CN107474979A - A kind of perfumed soap and preparation method thereof - Google Patents
A kind of perfumed soap and preparation method thereof Download PDFInfo
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- CN107474979A CN107474979A CN201710752120.0A CN201710752120A CN107474979A CN 107474979 A CN107474979 A CN 107474979A CN 201710752120 A CN201710752120 A CN 201710752120A CN 107474979 A CN107474979 A CN 107474979A
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- perfumed soap
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- water
- madder
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0068—Deodorant compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2006—Monohydric alcohols
- C11D3/201—Monohydric alcohols linear
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/667—Neutral esters, e.g. sorbitan esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention provides a kind of perfumed soap, is prepared by the raw material of following parts by weight：24 parts of plantain seed, 46 parts of madder, 13 parts of radix cynanchi atrati, 10 20 parts of cetyl sulfophenoxy benzenesulfonic acid disodium salt, 8 10 parts of coconut oil fatty acid monoethanolamide, N cocamidopropyl propyl amides N, 10 16 parts of N dimethylglycines inner salt, 24 parts of Glycerin, mixed triester with caprylic acid capric acid, 20 30 parts of distilled water, exquisiteness is stable, moderate performance, it is low to the excitant of skin, antiinflammation can be more played, the feature of environmental protection is good, goes removing fishy odor using effect good and conveniently.
Description
Technical field
The present invention relates to a kind of perfumed soap and preparation method thereof, belong to chemical technology field.
Background technology
Perfumed soap is a kind of indispensable daily washing product, and people can trace back to B.C. meaning using the history of perfumed soap
Big profit.Since last century the eighties, China gradually starts to widely use perfumed soap.There have been a kind of artificial synthesized during the Song Dynasty
Detergent, be to smash natural Chinese honey locust to pieces carefully to grind, add various medicinal petal powder, do globulate specialize in wash one's face bath body it
With.Have it is direct by Chinese honey locust with medicinal petal after water boiling, is added, carry out bathing.Plant weak base perfumed soap (soap) be skin,
One of hair washing and nursing article, it is a kind of daily necessities.And some manufacturers are with sodium soap and other surfaces activity
Agent is that primary raw material makes perfumed soap, adds quality improver and appearance modifying agents, after machine-shaping manufactured product, because
High for the content of these pH value, skin can not be resistant to for a long time, so can only be used for cleaning clothing.And the pH that plant weak base soap contains
Receiving low, that human skin can be long-term, and the various nutriments contained in plant, and the also nutritious care of vitamin
The effect of skin.
The content of the invention
Goal of the invention：It is an object of the invention to provide a kind of perfumed soap and preparation method thereof.
Technical scheme：The purpose of the present invention is realized by following scheme：
A kind of perfumed soap, it is prepared by the raw material of following parts by weight：Plantain seed 2-4 parts, madder 4-6 parts, radix cynanchi atrati 1-3 parts.
The perfumed soap, preparation method comprise the following steps：Plantain seed, madder and radix cynanchi atrati are taken, is added water to cook twice, is merged and decoct
Liquid, relative density is 1.20 medicinal extract when being concentrated under reduced pressure into 65 DEG C, adds ethanol the percent by volume of alcohol content is stirred up to 75%
Mix, stand, filtering, relative density is 1.25 when filtrate decompression is concentrated into 65 DEG C, and reclaims ethanol, concentrate is obtained, by concentrate
Spray drying, obtains extract powder, adds other auxiliary materials, be prepared into perfumed soap.
Other auxiliary materials are cetyl sulfophenoxy benzenesulfonic acid disodium salt 10-20 parts, coconut oil fat in the perfumed soap
Sour single ethanol amide 8-10 parts, N- cocamidopropyl propyl amides-N, N- dimethylglycine inner salt 10-16 parts, Glycerin, mixed triester with caprylic acid capric acid 2-4
Part, distilled water 20-30 parts.
The perfumed soap, in preparation method step, decocting condition is：Add 8-12 times that water is medicinal material weight to measure for the first time, decoct
1-2h is boiled, adds 6-10 times that water is medicinal material weight to measure for the second time, decocts 1-2h.
The application that the perfumed soap is gone in removing fishy odor detergent in preparation.
Perfumed soap preparation method, contains following steps：(a) spice is kneaded：The various raw materials of said components are weighed in proportion
It is added in the kneading machine of conventional soapmaking, kneading is uniformly mixed.(b) grind：The thing after being uniformly mixed will be kneaded
Material, into grinder, carry out soap body grinding.(c) vacuum press strip：By the soap body after grinding, into vacuum plodder, carry out true
Pneumatics bar.(d) print：The strip soap body that plodder extrudes is directly entered printer printing, the soap body being molded.
Beneficial effect：The perfumed soap of the present invention can remove removing fishy odor, and exquisiteness is stable, and moderate performance is low to the excitant of skin,
Antiinflammation can be played, the feature of environmental protection is good, and using effect is good and conveniently.
Embodiment
Form by the following examples, the above of the present invention is described in further detail again, but should not be by this
The scope for being interpreted as the above-mentioned theme of the present invention is only limitted to following example, and all technologies for being realized based on the above of the present invention are equal
Belong to the scope of the present invention.
