CN107489030A - 一种面料用抗紫外线处理液的制备方法 - Google Patents

一种面料用抗紫外线处理液的制备方法 Download PDF

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CN107489030A
CN107489030A CN201710911703.3A CN201710911703A CN107489030A CN 107489030 A CN107489030 A CN 107489030A CN 201710911703 A CN201710911703 A CN 201710911703A CN 107489030 A CN107489030 A CN 107489030A
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洪朝坑
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ANHUI DONGJIN GARMENT Co Ltd
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Abstract

本发明涉及面料技术领域，具体涉及一种面料用抗紫外线处理液的制备方法，包括以下步骤：秤取组成抗紫外线处理液的各原料：水溶性壳聚糖、萘啶酸和氟哌酸、异二醇单丁醚、异丙基苯磺酸钠、穿心莲内脂、夏枯草提取液、助剂、纯化水、纳米材料；将上述原料中除去纯化水的剩余原料按比例加入高压容器中进行高压混料，压力为2～3倍大气压，高压混料的温度为155‑180℃，高压混料的时间为8‑10分钟；取出上述混料然后与纯化水一起混合后搅拌均匀即得抗紫外线处理液。本发明制备的抗紫外线处理液性能稳定，效果持久，处理的面料经过多次水洗后其抗紫外线性能依旧稳定，而且还具有很好的抗静电性能。

