CN107432497B - Functional essence suitable for heating non-combustion tobacco products - Google Patents

Functional essence suitable for heating non-combustion tobacco products Download PDF

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Publication number
CN107432497B
CN107432497B CN201610353609.6A CN201610353609A CN107432497B CN 107432497 B CN107432497 B CN 107432497B CN 201610353609 A CN201610353609 A CN 201610353609A CN 107432497 B CN107432497 B CN 107432497B
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China
Prior art keywords
dimethoxyphenol
functional
tobacco
dimethoxybenzene
heating
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CN201610353609.6A
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Chinese (zh)
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CN107432497A (en
Inventor
杨君
胡安福
徐清泉
尹洁
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China Tobacco Zhejiang Industrial Co Ltd
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China Tobacco Zhejiang Industrial Co Ltd
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Classifications

    • A24F47/004
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/301Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/32Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0026Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms

Abstract

The invention belongs to the technical field of tobacco, and particularly relates to a functional essence suitable for heating a non-combustion tobacco product. A functional flavoring suitable for heating non-combustible tobacco products, the functional flavoring comprises the following components by weight percent: 1-3% of m-dimethoxyphenol, 0-5% of p-dimethoxyphenol, 0.5-2% of 2, 6-dimethoxyphenol, 0-3% of p-ethylphenol, 1-5% of 2-isopropylphenol, 0-4% of 3, 4-dimethylphenol, 0-0.5% of m-dimethoxybenzene, 0-0.5% of p-dimethoxybenzene, 0-0.5% of 1-methyl-3-methoxy-4-isopropylbenzene, 1-3% of eugenol, 0-1% of isoeugenol, 0.5-2% of guaiacol and 0.5-1% of propenyl ethyl guaiacol; 70-90% of solvent. The functional spice of the invention has stable property, strong pertinence, convenient use and simple production process.

