CN107469939A - A kind of method of the dry pupa albumen powder of temperature production degreasing insect - Google Patents
A kind of method of the dry pupa albumen powder of temperature production degreasing insect Download PDFInfo
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- CN107469939A CN107469939A CN201710731189.5A CN201710731189A CN107469939A CN 107469939 A CN107469939 A CN 107469939A CN 201710731189 A CN201710731189 A CN 201710731189A CN 107469939 A CN107469939 A CN 107469939A
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- insect
- degreasing
- dry pupa
- dry
- pupa
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C13/00—Disintegrating by mills having rotary beater elements ; Hammer mills
- B02C13/14—Disintegrating by mills having rotary beater elements ; Hammer mills with vertical rotor shaft, e.g. combined with sifting devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C13/00—Disintegrating by mills having rotary beater elements ; Hammer mills
- B02C13/26—Details
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/18—Adding fluid, other than for crushing or disintegrating by fluid energy
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/18—Adding fluid, other than for crushing or disintegrating by fluid energy
- B02C23/20—Adding fluid, other than for crushing or disintegrating by fluid energy after crushing or disintegrating
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/102—Production of fats or fatty oils from raw materials by extracting in counter-current; utilisation of an equipment wherein the material is conveyed by a screw
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- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fodder In General (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of method of the dry pupa albumen powder of temperature production degreasing insect, it comprises the following steps：(1) fresh and alive insect pupa is cleaned up, then be baked to；Then by the dry pupa coarse crushing of insect, by the dry pupa input rotation transmission extractor of the insect of coarse crushing, extraction temperature is 10 15 DEG C, and using liquefied butane as solvent, continuous countercurrent extraction is carried out to the dry pupa of insect；Then the filter residue obtained after rotation transmission extractor extraction is the dry pupa of degreasing insect；(2) the dry pupa of dried degreasing insect is sent into special flour mill, is milled to the dry pupa albumen powder of degreasing insect.The present invention can make requirement, long shelf-life and the high financial profit that feedstock oil residual is low, smashing fineness reaches food and medical protein powder raw material.
Description
Technical field
The present invention relates to insects deep-processing technical field of agricultural products, and in particular to a kind of dry pupa of temperature production degreasing insect
The method of albumen powder.
Background technology
With the insect of de-oiling processing albumen powder at home or the starting stage now, most of is all to use common grinder powder
It is broken, and feedstock oil residual is more, and smashing fineness difficulty reaches the requirement of food and medical protein powder raw material, and the shelf-life is short, economy effect
Benefit is low.
The content of the invention
In order to solve the above technical problems, it is an object of the invention to propose that one kind can make feedstock oil remain low, smashing fineness
Reach requirement, the dry pupa albumen of the temperature production degreasing insect of long shelf-life and high financial profit of food and medical protein powder raw material
The method of powder.
Used technical scheme is：
A kind of method of the dry pupa albumen powder of temperature production degreasing insect, comprises the following steps：
(1) fresh and alive insect pupa is cleaned up, then be baked to；Then by the dry pupa coarse crushing of insect, by the elder brother of coarse crushing
The dry pupa input rotation transmission extractor of worm, extraction temperature is 10-15 DEG C, and using liquefied butane as solvent, the dry pupa of insect is connected
Continuous counter-current extraction；Then the filter residue obtained after rotation transmission extractor extraction is the dry pupa of degreasing insect；
(2) the dry pupa of dried degreasing insect is sent into flour mill, is milled to the dry pupa albumen powder of degreasing insect；The mill
Broken machine includes body, is set in the body liquid nitrogen chamber, it is put into the crushing chamber of the liquid nitrogen indoor, into the crushing chamber
Rotary blade and the blower fan and charging aperture communicated with crushing chamber；The dry pupa of degreasing insect enters crushing chamber, liquid from charging aperture
Nitrogen room after the dry pupa of degreasing insect under liquid nitrogen cryogenics by cooling down the brittle easily crushing state of realization, is crushing using liquid nitrogen as low-temperature receiver
Intracavitary is rotated at a high speed by rotary blade, blade, the fluted disc of the dry pupa of degreasing insect and rotary blade, the dry pupa of degreasing insect and degreasing
Under mutual repeated stock, collision, shearing, friction comprehensive function between the dry pupa of insect, reach the powder of food and medical protein powder
Broken effect.
