CN107496287B - Whole plant synthetic surfactant-free cleansing product - Google Patents
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a full-plant synthetic surfactant-free face cleaning product, aiming at providing a face cleaning product which only contains natural surfactant, does not contain other chemical synthetic surfactant and has good skin cleaning effect, and the technical scheme is that the face cleaning product comprises 5-30% of soapberry extract, 10-30% of foam stabilizer, 0.8-1.2% of plant preservative and the balance of water according to 100% of the total mass; the foam stabilizer consists of hydrogenated starch hydrolysate and glycosyl trehalose according to the mass ratio of 0.5: 1.2-1.6; belongs to the technical field of skin care products.
Description
Technical Field
The invention discloses a face cleaning product, in particular to a full-plant synthetic surfactant-free face cleaning product, belonging to the technical field of skin care products.
Background
Cleansing as a basic project of skin care, along with the increasing deterioration of the environment and the decreasing air quality, the cleansing plays an essential and important role in daily life.
Most of common face cleaning products in the market at present are based on surfactants, and a considerable amount of surfactants interact with the horny layer in the face cleaning process, so that part of the horny layer lipid can be dissolved while cleaning, and the skin is dried; some surfactants also interact with stratum corneum proteins, causing protein denaturation and damage to sensitive skin.
The non-soap base type face cleaning product mainly containing amino acid type surfactant has good skin-friendly property and small irritation, but has weak detergency, and can obtain a face cleaning product with excellent foamability and water solubility only by reasonable compatibility with other surfactants, so the components are complex.
Under the trend of 'Chongshang green and returning to nature', the safe and reliable natural surfactant is used for replacing a chemical synthesis surfactant, and the future development trend of the face cleaning product is realized.
Sapindus mukorossi is a common washing product in China, and aril of the Sapindus mukorossi contains abundant glucoside substances (mainly triterpenoid saponin and sesquiterpene glucoside), has the content of about 4 percent, has good foamability and strong decontamination capability, and is called as natural plant soap. However, with the continuous progress of science and technology, more and more chemically synthesized detergents come out and soapberry becomes a dull proposition. The soapberry serving as a natural nonionic surfactant is easy to biodegrade, has good affinity with the skin, accords with the concept of 'Chongshang green and returning to nature', and can meet the ever-increasing psychological demands of consumers on green and safe face cleaning products.
The foam has surface tension which can increase the contact of the surfactant with the skin, and the dirt carrying capacity is increased to a certain extent, and the foam quality of the face cleansing product is closely related to the popularity. The foaming ability and foam stability of the soapberry extract increase with the increase of the pH value of the solution, and the soapberry extract exists in a non-ionic form in an acidic solution, so that the foam performance is poor. The existing research shows that the compounding of the soapberry extract and the nonionic surfactant can obviously enhance the foam stabilizing performance of the system, but the addition of other nonionic surfactants in the face cleaning formula has complex components and is not green and safe enough, and the soapberry saponin has the functions of expanding skin capillaries and hemolysis and particularly has strong stimulation to eyes, so that the soapberry extract can not be directly used for cleaning and washing the face even though the soapberry extract has good washing effect.
At present, no weak acid facial cleanser with good foam stabilizing performance by taking the soapberry extract as a surfactant alone exists.
Disclosure of Invention
In view of the above disadvantages, the present invention aims to provide a facial cleanser containing only natural surfactants, and no other chemically synthesized surfactants, and having good skin cleansing effect.
Therefore, the technical scheme provided by the invention is as follows:
a whole plant synthetic surfactant-free face cleaning product comprises, by total mass 100%, 5-30% of soapberry extract, 10-30% of foam stabilizer, 0.8-1.2% of plant preservative, and the balance of water; the foam stabilizer consists of hydrogenated starch hydrolysate and glycosyl trehalose according to the mass ratio of 0.5: 1.2-1.6.
As a further preferred aspect of the invention, the whole plant synthetic surfactant-free facial cleanser is a plant preservative A or a preservative B or a mixture of the preservative A and the preservative B, wherein the preservative A comprises a celandine extract, a cornflower extract and a myrobalan extract in a mass ratio of 3:2:3, and the preservative B comprises a zanthoxylum piperitum extract, a pulsatilla extract and a usnea barbata extract in a mass ratio of 3:2: 4.
