CN107513714B - 一种锄头防锈液及其制备方法 - Google Patents
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- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 30
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000843 powder Substances 0.000 claims abstract description 11
- 239000010456 wollastonite Substances 0.000 claims abstract description 11
- 229910052882 wollastonite Inorganic materials 0.000 claims abstract description 11
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 9
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 claims abstract description 9
- 235000019795 sodium metasilicate Nutrition 0.000 claims abstract description 9
- 235000015393 sodium molybdate Nutrition 0.000 claims abstract description 9
- 239000011684 sodium molybdate Substances 0.000 claims abstract description 9
- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 claims abstract description 9
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 9
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims abstract description 8
- 235000019799 monosodium phosphate Nutrition 0.000 claims abstract description 8
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims abstract description 8
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 claims abstract description 8
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 7
- 229960004025 sodium salicylate Drugs 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 6
- 238000000498 ball milling Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 2
- 239000011734 sodium Substances 0.000 claims 2
- 229910052708 sodium Inorganic materials 0.000 claims 2
- RZYKUPXRYIOEME-UHFFFAOYSA-N CCCCCCCCCCCC[S] Chemical compound CCCCCCCCCCCC[S] RZYKUPXRYIOEME-UHFFFAOYSA-N 0.000 claims 1
- SEGLCEQVOFDUPX-UHFFFAOYSA-N di-(2-ethylhexyl)phosphoric acid Chemical compound CCCCC(CC)COP(O)(=O)OCC(CC)CCCC SEGLCEQVOFDUPX-UHFFFAOYSA-N 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- DAJSVUQLFFJUSX-UHFFFAOYSA-M sodium;dodecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCS([O-])(=O)=O DAJSVUQLFFJUSX-UHFFFAOYSA-M 0.000 claims 1
- 230000007797 corrosion Effects 0.000 abstract description 3
- 238000005260 corrosion Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 2
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/08—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids
- C23F11/18—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using inorganic inhibitors
- C23F11/187—Mixtures of inorganic inhibitors
- C23F11/188—Mixtures of inorganic inhibitors containing phosphates
