the cream fragrance diacetate fiber as described in any one of claim 1 ~ 3, it is characterised in that the cream fragrance essence is oil Matter essence, in terms of mass fraction, concrete composition is as follows:
Vanillic aldehyde 0.1- ~ 0.3 part, 1.5 ~ 4.0 parts of ethyl butyrate, 0.5 ~ 2.0 part of diacetyl, 0.1 ~ 0.4 part of amyl butyrate, 1.0 ~ 3.0 parts of methylcoumarin, 60 ~ 100 parts of corn oil, 5.0 ~ 15.0 parts of butyric acid.
5. cream fragrance diacetate fiber as claimed in claim 4, it is characterised in that cream fragrance composition composition is:Chinese cymbidium 0.15 part of element, 2.5 parts of ethyl butyrate, 0.75 part of diacetyl, 0.35 part of amyl butyrate, 2.0 parts of methylcoumarin, corn 85 parts of oil, 9.5 parts of butyric acid.
6. application of the cream fragrance diacetate fiber in ramuscule cigarette described in claim 1, it is characterised in that for preparing ramuscule Filter bar for cigarette.
7. application of the cream fragrance diacetate fiber as claimed in claim 6 in ramuscule cigarette, it is characterised in that ramuscule cigarette is used Filter stick specification is:Length is 120mm, and a length of 16.90mm of circumference, pressure drop is 2800Pa ~ 4500Pa.
CN201611127542.0A 2016-12-09 2016-12-09 Butter-flavor cellulose acetate tow and application thereof in fine cigarettes Pending CN106690411A (en)

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Cited By (4)

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Publication number Priority date Publication date Assignee Title
CN107488513A (en) * 2017-09-19 2017-12-19 河南中烟工业有限责任公司 Fragrant line safranine extrait and its application in a kind of ramuscule filter stick
CN107541341A (en) * 2017-09-19 2018-01-05 河南中烟工业有限责任公司 Fragrant line fructus amomi essence and its application in a kind of ramuscule filter stick
CN111184253A (en) * 2018-11-14 2020-05-22 南通烟滤嘴有限责任公司 Method for selecting specification of tows for fine filter stick
EP3662770B1 (en) 2018-10-25 2021-02-24 Daicel Corporation Electronic cigarette tip tow band, electronic cigarette tip, method for producing electronic cigarette tip tow band, and method for producing electronic cigarette tip

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107488513A (en) * 2017-09-19 2017-12-19 河南中烟工业有限责任公司 Fragrant line safranine extrait and its application in a kind of ramuscule filter stick
CN107541341A (en) * 2017-09-19 2018-01-05 河南中烟工业有限责任公司 Fragrant line fructus amomi essence and its application in a kind of ramuscule filter stick
EP3662770B1 (en) 2018-10-25 2021-02-24 Daicel Corporation Electronic cigarette tip tow band, electronic cigarette tip, method for producing electronic cigarette tip tow band, and method for producing electronic cigarette tip
US11641873B2 (en) 2018-10-25 2023-05-09 Daicel Corporation Tow band for heated tobacco product tip, tip for heated tobacco product, method for manufacturing tow band for heated tobacco product tip, and method for manufacturing heated tobacco product tip
CN111184253A (en) * 2018-11-14 2020-05-22 南通烟滤嘴有限责任公司 Method for selecting specification of tows for fine filter stick

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Application publication date: 20170524