CN107467573A - A kind of lycopene extraction method and special diet tomato nutrient powder - Google Patents
A kind of lycopene extraction method and special diet tomato nutrient powder Download PDFInfo
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- CN107467573A CN107467573A CN201710759295.4A CN201710759295A CN107467573A CN 107467573 A CN107467573 A CN 107467573A CN 201710759295 A CN201710759295 A CN 201710759295A CN 107467573 A CN107467573 A CN 107467573A
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- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
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- A23L19/01—Instant products; Powders; Flakes; Granules
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- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
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Abstract
A kind of lycopene extraction method and special diet tomato nutrient powder, the method that lycopene is extracted using the enzymolysis ultrasound adverse current suitable for industrialized production, again to extract the slag after lycopene, juice as raw material, tomato meal is made using microwave vacuum drying technology, again using tomato meal as raw material, it is aided with the proportioning of soybean protein, dairy products and micronutrient hardening agent.Product of the present invention has anti-oxidant, cancer-resisting, improves immunity, anti-aging, protection skin, prevention cardiovascular and cerebrovascular disease and prostatitis function, can develop the special diet tomato nutrient powder product eaten suitable for all kinds of special populations.The extraction process that the present invention uses shortens extraction time, improve extraction yield, lycopene is set to reach 5~15%, raw material source is provided for the new product development based on lycopene, meanwhile, tomato meal can be used as food ingredient to apply into special meals nutrient powder, comprehensively utilize residue, juice, while avoiding environmental pollution, the nutritive loss of raw material is decreased, increases added value of product.
Description
One, technical fields：
The invention belongs to technical field of extraction of lycopene, is related to a kind of lycopene extraction method and special diet use kind
The preparation method of eggplant nutrient powder.
Two, technical backgrounds：
Lycopene is a kind of liposoluble natural pigment, is the activity for the most effective inoxidizability and Antiradiation being currently known
Material, there is stronger anti-oxidant and elimination free radical ability, atherosclerosis can be slowed down, prevent the oxygen of low density cholesterol
Change, can effectively prevent the generation of angiocardiopathy, also there is suppressor mutation, prevent the function of malignant tumour, it is solvable
In the grease of fat, and red is presented, is a kind of preferable colouring agent in food, therefore, lycopene is a kind of natural, green
The functional health care food of color medicine-food two-purpose, it is widely used in the fields such as medicine, health products, food, cosmetics.Lycopene is main
Exist in the fruit such as tomato, watermelon, grape, in chemical constitution service carotenoid.The extracting method of existing lycopene is main
Have：In solvent extraction method, supercritical CO2Extraction, enzymatic isolation method, microbe fermentation method.
Common organic solvent method, product quality are poor compared with other extracting methods, and product purity is low, production cycle length, energy consumption
And solvent loss is big, because lycopene is a kind of temperature-sensitive and photoactive substance, easily aoxidized in extraction process, so
Low to product purity, color value is low, supercritical CO2Extraction, the recovery rate of lycopene can be improved, and product purity is high, it is molten
Agent residual is low, but production equipment cost is high, and the operation and security requirement of equipment are high, are not suitable for big industrialized production.Micro- life
Thing fermentation method is harsher to working condition, environment, production operation, is not easy to separate and purify, production cycle length, and operates
Improper, easily failure, causes unnecessary loss, the method is not easy to promote.
The three, content of the invention
(1) is overcome the deficiencies in the prior art, and the invention provides a kind of enzymolysis ultrasound suitable for industrialized production is inverse
The method of stream extraction lycopene, then to extract the slag after lycopene, juice as raw material, be made using microwave vacuum drying technology
Tomato meal, then using tomato meal as raw material, it is aided with the proportioning of soybean protein, dairy products and micronutrient hardening agent, exploitation is applied to
The edible special diet tomato nutrient powder product of all kinds of special populations.