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/08—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids
- C23F11/10—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using organic inhibitors
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- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
本发明公开了一种锄头防锈液及其制备方法，按重量份计，其组成原料为：磷酸二氢钠6‑8、硅酸钠5.5‑6.0、硅灰石粉15‑17、钼酸钠3.5‑5.5、水杨酸钠3‑4、邻苯二甲酸二丁酯6‑8、十二烷基磺酸钠3‑5、硬脂酸锌8‑9、醋酸乙酯30‑35；与现有技术相比，本发明的防锈液中各组分环保，无毒，且制备方法简单，成本低，对锄头具有很好的防锈保护作用，延长了农具锄头的使用寿命。
Description
技术领域
本发明涉及一种防锈液，具体涉及一种锄头防锈液及其制备方法。
背景技术
农具是经常使用的工具之一，如果接触环境存在湿度高等情况，农具的生锈现象会比较严重，如何避免农具生锈有很多种方法，可以在农具表面喷涂防锈液，也可以在农具生锈后使用其他方式对锈迹进行处理，消除锈斑，目前的防锈液耐腐蚀性能较差，农具锄头在日常生活中经常性遇到生锈现象。
发明内容
为了缓解现有技术的不足和缺陷，本发明的目的在于提供一种锄头防锈液及其制备方法。
为了实现上述目的，本发明采用如下技术方案：
锄头防锈液，按重量份计，其组成原料为：磷酸二氢钠6-8、硅酸钠5.5-6.0、硅灰石粉15-17、钼酸钠3.5-5.5、水杨酸钠3-4、邻苯二甲酸二丁酯6-8、十二烷基磺酸钠3-5、硬脂酸锌8-9、醋酸乙酯30-35。
锄头防锈液，按重量份计，其组成原料为：磷酸二氢钠7、硅酸钠5.8、硅灰石粉16、钼酸钠4.5、水杨酸钠3.5、邻苯二甲酸二丁酯7、十二烷基磺酸钠4、硬脂酸锌8.5、醋酸乙酯32。
锄头防锈液的制备方法，具体包括以下内容：
(1)称取硅酸钠、硅灰石粉、钼酸钠，加入适量醋酸乙酯，球磨3-4小时，混合均匀；
(2)将上述步骤(1)混合料倒入醋酸乙酯中，然后再依次加入磷酸二氢钠、水杨酸钠、邻苯二甲酸二丁酯、十二烷基磺酸钠、硬脂酸锌，升温至体系60-70℃，搅拌使完全溶解，冷却即得。
所述的硅灰石粉为100-200目粉剂。
本发明的有益效果：
与现有技术相比，本发明的防锈液中各组分环保，无毒，且制备方法简单，成本低，对锄头具有很好的防锈保护作用，延长了农具锄头的使用寿命。
具体实施方式
实施例1：锄头防锈液，按重量份计，其组成原料为：磷酸二氢钠7、硅酸钠5.8、硅灰石粉16、钼酸钠4.5、水杨酸钠3.5、邻苯二甲酸二丁酯7、十二烷基磺酸钠4、硬脂酸锌8.5、醋酸乙酯32。
锄头防锈液的制备方法，具体包括以下内容：
(1)称取硅酸钠、硅灰石粉、钼酸钠，加入适量醋酸乙酯，球磨3-4小时，混合均匀；
(2)将上述步骤(1)混合料倒入醋酸乙酯中，然后再依次加入磷酸二氢钠、水杨酸钠、邻苯二甲酸二丁酯、十二烷基磺酸钠、硬脂酸锌，升温至体系60-70℃，搅拌使完全溶解，冷却即得。
所述的硅灰石粉为100-200目粉剂。
Claims (4)
1.一种锄头防锈液，其特征在于，按重量份计，其组成原料为：磷酸二氢钠6-8、硅酸钠5.5-6.0、硅灰石粉15-17、钼酸钠3.5-5.5、水杨酸钠3-4、邻苯二甲酸二丁酯6-8、十二烷基磺酸钠3-5、硬脂酸锌8-9、醋酸乙酯30-35。
2.根据权利要求1所述的锄头防锈液，其特征在于，按重量份计，其组成原料为：磷酸二氢钠7、硅酸钠5.8、硅灰石粉16、钼酸钠4.5、水杨酸钠3.5、邻苯二甲酸二丁酯7、十二烷基磺酸钠4、硬脂酸锌8.5、醋酸乙酯32。
3.一种如权利要求1所述的锄头防锈液的制备方法，其特征在于，具体包括以下内容：
(1)称取硅酸钠、硅灰石粉、钼酸钠，加入适量醋酸乙酯，球磨3-4小时，混合均匀；
(2)将上述步骤（1）混合料倒入醋酸乙酯中，然后再依次加入磷酸二氢钠、水杨酸钠、邻苯二甲酸二丁酯、十二烷基磺酸钠、硬脂酸锌，升温至体系60-70℃，搅拌使完全溶解，冷却即得。
4.根据权利要求1所述的锄头防锈液，其特征在于，所述的硅灰石粉为100-200目粉剂。
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| CN102372954A (zh) * | 2010-08-16 | 2012-03-14 | 南通市通州区金晨涂料厂 | 一种无味防锈底漆 |
| CN101967316B (zh) * | 2010-09-08 | 2013-01-09 | 中国乐凯胶片集团公司 | 一种用于海洋船舶与设施的无毒防污涂料及其制备方法 |
| CN103014740A (zh) * | 2011-09-20 | 2013-04-03 | 孙善家 | 一种新型除锈清洁剂 |
| CN102690558B (zh) * | 2012-05-31 | 2013-05-29 | 蓬莱蔚阳新材料有限公司 | 带锈防锈重防腐涂料的制备工艺 |
| CN104387972A (zh) * | 2014-11-14 | 2015-03-04 | 无锡伊佩克科技有限公司 | 一种船底彩色硬膜防锈油及其制备方法 |
| CN104479433A (zh) * | 2014-12-18 | 2015-04-01 | 无锡伊佩克科技有限公司 | 一种船底涂布用水性防锈涂料及其制备方法 |
| CN105174778A (zh) * | 2015-09-16 | 2015-12-23 | 桂林市和鑫防水装饰材料有限公司 | 一种硅酸钠防水剂 |
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