CN107549471A - A kind of preparation method of solid molasses feed - Google Patents
A kind of preparation method of solid molasses feed Download PDFInfo
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- CN107549471A CN107549471A CN201710946524.3A CN201710946524A CN107549471A CN 107549471 A CN107549471 A CN 107549471A CN 201710946524 A CN201710946524 A CN 201710946524A CN 107549471 A CN107549471 A CN 107549471A
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- molasses
- bagasse
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- solid
- feed
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- 235000013379 molasses Nutrition 0.000 title claims abstract description 124
- 239000007787 solid Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 241000609240 Ambelania acida Species 0.000 claims abstract description 50
- 239000010905 bagasse Substances 0.000 claims abstract description 50
- 239000000203 mixture Substances 0.000 claims abstract description 48
- 102000004190 Enzymes Human genes 0.000 claims abstract description 38
- 108090000790 Enzymes Proteins 0.000 claims abstract description 38
- 238000001035 drying Methods 0.000 claims abstract description 15
- 238000009472 formulation Methods 0.000 claims description 18
- 108010001682 Dextranase Proteins 0.000 claims description 14
- 108010051210 beta-Fructofuranosidase Proteins 0.000 claims description 12
- 239000001573 invertase Substances 0.000 claims description 12
- 235000011073 invertase Nutrition 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 108091005804 Peptidases Proteins 0.000 claims description 11
- 239000004365 Protease Substances 0.000 claims description 11
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 11
- 240000000111 Saccharum officinarum Species 0.000 claims description 10
- 235000007201 Saccharum officinarum Nutrition 0.000 claims description 10
- 239000000835 fiber Substances 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 9
- 239000012530 fluid Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 235000009508 confectionery Nutrition 0.000 claims description 6
- 239000007921 spray Substances 0.000 claims description 5
- 239000003595 mist Substances 0.000 claims description 4
- 241000282849 Ruminantia Species 0.000 claims description 3
- 239000002023 wood Substances 0.000 claims description 2
- 229930091371 Fructose Natural products 0.000 abstract description 9
- 239000005715 Fructose Substances 0.000 abstract description 9
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 4
- 235000019629 palatability Nutrition 0.000 abstract description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 10
- 229930006000 Sucrose Natural products 0.000 description 10
- 239000005720 sucrose Substances 0.000 description 10
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 7
- 239000008103 glucose Substances 0.000 description 7
- 238000001179 sorption measurement Methods 0.000 description 7
- 229920001277 pectin Polymers 0.000 description 6
- 239000001814 pectin Substances 0.000 description 6
- 235000010987 pectin Nutrition 0.000 description 6
- 241001465754 Metazoa Species 0.000 description 5
- 229920001503 Glucan Polymers 0.000 description 4
- 239000003292 glue Substances 0.000 description 4
- 229920001221 xylan Polymers 0.000 description 4
- 150000004823 xylans Chemical class 0.000 description 4
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 235000018102 proteins Nutrition 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- MIDXCONKKJTLDX-UHFFFAOYSA-N 3,5-dimethylcyclopentane-1,2-dione Chemical compound CC1CC(C)C(=O)C1=O MIDXCONKKJTLDX-UHFFFAOYSA-N 0.000 description 2
- 235000013736 caramel Nutrition 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 235000021050 feed intake Nutrition 0.000 description 2
- 235000012907 honey Nutrition 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- 235000016068 Berberis vulgaris Nutrition 0.000 description 1
- 241000335053 Beta vulgaris Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 235000019728 animal nutrition Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000002503 metabolic effect Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920001184 polypeptide Polymers 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- -1 which also needs to Chemical compound 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Abstract
The invention provides a kind of preparation method of solid molasses feed, comprise the following steps：After molasses are heated, handled with complex enzyme；Molasses after ferment treatment are well mixed with bagasse；By the drying of molasses bagasse mixture, crush.The preparation method of above-mentioned solid molasses feed, by the effect of complex enzyme, the viscosity of molasses is reduced, improves the palatability of the content and molasses of fructose as feed, and make molasses be easier to be well mixed with bagasse, it is easier to dried.
Description
Technical field
The present invention relates to the molasses field of deep of sugar industry, and liquid molasses are converted into solid more particularly to one kind
The preparation method of molasses feed.
Background technology
Molasses are the byproducts of sugar industry, are a kind of sticky, dark brown, semifluid object.Cane molasses contain 24
~36% sucrose, other sugar account for 12~24%；Beet molasses contains about 47% sucrose, soluble colloid (predominantly protein,
Xylan, glucan, pectin etc.）Account for 3~5%；Mineral matter accounts for 8~10%.
Often produce alcohol, glutamic acid, yeast, antibiotic, feed, surfactant by raw material of molasses both at home and abroad at present
Deng.