(2) the present invention is solves the problems, such as set forth above adopted the technical scheme that：
A kind of lycopene extraction method and special diet tomato nutrient powder, its making step are as follows：
Step a pretreatments of raw material：Raw material tomato, clear water cleaning tomato are taken, squeezing tomato obtains catsup；
Step b is digested：Tomato cleaning, after crushing, catsup is pre-processed using the combined-enzyme method of cellulase and pectase,
Cellulase: pectase=1-5: 3-8, complex enzyme addition 0.2-0.8mL/g, enzymolysis time 3-8h, hydrolysis temperature 25-50
℃；
Step c ultrasonic waves adverse current is extracted：By the obtained tomato slurries of step b and ethyl acetate according to mass ratio 1: 3~10,
It is put into single stage type continuous flow upstream ultrasonic extractor, 10-35min, extraction temperature is countercurrently extracted in the case where ultrasonic power is 150-250W
40-65 DEG C of degree, after filtering extraction, collection obtains filtrate and filter residue, and filter residue is repeated into ultrasound adverse current extraction 1~3 time, repeated
Filter, finally merges all filtrates；
Step d is concentrated：Gained filtrate is sent into the crystallization of vacuum refrigeration crystallizer, vacuum is 0.03~0.1Mpa, crystallization
Temperature is -22~-4 DEG C, and crystallization time is 3~13h, filters to obtain crystalline mixture, then gained crystalline mixture is carried out into vacuum
Concentration, vacuum are 0.03~0.1Mpa, and thickening temperature is 45~75 DEG C, 30~80min of concentration time；
Step e micro-wave vacuums：Material after gained is concentrated is sent into microwave vacuum dryer and dried, and drying time is
2~5h, vacuum are 0.03~0.09Mpa, and temperature is 25~60 DEG C；Resulting material is sent into micronizer to crush, obtained
The lycopene powder of 5-15% contents, fineness are 20-100 mesh, and the water content control of lycopene powder is in below 1-5%；
The preparation of step f special diets tomato nutrient powder product：To extract the skin slag after lycopene, juice as original
Material, is made tomato meal using microwave vacuum drying technology, is aided with soybean protein, dairy products and micronutrient (vitamin A, dimension
Raw plain B1, vitamin B2, vitamin C, vitamin D, vitamin E, folic acid, docosahexaenoic acid, calcium, iron, zinc, the nutrition such as selenium
Hardening agent forms), exploitation is applied to the special diet tomato nutrient powder product that all kinds of special populations are eaten, and optimization formula is such as
Under：
Tomato meal 10-40g, soybean protein 10-30g, dairy products 5-15g, 500-1000ug containing vitamin A, vitamin B1
500-1500ug, vitamin B2400-600ug, vitamin C 100-350mg, vitamin D 60-150IU, vitamin E 10-
25mga-TE Cernevit-12；And the foliamin of the 200-450ug containing folic acid；Docosahexaenoic acid 500-
1000mg；Calcic 100-250mg, iron 3-9mg, zinc 3-8mg, selenium 100-350ug composite trace element preparation.
(3) beneficial effects of the present invention：
1. the present invention has carried out industrialization key technology research based on raw tomatoes material, promote lycopene and eaten in processing
Application in product, Medicines and Health Product.
2. the chemical reagent corrosive very little that the present invention uses, security is good, and is easily recycled processing, reduces equipment
Anti-corrosion and pollution treatment processing cost.
3. the present invention is made kind using immobilized cellulase and pectase degraded or the cellulose, the pectin that destroy in tomato
Lycopene fully overflows, and in conjunction with ultrasonic assistant extractive technique, accelerates the speed of extraction process infiltration dissolving and diffusion, shortens
Extraction time, extraction yield is improved, lycopene is reached 5~15%, is opened for the new product based on lycopene
Hair provides raw material source.
4. the present invention can be applied to special meals by the use of tomato meal made from microwave vacuum low-temperature dry technology as food ingredient
In nutrient powder, comprehensive utilization residue, juice, while avoiding environmental pollution, the nutritive loss of raw material is decreased, increase product is attached
It is value added.
4th, embodiment
Specific embodiment one
A kind of lycopene extraction method and special diet tomato nutrient powder, its making step are as follows：
Step a pretreatments of raw material：Raw material tomato, clear water cleaning tomato are taken, squeezing tomato obtains catsup；
Step b is digested：Catsup is pre-processed using the combined-enzyme method of cellulase and pectase, complex enzyme addition is
2L, cellulase addition are 0.4L, and the addition of pectase is 1.6L, enzymolysis time 6h, 45 DEG C of hydrolysis temperature.