Further, in addition to albumen powder is classified by step (3) by gas flow sizing machine, the grader and the milling
The crushing chamber connection of machine, and form closed-circuit system with flour mill.
Further, in step (1), dried with micro-wave oven, wherein microwave is 10-15kg/KWh, temperature 40-50
DEG C, it is 5%-9% to be dried to water content.
Further, in step (2), the water content of the dried dry pupa of degreasing insect is 5%-9%.
Further, in step (1), the rotation transmission extractor includes vertical rotary conveyer and inclined rotation transmission
Device, the bottom of the inclined rotational transmitter are connected with the bottom of the vertical rotary conveyer, the inclined rotation transmission
The top of device is higher than the top of the vertical rotary conveyer；The vertical rotary conveyer and the inclined rotational transmitter two
The screw rod that person includes is driven with motor respectively.
Further, the angle between the inclined rotational transmitter and the vertical rotary conveyer is 35-55 degree.
Further, the rotation transmission extractor is immersed to the constant temperature being adapted with the rotation transmission extractor structure
In water bath.
Further, the dry pupa of the insect is the dry pupa of yellow meal worm or the dry pupa of barley worm.
Further, in step (1), the addition of butane is 6-10 times of the dry pupa weight of insect.
The beneficial effects of the present invention are：
1. the present invention uses the dry pupal fat fat of continuous countercurrent extraction insect, continuous countercurrent extraction refers to that extraction phase is opposite with raffinate
The extraction that opposite direction flows and carried out.In the process, rich solvent-laden extract before outflow system with extract (elder brother
The dry pupa of worm) contact, make extract and separate more complete.Because it is compared with conventional extraction, the screw rod of rotation is taken as separation
Place, therefore in the presence of multidimensional centrifugal force field force, the mixing of extraction phase and raffinate phase is more thorough, and extraction efficiency is higher, extraction
Take and (carry oil) rate to be up to 90-96%, so as to make the oily residual rate of the dry pupa of degreasing insect very low.
It is low-temperature receiver with liquid nitrogen 2. the present invention uses special flour mill, send the dry pupa of the degreasing insect after oil is carried into milling
In machine, by under the comprehensive functions such as the mutual repeated stock between material and material, collision, shearing, reaching crushing effect.Advantage
It is that smashing fineness is big, the use standard of food, medicine can be reached.Energy industrialized production, technology is strict, and quality is guaranteed.Production
Process temperature is low, does not destroy protein active agent, keeps phase length, more economic benefits can be brought to manufacturer.
Brief description of the drawings
Fig. 1 is rotation transmission extractor structural representation；
Fig. 2 is the structural representation of flour mill；
Fig. 3 is the structural representation for including the gentle flow fan of flour mill.
Embodiment
The present invention is further illustrated below by embodiment, but protection scope of the present invention is not limited thereto.