As a further preferred aspect of the present invention, in the above all-plant synthetic surfactant-free facial cleanser, the soapberry extract is prepared by sequentially performing the following steps: weighing 20-40 parts by weight of soapberry peel, placing the soapberry peel in 280 parts by weight of plant fermentation liquor for soaking for 20 days, carrying out low-temperature vacuum drying on the soaked soapberry peel at 0-4 ℃, carrying out superfine grinding on the frozen soapberry, adding 20-80% of ethanol into the soapberry fine powder at a material-liquid ratio of 1:40-60, carrying out ultrasonic extraction at 25 ℃ for 20min at an ultrasonic frequency of 1.5-2.0MHz, filtering with a microporous filter membrane, collecting filtrate, loading the filtrate into a macroporous adsorption resin column, washing with water until the filtrate is colorless, eluting with 20-80% of ethanol until the eluate is colorless, collecting ethanol eluate, carrying out membrane concentration to remove ethanol, and carrying out spray drying to obtain the soapberry extract.
As a further preferred aspect of the present invention, the whole plant synthetic surfactant-free facial cleanser is prepared by sequentially performing the following steps of: weighing 25-40 parts by weight of roselle flower and 30-50 parts by weight of ailanthus altissima, drying, crushing to 20-80 meshes, and uniformly mixing to obtain mixed powder; adding water 40-50 times the weight of the mixed powder, adding lactobacillus liquid 10-30% of the total volume of the mixed solution, fermenting at 25-30 deg.C for 2-3 months, filtering, centrifuging, collecting supernatant, and vacuum concentrating to 1/4 of the original volume to obtain plant fermentation liquid.
In a further preferred embodiment of the present invention, the above all-plant synthetic surfactant-free cleansing product is a lactobacillus liquid having a concentration of 105-108CFU/ml。
Compared with the prior art, the technical scheme provided by the invention has the following beneficial effects:
1. the technical scheme provided by the invention only contains a plurality of components of soapberry extract, hydrogenated starch hydrolysate, glycosyl trehalose, loosestrife extract, cornflower extract and myrobalan extract (or zanthoxylum fruit extract, pulsatilla extract and usnea extract), and the components are simple, all of the components are derived from natural plants, and the surfactant does not contain other chemically synthesized surfactants and has no harm to skin.
2. The soapberry extract provided by the invention is soapberry saponin, and the minimum addition amount of the soapberry extract is 5%, namely the soapberry extract has the advantages of small dosage, good effect and low cost.
3. According to the technical scheme provided by the invention, the hydrogenated starch hydrolysate and the glycosyl trehalose are conventional moisturizing agents in the field, but the hydrogenated starch hydrolysate and the glycosyl trehalose are compounded according to a specific ratio of 0.5:1.4 and then are used as a foam stabilizer to be used, and are synergized with the soapberry extract, so that a abundant, three-dimensional, dense and good-lasting facial cleaning product is obtained.
Wherein, the hydrogenated starch hydrolysate is a polyhydric sugar alcohol mixture obtained by hydrolyzing and hydrogenating starch, contains not only mono-polyhydric sugar alcohol and bi-polyhydric sugar alcohol, but also a large amount of hydrogenated oligosaccharide and hydrogenated polysaccharide, and has physicochemical properties of moisture retention and crystallization prevention; glycosyl trehalose (glycotrehalose trehalase) is a polysaccharide from maize; the two components interact with the soapberry extract, and also play a good role in moisturizing.
4. According to the technical scheme, the plant preservative is a preservative combination A or a preservative combination B or a preservative combination A and a preservative combination B, the preservative combination A is composed of a loosestrife extract, a cornflower extract and a myrobalan extract according to a specific ratio of 3:2:3, the preservative combination B is composed of a zanthoxylum piperitum extract, a pulsatilla chinensis extract and a usnea barbata extract according to a specific ratio of 3:2:4, and the preservative combination A or the preservative combination B interacts with the soapberry extract, a hydrogenated starch hydrolysate and glycosyl trehalose, so that the preservative can be used as a preservative of a face cleaning product, can assist the soapberry extract in inhibiting harmful bacteria after face cleaning, and can regulate microbial ecological balance of the face.