Description

Functional essence suitable for heating non-combustion tobacco products
Technical Field
The invention belongs to the technical field of tobacco, and particularly relates to a functional essence suitable for heating a non-combustion tobacco product.
Background
Heated non-combustible smoking articles have originated in the eighties of the last century and have been known to have a history of nearly 30 years since the appearance of the product. Through continuous technical innovation and product popularization, the tobacco product is one of important types of novel tobacco products. The smoke generated by the product is closer to the traditional cigarette, and the sidestream smoke and partial harmful components are obviously reduced, so that the cigarette has certain market potential, and the related technology becomes the hot spot of the research of foreign tobacco companies at present. In recent years, with the increasing of the smoke control strength, foreign tobacco companies have increased research and development strength of heating non-combustion type tobacco products as substitute products of traditional cigarettes and started to popularize the tobacco products to public health departments and consumers in the world, which also draws wide attention to the heating non-combustion type tobacco products in the international tobacco field and defines the tobacco products as 'real harm reduction products'. Chinese patent application CN88101196, 89108679.X of Reynolds tobacco corporation and Chinese patent application CN02826243.3, CN200980159916.9 of Japanese tobacco corporation disclose product constitution of carbon heating type heating non-combustion tobacco product and related technology. Chinese patents CN94102530.6, CN96194107.3, CN96195594.5, CN200380102439.5 and CN200580036230.2 applied by the famo tobacco company disclose product compositions of electric heating type heating non-combustion tobacco products and related technologies. However, the analysis of the existing products shows that the sensory quality of the smoke is not satisfactory, and the smoke is to be further improved, which may be the main reason that the products cannot be completely accepted by the market at present. Therefore, the invention discloses a functional essence formula capable of effectively improving the sensory quality of the heating non-combustion tobacco products, and has important significance for the development of the heating non-combustion tobacco products.
Disclosure of Invention
In order to solve the above technical problems, the present invention aims to provide a functional flavor suitable for a heated non-combustible tobacco product, which improves the sensory quality of the heated non-combustible tobacco product.
In order to achieve the purpose, the invention adopts the following technical scheme:
a functional flavoring suitable for heating non-combustible tobacco products, the functional flavoring comprises the following components by weight percent: 1-3% of m-dimethoxyphenol, 0-5% of p-dimethoxyphenol, 0.5-2% of 2, 6-dimethoxyphenol, 0-3% of p-ethylphenol, 1-5% of 2-isopropylphenol, 0-4% of 3, 4-dimethylphenol, 0-0.5% of m-dimethoxybenzene, 0-0.5% of p-dimethoxybenzene, 0-0.5% of 1-methyl-3-methoxy-4-isopropylbenzene, 1-3% of eugenol, 0-1% of isoeugenol, 0.5-2% of guaiacol and 0.5-1% of propenyl ethyl guaiacol; 70-95% of solvent.
Preferably, the functional perfume consists of the following components in percentage by weight: m-dimethoxyphenol 1.5-2.5%, p-dimethoxyphenol 2-4%, 2, 6-dimethoxyphenol 1-2%, p-ethylphenol 0.5-2.5%, 2-isopropylphenol 2-4%, 3, 4-dimethylphenol 1-3%, m-dimethoxybenzene 0.2-0.4%, p-dimethoxybenzene 0.2-0.4%, 1-methyl-3-methoxy-4-isopropylbenzene 0.2-0.4%, eugenol 1-3%, isoeugenol 0.5-1%, guaiacol 1-1.5%, propenyl ethylguaiacol 0.5-1%; 70-90% of solvent.
Preferably, the solvent is one or a mixture of glycerol, propylene glycol and ethanol.
Preferably, the functional perfume consists of the following components in percentage by weight: m-dimethoxyphenol 1%, p-dimethoxyphenol 2%, 2, 6-dimethoxyphenol 1.5%, p-ethylphenol 1%, 2-isopropylphenol 2%, 3, 4-dimethylphenol 1%, m-dimethoxybenzene 0.2%, p-dimethoxybenzene 0.3%, eugenol 2%, isoeugenol 0.5%, guaiacol 1%, propenyl ethylguaiacol 0.8%; and 86.7 percent of ethanol.
Preferably, the functional perfume consists of the following components in percentage by weight: m-dimethoxyphenol 2%, p-dimethoxyphenol 3%, 2, 6-dimethoxyphenol 1%, p-ethylphenol 0.5%, 2-isopropylphenol 0.5%, 3, 4-dimethylphenol 0.5%, m-dimethoxybenzene 0.2%, p-dimethoxybenzene 0.1%, 1-methyl-3-methoxy-4-isopropylbenzene 0.2%, eugenol 1%, isoeugenol 0.5%, guaiacol 1%, propenyl guaethol 0.7%; 60% of ethanol and 29.5% of propylene glycol.
The functional spice provided by the invention can endow the heated non-combustion tobacco products with obvious smoking aroma, enrich aroma and improve sensory quality, and can enable the sensory characteristics of the heated non-combustion tobacco products to be closer to that of the traditional cigarettes, thereby being beneficial to improving the market acceptance of the heated non-combustion tobacco products. The functional spice of the invention has stable property, strong pertinence, convenient use and simple production process.
Detailed Description
The invention is further described below with reference to examples of embodiment but without in any way limiting the scope of the invention.
Example 1
Functional essence formula (mass percentage)
M-dimethoxyphenol 1%, p-dimethoxyphenol 2%, 2, 6-dimethoxyphenol 1.5%, p-ethylphenol 1%, 2-isopropylphenol 2%, 3, 4-dimethylphenol 1%, m-dimethoxybenzene 0.2%, p-dimethoxybenzene 0.3%, eugenol 2%, isoeugenol 0.5%, guaiacol 1%, propenyl ethylguaiacol 0.8%; and 86.7 percent of ethanol.
Adding the functional essence module solution into cured tobacco shreds according to the addition of 50 ppm, balancing for 48 h, heating blank tobacco shreds and flavored tobacco shreds at 300 deg.C by using a laboratory heating device, and performing sensory evaluation on the released smoke. The result shows that after the functional essence module is added, the smoking aroma of the flue gas released by the flue-cured tobacco shreds in a non-combustion state is prominent, the aroma is rich, the aroma quality is improved, and the aroma characteristic of the flue-cured tobacco shreds is closer to that of the traditional cigarette.
Example 2
Functional essence formula (mass percentage)
M-dimethoxyphenol 2%, p-dimethoxyphenol 3%, 2, 6-dimethoxyphenol 1%, p-ethylphenol 0.5%, 2-isopropylphenol 0.5%, 3, 4-dimethylphenol 0.5%, m-dimethoxybenzene 0.2%, p-dimethoxybenzene 0.1%, 1-methyl-3-methoxy-4-isopropylbenzene 0.2%, eugenol 1%, isoeugenol 0.5%, guaiacol 1%, propenyl guaethol 0.7%; 60% of ethanol and 29.5% of propylene glycol.
Adding the functional essence module solution into cured tobacco shreds according to the addition of 50 ppm, balancing for 48 h, heating blank tobacco shreds and flavored tobacco shreds at 300 deg.C by using a laboratory heating device, and performing sensory evaluation on the released smoke. The result shows that after the functional essence module is added, the smoking aroma of the flue gas released by the flue-cured tobacco shreds in a non-combustion state is prominent, the aroma is rich, the aroma quality is improved, and the aroma characteristic of the flue-cured tobacco shreds is closer to that of the traditional cigarette.