Embodiment 1
Referring to shown in Fig. 1-Fig. 3, a kind of method of the dry pupa albumen powder of temperature production degreasing insect, comprise the following steps：
(1) fresh and alive yellow meal worm is cleaned up, then be baked to, wherein microwave is 10kg/KWh, and temperature is 40 DEG C,
Water content is dried to as 9%；Then it is yellow meal worm dry pupa powder is broken, the dry pupa input rotation of the yellow meal worm of crushing is transmitted into extractor,
Extraction temperature is 10 DEG C, and using liquefied butane as solvent, addition is 6 times of the dry pupa weight of yellow meal worm, and the dry pupa of yellow meal worm is carried out
Continuous countercurrent extraction；Wherein, rotation transmission extractor is shown in Figure 1, and rotation transmission extractor includes vertical rotary conveyer 1
With inclined rotational transmitter 2, the bottom of inclined rotational transmitter 2 is connected with the bottom of vertical rotary conveyer 1, inclined rotation
The top of conveyer 2 is higher than the top of vertical rotary conveyer 1；In both vertical rotary conveyer 1 and inclined rotational transmitter 2
The screw rod 3,4 contained is driven with motor respectively；Angle between inclined rotational transmitter 2 and vertical rotary conveyer 1 is 45 degree；
During work, rotation transmission extractor immerse to in the constant water bath box that is adapted of rotation transmission extractor structure, can be with
Ensure whole low-temperature extraction.And whole low-temperature extraction ensure that the nutriment not destroyed in oil product and bioprotein are lived
Property；
Then the filter residue obtained after rotation transmission extractor extraction is the dry pupa of degreasing insect；
(2) the dry pupa of degreasing yellow meal worm is dried, and it is 9% to make its water content；The dried dry pupa of degreasing yellow meal worm is sent
Enter in flour mill, be milled to the dry pupa albumen powder of degreasing yellow meal worm；Shown in Figure 2, the grater includes body 5, described
The liquid nitrogen chamber 6 that sets in body 5, the crushing chamber 7 being put into the liquid nitrogen chamber 6, into the rotary blade 8 in the crushing chamber 7 and
The blower fan 9 and charging aperture 10 communicated with crushing chamber 7；The dry pupa of degreasing yellow meal worm enters crushing chamber from charging aperture, liquid nitrogen chamber with
Liquid nitrogen is low-temperature receiver, and the dry pupa of degreasing yellow meal worm realizes brittle easily crushing state by being cooled down under liquid nitrogen cryogenics (reachable -196 DEG C)
Afterwards, rotated at a high speed by rotary blade in crushing chamber, blade, the fluted disc of the dry pupa of degreasing yellow meal worm and rotary blade, degreasing is yellow
Under mutual repeated stock, collision, shearing, friction comprehensive function between the dry pupa of mealworm and the dry pupa of degreasing yellow meal worm, reach food
And the crushing effect of medical protein powder.Wherein, under the rotation of rotary blade, the dry pupa of degreasing yellow meal worm and rotary blade 8 are realized
Blade 15, fluted disc 16 collision, while under the cooperation of blower fan, realize mutually touching between the dry pupa of degreasing yellow meal worm itself
Hit, and the collision of the blade, fluted disc of the dry pupa of aggravation degreasing yellow meal worm and rotary blade.
(3) albumen powder is classified by gas flow sizing machine, shown in Figure 3, the grader 11 and the flour mill
Crushing chamber 7 connects, and forms closed-circuit system with flour mill.Gas flow sizing machine is mainly by motor 12, grader housing 13 and classification
The composition of wheel 14.Grading wheel is set in grader housing, and grading wheel is driven by motor.Motor driven grading wheel is in grader housing
High-speed rotation (rotating speed can be adjusted arbitrarily), forms powerful centrifugal force in grader.The gas powder mixing entered in grader
Thing is introduced into inside grading wheel, and under the influence of centrifugal force, big or weight particle centrifugalization power is big, therefore is got rid of to grading wheel
Periphery is no longer influenceed to grader side wall by centrifugal force, and falling on discharging opening under nature is collected；Small or light material by
Centrifugal action is small, is hovered inside grading wheel, and eminence is taken to by the windage of blower fan, in pipeline to next component
It is graded or collects.The size of centrifugal force in grader can be adjusted by the rotating speed of variable frequency adjustment grading wheel, reach and separate finger
Determine the purpose of the material of granularity.Gas flow sizing machine forms closed-circuit system with flour mill, and wind can be made to be back in crushing chamber and used.
If being classified the material being collected into is not reaching to fineness requirement, can also be back to by charging aperture in crushing chamber further
Crush.