In summary, the whole-plant synthetic surfactant-free facial cleanser provided by the invention successfully applies the soapberry extract as a surfactant alone to a weakly acidic facial cleanser, has good foam density, foam persistence and cleaning power, and is mild and non-irritant to skin during cleaning.
Detailed Description
The following claims are further defined in conjunction with the detailed description of the invention and are not to be construed as limiting the invention in any way, as any number of variations may be made by anyone within the scope of the claims.
It should be noted that the process parameters, raw materials and the like which are not described in detail in the present invention are performed according to the conventional technical means in the art.
Example 1
The invention provides a full-plant synthetic surfactant-free face cleaning product, which comprises 30g of soapberry extract, 23.5g of foam stabilizer, 0.8g of plant preservative and the balance of water, wherein the total mass is 100 g.
Wherein: the foam stabilizer consists of hydrogenated starch hydrolysate and glycosyl trehalose according to the mass ratio of 0.5: 1.2; the plant preservative comprises a zanthoxylum bungeanum maxim fruit extract, a pulsatilla chinensis bunge extract and an usnea barbata extract according to a ratio of 3:2: 4.
The soapberry extract is prepared by the following steps in sequence: weighing 40 parts by weight of soapberry pericarp, placing the soapberry pericarp in 150 parts by weight of plant fermentation liquor for soaking for 20 days, carrying out vacuum drying on the soaked soapberry pericarp at the low temperature of 0 ℃, carrying out superfine grinding on the frozen soapberry, adding 60mL of 20% ethanol (the material-liquid ratio is 1:60) into each gram of soapberry fine powder, carrying out ultrasonic extraction at the temperature of 25 ℃ for 20min, wherein the ultrasonic frequency is 2.0MHz, filtering by using a microporous filter membrane, collecting filtrate, loading the filtrate onto a macroporous adsorption resin column, washing by using water until the filtrate is colorless, eluting by using 80% ethanol until the eluent is colorless, collecting ethanol eluent, carrying out membrane concentration to remove ethanol, and carrying out spray drying to obtain the soapberry extract.
The plant fermentation liquor is prepared by the following steps in sequence: weighing 40 parts by weight of roselle flower and 50 parts by weight of ailanthus altissima, drying, crushing to 80 meshes, and uniformly mixing to obtain mixed powder; adding water with the volume 50 times of the weight of the mixed powder, and then adding lactobacillus liquid with the concentration of 10 percent in the total volume of the mixed liquid8CFU/ml, fermenting at 25 deg.C for 3 months, filtering, centrifuging, collecting supernatant, and vacuum concentrating to 1/4 to obtain plant fermentation liquid.
Example 2
The invention provides a full-plant synthetic surfactant-free face cleaning product, which comprises 20g of soapberry extract, 14.5g of foam stabilizer, 1.2g of plant preservative and the balance of water, wherein the total mass is 100 g.
Wherein: the foam stabilizer consists of hydrogenated starch hydrolysate and glycosyl trehalose according to the mass ratio of 0.5: 1.6; the plant preservative comprises a zanthoxylum bungeanum maxim fruit extract, a pulsatilla chinensis bunge extract and an usnea barbata extract according to the mass ratio of 3:2: 4.
The soapberry extract is prepared by the following steps in sequence: weighing 40 parts by weight of soapberry pericarp, placing the soapberry pericarp in 280 parts by weight of plant fermentation liquor for soaking for 20 days, carrying out vacuum drying on the soaked soapberry pericarp at a low temperature of 4 ℃, carrying out superfine grinding on the frozen soapberry, adding 60mL of 80% ethanol (the material-liquid ratio is 1:60) into each gram of soapberry fine powder, carrying out ultrasonic extraction at a temperature of 25 ℃ for 20min, wherein the ultrasonic frequency is 2.0MHz, filtering by using a microporous filter membrane, collecting filtrate, placing the filtrate on a macroporous adsorption resin column, washing the filtrate until the filtrate is colorless, eluting the filtrate by using 80% ethanol until the eluate is colorless, collecting ethanol eluate, carrying out membrane concentration to remove ethanol, and carrying out spray drying to obtain the soapberry extract.
