CN107556902A - A kind of preparation method of switch cubicle spray-applied primer - Google Patents
A kind of preparation method of switch cubicle spray-applied primer Download PDFInfo
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- CN107556902A CN107556902A CN201710879615.XA CN201710879615A CN107556902A CN 107556902 A CN107556902 A CN 107556902A CN 201710879615 A CN201710879615 A CN 201710879615A CN 107556902 A CN107556902 A CN 107556902A
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- switch cubicle
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Abstract
The present invention relates to a kind of preparation method of switch cubicle spray-applied primer, by weight, 100 parts of mould proof modified urethane acrylate, 10 25 parts of epoxy acrylate, 15 parts of esterase, 10 20 parts of white oil, 15 parts of Diisopentyl Maleate Using, 1 5h of stirring obtained by step 1 are added in stirred tank, that is, obtains switch cubicle spray-applied primer.
Description
Technical field
The present invention relates to a kind of preparation method of paint, especially a kind of preparation method of switch cubicle spray-applied primer.
Background technology
Switch cubicle（switch cabinet）It is a kind of electrical equipment, controls the Push And Release of various equipment.Switch cubicle outside line
Master switch in cabinet is introduced into, is switched subsequently into sub-control, each branch is needed to set by it.Such as instrument, automatic control, motor magnetic force
Switch, various A.C. contactors etc., some also sets hyperbaric chamber and low-pressure chamber switch cubicle, provided with high voltage bus, such as power plant, has
Be additionally provided with for protect capital equipment low-frequency load reduction.Part in switch cubicle mainly have breaker, disconnecting switch, on-load switch,
Operating mechanism, transformer and various protection devices etc..The sorting technique of switch cubicle is a lot, such as can by breaker mounting means
To be divided into withdraw-type switch cabinet and fixed switching cabinet；Or the difference according to cabinet body structure, open type switch cubicle, metal can be divided into
Closed switch cabinet and metal enclosed armoured switch cabinet；It can be divided into high-tension switch cabinet, Medium voltage switch or circuit breaker again according to voltage class is different
Cabinet and low-tension switch cabinet etc..
CN104004450A discloses a kind of switch cubicle spray-applied primer, it is characterised in that by the raw material system of following parts by weight
Prepare into：Urethane acrylate 40-45, epoxy acrylate 23-28, titanium dioxide 3-4, hydrophobic silica 2-3, cyanuric acid
Zinc 2-3, zinc oxide 3-4, alum powder 2-3, isopropyl thioxanthone 1-2, benzoin dimethylether 3-4, methyl methacrylate 1-
2nd, ethylene glycol ether acetate 3-5, esterase 8-10, ethyl acetate 7-9, dispersing aid 3-4；Dispersing aid improves light
Performance is learned, paint is uniformly dispersed, and maintain the stability of paint；Resist sagging, film enrich, and adhesive force is strong, can be fast
Speed solidification, substantially increases operating efficiency.
CN106085225A is related to a kind of switch cubicle protective paint, the protective paint by weight, by following components group
Into：Fatty alcohol-ether sodium sulfate 2-4 parts, hydroxyacetic acid 1-3 parts, attapulgite 0.5-0.7 parts, potassium hydroxide 0.8-1.0 parts, sulfuric acid
Barium 1-2 parts, hexyl decyl alcohol 1-3 parts and epoxy silicone 11-15 parts.
CN103555138A is related to a kind of Switch cabinet spray paint, is made from the following raw materials in parts by weight：E-12 epoxy resin
55-60, amino resins 30-35, polyester resin（EL-1000H）20-24, ethylene bis stearic acid amide 2-3, ethyl thioglycollic acid are different pungent
Ester 2-3, polyvinyl butyral resin 3-4, Di(dioctylpyrophosphato) ethylene titanate 2-3, magnesium hydroxide 6-8, dioxy
Change titanium 4-5, zinc oxide 1-2, calcium carbonate 10-12, ethyl acetate 15-18, auxiliary agent 4-5；Auxiliary agent of the present invention improves optical property,
Paint is uniformly dispersed, and maintain the stability of paint, improve film-formation result.
Existing Switch cabinet heatproof anticorrosion paint, it is larger in humidity, in the environment of easy mould growth, easily produce mould
Bacterium, generate mildew.
The content of the invention
The purpose of the present invention is：There is provided a kind of preparation method of switch cubicle spray-applied primer, it is characterised in that following steps：
The preparation of the mould proof modified urethane acrylate of step 1.
By weight, urethane acrylate is added in a kettle, and tributyl-methyl phosphonium ammonium is double（Fluoroform sulphonyl）Imines
Salt, 2- amino -4- Methyl-N-phenyl thiazole -5- formamides, trifluoroacetylacetone (TFA) cerium hydrate, titanium dioxide, silica,
50-70 DEG C is warming up to, 3-10h is reacted, obtains mould proof modified urethane acrylate.