The dry pupa albumen powder of yellow meal worm of this method production, the activity that it is remained in whole production process are not damaged, energy
As Edible protein flour and the raw material or directly edible of medical protein powder.
Embodiment 2
Implement with reference to embodiment 1, as different from Example 1：
In step (1), microwave 12kg/KWh, temperature is 45 DEG C, is dried to water content as 7%；Extraction temperature is 12
DEG C, butane addition is 8 times of the dry pupa weight of yellow meal worm.
In step (2), the dry pupa water content of dry yellow meal worm is 7%.
Embodiment 3
Implement with reference to embodiment 1, as different from Example 1：
In step (1), microwave 15kg/KWh, temperature is 50 DEG C, is dried to water content as 5%；Extraction temperature is 15
DEG C, butane addition is 10 times of the dry pupa weight of yellow meal worm.
In step (2), the dry pupa water content of dry yellow meal worm is 5%.
Embodiment 4- embodiments 6
Respectively to should refer to embodiment 1- embodiments 3, unlike, the insect pupa of embodiment 4- embodiments 6 is big
Wheat worm pupa.
The content of the tenebrio oil that the step (1) of embodiment 1- embodiments 6 is obtained by continuous extraction and barley worm oil is entered
Row is weighed, and compared with the theoretic grease weight of raw material, extraction yield is calculated, as shown in table 1 below：
Table 1
| Embodiment | Extraction yield |
| Embodiment 1 | 94% |
| Embodiment 2 | 96% |
| Embodiment 3 | 91% |
| Embodiment 4 | 93% |
| Embodiment 5 | 95% |
| Embodiment 6 | 90% |
The present invention is it is not intended that pH value, influence of the pH value to extraction yield are little.Butane is with liquefied butane (- 0.5 DEG C of boiling point)
Solvent, continuous multi-stage extraction, whole low-temperature extraction being carried out using rotation transmission extractor, extraction yield is up to 90-96%, so that
The oily residual rate of the dry pupa of degreasing insect is very low.
The dry pupa albumen powder of insect that the step (2) of embodiment 1- embodiments 6 is obtained, measure and the amino acid for carrying out particle diameter are total
The measure of amount, measurement result are as shown in table 2 below：
Table 2
The smashing fineness of the present invention is big, can reach the use standard of food, medicine.
In addition, if moisture content is too high in step (1), continuous phase moisture film easily is formed in particle surface, influences degreasing rate
(extraction yield), in step (2), if moisture content is too high, cohesive bonding phenomenon occurs when being processed into albumen powder, so aqueous
Measure and obtain controlling the quality that can make product more stable in step (1) neutralization procedure (2).
Those listed above is a series of to describe illustrating only for possible embodiments of the invention in detail,
They simultaneously are not used to limit the scope of the invention, all equivalent embodiments made without departing from skill spirit of the present invention or change
It should be included in the scope of the protection.
Claims (9)
- A kind of 1. method of the dry pupa albumen powder of temperature production degreasing insect, it is characterised in that comprise the following steps：(1) fresh and alive insect pupa is cleaned up, then be baked to；Then by the dry pupa coarse crushing of insect, the insect of coarse crushing is done Pupa input rotation transmission extractor, extraction temperature is 10-15 DEG C, using liquefied butane as solvent, the dry pupa of insect is carried out continuous inverse Stream extraction；Then the filter residue obtained after rotation transmission extractor extraction is the dry pupa of degreasing insect；(2) the dry pupa of dried degreasing insect is sent into flour mill, is milled to the dry pupa albumen powder of degreasing insect；The grater The liquid nitrogen chamber that is set including body, in the body, the crushing chamber for being put into the liquid nitrogen indoor, into the rotation in the crushing chamber Impeller and the blower fan and charging aperture communicated with crushing chamber；The dry pupa of degreasing insect enters crushing chamber, liquid nitrogen chamber from charging aperture Using liquid nitrogen as low-temperature receiver, after the dry pupa of degreasing insect under liquid nitrogen cryogenics by cooling down the brittle easily crushing state of realization, in crushing chamber Rotated at a high speed by rotary blade, blade, the fluted disc of the dry pupa of degreasing insect and rotary blade, the dry pupa of degreasing insect and degreasing insect Under mutual repeated stock, collision, shearing, friction comprehensive function between dry pupa, reach the crushing effect of food and medical protein powder Fruit.