The plant fermentation liquor is prepared by the following steps in sequence: weighing 25 parts by weight of roselle flower and 50 parts by weight of ailanthus altissima, drying, crushing to 20 meshes, and uniformly mixing to obtain mixed powder; adding water with the volume 40 times of the weight of the mixed powder, and then adding lactobacillus liquid with the concentration of 10 percent in the total volume of the mixed liquid8CFU/ml, fermenting at 25 deg.C for 2 months, filtering, centrifuging, collecting supernatant, and vacuum concentrating to 1/4 to obtain plant fermentation liquid.
Example 3
The invention provides a full-plant synthetic surfactant-free face cleaning product, which comprises 5g of soapberry extract, 15g of foam stabilizer, 1g of plant preservative and the balance of water, wherein the total mass is 100 g.
Wherein: the foam stabilizer consists of hydrogenated starch hydrolysate and glycosyl trehalose according to the mass ratio of 0.5: 1.4; the plant preservative comprises a loosestrife extract, a cornflower extract and a myrobalan fruit extract according to a mass ratio of 3:2: 3.
The soapberry extract is prepared by the following steps in sequence: weighing 30 parts by weight of soapberry pericarp, placing the soapberry pericarp in 200 parts by weight of plant fermentation liquor for soaking for 20 days, carrying out vacuum drying on the soaked soapberry pericarp at the low temperature of 2 ℃, carrying out superfine grinding on the frozen soapberry, adding 50mL of 50% ethanol (the material-liquid ratio is 1:50) into each gram of soapberry fine powder, carrying out ultrasonic extraction at the temperature of 25 ℃ for 20min, wherein the ultrasonic frequency is 1.8MHz, filtering by using a microporous filter membrane, collecting filtrate, loading the filtrate onto a macroporous adsorption resin column, washing by using water until the filtrate is colorless, eluting by using 50% ethanol until the eluent is colorless, collecting ethanol eluent, carrying out membrane concentration to remove ethanol, and carrying out spray drying to obtain the soapberry extract.
The plant fermentation liquor is prepared by the following steps in sequence: weighing 30 parts by weight of roselle flower and 40 parts by weight of ailanthus altissima, drying, crushing to 50 meshes, and uniformly mixing to obtain mixed powder; adding water with the volume 40 times of the weight of the mixed powder, and then adding lactobacillus liquid with the concentration of 10 percent in the total volume of the mixed liquid6CFU/ml, fermenting at 28 deg.C for 2 months, filtering, centrifuging, collecting supernatant, and vacuum concentrating to 1/4 to obtain plant fermentation liquid.
Example 4
The invention provides a full-plant synthetic surfactant-free face cleaning product, which comprises 10g of soapberry extract, 21g of foam stabilizer, 0.9 of plant preservative and the balance of water, wherein the total mass is 100 g.
Wherein: the foam stabilizer consists of hydrogenated starch hydrolysate and glycosyl trehalose according to the mass ratio of 0.5: 1.5; the plant preservative is prepared by mixing a preservative A and a preservative B according to the mass ratio of 1: 1; the plant preservative A consists of a loosestrife extract, a cornflower extract and a myrobalan fruit extract according to the mass ratio of 3:2: 3; the plant preservative B is prepared from a zanthoxylum bungeanum fruit extract, a pulsatilla chinensis extract and a usnea barbata extract according to a ratio of 3:2: 4.
The soapberry extract is prepared by the following steps in sequence: weighing 35 parts by weight of soapberry pericarp, placing the soapberry pericarp in 250 parts by weight of plant fermentation liquor for soaking for 20 days, carrying out vacuum drying on the soaked soapberry pericarp at a low temperature of 3 ℃, carrying out superfine grinding on the frozen soapberry, adding 50mL of 60% ethanol (the material-liquid ratio is 1:50) into each gram of soapberry fine powder, carrying out ultrasonic extraction at a temperature of 25 ℃ for 20min, wherein the ultrasonic frequency is 1.6MHz, filtering by using a microporous filter membrane, collecting filtrate, loading the filtrate onto a macroporous adsorption resin column, washing with water until the filtrate is colorless, eluting with 40% ethanol until the eluate is colorless, collecting ethanol eluate, carrying out membrane concentration to remove ethanol, and carrying out spray drying to obtain the soapberry extract.