Step c ultrasonic waves adverse current is extracted：Obtained tomato slurries and ethyl acetate will be digested according to mass ratio 1g: 6g, put
Enter in single stage type continuous flow upstream ultrasonic extractor, extractor there are 6 section pipes, wherein 1 section is soak extraction pipe, 5 sections are ultrasonic extraction
Pipe, single stage type continuous flow upstream ultrasonic extractor is is in pipeline closed state in extraction process, in the case where ultrasonic power is 245W
Adverse current extraction 20min, 53 DEG C of Extracting temperature, after filtering extraction, collection obtains filtrate and filter residue, and filter residue is repeated into ultrasound adverse current carries
Take 3 times, repeat to filter, finally merge all filtrates；
Step d is concentrated：Gained filtrate is sent into the crystallization of vacuum refrigeration crystallizer, vacuum 0.05Mpa, crystallization temperature
For -17 DEG C, crystallization time 4h, crystalline mixture is filtered to obtain, then gained crystalline mixture is concentrated in vacuo, vacuum is
0.06Mpa, thickening temperature are 50 DEG C, concentration time 45min；
Step e micro-wave vacuums：Material after gained is concentrated is sent into microwave vacuum dryer and dried, and drying time is
2h, vacuum 0.04Mpa, temperature are 50 DEG C；Resulting material is sent into micronizer to crush, obtains kind of 5-15% contents
Lycopene powder, fineness are 20-100 mesh, and lycopene powder moisture control is in 1-5%；
The preparation of step f special diets tomato nutrient powder product：To extract the skin slag after lycopene, juice as original
Material, is made tomato meal using microwave vacuum drying technology, is aided with soybean protein, dairy products and micronutrient (vitamin A, dimension
Raw plain B1, vitamin B2, vitamin C, vitamin D, vitamin E, folic acid, docosahexaenoic acid, calcium, iron, zinc, the nutrition such as selenium
Hardening agent forms), exploitation is applied to the special diet tomato nutrient powder product that all kinds of special populations are eaten, and optimization formula is such as
Under：
Tomato meal 40g, soybean protein 25g, dairy products 15g, 600ug containing vitamin A, vitamin B11500ug, dimension life
Plain B2400ug, vitamin C 350mg, vitamin D 150IU, vitamin E 25mga-TE Cernevit-12；And
The foliamin of the 450ug containing folic acid；Docosahexaenoic acid 1000mg；Calcic 250mg, iron 9mg, zinc 8mg, selenium 350ug are answered
Close Rare Elements Preparations.
Specific embodiment two
A kind of lycopene extraction method and special diet tomato nutrient powder, its making step are as follows：
Step a pretreatments of raw material：Raw material tomato, clear water cleaning tomato are taken, squeezing tomato obtains catsup；
Step b is digested：Catsup is pre-processed using the combined-enzyme method of cellulase and pectase, complex enzyme addition is
1.5L, cellulase addition are 0.3L, and the addition of pectase is 1.2L, enzymolysis time 5.5h, 45 DEG C of hydrolysis temperature；
Step c ultrasonic waves adverse current is extracted：Obtained tomato slurries and ethyl acetate will be digested according to mass ratio 1g: 5g, put
Enter in single stage type continuous flow upstream ultrasonic extractor, extractor there are 6 section pipes, wherein 1 section is soak extraction pipe, 5 sections are ultrasonic extraction
Pipe, single stage type continuous flow upstream ultrasonic extractor is is in pipeline closed state in extraction process, in the case where ultrasonic power is 200W
Adverse current extraction 25min, 55 DEG C of Extracting temperature, after filtering extraction, collection obtains filtrate and filter residue, and filter residue is repeated into ultrasound adverse current carries
Take 3 times, repeat to filter, finally merge all filtrates；
Step d is concentrated：Gained filtrate is sent into the crystallization of vacuum refrigeration crystallizer, vacuum 0.08Mpa, crystallization temperature
For -16 DEG C, crystallization time 5h, crystalline mixture is filtered to obtain, then gained crystalline mixture is concentrated in vacuo, vacuum is
0.03Mpa, thickening temperature are 45 DEG C, concentration time 50min；
Step e micro-wave vacuums：Material after gained is concentrated is sent into microwave vacuum dryer and dried, and drying time is
2.5h, vacuum 0.03Mpa, temperature are 55 DEG C；Resulting material is sent into micronizer to crush, obtains 5-15% contents
Lycopene powder, fineness are 20-100 mesh, and lycopene powder moisture control is in 1-5%；
The preparation of step f special diets tomato nutrient powder product：To extract the skin slag after lycopene, juice as original
Material, is made tomato meal using microwave vacuum drying technology, is aided with soybean protein, dairy products and micronutrient (vitamin A, dimension
Raw plain B1, vitamin B2, vitamin C, vitamin D, vitamin E, folic acid, docosahexaenoic acid, calcium, iron, zinc, the nutrition such as selenium
Hardening agent forms), exploitation is applied to the special diet tomato nutrient powder product that all kinds of special populations are eaten, and optimization formula is as follows：
Tomato meal 20g, soybean protein 10g, dairy products 7g, 500ug containing vitamin A, vitamin B11000ug, vitamin
B2450ug, vitamin C 300mg, vitamin D 100IU, vitamin E 13mga-TE Cernevit-12；And contain
Folic acid 220ug foliamin；Docosahexaenoic acid 500mg；Calcic 180mg, iron 4.5mg, zinc 4mg, selenium 150ug it is compound
Rare Elements Preparations.