As feedstuff, molasses are not only a kind of energy feedstuff, but also fast, raising is agreeable to the taste with digesting and assimilating
Property, reduce dust, improve granular mass the advantages that.But have the following disadvantages simultaneously：（1）Liquid molasses viscosity is big, poor fluidity,
It is difficult to be well mixed, influences the homogeneity of feed.（2）Liquid molasses are unfavorable for preserving under the high temperature conditions, due to its contain it is micro-
Nutritional ingredient needed for biological growth, easy moldy metamorphism, with the extension of pot-life, the quality of cane molasses（It can ferment
Property sugar/non-fermentable sugar）Reduce.（3）Liquid molasses need to use special tank car to be transported, and cost of transportation is high.
It is a kind of effective way for solving the above problems that liquid molasses are converted into solid molasses, but existing method for transformation
The shortcomings of power consumption is high, efficiency is low, cost is high mostly be present.
The content of the invention
The greatest problem that liquid molasses are applied to feed is that its viscosity is big, poor fluidity, is difficult to other feedstuffs
It is well mixed.The greatest problem for being converted into solid is that easily absorption is bonded in equipment and coking occurs at high temperature molasses,
So as to influence the quality of the continuous operation of equipment and solid molasses.Molasses can be reduced it is an object of the invention to provide one kind to glue
Spend, improve the solid molasses feed producing method of its feeding value.
A kind of preparation method of solid molasses feed, comprises the following steps：
（1）Molasses are heated to 40~60 DEG C, then add 0.05~0.1% complex enzyme formulation（Based on molasses weight）, stirring is
It is even, 2~5h is reacted, wherein complex enzyme formulation is made up of each component of following mass percent：25 ~ 40% invertase, 5 ~ 10%
Protease, 10 ~ 20% pectase, 10 ~ 20% zytase, 20 ~ 30% dextranase；
（2）Molasses after will be enzyme treated press 1 with bagasse：0.5~1 mixing, and 15~30min is stirred, molasses is uniformly inhaled
It is attached on sugarcane fibre；
（3）Molasses bagasse mixture is broken up, is dried with fluid bed, controls 70~90 DEG C of EAT, controls drying
Molasses bagasse mixture moisture content is 3~8% afterwards；
（4）Dried molasses bagasse mixture is crushed, produces a kind of solid molasses feed.
In one of the embodiments, step（1）In complex enzyme formulation be made up of each component of following mass percent：
30% invertase, 10% protease, 10% pectase, 20% zytase, 30% dextranase.
In one of the embodiments, step（2）The hybrid mode of middle molasses and bagasse is to be made with high pressure Fine spray shower nozzle
Liquid molasses are mixed with mist with bagasse.
In one of the embodiments, step（3）In dried molasses bagasse mixture to can be directly used for feeding anti-
Hay animal.
Above-mentioned solid molasses preparation method, the viscosity of molasses is reduced by compound enzyme effect, makes it easier for uniform adsorption
On bagasse, while the fluff structure of bagasse, drying efficiency can be improved, realizes and is dried with lower temperature, prevents sugar
Honey produces caramel at high temperature.
Embodiment
In order to facilitate the understanding of the purposes, features and advantages of the present invention, below to the specific embodiment party of the present invention
Formula is described in detail.Many details are elaborated in the following description in order to fully understand the present invention.But this hair
Bright to be implemented with being much different from other manner described here, those skilled in the art can be without prejudice in the present invention
Similar improvement is done in the case of culvert, therefore the present invention is not limited to the specific embodiments disclosed below.
The preparation method of the solid molasses feed of one embodiment, comprises the following steps:
Step S100, molasses are heated to 40~60 DEG C, then add 0.05~0.1% complex enzyme formulation（Based on molasses weight）,
Stir, react 2~5h, wherein complex enzyme formulation is made up of each component of following mass percent：25 ~ 40% invertase,
5 ~ 10% protease, 10 ~ 20% pectase, 10 ~ 20% zytase, 20 ~ 30% dextranase；
Preferably, the complex enzyme formulation is made up of each component of following mass percent：30% invertase, 10% albumen
Enzyme, 10% pectase, 20% zytase, 30% dextranase；
After heating, molasses viscosity reduces, and is advantageous to the dispersed of complex enzyme and effect.Pectin, xylan, glucan are not
Only increase the viscosity of molasses, and absorbing for other nutritional ingredients can be also influenceed in entrance animal body, pass through pectase, wood
The degradation of dextranase, dextranase, molasses viscosity can be reduced, improve the utilization rate of other nutritional ingredients.
Protease can be more beneficial for absorbing for animal the degradation of proteins into polypeptide, amino acid.
