CN107488513A - Fragrant line safranine extrait and its application in a kind of ramuscule filter stick - Google Patents
Fragrant line safranine extrait and its application in a kind of ramuscule filter stick Download PDFInfo
- Publication number
- CN107488513A CN107488513A CN201710846822.5A CN201710846822A CN107488513A CN 107488513 A CN107488513 A CN 107488513A CN 201710846822 A CN201710846822 A CN 201710846822A CN 107488513 A CN107488513 A CN 107488513A
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- Prior art keywords
- safranine
- extrait
- line
- ramuscule
- built
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to ramuscule cigarette filter rod production technical field, and in particular to fragrant line safranine extrait and its patent application of application in a kind of ramuscule filter stick.It is calculated in mass percent, it is composed of the following components：2.0 ~ 5.0% safflower essential oil, 1.0 ~ 2.0% Leaf Acetate, 0.5 ~ 1.0% benzyl carbinol, 0.5 ~ 1.0% nerol, 0.05 ~ 0.1% lavender oil, 0.1 ~ 0.2% isophorone, 0.2 ~ 0.5% β damascones, 90.2 ~ 95.65% Glycerin, mixed triester with caprylic acid capric acid.The application is while fragrant line is with safranine extrait in providing a kind of ramuscule cigarette with peat-reek, coordinate the improvement of ramuscule cigarette filter rod structure, ramuscule cigarette can preferably be improved sucks effect, and improvement effect is obvious, with preferable practical value, design, exploitation and production and sales for new ramuscule cigarette have preferable Demonstration And Extension application value.
Description
Technical field
The invention belongs to ramuscule cigarette filter rod production technical field, and in particular to fragrant line safflower in a kind of ramuscule filter stick
Essence and its patent application of application.
Background technology
With the continuous improvement of people's living standards, the cigarette kind on cigarette market is also increasingly abundanter, also it is consumption
Person provides more choices, and ramuscule cigarette is exactly typical case therein.From the point of view of effective sale effect, ramuscule cigarette is unique with it
Glamour conquered increasing consumer.
From the point of view of cigarette quality, the tar content of ramuscule cigarette is more general than regular-size cigarette low, and suction taste is also thin, thus comparison operators
The demand of particular consumer is closed, the urban woman for being particularly subject to follow the fashion, graceful, fashion is lived consumes the especially blue or green of family
Look at.And as the fast development of low-coke tar cigarette, advantage of the ramuscule cigarette in terms of " tar reduction is protected fragrant " just seem especially noticeable.
Due to occupying the relatively small number of innate advantage of cigarette small volume, releasing content of coke tar, ramuscule cigarette also goes out simultaneously
The problems such as smoke is light, fragrance is insufficient is showed, thus it is promoted the crowd of being applicable and certain limitation be present.Therefore, existing cigarette
Manufacturing enterprise is also cracking this technical barrier by reducing many technological means such as filter stick pressure drop, optimization tobacco structure.
In terms of the ramuscule cigarette flavouring, in prior art thinking, mainly using the forms such as perfume particles, essence capsule come
Supplement or increase cigarette fragrance, but this release of several ramuscule cigarette flavouring mode generally existing fragrance is uneven, the resting period is short,
The defects of with flue gas inaccurate coordination, so that improving fragrance effect is not obvious enough.Thus pole is necessary in existing flavouring mode
On the basis of, comprehensive means are further improved etc. by composition, flavouring mode, further to improve the uniformity of flavouring, steady
Qualitative and harmony.
The content of the invention
Present invention aims at a kind of safranine extrait for fragrant line in ramuscule filter stick of offer, while ramuscule is coordinated to filter
The improvement of rod configuration aspects, while abundant ramuscule cigarette type, further improve the flavouring effect of ramuscule cigarette.
Details are as follows for the technical scheme that the application is taken.