Claims (1)

1. A functional flavoring suitable for heating non-combustible tobacco products, which is characterized by comprising the following components in percentage by weight: m-dimethoxyphenol 1%, p-dimethoxyphenol 2%, 2, 6-dimethoxyphenol 1.5%, p-ethylphenol 1%, 2-isopropylphenol 2%, 3, 4-dimethylphenol 1%, m-dimethoxybenzene 0.2%, p-dimethoxybenzene 0.3%, eugenol 2%, isoeugenol 0.5%, guaiacol 1%, propenyl ethylguaiacol 0.8%; and 86.7 percent of ethanol.
CN201610353609.6A 2016-05-25 2016-05-25 Functional essence suitable for heating non-combustion tobacco products Active CN107432497B (en)

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Publication number Priority date Publication date Assignee Title
CN108893195A (en) * 2018-06-08 2018-11-27 南通金源新材料有限公司 A kind of composition suitable for heating the cigarette that do not burn
CN109156868A (en) * 2018-10-23 2019-01-08 云南中烟工业有限责任公司 A kind of essence with tongue fur note style and features and include the cigarette of the essence
CN109156870B (en) * 2018-10-23 2021-01-29 云南中烟工业有限责任公司 Additive with moss aroma style characteristics and cigarette containing additive

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US7576170B2 (en) * 2003-12-19 2009-08-18 Momentive Performance Materials Cyclic siloxane compositions for the release of active ingredients
CN101416773B (en) * 2007-10-22 2011-08-24 武汉烟草(集团)有限公司 Method for increasing the quality of flavoring essences for tobacco using oak
CN102304430B (en) * 2011-03-17 2013-06-05 广州市澳键丰泽生物科技有限公司 Formula of tobacco flavoring essence with sweet fragrance
CN102230918A (en) * 2011-06-22 2011-11-02 红云红河烟草(集团)有限责任公司 Method for determining benzene and benzene series contents in flavor and spices for cigarettes
CN104498186B (en) * 2014-12-28 2017-10-13 中国烟草总公司郑州烟草研究院 A kind of electronic cigarette fragrance formulations
CN104479873B (en) * 2014-12-28 2018-03-09 中国烟草总公司郑州烟草研究院 A kind of electronic cigarette smoke flavour spices module formula
CN105146734A (en) * 2015-08-14 2015-12-16 贵州中烟工业有限责任公司 Maotai-flavor tobacco product capable of avoiding burning as being heated and preparation method of tobacco product

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