CN107522403A - A kind of blue chun glaze - Google Patents
A kind of blue chun glaze Download PDFInfo
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- CN107522403A CN107522403A CN201710962909.9A CN201710962909A CN107522403A CN 107522403 A CN107522403 A CN 107522403A CN 201710962909 A CN201710962909 A CN 201710962909A CN 107522403 A CN107522403 A CN 107522403A
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- glaze
- blue
- blue chun
- chun glaze
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Glass Compositions (AREA)
- Dental Preparations (AREA)
Abstract
A kind of blue chun glaze, is prepared by the raw material of following parts by weight：40 50 parts of this medicine, 10 14 parts of quartz, 14 18 parts of calcite, 46 parts of talcum, 1.4 1.6 parts of iron oxide, 0.4 0.6 parts of cobalt oxide, 46 parts of Copper Ores, 8 12 parts of zinc frit, 0.4 0.6 parts of bone ash, 6 10 parts of plant ash.Feldspar conventional in conventional formulation is replaced in glaze of the present invention using this medicine, part raw glaze material is replaced using zinc frit, using iron oxide and cobalt oxide coloring and assistant toner, improve aluminium, potassium content in formula, expand firing range, the present invention is burnt traditional process for calcining while high-quality orchid chun glaze is obtained using coal burning or charcoal, can also obtain higher yield rate, improve economy and artistic value.
Description
Technical field
The invention belongs to pottery production technical field, and in particular to a kind of blue chun glaze and preparation method thereof.
Background technology
Pottery is one of five big porcelain of China's Song Dynasty, is world-famous for " transmutation " glaze colours of uniqueness, is Henan Province of China
The exclusive national treasure porcelain in Yuzhou City god Hou towns.Traditional blue glaze in pottery, using natural earthy cobalt as colouring agent, except containing cobalt oxide
Outside, iron oxide is also contained.Modern an ancient unit of weight orchid glaze is general to be adopted using the method for adding oxidation industrial chemicals in order to obtain high yield rate
Firing is burnt with gas to form, because gas burns, firing atmosphere is relatively simple, and plus using industrial chemicals, shortage is using natural crystal coloring
The Determination of multiple metal elements of agent, the blue chun glaze glaze colours dullness for causing firing to form is gorgeous, lacks simple and unsophisticated cultured wind.
The content of the invention
The purpose of the present invention is that provides one kind using traditional method for cooking, yield rate to solve the deficiencies in the prior art
High, glaze colours primitive simplicity and nature blue chun glaze and preparation method thereof.
The purpose of the present invention is realized with following technical proposals：
A kind of blue chun glaze, is prepared by the raw material of following parts by weight：This medicine 40-50 parts, quartzy 10-14 parts, calcite 14-18
Part, talcum 4-6 parts, iron oxide 1.4-1.6 parts, cobalt oxide 0.4-0.6 parts, Copper Ores 4-6 parts, zinc frit 8-12 parts, bone ash
0.4-0.6 parts, plant ash 6-10 parts.
Preferably, it is prepared by the raw material of following parts by weight：45 parts of this medicine, 12 parts of quartz, 16 parts of calcite, talcum 5
Part, 1.5 parts of iron oxide, 0.5 part of cobalt oxide, 5 parts of Copper Ores, 10 parts of zinc frit, 0.5 part of bone ash, 8 parts of plant ash.
The zinc frit Zn content is more than 15%.
The preparation method of blue chun glaze as described above, it is characterised in that comprise the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Glazing；
（3）Burnt using coal or charcoal firing method is burnt till, firing temperature is 1260-1300 DEG C.
Step（1）Middle glaze slip mass concentration is 54-56%.
Step（2）It is middle to use leaching glaze method glazing, and soak glaze twice.
Step（3）Specifically burning till step is：1. oxidation stage：Base substrate after glazing is put into kiln, under oxidizing atmosphere
Fire, temperature is ramped up 1000-1050 DEG C in 4-6h；2. reduction phase：Under reducing atmosphere, make temperature uniform in 5-6h
Rise to 1260-1300 DEG C；3. cooling stage：Room temperature is naturally cooled to, is made.
Feldspar conventional in conventional formulation is replaced in glaze of the present invention using this medicine, part raw glaze is replaced using zinc frit
Material, using iron oxide and cobalt oxide coloring and assistant toner, aluminium, potassium content in formula are improved, expands firing range, adopts the present invention
Burnt with coal or charcoal burns traditional process for calcining while high-quality orchid chun glaze is obtained, can also obtained higher yield rate, improve warp
Ji and artistic value.
