CN107410808A - A kind of preparation method of chrysanthemum concrete - Google Patents
A kind of preparation method of chrysanthemum concrete Download PDFInfo
- Publication number
- CN107410808A CN107410808A CN201710271005.1A CN201710271005A CN107410808A CN 107410808 A CN107410808 A CN 107410808A CN 201710271005 A CN201710271005 A CN 201710271005A CN 107410808 A CN107410808 A CN 107410808A
- Authority
- CN
- China
- Prior art keywords
- chrysanthemum
- extraction
- extract
- water
- filtering
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000007516 Chrysanthemum Nutrition 0.000 title claims abstract description 63
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 244000189548 Chrysanthemum x morifolium Species 0.000 title 1
- 239000000284 extract Substances 0.000 claims abstract description 39
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 26
- 238000000605 extraction Methods 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000001914 filtration Methods 0.000 claims abstract description 11
- 238000003809 water extraction Methods 0.000 claims abstract description 9
- 241000723353 Chrysanthemum Species 0.000 claims abstract 19
- 240000005250 Chrysanthemum indicum Species 0.000 claims description 45
- 238000010992 reflux Methods 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- 239000012141 concentrate Substances 0.000 claims description 3
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 3
- 230000008719 thickening Effects 0.000 claims description 3
- 235000018959 Chrysanthemum indicum Nutrition 0.000 claims description 2
- 235000008495 Chrysanthemum leucanthemum Nutrition 0.000 claims description 2
- 235000000604 Chrysanthemum parthenium Nutrition 0.000 claims description 2
- 241000628997 Flos Species 0.000 claims description 2
- 235000008384 feverfew Nutrition 0.000 claims description 2
- VYQNWZOUAUKGHI-UHFFFAOYSA-N monobenzone Chemical compound C1=CC(O)=CC=C1OCC1=CC=CC=C1 VYQNWZOUAUKGHI-UHFFFAOYSA-N 0.000 claims description 2
- 244000035851 Chrysanthemum leucanthemum Species 0.000 claims 1
- 239000000796 flavoring agent Substances 0.000 abstract description 13
- 235000019634 flavors Nutrition 0.000 abstract description 13
- 238000000034 method Methods 0.000 abstract description 8
- 239000000463 material Substances 0.000 abstract description 5
- 239000000126 substance Substances 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 description 5
- 206010019233 Headaches Diseases 0.000 description 2
- 244000269722 Thea sinensis Species 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 231100000869 headache Toxicity 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 244000192528 Chrysanthemum parthenium Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 208000009205 Tinnitus Diseases 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 208000013403 hyperactivity Diseases 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000001223 reverse osmosis Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
- 231100000886 tinnitus Toxicity 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses a kind of preparation method of chrysanthemum concrete, including alcohol extracting, filtering, filter residue water extraction, filtering, concentrated extract again, the problem of present invention easily scatters and disappears for chrysanthemum-flavored, propose two-step extraction, it is the extraction for carrying out volatile flavor substance first, it is stripped using ethanol, its alcohol extract uses directly as formula；Then water extraction is carried out again, preferably selects inverse concentration gradient, and combines vacuum concentration process and obtains the water extracted immersing paste, as one of formula material；Using above-mentioned two steps extraction process, two kinds of extracts of chrysanthemum alcohol extract and water extract can be obtained, wherein water extract mainly provides the main body flavour and nutriment of drink, and alcohol extract mainly provides the main body flavor of chrysanthemum.
Description
Technical field
The present invention relates to a kind of preparation method of chrysanthemum concrete, belongs to food processing technology field.