Description

一种面料用抗紫外线处理液的制备方法
技术领域：
本发明涉及面料技术领域，具体涉及一种面料用抗紫外线处理液的制备方法。
背景技术：
随着人们生活水平逐渐升高，对于穿着质量的要求也就越高，不只要求舒适，还需兼具多功能，依据不同的生活型态，所穿着衣服的功能也不同，举凡登山时，因应环境的低温、多雨及高山暴露的紫外线，则所穿着的服装则须具备保温、防水及抗紫外线等功能；当进行户外运动时，则需要轻巧、吸湿排汗、速干及透气等功能的面料，而传统运用于运动系列的针织面料大都采用普通的圆形截面涤纶低弹丝原料，采用原始的染色后制作工艺，水洗浮色较多和耐光照牢度差，经长期户外运动着装后颜色变得萎暗，手感变硬且吸湿导汗性能差，穿着闷热不透气，舒适感差；即使一般人未进行任何活动的情况下，仍要求所穿着的服装须具备高质量的质量，另外，随着周遭环境污染日益严重，文明病也相继出现，例如太粗糙的衣服面料会导致一部分人皮肤产生过敏，或者是对外在环境容易产生过敏的体质，导致现代人对于抗菌的观念也逐渐重视，以往只有医护人员所需的抗菌衣及抗菌器具，也逐渐被应用在日常生活的用品。
对人体而言，适量的紫外线辐射具有杀菌作用并能促进维生素D的合成，有利于人体健康。但在烈日持续照射下，人体皮肤会失去抵御能力，易发生灼伤，出现红斑或水泡。过量的紫外线照射还会诱发皮肤病(如皮炎，色素干皮症)，甚至皮肤癌，促进白内障的生成并降低人体的免疫功能。
从光学原理上讲，紫外线辐射到织物上，部分在表面被反射，部分被织物吸收，其余的则透过织物。一般情况下，紫外线的透过率+反射率+吸收率＝100％。因此，提高织物对紫外线的吸收率和反射率就可以降低紫外线的透过率。目前现有的抗紫外线处理液虽然会赋予织物一定的紫外线反射率和吸收率，但是经过长时间清洗后，抗紫外线性能会逐渐减弱直至消失。
而织物的抗静电性也尤为重要，尤其在特殊场合，织物产生的静电往往会产生致命的危害，因此，对织物的抗静电性的研究也显得尤为重要。
发明内容：
本发明所要解决的技术问题在于克服现有的技术缺陷，提供一种面料用抗紫外线处理液的制备方法。
本发明所要解决的技术问题采用以下的技术方案来实现：
一种面料用抗紫外线处理液的制备方法，包括以下步骤：
(1)秤取组成抗紫外线处理液的各原料：水溶性壳聚糖、萘啶酸和氟哌酸、异二醇单丁醚、异丙基苯磺酸钠、穿心莲内脂、夏枯草提取液、助剂、纯化水、纳米材料；
(2)将上述原料中除去纯化水的剩余原料按比例加入高压容器中进行高压混料，压力为2～3倍大气压，高压混料的温度为155-180℃，高压混料的时间为8-10分钟；
(3)取出上述混料然后与纯化水一起混合后搅拌均匀即得抗紫外线处理液。
更进一步地，所述抗紫外线处理液由以下重量份原料制成：水溶性壳聚糖4份、萘啶酸和氟哌酸4份、异二醇单丁醚2.2份、异丙基苯磺酸钠0.3份、穿心莲内脂1.3份、夏枯草提取液3.6份、助剂1.5份、纯化水100份、纳米材料0.2份。
更进一步地，所述助剂为蛋氨酸、珠光脂酸、蜂花酸、纳米石墨烯粉、医用白矿油按等比例混合的混合物。
更进一步地，所述纳米材料包括以下重量份原料制成：纳米石墨烯0.1份、纳米二氧化钛0.2份、纳米氧化铝0.1份，各原料混合均匀即可。
本发明的有益效果为：本发明制备的抗紫外线处理液性能稳定，效果持久，处理的面料经过多次水洗后其抗紫外线性能依旧稳定，而且还具有很好的抗静电性能。
附图说明：
图1为本发明的结构示意图；
图2为本发明基面和黏胶的结构示意图。
具体实施方式：
下面将结合本发明实施例中的附图，对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
本发明的描述中，需要说明的是，术语“竖直”、“上”、“下”、“水平”等指示的方位或者位置关系为基于附图所示的方位或者位置关系，仅是为了便于描述本实用和简化描述，而不是指示或者暗示所指的装置或者元件必须具有特定的方位，以特定的方位构造和操作，因此不能理解为对本发明的限制。此外，“第一”、“第二”、“第三”、“第四”仅用于描述目的，而不能理解为指示或者暗示相对重要性。
本发明的描述中，还需要说明的是，除非另有明确的规定和限制，术语“设置”、“安装”、“相连”、“连接”应做广义理解，例如，可以是固定连接，也可以是可拆卸连接，或一体地连接，可以是机械连接，也可以是电连接，可以是直接连接，也可以是通过中间媒介相连，可以是两个元件内部的连通。对于本领域的普通技术人员而言，可以根据具体情况理解上述术语在本发明中的具体含义。
实施例一
如附图1、2所示，一种防紫外线面料，面料包括依次复合的底层1、中间层2、上层3；
底层1由经纱、纬纱机织而成，经纱为竹炭纤维、红薯纤维混纺而成；
中间层2为混纺纺织物，将聚氯乙烯接枝马来酸酐、二硫化二苯并噻唑、聚芳烯烃、二硫化四苄基秋兰姆各自的共聚酯共同与石墨粉混合均匀进行纺中空纤维丝，该中空纤维丝进行混纺得混纺纺织物；
上层3由棉纤维、麻纤维混纺而成；
面料用抗紫外线处理液浸泡处理后再烘干即得防紫外线面料。
抗紫外线处理液由以下重量份原料制成：水溶性壳聚糖4份、萘啶酸和氟哌酸4份、异二醇单丁醚2.2份、异丙基苯磺酸钠0.3份、穿心莲内脂1.3份、夏枯草提取液3.6份、助剂1.5份、纯化水100份。
助剂为蛋氨酸、珠光脂酸、蜂花酸、纳米石墨烯粉、医用白矿油按等比例混合的混合物。
一种面料用抗紫外线处理液的制备方法，包括以下步骤：
(1)秤取组成抗紫外线处理液的各原料：水溶性壳聚糖、萘啶酸和氟哌酸、异二醇单丁醚、异丙基苯磺酸钠、穿心莲内脂、夏枯草提取液、助剂、纯化水；
(2)将上述原料中除去纯化水的剩余原料按比例加入高压容器中进行高压混料，压力为2～3倍大气压，高压混料的温度为155-180℃，高压混料的时间为8-10分钟；
(3)取出上述混料然后与纯化水一起混合后搅拌均匀即得抗紫外线处理液。
实施例二
如附图1、2所示，一种防紫外线面料，面料包括依次复合的底层1、中间层2、上层3；
底层1由经纱、纬纱机织而成，经纱为竹炭纤维、红薯纤维混纺而成；
中间层2为混纺纺织物，将聚氯乙烯接枝马来酸酐、二硫化二苯并噻唑、聚芳烯烃、二硫化四苄基秋兰姆各自的共聚酯共同与石墨粉混合均匀进行纺中空纤维丝，该中空纤维丝进行混纺得混纺纺织物；
上层3由棉纤维、麻纤维混纺而成；
面料用抗紫外线处理液浸泡处理后再烘干即得防紫外线面料。
抗紫外线处理液由以下重量份原料制成：水溶性壳聚糖4份、萘啶酸和氟哌酸4份、异二醇单丁醚2.2份、异丙基苯磺酸钠0.3份、穿心莲内脂1.3份、夏枯草提取液3.6份、助剂1.5份、纯化水100份、纳米材料0.2份。
助剂为蛋氨酸、珠光脂酸、蜂花酸、纳米石墨烯粉、医用白矿油按等比例混合的混合物。
纳米材料包括以下重量份原料制成：纳米石墨烯0.1份、纳米二氧化钛0.2份、纳米氧化铝0.1份，各原料混合均匀即可。
一种面料用抗紫外线处理液的制备方法，包括以下步骤：
(1)秤取组成抗紫外线处理液的各原料：水溶性壳聚糖、萘啶酸和氟哌酸、异二醇单丁醚、异丙基苯磺酸钠、穿心莲内脂、夏枯草提取液、助剂、纯化水、纳米材料；
(2)将上述原料中除去纯化水的剩余原料按比例加入高压容器中进行高压混料，压力为2～3倍大气压，高压混料的温度为155-180℃，高压混料的时间为8-10分钟；
(3)取出上述混料然后与纯化水一起混合后搅拌均匀即得抗紫外线处理液。
实施例三
如附图1、2所示，一种防紫外线面料，面料包括依次复合的底层1、中间层2、上层3；
底层1由经纱、纬纱机织而成，经纱为竹炭纤维、红薯纤维混纺而成；
中间层2为混纺纺织物，将聚氯乙烯接枝马来酸酐、二硫化二苯并噻唑、聚芳烯烃、二硫化四苄基秋兰姆各自的共聚酯共同与石墨粉混合均匀进行纺中空纤维丝，该中空纤维丝进行混纺得混纺纺织物；
上层3由棉纤维、麻纤维混纺而成；
面料用抗紫外线处理液浸泡处理后再烘干即得防紫外线面料。
抗紫外线处理液由以下重量份原料制成：水溶性壳聚糖4份、萘啶酸和氟哌酸4份、异二醇单丁醚2.2份、异丙基苯磺酸钠0.3份、穿心莲内脂1.3份、夏枯草提取液3.6份、助剂1.5份、纯化水100份、纳米材料0.2份。
助剂为蛋氨酸、珠光脂酸、蜂花酸、纳米石墨烯粉、医用白矿油按等比例混合的混合物。
纳米材料包括以下重量份原料制成：纳米石墨烯0.1份、纳米二氧化钛0.2份、纳米氧化铝0.1份，各原料混合均匀即可。
一种面料用抗紫外线处理液的制备方法，包括以下步骤：
(1)秤取组成抗紫外线处理液的各原料：水溶性壳聚糖、萘啶酸和氟哌酸、异二醇单丁醚、异丙基苯磺酸钠、穿心莲内脂、夏枯草提取液、助剂、纯化水、纳米材料；
(2)将上述原料中除去纯化水的剩余原料按比例加入高压容器中进行高压混料，压力为2～3倍大气压，高压混料的温度为155-180℃，高压混料的时间为8-10分钟；
(3)取出上述混料然后与纯化水一起混合后搅拌均匀即得抗紫外线处理液。
使用时将面料浸泡到抗紫外线处理液中10-20分钟，然后捞出干燥即可。
试验
对实施例1至3所得抗紫外线抗静电面料进行抗紫外线和抗静电性能检测，其中，抗紫外线性能测试面料对紫外线(尤其波长290-400nm的紫外线)的透过率，抗静电性能以面料表面的比电阻Rs(每平方单位试样对应边间的电阻)来表示，同时，在面料被洗涤20次后再次测试面料的抗静电性能和抗紫外线性能，并与中国发明专利申请公布号：CN105088750 A，申请公布日：2015.11.25的实施例1进行比较，结果如下：
可见，本发明防紫外线面料性能优越，紫外线透过率低，而且经过多次洗涤后其抗紫外线能力依旧很强，且抗静电性能也较稳定，实施例2、3的紫外线透过率明细比实施例1低，正是因为抗紫外线处理液中添加了纳米材料，从而提升了抗紫外线性能和抗静电性能。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (4)