Embodiment
Embodiment 1
A kind of blue chun glaze, is prepared by the raw material of following parts by weight：This medicine 40-50 parts, quartzy 10-14 parts, calcite 14-18
Part, talcum 4-6 parts, iron oxide 1.4-1.6 parts, cobalt oxide 0.4-0.6 parts, Copper Ores 4-6 parts, zinc frit 8-12 parts, bone ash
0.4-0.6 parts, plant ash 6-10 parts.Zn content is more than 15% in zinc frit.
The preparation method of above-mentioned blue chun glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；Glaze slip mass concentration is 54-56%；
（2）Using leaching glaze method glazing, and soak glaze twice；
（3）Burnt using coal or charcoal firing method is burnt till, specifically burning till step is：1. oxidation stage：Base substrate after glazing is put into kiln
In, fired under oxidizing atmosphere, temperature is ramped up 1000-1050 DEG C in 4-6h；2. reduction phase：Under reducing atmosphere,
Temperature is set to be ramped up 1260-1300 DEG C in 5-6h；3. cooling stage：Room temperature is naturally cooled to, is made.
This medicine, quartz, calcite, talcum, Copper Ores originate from Yuzhou in the present invention, wherein, this medicine is Yuzhou
A kind of natural glaze stone, its essential mineral is anorthite, quartz and albite, and iron-holder is higher, and feldspar is compared in this formula
Glaze colours is more conducive to be formed；The predominant amount of quartz is silica, it is possible to increase the melting temperature and viscosity of glaze, can be more
Lyotrope CaO, Na2O、K2O, MgO meltings generation transparence quartz glass, make glaze paint bright, improve the glossiness of pottery；Side
It is calcium oxide to solve stone main component, is cosolvent, by increasing capacitance it is possible to increase hardness, abrasion resistance and the corrosion resistance of glaze, reduces the molten of glaze
Melt temperature, increase the glossiness and transparency of glaze colours, the cracking of preventing and treating glaze paint and accumulation；Talcum is magnesium silicate mineral, plays milkiness
And fluxing action；Bone ash is preferably the ash after ox bone burns, and its main component is calcium phosphate, calcium carbonate etc., had both been opacifiers, and had made again
Glaze colours primitive simplicity and nature after burning till；Plant ash is introduced primarily into phosphorus, magnesium, calcium constituent, both makees cosolvent, and helps together with bone ash simple and unsophisticated
Glaze colours is formed, meanwhile, the potassium that plant ash introduces can expand firing range；Zinc frit replaces part raw glaze material, can reduce glaze slip
Layering, contribute to cover-coat enamel and ground-coat enamel to merge, while reduce glaze layer surface and bubble be present, influence yield rate, zinc in zinc frit and
Copper in iron oxide, cobalt oxide and Copper Ores is main colouring agent, toner, can improve burnt using coal, charcoal burns the side of burning till
The yield rate of method, meanwhile, the raw material compared with multiple metallic element is contained using this medicine, Copper Ores, plant ash etc., contributes to transmutation glaze colours
Formation；Therefore, the present invention is by optimizing glaze formula, and by improving firing range, and synthesis using chemical industry colouring agent and is drawn
In the case of entering other more metallic elements, using traditional process for calcining, high yield rate, blue an ancient unit of weight of glaze colours primitive simplicity and nature are obtained
Glaze, its yield rate is typically more than 85%.
Embodiment 2
A kind of blue chun glaze, is prepared by the raw material of following parts by weight：45 parts of this medicine, 12 parts of quartz, 16 parts of calcite, talcum 5
Part, 1.5 parts of iron oxide, 0.5 part of cobalt oxide, 5 parts of Copper Ores, 10 parts of zinc frit, 0.5 part of bone ash, 8 parts of plant ash.
The preparation method of above-mentioned blue chun glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；Glaze slip mass concentration is 55%；
（2）Using leaching glaze method glazing, and soak glaze twice；
（3）Burnt using coal or charcoal firing method is burnt till, specifically burning till step is：1. oxidation stage：Base substrate after glazing is put into kiln
In, fired under oxidizing atmosphere, temperature is ramped up 1020 DEG C in 5h；2. reduction phase：Under reducing atmosphere, temperature is made to exist
5-6h is ramped up 1260-1300 DEG C；3. cooling stage：Room temperature is naturally cooled to, is made.The firing temperature of general chun glaze is
1280-1300 DEG C, burnt using coal, traditional process for calcining difficult point is that the unmanageable of firing temperature such as charcoal burns, the present invention is logical
Expansion firing range is crossed, improves yield rate.
The formula for the blue chun glaze that 3-18 of the embodiment of the present invention is provided is shown in Table 1-2, and other are the same as embodiment 2.