- 2. the method for the dry pupa albumen powder of temperature production degreasing insect according to claim 1, it is characterised in that also include step Suddenly albumen powder is classified by (3) by gas flow sizing machine, and the grader connects with the crushing chamber of the flour mill, and and flour mill Form closed-circuit system.
- 3. it is to use microwave in step (1) method of the dry pupa albumen powder of temperature production degreasing insect according to claim 1 Baking oven is done, and wherein microwave is 10-15kg/KWh, and temperature is 40-50 DEG C, and it is 5%-9% to be dried to water content.
- It is dried in step (2) 4. the method for the dry pupa albumen powder of temperature production degreasing insect according to claim 1 The water content of the dry pupa of degreasing insect is 5%-9%.
- 5. the method for the dry pupa albumen powder of temperature production degreasing insect according to claim 1, it is characterised in that step (1) In, the rotation transmission extractor includes vertical rotary conveyer and inclined rotational transmitter, the inclined rotational transmitter Bottom is connected with the bottom of the vertical rotary conveyer, and the top of the inclined rotational transmitter passes than the vertical rotary Send the top of device high；The screw rod that both the vertical rotary conveyer and the inclined rotational transmitter include uses motor respectively Transmission.
- 6. the method for the dry pupa albumen powder of temperature production degreasing insect according to claim 5, it is characterised in that the inclined Angle between rotational transmitter and the vertical rotary conveyer is 35-55 degree.
- 7. the method for the dry pupa albumen powder of temperature production degreasing insect according to claim 6, it is characterised in that the rotation Transmission extractor is immersed into the constant water bath box being adapted with the rotation transmission extractor structure.
- 8. the method for the dry pupa albumen powder of temperature production degreasing insect according to claim 1, it is characterised in that the insect Dry pupa is the dry pupa of yellow meal worm or the dry pupa of barley worm.
- 9. the method for the dry pupa albumen powder of temperature production degreasing insect according to claim 1, it is characterised in that step (1) In, the addition of butane is 6-10 times of the dry pupa weight of insect.
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Cited By (4)
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| CN111000021A (en) * | 2019-10-21 | 2020-04-14 | 长沙理工大学 | Production equipment and method of insect protein powder |
| CN113198590A (en) * | 2021-04-30 | 2021-08-03 | 青岛新农康源生物工程有限公司 | Method for producing defatted tenebrio molitor protein powder at low temperature |
| CN115254353A (en) * | 2021-04-30 | 2022-11-01 | 青岛新农康源生物工程有限公司 | Low-temperature production process of dry tenebrio molitor powder |
| CN117941830A (en) * | 2024-03-14 | 2024-04-30 | 江苏省农业科学院 | Eucommia ulmoides and cordyceps militaris compound product and preparation method thereof |
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| CN113198590A (en) * | 2021-04-30 | 2021-08-03 | 青岛新农康源生物工程有限公司 | Method for producing defatted tenebrio molitor protein powder at low temperature |
| CN115254353A (en) * | 2021-04-30 | 2022-11-01 | 青岛新农康源生物工程有限公司 | Low-temperature production process of dry tenebrio molitor powder |
| CN117941830A (en) * | 2024-03-14 | 2024-04-30 | 江苏省农业科学院 | Eucommia ulmoides and cordyceps militaris compound product and preparation method thereof |
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Denomination of invention: A method of producing degreased insect dried pupa protein powder at low temperature Effective date of registration: 20230116 Granted publication date: 20190614 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: QINGDAO XINNONG KANGYUAN BIOENGINEERING CO.,LTD. Registration number: Y2023370010015 |