Fragrant line safranine extrait, is calculated in mass percent in a kind of ramuscule filter stick, composed of the following components：
2.0 ~ 5.0% safflower essential oil, 1.0 ~ 2.0% Leaf Acetate,
0.5 ~ 1.0% benzyl carbinol, 0.5 ~ 1.0% nerol, 0.05 ~ 0.1% lavender oil, 0.1 ~ 0.2% isophorone,
0.2 ~ 0.5% β-damascone, 90.2 ~ 95.65% Glycerin, mixed triester with caprylic acid capric acid.
The safflower essential oil, existing finished product can be used, or be prepared with reference to following preparation method：
（1）After safflower crushes after drying, 40-60 mesh sieves are crossed, obtain saffron；
（2）A certain amount of saffron is taken to insert in distilling flask, after adding a certain amount of distilled water, 3 ~ 5h of steam distillation obtains profit
The distillate of layering；
（3）With the oil phase in dichloromethane extractive distillation liquid, and use anhydrous sodium sulfate drying；
（4）By step（3）Rotation evaporates solvent under 50 DEG C of water bath conditions after middle gained finish filtering, obtains crocein
Oil.
Fragrant line safranine extrait, specific formula are, for example, in the ramuscule filter stick：3.5% safflower essential oil, 1.5%
Leaf Acetate, 0.7% benzyl carbinol, 0.7% nerol, 0.08% lavender oil, 0.15% isophorone, 0.35%
β-damascone, 93.02% Glycerin, mixed triester with caprylic acid capric acid.
Application of the fragrant line with safranine extrait in cigarette in the ramuscule filter stick, for fragrant line in ramuscule cigarette filter rod.
A kind of ramuscule composite filter of built-in safranine extrait perfume (or spice) line, the composite filter outer wrap has forming paper, interior
Portion is combined by common vinegar fibre filter rod segments and built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments, wherein built-in safranine extrait is fragrant
Line vinegar fibre filter rod segments are close to pipe tobacco section；
Common vinegar fibre filter rod segments and built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments, the cross sectional shape of diacetate fiber used is Y types,
Strand specification requires：Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den；
Common vinegar fibre filter rod segments and the length ratio of built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments, can be according to resistance to suction or flavouring need
Ask and be adjusted, length ratio is, for example, specifically 1:1；
The built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments, its middle part are built-in with fragrant line, and fragrant line is adsorbed with safranine extrait；Its
Preparation process is prepared by prior art, is specially：Before fragrant line enters filter-stick forming device after being come out from line roller, by equipped with one
The flavoring system for determining concentration safranine extrait applies essence；
The The concrete specification of the composite filter, it is, for example,：Length is 120mm, a length of 16.90mm of circumference, pressure drop be 2600Pa ~
4200Pa。
The essence applied amount of the ramuscule perfume (or spice) line filter stick list branch filter stick is 10mg ~ 30mg.
Utilize ramuscule cigarette prepared by the ramuscule composite filter of the built-in safranine extrait perfume (or spice) line.
The present invention prepares a kind of saffron flavoured essence with peat-reek first by autonomous Design composition,
As the flavouring additive in ramuscule perfume (or spice) line filter stick, the ramuscule composite filter with safranine flowery odour has been prepared.Hide
Safflower is sweet, micro-pungent, mild-natured；The thoughts of returning home, Liver Channel；Body lightweight is moistened, and is entered blood and is dissipated；Possess and activate blood circulation and disperse blood clots, dissipate Yu Kaijie, removing pattogenic heat from the blood and toxic material from the body
Function.Thus the application can partly reduce the harmfulness of tobacco while abundant essence type.
Preliminary Applications show, after the ramuscule perfume (or spice) line composite filter is used for ramuscule cigarette, not only increase the equal of essence application
Even property and the stability of release, also improve the harmony of fragrance and product sensory quality.By the safranine extrait applied
Allocate and obtain for natural materials, therefore these aroma substances can be highlighted more " the roasting sweet tea " of cigarette after cigarette smoke is entered
Note, lifts the fragrance richness and plumpness of ramuscule cigarette, and then improves its sucking quality and sense organ comfort level.