Claims (7)
1. a kind of blue chun glaze, it is characterised in that be prepared by the raw material of following parts by weight：This medicine 40-50 parts, quartzy 10-14
Part, calcite 14-18 parts, talcum 4-6 parts, iron oxide 1.4-1.6 parts, cobalt oxide 0.4-0.6 parts, Copper Ores 4-6 parts, zinc frit
8-12 parts, bone ash 0.4-0.6 parts, plant ash 6-10 parts.
2. blue chun glaze as claimed in claim 1, it is characterised in that be prepared by the raw material of following parts by weight：45 parts of this medicine,
12 parts of quartz, 16 parts of calcite, 5 parts of talcum, 1.5 parts of iron oxide, 0.5 part of cobalt oxide, 5 parts of Copper Ores, 10 parts of zinc frit, bone ash
0.5 part, 8 parts of plant ash.
3. the blue chun glaze as described in claim any one of 1-2, it is characterised in that the zinc frit Zn content is more than 15%.
4. the preparation method of the blue chun glaze as described in claim any one of 1-3, it is characterised in that comprise the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Glazing；
（3）Burnt using coal or charcoal firing method is burnt till, firing temperature is 1260-1300 DEG C.
5. the preparation method of blue chun glaze as claimed in claim 4, it is characterised in that step（1）Middle glaze slip mass concentration is 54-
56%。
6. the preparation method of blue chun glaze as claimed in claim 4, it is characterised in that step（2）It is middle to use leaching glaze method glazing,
And soak glaze twice.
7. the preparation method of blue chun glaze as claimed in claim 4, it is characterised in that step（3）Specifically burning till step is：1. oxygen
The change stage：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, temperature is ramped up 1000-1050 in 4-6h
℃；2. reduction phase：Under reducing atmosphere, temperature is made to be ramped up 1260-1300 DEG C in 5-6h；3. cooling stage：Naturally it is cold
But to room temperature, it is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710962909.9A CN107522403A (en) | 2017-10-16 | 2017-10-16 | A kind of blue chun glaze |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710962909.9A CN107522403A (en) | 2017-10-16 | 2017-10-16 | A kind of blue chun glaze |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107522403A true CN107522403A (en) | 2017-12-29 |
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ID=60685281
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710962909.9A Withdrawn CN107522403A (en) | 2017-10-16 | 2017-10-16 | A kind of blue chun glaze |
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| Country | Link |
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| CN (1) | CN107522403A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109020227A (en) * | 2018-09-19 | 2018-12-18 | 张诚明 | A kind of production method of the blue chun glaze pottery with asterism pattern |
| CN109627055A (en) * | 2019-02-15 | 2019-04-16 | 天津水泥工业设计研究院有限公司 | A kind of additive and potassium-bearing mineral fertilizer for widening potassium-bearing mineral fertilizer firing range |
| CN113896422A (en) * | 2021-11-18 | 2022-01-07 | 福建省德化县顺华达瓷业有限责任公司 | Furnace transmutation blue glaze, preparation method thereof and glaze firing method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106145683A (en) * | 2016-08-18 | 2016-11-23 | 温书强 | A kind of peacock blue pottery glaze and preparation method thereof |
| CN107010834A (en) * | 2017-05-24 | 2017-08-04 | 禹州市神器钧窑有限公司 | A kind of Lu's chun glaze |
-
2017
- 2017-10-16 CN CN201710962909.9A patent/CN107522403A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106145683A (en) * | 2016-08-18 | 2016-11-23 | 温书强 | A kind of peacock blue pottery glaze and preparation method thereof |
| CN107010834A (en) * | 2017-05-24 | 2017-08-04 | 禹州市神器钧窑有限公司 | A kind of Lu's chun glaze |
Non-Patent Citations (2)
| Title |
|---|
| （美）泰勒: "《釉 釉料及陶瓷颜色配制手册》", 30 November 2015, 上海科学技术出版社 * |
| 孙彦春等: "《中国钧窑研究与探索》", 31 July 2011, 中州古籍出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109020227A (en) * | 2018-09-19 | 2018-12-18 | 张诚明 | A kind of production method of the blue chun glaze pottery with asterism pattern |
| CN109627055A (en) * | 2019-02-15 | 2019-04-16 | 天津水泥工业设计研究院有限公司 | A kind of additive and potassium-bearing mineral fertilizer for widening potassium-bearing mineral fertilizer firing range |
| CN109627055B (en) * | 2019-02-15 | 2021-09-14 | 天津水泥工业设计研究院有限公司 | Additive for widening firing range of potassium-containing mineral fertilizer and potassium-containing mineral fertilizer |
| CN113896422A (en) * | 2021-11-18 | 2022-01-07 | 福建省德化县顺华达瓷业有限责任公司 | Furnace transmutation blue glaze, preparation method thereof and glaze firing method |
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Application publication date: 20171229 |