Embodiment 1：Take 2 parts of plantain seed, 6 parts of madder, 1 part of radix cynanchi atrati, cetyl sulfophenoxy benzenesulfonic acid disodium salt 10
Part, 10 parts of coconut oil fatty acid monoethanolamide, 10 parts of N- cocamidopropyl propyl amides-N, N- dimethylglycine inner salt, pungent capric acid
4 parts of glyceride, 20 parts of distilled water, plantain seed, madder and radix cynanchi atrati, are added water to cook twice, collecting decoction, when being concentrated under reduced pressure into 65 DEG C
Relative density is 1.20 medicinal extract, adds ethanol the percent by volume of alcohol content is stirred, is stood, filter, filtrate decompression up to 75%
Relative density is 1.25 when being concentrated into 65 DEG C, and reclaims ethanol, obtains concentrate, concentrate is spray-dried, obtain extract powder, is added
Other auxiliary materials, are prepared into perfumed soap.In preparation method step, decocting condition is：For the first time plus water is 8 times of amounts of medicinal material weight, is decocted
2h is boiled, for the second time plus water is 6 times of amounts of medicinal material weight, decocts 2h.
Embodiment 2：Take 4 parts of plantain seed, 4 parts of madder, 3 parts of radix cynanchi atrati, cetyl sulfophenoxy benzenesulfonic acid disodium salt 20
Part, 8 parts of coconut oil fatty acid monoethanolamide, 16 parts of N- cocamidopropyl propyl amides-N, N- dimethylglycine inner salt, pungent capric acid are sweet
2 parts of grease, 30 parts of distilled water, take plantain seed, madder and radix cynanchi atrati, add water to cook twice, collecting decoction, when being concentrated under reduced pressure into 65 DEG C
Relative density is 1.20 medicinal extract, adds ethanol the percent by volume of alcohol content is stirred, is stood, filter, filtrate decompression up to 75%
Relative density is 1.25 when being concentrated into 65 DEG C, and reclaims ethanol, obtains concentrate, concentrate is spray-dried, obtain extract powder, is added
Other auxiliary materials, are prepared into perfumed soap.In preparation method step, decocting condition is：For the first time plus water is 12 times of amounts of medicinal material weight, is decocted
1h is boiled, for the second time plus water is 10 times of amounts of medicinal material weight, decocts 1h.
Embodiment 3：Take 3 parts of plantain seed, 5 parts of madder, 2 parts of radix cynanchi atrati, cetyl sulfophenoxy benzenesulfonic acid disodium salt 15
Part, 9 parts of coconut oil fatty acid monoethanolamide, 13 parts of N- cocamidopropyl propyl amides-N, N- dimethylglycine inner salt, pungent capric acid are sweet
3 parts of grease, 25 parts of distilled water, take plantain seed, madder and radix cynanchi atrati, add water to cook twice, collecting decoction, when being concentrated under reduced pressure into 65 DEG C
Relative density is 1.20 medicinal extract, adds ethanol the percent by volume of alcohol content is stirred, is stood, filter, filtrate decompression up to 75%
Relative density is 1.25 when being concentrated into 65 DEG C, and reclaims ethanol, obtains concentrate, concentrate is spray-dried, obtain extract powder, is added
Other auxiliary materials, are prepared into perfumed soap.In preparation method step, decocting condition is：For the first time plus water is 10 times of amounts of medicinal material weight, is decocted
1.5h is boiled, for the second time plus water is 8 times of amounts of medicinal material weight, decocts 1.5h.
Embodiment 4, effect example
The preparation of bacteriostatic solution：The perfumed soap of the present invention made and conventional perfumed soap (non-antimicrobial form perfumed soap) are configured to respectively
1：10 solution.Diameter 4mm circular filter paper piece is made into 102 type middling speed qualitative filter papers, is placed in 121 DEG C of sterilizings in culture dish
20min, with matched somebody with somebody solution respectively toward 20 μ l, 25 DEG C of drying for standby are quantitatively added dropwise on filter paper after cooling.Test strain is：It is golden yellow
Color staphylococcus, Escherichia coli, beta streptococcus, Candida albicans.Test organisms after activation is inoculated in MH sausage culture mediums
In, 24h is cultivated at 37 DEG C, the bacteria suspension that concentration is 105~108CFU/ml is diluted to MH culture mediums.In diameter 9cm culture
15mlMHA culture mediums are added in ware, it is 10 that 1ml concentration is added per ware5~108CFU/ml bacteria suspension, with spreader even spread
Flat board table is uniformly attached to successively on MHA culture mediums, then by the filter paper of the filter paper added with bacteriostatic solution, contrast solution
Face, every kind of bacterium do 5 parallel tests.Observed after cultivating 24h at 37 DEG C and record inhibition zone (transparent circle) size, inhibition zone is big
It is small to average.It is antibacterial to the results are shown in Table.