The plant fermentation liquor is prepared by the following steps in sequence: weighing 35 parts by weight of roselle flower and 40 parts by weight of ailanthus altissima, drying, crushing to 50 meshes, and uniformly mixing to obtain mixed powder; adding water with the volume being 45 times of the weight of the mixed powder, then adding lactobacillus liquid with the concentration being 105CFU/ml and the total volume being 20% of the total volume of the mixed liquid, fermenting for 2 months at the temperature of 28 ℃, filtering, centrifuging, taking supernatant, and concentrating in vacuum to 1/4 with the original volume to obtain the plant fermentation liquid.
The preparation method of the all-plant synthetic surfactant-free face cleaning product comprises adding soapberry extract, foam stabilizer and plant preservative into water, and mixing uniformly to obtain the product.
To better illustrate the beneficial effects of the present invention, comparative examples 1-4 are given below and are tested in human trials with examples 1-4:
the cleansing product provided in comparative example 1, in which the soapberry peel was not soaked with the plant fermentation broth, the rest was the same as in example 3;
the cleansing product provided in comparative example 2 was prepared by replacing the soapberry extract with theasaponin, and the remainder was the same as in example 3;
the cleansing product provided in comparative example 3 was prepared by changing the ratio of the hydrogenated starch hydrolysate to the glycosyl trehalose to 1:1, and the rest was the same as in example 3;
the cleansing product provided in comparative example 4 was prepared by changing the ratio of the loosestrife extract, cornflower extract, and myrobalan fruit extract to 3:1:4, and the rest was the same as in example 3.
The test population: 160 subjects, aged 20-40 years, were selected and randomized sex and divided into 8 groups of 20 subjects each.
Test samples: the cleansing products of examples 1 to 4 and the cleansing products of comparative examples 1 to 4.
The test method comprises the following steps: the test samples were distributed to the subjects for use, the subjects used the morning and evening daily, the facial skin was first moistened with clear water, the test products were applied to the face in an appropriate amount, gently rubbed for about one minute, then rinsed with clear water, and the above steps were repeated each morning and evening, and the test samples were scored two weeks after each test sample was used, with the results shown in table 1. The score was taken as 10 points, 1 point being the worst and 10 points being the best.
TABLE 1
The results show that the cleansing products provided by the invention in the examples 1 to 4 have an average foam density score of 8.54, an average foam duration score of 8.28, an average cleanliness score of 7.63, an average mildness score of 7.41, an average moisturizing score of 7.56 and an average acne prevention score of 6.59, do not react to cause phenomena such as allergy, skin discomfort and the like, and show that the whole-plant synthetic surfactant-free cleansing products provided by the invention not only have good foam density, foam duration and cleanliness, but also are mild and non-irritant to skin during cleansing.
Compared with the comparative example 1, the method has higher average score in the example 3, which shows that the soapberry peel is soaked in the plant fermentation liquid, so that the influence on the foam density, the foam duration, the cleanliness, the temperature and humidity, the humidity preservation and the acne prevention of the product is realized; compared with the comparative example 2, the soapberry extract in the example 3 has higher average score, which indicates that the synergy of the soapberry extract, the foam stabilizer and the plant preservative has influence on the foam density, the foam durability, the cleanness, the temperature and the humidity, the moisture retention and the acne prevention of the product; compared with the comparative example 3, the average score of the product of the embodiment 3 of the invention is higher, which shows that the compounding ratio of the hydrogenated starch hydrolysate and the glycosyl trehalose has influence on the foam density, the foam durability, the cleanliness, the temperature and the humidity, the moisture retention and the acne prevention of the product; compared with the comparative example 4, the compound preparation of the invention in the example 3 has higher average score, which shows that the compound proportion of the loosestrife extract, the cornflower extract and the myrobalan fruit extract has influence on the foam density, the foam durability, the cleanliness, the temperature and the humidity, the moisture retention and the acne prevention of the product.