The preparation method of step 2. switch cubicle spray-applied primer
By weight, 100 parts of mould proof modified urethane acrylate, the epoxy third obtained by step 1 are added in stirred tank
Olefin(e) acid ester 10-25 parts, esterase 1-5 parts, white oil 10-20 parts, Diisopentyl Maleate Using 1-5 parts, stirring 1-5h, that is, obtain
Switch cubicle spray-applied primer.
Described mould proof modified urethane acrylate, its material quality amount ratio are epoxy resin：Tributyl-methyl phosphonium ammonium
It is double（Fluoroform sulphonyl）Inferior amine salt：2- amino -4- Methyl-N-phenyl thiazole -5- formamides：Trifluoroacetylacetone (TFA) cerium is hydrated
Thing:Titanium dioxide:Silica=100：0.01-0.1：0.5-1.5:0.1-1:4-9:5-15.
Described epoxy resin, tributyl-methyl phosphonium ammonium are double（Fluoroform sulphonyl）Inferior amine salt, 2- amino -4- methyl-N- benzene
Base thiazole -5- formamides, trifluoroacetylacetone (TFA) cerium (hydrate, urethane acrylate, epoxy acrylate, rosin glycerin ester
Ester, white oil, Diisopentyl Maleate Using are commercially available prod.
The product of the present invention has the advantages that：
The switch cubicle spray-applied primer that the present invention is produced, its main material resin crosslinks degree is big, non-aging, the mechanics of product
It is functional, there is permanent and potent bactericidal effect simultaneously for bacteriums such as moulds.
Embodiment
Following instance is only to further illustrate the present invention, is not limitation the scope of protection of the invention.
Embodiment 1
The preparation of the mould proof modified urethane acrylate of step 1.
By weight, urethane acrylate is added in a kettle, and tributyl-methyl phosphonium ammonium is double（Fluoroform sulphonyl）Imines
Salt, 2- amino -4- Methyl-N-phenyl thiazole -5- formamides, trifluoroacetylacetone (TFA) cerium hydrate, 65 DEG C are warming up to, reaction
5h, obtain mould proof modified urethane acrylate.
The preparation method of step 2. switch cubicle spray-applied primer
By weight, 100 parts of mould proof modified urethane acrylate, the epoxy third obtained by step 1 are added in stirred tank
14 parts of olefin(e) acid ester, 3 parts of esterase, 15 parts of white oil, 3 parts of Diisopentyl Maleate Using, stirring 3h, that is, obtain switch cubicle spraying bottom
Paint.
Described mould proof modified urethane acrylate, its material quality amount ratio are epoxy resin：Tributyl-methyl phosphonium ammonium
It is double（Fluoroform sulphonyl）Inferior amine salt：2- amino -4- Methyl-N-phenyl thiazole -5- formamides：Trifluoroacetylacetone (TFA) cerium is hydrated
Thing:Titanium dioxide:Silica=100：0.02：1:0.2:6:8.
Embodiment 2
The preparation of the mould proof modified urethane acrylate of step 1.
By weight, urethane acrylate is added in a kettle, and tributyl-methyl phosphonium ammonium is double（Fluoroform sulphonyl）Imines
Salt, 2- amino -4- Methyl-N-phenyl thiazole -5- formamides, trifluoroacetylacetone (TFA) cerium hydrate, 50 DEG C are warming up to, reaction
10h, obtain mould proof modified urethane acrylate.
The preparation method of step 2. switch cubicle spray-applied primer
By weight, 100 parts of mould proof modified urethane acrylate, the epoxy third obtained by step 1 are added in stirred tank
10 parts of olefin(e) acid ester, 1 part of esterase, 10 parts of white oil, 1 part of Diisopentyl Maleate Using, stirring 1h, that is, obtain switch cubicle spraying bottom
Paint.
Described mould proof modified urethane acrylate, its material quality amount ratio are epoxy resin：Tributyl-methyl phosphonium ammonium
It is double（Fluoroform sulphonyl）Inferior amine salt：2- amino -4- Methyl-N-phenyl thiazole -5- formamides：Trifluoroacetylacetone (TFA) cerium is hydrated
Thing:Titanium dioxide:Silica=100：0.01：0.5:0.1:4:5.
The preparation of the mould proof modified urethane acrylate of step 1.
By weight, urethane acrylate is added in a kettle, and tributyl-methyl phosphonium ammonium is double（Fluoroform sulphonyl）Imines
Salt, 2- amino -4- Methyl-N-phenyl thiazole -5- formamides, trifluoroacetylacetone (TFA) cerium hydrate, 70 DEG C are warming up to, reaction
3h, obtain mould proof modified urethane acrylate.
The preparation method of step 2. switch cubicle spray-applied primer
By weight, 100 parts of mould proof modified urethane acrylate, the epoxy third obtained by step 1 are added in stirred tank
25 parts of olefin(e) acid ester, 5 parts of esterase, 20 parts of white oil, 5 parts of Diisopentyl Maleate Using, stirring 5h, that is, obtain switch cubicle spraying bottom
Paint.