As a result malignant bacteria staphylococcus aureus, Escherichia coli, B-mode chain of the perfumed soap of the present invention to participation test are shown
Coccus, Candida albicans have a certain degree of fungistatic effect, and compared to conventional perfumed soap, the fungistatic effect of perfumed soap of the present invention obtains
Significantly improve.
Embodiment 5：Influence of the present invention to fishlike smell
Test method：Embodiment 1-3 will be prepared, 20 testers is respectively issued to and uses, before tester uses sample
Both hands speckle with fishlike smell, and the specific clean method of tester is：After first drenching skin using clear water, fitted using product of the present invention
Measure in the palm of the hand, gently rub out foam one minute；Then rinsed well with clear water, another tester according to oneself feel commented
Than.Content on probation includes：Whether there is excitement, whether there is itch, that arm skin whether there is is general red.Evaluation criterion takes ten point system.
Perfumed soap using effect evaluation table of the present invention
| Sample source | Skin comfort degree | Remove removing fishy odor | Foaming abundancy sense |
| Embodiment 1 | 9.9 | 9.8 | 9.6 |
| Embodiment 2 | 9.6 | 9.6 | 9.4 |
| Embodiment 3 | 9.5 | 9.4 | 9.2 |
| Conventional perfumed soap | 8.1 | 7.1 | 7.4 |
As a result show：Embodiment 1-3 skin comforts degree, go removing fishy odor, foaming abundancy sense to be significantly better than conventional perfumed soap, say
The bright present invention works well.
Claims (5)
1. a kind of perfumed soap, it is characterised in that be prepared by the raw material of following parts by weight：It is plantain seed 2-4 parts, madder 4-6 parts, white
Common vetch 1-3 parts.
2. perfumed soap as claimed in claim 1, it is characterised in that preparation method comprises the following steps：Take plantain seed, madder and white
Common vetch, add water to cook twice, collecting decoction, relative density is 1.20 medicinal extract when being concentrated under reduced pressure into 65 DEG C, adds ethanol to make alcohol content
Percent by volume up to 75%, stir, stand, filtering, relative density is 1.25 when filtrate decompression is concentrated into 65 DEG C, and reclaims second
Alcohol, concentrate is obtained, concentrate is spray-dried, obtain extract powder, added other auxiliary materials, be prepared into perfumed soap.
3. perfumed soap as claimed in claim 2, it is characterised in that other described auxiliary materials are cetyl sulfophenoxy benzene sulfonic acid two
Sodium salt 10-20 parts, coconut oil fatty acid monoethanolamide 8-10 parts, N- cocamidopropyl propyl amides-N, N- dimethylglycine inner salt
10-16 parts, Glycerin, mixed triester with caprylic acid capric acid 2-4 parts, distilled water 20-30 parts.
4. perfumed soap as claimed in claim 2, it is characterised in that in preparation method step, decocting condition is：For the first time plus water is medicine
8-12 times of material weight is measured, and decocts 1-2h, is added 6-10 times that water is medicinal material weight to measure for the second time, is decocted 1-2h.
5. application of the perfumed soap as claimed in claim 1 in removing fishy odor detergent is removed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710752120.0A CN107474979A (en) | 2017-08-28 | 2017-08-28 | A kind of perfumed soap and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710752120.0A CN107474979A (en) | 2017-08-28 | 2017-08-28 | A kind of perfumed soap and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107474979A true CN107474979A (en) | 2017-12-15 |
Family
ID=60603884
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710752120.0A Pending CN107474979A (en) | 2017-08-28 | 2017-08-28 | A kind of perfumed soap and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107474979A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1030606A (en) * | 1987-05-18 | 1989-01-25 | 肖兴寿 | deodorant soap |
| CN1456651A (en) * | 2003-03-07 | 2003-11-19 | 吴燕娇 | Deodorant healthy metal soap and producing method thereof |
| CN102784350A (en) * | 2012-08-07 | 2012-11-21 | 孙雅儒 | Mite killing bactericide and preparation method of mite killing bactericide |
| CN104257563A (en) * | 2014-10-16 | 2015-01-07 | 李正梅 | Creeping falsepimpernel herb hand sanitizer and preparation method thereof |
| CN104263569A (en) * | 2014-10-14 | 2015-01-07 | 李正梅 | Anti-inflammatory homalocladium platycladium soap and preparation method thereof |
-
2017
- 2017-08-28 CN CN201710752120.0A patent/CN107474979A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1030606A (en) * | 1987-05-18 | 1989-01-25 | 肖兴寿 | deodorant soap |
| CN1456651A (en) * | 2003-03-07 | 2003-11-19 | 吴燕娇 | Deodorant healthy metal soap and producing method thereof |
| CN102784350A (en) * | 2012-08-07 | 2012-11-21 | 孙雅儒 | Mite killing bactericide and preparation method of mite killing bactericide |
| CN104263569A (en) * | 2014-10-14 | 2015-01-07 | 李正梅 | Anti-inflammatory homalocladium platycladium soap and preparation method thereof |
| CN104257563A (en) * | 2014-10-16 | 2015-01-07 | 李正梅 | Creeping falsepimpernel herb hand sanitizer and preparation method thereof |
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Application publication date: 20171215 |