Compared with existing perfuming technology, main advantages of the present invention have：
(1) simple process：Preparation technology of the present invention is simple, without making notable adjustment to current production technology and equipment, without
Large-scale instrument and equipment and expensive reagent, it is simple to operate, it is easily controllable；
(2) safety and sanitation：Raw and auxiliary material of the present invention is widely used in food processing field, in the absence of toxic reagent
Residue problem, thus securely and reliably；
（3）Release is stable：Built-in fragrant line composite filter form of the present invention, the same of fragrant line is directly contacted avoiding oral cavity
When, help to slow down the loss of fragrance.
In general, a kind of the application fragrant line in the ramuscule cigarette with peat-reek is provided is same with safranine extrait
When, coordinate the improvement of ramuscule cigarette filter rod structure, can preferably improve the effect of sucking of ramuscule cigarette, and improvement effect is obvious,
With preferable practical value, while abundant cigarette product type, design, exploitation and production for new ramuscule cigarette
Sale has preferable Demonstration And Extension application value.
Brief description of the drawings
Fig. 1 is the ramuscule composite filter structural representation of built-in safranine extrait perfume (or spice) line provided by the present invention；
Fig. 2 is ramuscule cigarette structure schematic diagram prepared by the ramuscule composite filter of safranine extrait perfume (or spice) line built in utilization.
Embodiment
Explanation is further explained to the application with reference to embodiment., it is necessary to illustrate before specific embodiment is introduced
, safflower essential oil employed in following embodiments, benzyl carbinol, nerol, lavender oil, isophorone, Leaf Acetate,
The materials such as β-damascone, Glycerin, mixed triester with caprylic acid capric acid are Shanghai Huabao Biotechnology Co., Ltd.'s Products；Fragrant line, ramuscule filter stick
Carried out Deng also prior art production is pressed.
Embodiment 1
The present embodiment provides fragrant line safranine extrait in ramuscule filter stick, is calculated in mass percent, composed of the following components：
2.0% safflower essential oil, 0.5% benzyl carbinol, 0.5% nerol, 0.05% lavender oil, 0.1% different Fo Er
Ketone, 1.0% Leaf Acetate, 0.2% β-damascone, 95.65% Glycerin, mixed triester with caprylic acid capric acid.
By prior art, the ramuscule composite filter of safranine extrait perfume (or spice) line built in preparation is as shown in Figure 1, 2, prepared multiple
Filter stick 3 is closed, outer wrap has forming paper, and inside is by common vinegar fibre filter rod segments 2 and built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments 1
It is combined, wherein built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments 1 are close to pipe tobacco section 4；
Common vinegar fibre filter rod segments 2, the cross sectional shape of diacetate fiber used is Y types, and strand specification requirement is：6.0Y/17000
（den/den）；
Built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments 2, the cross sectional shape of diacetate fiber used is Y types, and strand specification requirement is：
8.0Y/15000（den/den）；
The length ratio of common vinegar fibre filter rod segments and built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments, it is 1:1；The composite filter
The concrete specification be：Length is 120mm, a length of 16.90mm of circumference（In Fig. 2, during actual use, filter length 30mm（Scheme
1+2 part-structures length in 2））, the filter lengths of 1+2 structures are 30mm in Fig. 2.
When preparing the ramuscule composite filter of the built-in safranine extrait perfume (or spice) line, carried out by existing filter stick production technology, it is first
First pass through filter-stick forming device the fragrant line for being applied with safranine extrait is inserted into filter stick center and fragrant line filter stick is made, then pass through filter again
Rod compounding machine and common vinegar fibre filter stick formation are ramuscule perfume (or spice) line binary compound filter candle（The ramuscule for stating built-in safranine extrait perfume (or spice) line is answered
Close filter stick）.After shaping, measurement result shows, fragrant line is 20mg or so with safranine extrait applied amount in every composite filter（I.e.
The dosage of the long filter sticks of 120mm is 20mg）.
It is ramuscule by the ramuscule composite filter of the built-in safranine extrait perfume (or spice) line and tobacco sample cigarette by prior art
Cigarette sample sets blank control sample as test sample（Blank perfume (or spice) line is added at filter stick same position）As control
Sample, evaluation is detected and is aspirated respectively to test sample and control sample by 7 professional sensory evaluation personnel.Specific flue gas inspection knot
Fruit and specific suction evaluate score value referring to form hereinafter.