Described mould proof modified urethane acrylate, its material quality amount ratio are epoxy resin：Tributyl-methyl phosphonium ammonium
It is double（Fluoroform sulphonyl）Inferior amine salt：2- amino -4- Methyl-N-phenyl thiazole -5- formamides：Trifluoroacetylacetone (TFA) cerium is hydrated
Thing:Titanium dioxide:Silica=100：0.1：1.5:1:9:15.
Comparative example 1
It is double that step 1 is added without tributyl-methyl phosphonium ammonium（Fluoroform sulphonyl）Inferior amine salt, other conditions are the same as embodiment 1.
Comparative example 2
Step 1 is added without 2- amino -4- Methyl-N-phenyl thiazole -5- formamides, and other conditions are the same as embodiment 1.
Comparative example 3
Step 1 is added without trifluoroacetylacetone (TFA) cerium hydrate, and other conditions are the same as embodiment 1.
Comparative example 4
Step 1 is cancelled, and urethane acrylate is not modified, and other conditions are the same as embodiment 1.
Embodiment 4
The switch cubicle spray-applied primer for respectively being produced embodiment 1-3 and comparative example 1-4, reference standard QBT2591-2003 are carried
The method of confession examines its antifungi ability and two months later antifungi abilities.It is shown in Table 1.
Table 1：The Anti-mildew capability for the switch cubicle spray-applied primer that different process is produced.
| Production code member | Antifungi rate/% | Antifungi rate/% after two months |
| Embodiment 1 | 98 | 98 |
| Embodiment 2 | 98 | 97 |
| Embodiment 3 | 99 | 99 |
| Comparative example 1 | 93 | 89 |
| Comparative example 2 | 92 | 88 |
| Comparative example 3 | 95 | 92 |
| Comparative example 4 | 87 | 81 |
Claims (3)
1. a kind of preparation method of switch cubicle spray-applied primer, it is characterised in that comprise the following steps：
By weight, 100 parts of mould proof modified urethane acrylate, the epoxy third obtained by step 1 are added in stirred tank
Olefin(e) acid ester 10-25 parts, esterase 1-5 parts, white oil 10-20 parts, Diisopentyl Maleate Using 1-5 parts, stirring 1-5h, that is, obtain
Switch cubicle spray-applied primer.
A kind of 2. preparation method of switch cubicle spray-applied primer according to claim 1, it is characterised in that：It is described mould proof to change
The preparation method of property urethane acrylate is：
By weight, urethane acrylate is added in a kettle, and tributyl-methyl phosphonium ammonium is double（Fluoroform sulphonyl）Imines
Salt, 2- amino -4- Methyl-N-phenyl thiazole -5- formamides, trifluoroacetylacetone (TFA) cerium hydrate, is warming up to 50-70 DEG C, instead
3-10h is answered, obtains mould proof modified urethane acrylate.
A kind of 3. preparation method of switch cubicle spray-applied primer according to claim 2, it is characterised in that：It is described mould proof to change
Property urethane acrylate, its material quality amount ratio is epoxy resin：Tributyl-methyl phosphonium ammonium is double（Fluoroform sulphonyl）Imines
Salt：2- amino -4- Methyl-N-phenyl thiazole -5- formamides：Trifluoroacetylacetone (TFA) cerium hydrate:Titanium dioxide:Silica ,=
100：0.01-0.1：0.5-1.5:0.1-1:4-9:5-15.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710879615.XA CN107556902A (en) | 2017-09-26 | 2017-09-26 | A kind of preparation method of switch cubicle spray-applied primer |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710879615.XA CN107556902A (en) | 2017-09-26 | 2017-09-26 | A kind of preparation method of switch cubicle spray-applied primer |
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| Publication Number | Publication Date |
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| CN107556902A true CN107556902A (en) | 2018-01-09 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710879615.XA Pending CN107556902A (en) | 2017-09-26 | 2017-09-26 | A kind of preparation method of switch cubicle spray-applied primer |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102732133A (en) * | 2012-06-29 | 2012-10-17 | 惠州市长润发涂料有限公司 | Anti-sagging spraying prime coat |
| CN104004450A (en) * | 2014-04-25 | 2014-08-27 | 安徽祈艾特电子科技有限公司 | Switch cabinet spraying priming paint and preparation method thereof |
-
2017
- 2017-09-26 CN CN201710879615.XA patent/CN107556902A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102732133A (en) * | 2012-06-29 | 2012-10-17 | 惠州市长润发涂料有限公司 | Anti-sagging spraying prime coat |
| CN104004450A (en) * | 2014-04-25 | 2014-08-27 | 安徽祈艾特电子科技有限公司 | Switch cabinet spraying priming paint and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 中国化工信息中心市场信息部: "《中国化工产品目录（上）》", 31 January 1993, 中国化工信息中心 * |
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Application publication date: 20180109 |