Sucrose inversion can be glucose, fructose by invertase, and one side glucose, the viscosity of fructose are less than sucrose, can dropped
The viscosity of low sugar honey, on the other hand, the distinctive flavor of fructose, and it is further with glucose, the synergistic function of sucrose, energy
The palatability of molasses is improved, increases feed intake.Other glucose, fructose compare sucrose, directly can be absorbed by animal, and
It is in animal body glucose by metabolic conversion that sucrose, which also needs to, fructose can just be used.
Cane molasses through complex enzyme before and after the processing viscosity and sucrose, glucose, fructose the situation of change of content see the table below：
| Before processing | After processing | |
| Sucrose（%） | 28 | 12 |
| Glucose（%） | 12 | 20 |
| Fructose（%） | 10 | 18 |
| Viscosity（cp） | 4920 | 1829 |
Step S200, the molasses after will be enzyme treated press 1 with bagasse：0.5~1 mixing, and 15~30min is stirred, make molasses
Uniform adsorption is on sugarcane fibre；
Preferably, the hybrid mode of molasses and bagasse is to make liquid molasses with high pressure Fine spray shower nozzle with mist and bagasse
Mixing；
Bagasse structure is fluffy, and space is big, and strong to sugared adsorptivity, but the molasses with being treated by conventional method mix
When, still it is difficult to be well mixed, and be easy to agglomerating.Molasses viscosity after ferment treatment is decreased obviously so that it more holds
Easily it is well mixed with bagasse fibre.The conversion of molasses high pressure Fine spray shower nozzle is nebulized, can preferably make molasses and bagasse
Fiber uniformly contacts, and improves mixing efficiency.Ensure certain mixing time, the partial moisture that can be allowed in molasses is transferred to sugarcane
In slag fiber, be advantageous to follow-up drying.
Step S300, molasses bagasse mixture is broken up, be dried with fluid bed, control EAT 70~90
DEG C, it is 3~8% to control molasses bagasse mixture moisture content after drying；
Preferably, dried molasses bagasse mixture can be directly used for feeding ruminants；
After the molasses bagasse mixture of part conglomeration is broken up, hot blast contact area can be increased, improve drying efficiency, so as to
Drying is completed with lower temperature, in case sugar coking in the drying process, produces caramel.
Step S400, dried molasses bagasse mixture is crushed, produces a kind of solid molasses feed；
Main advantages of the present invention are：
1st, degraded sucrose, pectin, xylan, glucan, protein, effectively reduce molasses viscosity, are easy to follow-up molasses and sugarcane
The mixing of slag.
2nd, the adverse effect that pectin, xylan, glucan absorb to Animal nutrition is reduced.
3rd, increase fructose content, further improve the palatability of molasses, increase feed intake.
4th, drying temperature is low, reduces the generation for being charred taste.
With reference to specific embodiment, the invention will be further elaborated.
Embodiment 1
A kind of preparation method of solid molasses feed, comprises the following steps：
（1）Molasses are heated to 40 DEG C, then add 0.1% complex enzyme formulation（Based on molasses weight）, stir, react 5h,
Wherein complex enzyme formulation is made up of each component of following mass percent：40% invertase, 5% protease, 10% pectin
Enzyme, 20% zytase, 25% dextranase；
（2）Molasses after will be enzyme treated press 1 with bagasse：1 mixing, and 30min is stirred, make molasses uniform adsorption fine in sugarcane
In dimension；
（3）Molasses bagasse mixture is broken up, is dried with fluid bed, controls 90 DEG C of EAT, control sugared after drying
Sweet bagasse mixture moisture content is 3%；
（4）Dried molasses bagasse mixture is crushed, produces a kind of solid molasses feed；
Embodiment 2
A kind of preparation method of solid molasses feed, comprises the following steps：
（1）Molasses are heated to 60 DEG C, then add 0.05% complex enzyme formulation（Based on molasses weight）, stir, react
2h, wherein complex enzyme formulation are made up of each component of following mass percent：25% invertase, 10% protease, 20% fruit
Glue enzyme, 15% zytase, 30% dextranase；
（2）Molasses after will be enzyme treated press 1 with bagasse：0.5 mixing, and 15min is stirred, make molasses uniform adsorption in sugarcane
On fiber；
（3）Molasses bagasse mixture is broken up, is dried with fluid bed, controls 70 DEG C of EAT, control sugared after drying
Sweet bagasse mixture moisture content is 8%；
（4）Dried molasses bagasse mixture is crushed, produces a kind of solid molasses feed；
Embodiment 3
A kind of preparation method of solid molasses feed, comprises the following steps：
（1）Molasses are heated to 50 DEG C, then add 0.08% complex enzyme formulation（Based on molasses weight）, stir, react
3h, wherein complex enzyme formulation are made up of each component of following mass percent：30% invertase, 10% protease, 10% fruit
Glue enzyme, 20% zytase, 30% dextranase；