Claims (6)
1. A whole plant synthetic surfactant-free cleansing product is characterized in that, by 100 percent of the total mass, 5 to 30 percent of soapberry extract, 10 to 30 percent of foam stabilizer, 0.8 to 1.2 percent of plant preservative and the balance of water; the foam stabilizer consists of hydrogenated starch hydrolysate and glycosyl trehalose according to the mass ratio of 0.5: 1.2-1.6; the plant preservative is a preservative combination A or a preservative combination B or a mixture of the preservative combination A and the preservative combination B, wherein the preservative combination A comprises a celandine extract, a cornflower extract and a myrobalan extract according to a mass ratio of 3:2:3, and the preservative combination B comprises a zanthoxylum fruit extract, a pulsatilla extract and a usnea extract according to a mass ratio of 3:2: 4;
the soapberry extract is prepared by the following steps in sequence: weighing 20-40 parts by weight of soapberry pericarp, soaking in 150-280 parts by weight of plant fermentation liquor, drying the soaked soapberry pericarp at low temperature of 0-4 ℃ in vacuum, then carrying out superfine grinding on the soapberry pericarp, adding 20-80% ethanol into the soapberry pericarp fine powder, carrying out ultrasonic extraction at 25 ℃, filtering by using a microporous filter membrane, collecting filtrate, then loading the filtrate on a macroporous adsorption resin column, washing the filtrate until the filtrate is colorless, eluting the filtrate by using 20-80% ethanol until the eluate is colorless, collecting ethanol eluate, carrying out membrane concentration to remove ethanol, and carrying out spray drying to obtain a soapberry extract;
the plant fermentation liquid is prepared by the following steps in sequence: weighing 25-40 parts by weight of roselle flower and 30-50 parts by weight of ailanthus altissima, drying, crushing, and uniformly mixing to obtain mixed powder; adding water 40-50 times the volume of the mixed powder, adding lactobacillus bacteria solution 10-30% of the total volume of the mixed solution, fermenting at 25-30 deg.C for 2-3 months, filtering, centrifuging, collecting supernatant, and vacuum concentrating to 1/4 of the original volume to obtain plant fermentation liquid.
2. The whole plant, additive-free synthetic surfactant cleanser product of claim 1, wherein said soapberry fruit peel is soaked in plant broth for 20 days.
3. The whole plant synthetic surfactant-free facial cleaning product according to claim 1, wherein the feed-liquid ratio of the fine powder of soapberry to ethanol is 1: 40-60.
4. The whole plant no-additive synthetic surfactant cleanser product of claim 1, wherein said ultrasonic extraction process parameters are: the ultrasonic treatment time is 20min, and the ultrasonic frequency is 1.5-2.0 MHz.
5. The whole-plant synthetic surfactant-free facial cleanser product according to claim 1, wherein the roselle flower and the ailanthus altissima are ground, sieved by a 20-80-mesh sieve and then mixed uniformly.
6. The whole plant synthetic surfactant-free cleansing product according to claim 1 wherein the lactobacillus solution has a concentration of 105-108CFU/ml。
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| CN109620746A (en) * | 2018-12-06 | 2019-04-16 | 澳宝化妆品（惠州）有限公司 | A kind of Calyx Hibisci Sabdariffae extract and its application in facial-care composition |
| CN111110607B (en) * | 2020-02-26 | 2020-12-15 | 李应坤 | Mild moisturizing type foam facial cleanser and preparation method thereof |
| CN113214913A (en) * | 2021-04-29 | 2021-08-06 | 浙江吉叶生物科技有限公司 | Natural surfactant and preparation method thereof |
| CN113425661B (en) * | 2021-08-11 | 2023-02-10 | 广州睿森生物科技有限公司 | Plant composition with cleaning and repairing effects and application thereof |
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| CN105581956A (en) * | 2014-10-22 | 2016-05-18 | 曹涛 | Food-grade anti-wrinkle anti-aging facial cleanser |
| CN105029603A (en) * | 2015-06-24 | 2015-11-11 | 陈琳仁 | Composite fresh flower, fruit, vegetable and herb enzyme, and preparation method and application thereof |
| CN106176337A (en) * | 2016-07-07 | 2016-12-07 | 黄献疆 | A kind of shampoo and preparation technology thereof |
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