1.一种面料用抗紫外线处理液的制备方法，其特征在于，包括以下步骤：
(1)秤取组成抗紫外线处理液的各原料：水溶性壳聚糖、萘啶酸和氟哌酸、异二醇单丁醚、异丙基苯磺酸钠、穿心莲内脂、夏枯草提取液、助剂、纯化水、纳米材料；
(2)将上述原料中除去纯化水的剩余原料按比例加入高压容器中进行高压混料，压力为2～3倍大气压，高压混料的温度为155-180℃，高压混料的时间为8-10分钟；
(3)取出上述混料然后与纯化水一起混合后搅拌均匀即得抗紫外线处理液。
2.根据权利要求1所述的一种面料用抗紫外线处理液的制备方法，其特征在于，所述抗紫外线处理液由以下重量份原料制成：水溶性壳聚糖4份、萘啶酸和氟哌酸4份、异二醇单丁醚2.2份、异丙基苯磺酸钠0.3份、穿心莲内脂1.3份、夏枯草提取液3.6份、助剂1.5份、纯化水100份、纳米材料0.2份。
3.根据权利要求1或2所述的一种面料用抗紫外线处理液的制备方法，其特征在于，所述助剂为蛋氨酸、珠光脂酸、蜂花酸、纳米石墨烯粉、医用白矿油按等比例混合的混合物。
4.根据权利要求1或2所述的一种面料用抗紫外线处理液的制备方法，其特征在于，所述纳米材料包括以下重量份原料制成：纳米石墨烯0.1份、纳米二氧化钛0.2份、纳米氧化铝0.1份，各原料混合均匀即可。
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CN108705818A (zh) * 2018-05-29 2018-10-26 安徽英士博纺织发展有限公司 一种用于冲锋衣生产的服装面料

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CN104975503A (zh) * 2015-06-29 2015-10-14 安徽东锦服饰有限公司 防紫外线隔热服装加工方法

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CN104975503A (zh) * 2015-06-29 2015-10-14 安徽东锦服饰有限公司 防紫外线隔热服装加工方法

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CN108705818A (zh) * 2018-05-29 2018-10-26 安徽英士博纺织发展有限公司 一种用于冲锋衣生产的服装面料

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