Claims (3)
1. a kind of lycopene extraction method and special diet tomato nutrient powder, it is characterised in that using cellulase and pectin
The combined-enzyme method pretreatment tomato of enzyme, then using ethyl acetate as extractant, extract solution is obtained through centrifugal concentrating, it is finally true using microwave
Empty dry technology obtains lycopene powder, and wherein lycopene content is 5-15%, extracts slag, juice after lycopene, uses
Microwave vacuum drying technology produces the full powder of kind Jia, using the full powder of tomato as raw material, is aided with soybean protein isolate, maltodextrin, compound
Tomato nutrient powder is made in the production technology such as vitamin and composite mineral matter, preprocessed, mixing, allotment.
A kind of a kind of 2. preparation method of lycopene powder according to claim 1, it is characterised in that described tomato red
Plain extracting method comprises the following steps：
Step a pretreatments of raw material：Raw material tomato, clear water cleaning tomato are taken, squeezing tomato obtains catsup；
Step b is digested：Catsup, cellulase: pectase=1-5 are pre-processed using the combined-enzyme method of cellulase and pectase
: 3-8, complex enzyme addition 0.2-0.8mL/g, enzymolysis time 3-8h, 25-50 DEG C of hydrolysis temperature；
Step c ultrasonic waves adverse current is extracted：By the obtained tomato slurries of step b and ethyl acetate according to mass ratio 1: 3~10, it is put into
In single stage type continuous flow upstream ultrasonic extractor, 10-35min, Extracting temperature 40- are countercurrently extracted in the case where ultrasonic power is 150-250W
65 DEG C, after filtering extraction, collection obtains filtrate and filter residue, and filter residue is repeated into ultrasound adverse current extraction 1-3 times, repeats to filter, finally
Merge all filtrates；
Step d is concentrated：Gained filtrate is sent into the crystallization of vacuum refrigeration crystallizer, vacuum 0.03-0.1Mpa, crystallization temperature
For -22--4 DEG C, crystallization time 3-13h, crystalline mixture is filtered to obtain, then gained crystalline mixture is concentrated in vacuo, very
Reciprocal of duty cycle is 0.03-0.1Mpa, and thickening temperature is 45-75 DEG C, concentration time 30-80min；
Step e micro-wave vacuums：Material after gained is concentrated is sent into microwave vacuum dryer and dried, drying time 2-
5h, vacuum 0.03-0.09Mpa, temperature are 25-60 DEG C；Resulting material is sent into micronizer to crush, obtains 5-15%
The lycopene powder of content, fineness are 20-100 mesh, and the water content control of lycopene powder is in below 1-5%.
A kind of a kind of 3. preparation method of lycopene powder according to claim 1, it is characterised in that described special meals
Edible tomato nutrient powder, preparation method are as follows：
To extract the skin slag after lycopene, juice as raw material, tomato meal is made using microwave vacuum drying technology, is aided with soybean
Albumen, dairy products and micronutrient (vitamin A, vitamin B1, vitamin B2, vitamin C, vitamin D, vitamin E, leaf
The nutrition fortifiers such as acid, docosahexaenoic acid, calcium, iron, zinc, selenium form), exploitation is applied to the spy that all kinds of special populations are eaten
Different meals tomato nutrient powder product, optimization formula are as follows：
Tomato meal 10-40g, soybean protein 10-30g, dairy products 5-15g, 500-1000ug containing vitamin A, vitamin B1 500-
1500ug, vitamin B2400-600ug, vitamin C 100-350mg, vitamin D 60-150IU, vitamin E 10-
25mga-TE Cernevit-12；And the foliamin of the 200-450ug containing folic acid；Docosahexaenoic acid 500-
1000mg；Calcic 100-250mg, iron 3-9mg, zinc 3-8mg, selenium 100-350ug composite trace element preparation.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115316665A (en) * | 2022-06-24 | 2022-11-11 | 万宝甲由(北京)科技有限责任公司 | Composition preparation containing water-soluble dietary fiber of tomato and lycopene and preparation method thereof |
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| CN1463623A (en) * | 2002-06-20 | 2003-12-31 | 中国科学院新疆理化技术研究所 | Tomato product finely processing method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115316665A (en) * | 2022-06-24 | 2022-11-11 | 万宝甲由(北京)科技有限责任公司 | Composition preparation containing water-soluble dietary fiber of tomato and lycopene and preparation method thereof |
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