Suction evaluation result shows that after it with the addition of safranine extrait, " safflower " fragrance of cigarette sample is obvious, flue gas
Fragrance it is rich have certain lifting, excitant is reduced, and miscellaneous gas is reduced, and flue gas sophistication improves, and pleasant impression makes moderate progress.
Embodiment 2
The present embodiment provides fragrant line safranine extrait in ramuscule filter stick, is calculated in mass percent, composed of the following components：
3.5% safflower essential oil, 0.7% benzyl carbinol, 0.7% nerol, 0.08% lavender oil, 0.15% different Fo Er
Ketone, 1.5% Leaf Acetate, 0.35% β-damascone, 93.02% Glycerin, mixed triester with caprylic acid capric acid.
With the filter stick specification of embodiment 1, the ramuscule composite filter of safranine extrait perfume (or spice) line built in preparation.After shaping, measure
As a result show, fragrant line is 20mg or so with safranine extrait applied amount in every composite filter.
The ramuscule composite filter of the built-in safranine extrait perfume (or spice) line and tobacco sample cigarette are made for ramuscule cigarette sample
For test sample, suction evaluation is carried out.
Suction evaluation result shows, after it with the addition of safranine extrait, " the safranine fragrance of a flower " obvious, cigarette of cigarette sample
Gas fragrance is rich to be dramatically increased, and excitant significantly reduces, and miscellaneous gas is reduced, and flue gas sophistication is significantly improved, and pleasant impression is obviously improved.
Embodiment 3
The present embodiment provides fragrant line safranine extrait in ramuscule filter stick, is calculated in mass percent, composed of the following components：
5.0% safflower essential oil, 1.0% benzyl carbinol, 1.0% nerol, 0.1% lavender oil, 0.2% isophorone,
2.0% Leaf Acetate, 0.5% β-damascone, 90.2% Glycerin, mixed triester with caprylic acid capric acid.
With the filter stick specification of embodiment 1, the ramuscule composite filter of safranine extrait perfume (or spice) line built in preparation.After shaping, measure
As a result show, fragrant line is 20mg or so with safranine extrait applied amount in every composite filter.
The ramuscule composite filter of the built-in safranine extrait perfume (or spice) line and tobacco sample cigarette are made for ramuscule cigarette sample
For test sample, suction evaluation is carried out.
Suction evaluation result shows, after it with the addition of safranine extrait, " the safranine fragrance of a flower " fairly obvious, cigarette of cigarette sample
Gas fragrance harmony is reduced, and excitant increase, miscellaneous gas is reduced, and flue gas inaccurate coordination and has uncomfortable sweet sense, pleasant impression
Not as normal cigarette（Compared with control sample cigarette）.
Composite filter prepared by different embodiments is detected, further according to《The cigarette of GB/T 19609-2004 is used
Conventional analysis determines TPM and tar with smoking machine》Method measure cigarette mainstream flue gas in TPM, tar, nicotine
Detected with indexs such as moisture, concrete outcome is as shown in the table.
Table 1, the testing result of the ramuscule composite filter of built-in safranine extrait perfume (or spice) line prepared by different embodiments：
；
Table 2, the physical index and main flume testing result of kinds of cigarettes sample：
；
It is can be seen that from the above-mentioned data of table 1 compared with normal diacetate fiber filter stick, place the filter stick physical index of safranine fragrance of a flower line
Without significant difference.As can be seen from Table 2, compared with the normal cigarette of reference examples, the main flume of safranine fragrance of a flower coil of wire cigarette without
Significant change, the key index tar and nicotine for influenceing cigarette sense organ do not have significant changes.
Table 3, kinds of cigarettes sample sensory quality assessment result：
。
As can be seen from Table 3, it can obtain cigarette sensory quality by using safranine extrait perfume (or spice) line composite filter
Significantly improve, its sensory evaluation scores highest can improve 0.81 point, and fragrance significantly improves, and pleasant impression improves, excitant and miscellaneous gas also have compared with
It is big to reduce.