（2）Molasses after will be enzyme treated press 1 with bagasse：1 mixing, and 20min is stirred, make molasses uniform adsorption fine in sugarcane
In dimension；
（3）Molasses bagasse mixture is broken up, is dried with fluid bed, controls 80 DEG C of EAT, control sugared after drying
Sweet bagasse mixture moisture content is 5%；
（4）Dried molasses bagasse mixture is crushed, produces a kind of solid molasses feed；
Embodiment 4
A kind of preparation method of solid molasses feed, comprises the following steps：
（1）Molasses are heated to 40 DEG C, then add 0.05% complex enzyme formulation（Based on molasses weight）, stir, react
4h, wherein complex enzyme formulation are made up of each component of following mass percent：25% invertase, 10% protease, 20% fruit
Glue enzyme, 20% zytase, 25% dextranase；
（2）Molasses high pressure Fine spray shower nozzle after will be enzyme treated makes molasses with mist and bagasse by 1：0.75 mixing,
And 20min is stirred, make molasses uniform adsorption on sugarcane fibre；
（3）Molasses bagasse mixture is broken up, is dried with fluid bed, controls 70 DEG C of EAT, control sugared after drying
Sweet bagasse mixture moisture content is 8%；
（4）Dried molasses bagasse mixture is crushed, produces a kind of solid molasses feed；
Embodiment 5
A kind of preparation method of solid molasses feed, comprises the following steps：
（1）Molasses are heated to 60 DEG C, then add 0.1% complex enzyme formulation（Based on molasses weight）, stir, react 2h,
Wherein complex enzyme formulation is made up of each component of following mass percent：40% invertase, 10% protease, 10% pectin
Enzyme, 20% zytase, 20% dextranase；
（2）Molasses after will be enzyme treated press 1 with bagasse：0.5 mixing, and 30min is stirred, make molasses uniform adsorption in sugarcane
On fiber；
（3）Molasses bagasse mixture is broken up, is dried with fluid bed, controls 70 DEG C of EAT, control sugared after drying
Sweet bagasse mixture moisture content is 5%（This molasses bagasse mixture can be directly used for feeding ruminants）；
Embodiment described above only expresses the several embodiments of the present invention, and its description is more specific and detailed, but can not
Therefore it is interpreted as the limitation to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art,
Without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the protection model of the present invention
Enclose.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (4)
1. a kind of preparation method of solid molasses feed, it is characterised in that comprise the following steps：
（1）Molasses are heated to 40~60 DEG C, then add 0.05~0.1% complex enzyme formulation（Based on molasses weight）, stirring is
It is even, 2~5h is reacted, wherein complex enzyme formulation is made up of each component of following mass percent：25 ~ 40% invertase, 5 ~ 10%
Protease, 10 ~ 20% pectase, 10 ~ 20% zytase, 20 ~ 30% dextranase；
（2）Molasses after will be enzyme treated press 1 with bagasse：0.5~1 mixing, and 15~30min is stirred, molasses is uniformly inhaled
It is attached on sugarcane fibre；
（3）Molasses bagasse mixture is broken up, is dried with fluid bed, controls 70~90 DEG C of EAT, controls drying
Molasses bagasse mixture moisture content is 3~8% afterwards；
（4）Dried molasses bagasse mixture is crushed, produces a kind of solid molasses feed.
2. the preparation method of solid molasses feed according to claim 1, it is characterised in that step（1）In complex enzyme
Preparation is made up of each component of following mass percent：30% invertase, 10% protease, 10% pectase, 20% wood
Dextranase, 30% dextranase.
3. the preparation method of solid molasses feed according to claim 1, it is characterised in that step（2）Middle molasses with it is sweet
The hybrid mode of bagasse is liquid molasses is mixed with mist with bagasse with high pressure Fine spray shower nozzle.
4. the preparation method of solid molasses feed according to claim 1, it is characterised in that step（3）In it is dried
Molasses bagasse mixture can be directly used for feeding ruminants.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112825962A (en) * | 2021-01-19 | 2021-05-25 | 唐山隆牧饲料有限公司 | Molasses tabletting corn mixed feed and molasses preparation method |
| CN114513962A (en) * | 2019-10-11 | 2022-05-17 | 中部饲料株式会社 | Method for producing cattle feed and cattle feed |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112825962A (en) * | 2021-01-19 | 2021-05-25 | 唐山隆牧饲料有限公司 | Molasses tabletting corn mixed feed and molasses preparation method |
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Effective date of registration: 20240419 Address after: 1901, Building A3, Wealth Center, Third City, Economic Development Zone, Kunming City, Yunnan Province, 650000 Patentee after: Yunnan New Glycogen Bioengineering Co.,Ltd. Country or region after: China Address before: Room 229, A2 / F, biological nano Park, 218 Xinghu street, Suzhou Industrial Park, Jiangsu Province Patentee before: SUZHOU KUNLAN BIOTECHNOLOGY Co.,Ltd. Country or region before: China |