To sum up, by targetedly designing the fragrant line filter stick composition of specific fragrance, after being applied to cigarette, energy
Odor characteristic during smoking property of cigarette is enough obviously improved, impression is sucked in abundant and raising, simultaneously because the present invention uses special construction
Fragrant line filter stick, conventional fragrant line filter stick can be avoided quickly to be lost in, while safety and sanitation.Therefore the application highlights cigarette as one kind
" safflower " note, the new saffron flavoured ramuscule perfume (or spice) line composite filter for improving sucking quality, in industry have and definitely push away
Wide application value.
Claims (5)
1. fragrant line safranine extrait in a kind of ramuscule filter stick, it is characterised in that be calculated in mass percent, by following components group
Into：
2.0 ~ 5.0% safflower essential oil, 1.0 ~ 2.0% Leaf Acetate,
0.5 ~ 1.0% benzyl carbinol, 0.5 ~ 1.0% nerol, 0.05 ~ 0.1% lavender oil, 0.1 ~ 0.2% isophorone,
0.2 ~ 0.5% β-damascone, 90.2 ~ 95.65% Glycerin, mixed triester with caprylic acid capric acid.
2. fragrant line safranine extrait in ramuscule filter stick as claimed in claim 1, it is characterised in that specific formula is：3.5%
Safflower essential oil, 1.5% Leaf Acetate, 0.7% benzyl carbinol, 0.7% nerol, 0.08% lavender oil, 0.15%
Isophorone, 0.35% β-damascone, 93.02% Glycerin, mixed triester with caprylic acid capric acid；
Or it is：
2.0% safflower essential oil, 0.5% benzyl carbinol, 0.5% nerol, 0.05% lavender oil, 0.1% different Fo Er
Ketone, 1.0% Leaf Acetate, 0.2% β-damascone, 95.65% Glycerin, mixed triester with caprylic acid capric acid；
Or it is：
5.0% safflower essential oil, 1.0% benzyl carbinol, 1.0% nerol, 0.1% lavender oil, 0.2% isophorone,
2.0% Leaf Acetate, 0.5% β-damascone, 90.2% Glycerin, mixed triester with caprylic acid capric acid.
3. application of the fragrant line with safranine extrait in cigarette in the ramuscule filter stick of claim 1 or 2, it is characterised in that use
The fragrant line in ramuscule cigarette filter rod.
4. a kind of ramuscule composite filter of built-in safranine extrait perfume (or spice) line, it is characterised in that the composite filter outer wrap has
Forming paper, inside is combined by common vinegar fibre filter rod segments and built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments, wherein built-in Tibetan
Safflower essence perfume (or spice) line vinegar fibre filter rod segments are close to pipe tobacco section；
Common vinegar fibre filter rod segments and built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments, the cross sectional shape of diacetate fiber used is Y types,
Strand specification requires：Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den；
The length ratio of common vinegar fibre filter rod segments and built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments is 1:1；
The built-in safranine extrait perfume (or spice) line vinegar fibre filter rod segments, its middle part are built-in with fragrant line, and fragrant line is adsorbed with safranine extrait.
5. utilize ramuscule cigarette, its feature prepared by the ramuscule composite filter of built-in safranine extrait perfume (or spice) line described in claim 4
It is, the essence applied amount of single branch filter stick is 10mg ~ 30mg.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710846822.5A CN107488513A (en) | 2017-09-19 | 2017-09-19 | Fragrant line safranine extrait and its application in a kind of ramuscule filter stick |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710846822.5A CN107488513A (en) | 2017-09-19 | 2017-09-19 | Fragrant line safranine extrait and its application in a kind of ramuscule filter stick |
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|---|---|
| CN107488513A true CN107488513A (en) | 2017-12-19 |
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ID=60651753
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|---|---|---|---|
| CN201710846822.5A Pending CN107488513A (en) | 2017-09-19 | 2017-09-19 | Fragrant line safranine extrait and its application in a kind of ramuscule filter stick |
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Application publication date: 20171219 |
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