Background technology
Chrysanthemum is one of conventional Chinese medicine, recorded according to ancient books as one of ten big famous flower of China, chrysanthemum sweet-bitter flavor, property
It is slightly cold；There is scattered wind heat-clearing, clear liver and improve vision and detoxicating, relieving inflammation etc. acts on, it is puckery to dry, hyperactivity of fire, mesh, or take out caused by wind, cold, wet
Limbs pain, numb disease have the effect of certain；Cold anemopyretic, headache etc. are cured mainly, is had to dizziness, headache, tinnitus anti-
Effect is controlled, chrysanthemum steeps the function that the chrysanthemum tea after boiling is quenched one's thirst with its strong chrysanthemum perfume, plurality of health care functions and heat-clearing, deep by the masses
Welcome, China's chrysanthemum resources have developed rapidly, and four big chrysanthemums have been respectively formed industry development base, be used every year as medicine food resource
Drying chrysanthemum yield more than 3000 tons.But the deep processing of chrysanthemum resources more lags, in the market is mainly carried out with dried flower
Sale, jasmine tea is turned into by compounding on a small quantity, separately there are the solid beverages such as some chrysanthemum particles, because of process technology problem, market acceptance
Degree is not high.Subject matter is that these deep processing drinks lack typical chrysanthemum-flavored, and the chrysanthemum active material contained is total
Body is not high.
Because Scent of Chrysanthemum is simple and elegant, compared with other drinks are spent, main body flavor does not protrude, in addition in the drying processing phase
Between, some volatile compounds have lost, if using common water extraction concentration technology, it is easy to cause entering for volatile flavor
One step is scattered and disappeared；And solvent extraction is carried out to chrysanthemum, generally need the solvent for adding more than 20 times just to can guarantee that extraction is abundant every time,
This just needs subsequently to carry out substantial amounts of concentration operation；And concentration operation, easily cause scattering and disappearing for volatile ingredient, during it
It is difficult to carry out the recovery of flavor, carrying out concentration using counter-infiltration contributes to the flavor of reservation chrysanthemum, but reverse osmosis concentration is not thorough
Bottom, to obtain medicinal extract sample product, it is still desirable to heat concentration.
The content of the invention
The problem of easily being scattered and disappeared for chrysanthemum-flavored, the present invention proposes two-step extraction, is to carry out volatility wind first
The extraction of taste material, is stripped using ethanol, and its alcohol extract uses directly as formula；Then water extraction is carried out again, is preferably selected
Inverse concentration gradient is selected, and combines vacuum concentration process and obtains the water extracted immersing paste, as one of formula material；Extracted using above-mentioned two step
Technique, can obtain two kinds of extracts of chrysanthemum alcohol extract and water extract, wherein water extract mainly provide drink main body flavour and
Nutriment, alcohol extract mainly provide the main body flavor of chrysanthemum.
Technical scheme is as follows：
The preparation method of chrysanthemum concrete, including alcohol extracting, filtering, filter residue water extraction, filtering, concentrated extract again, are specifically included following
Content：
（1）Chrysanthemum is crushed to 10-20 mesh, is put into the extraction equipment with reflux cooler, adds volume ratio 50%-95%'s
Ethanol water, addition are 10-30 times of volume of chrysanthemum quality, are warming up to 35 DEG C -80 DEG C, refluxing extraction 0.2h-2.0h；Carry
After taking end, first of chrysanthemum alcohol extract is filtered out；For alcohol extract through being concentrated under reduced pressure into 1-2 times of volume of chrysanthemum quality, it concentrates temperature
40 DEG C -50 DEG C of degree；
（2）In above-mentioned steps（1）Water is added in chrysanthemum filter residue and carries out second extraction, amount of water is the 10- of raw material chrysanthemum quality
30 times of volumes, 50 DEG C -100 DEG C are warming up to, extract 0.2h-2.0h；After extraction terminates, second extract solution is filtered out；Extract solution passes through
Vacuum filter or plate-frame filtering, are concentrated in vacuo, 50 DEG C -70 DEG C of its thickening temperature, concentration volume to raw material chrysanthemum quality
0.3-1.0 times, obtain chrysanthemum concrete.
Described chrysanthemum can arbitrarily select Bo feverfew, tribute chrysanthemum, chrysanthemum indicum, chu chrysanthemum, FLOS CHRYSANTHEMI ALBA from Haizhou of China.
Described chrysanthemum can include the complete chrysanthemum of each kind condition or inferior flower.
The key problem in technology of the present invention is two aspects：（1）Extracted using alcohol reflux, obtain high concentration extract solution.But
Extraction time is unsuitable long, and otherwise insoluble substance dissolution is more, and bad pungent also can dissolution；（2）Water extraction process
Solid-liquid ratio should be controlled, too big solid-liquid ratio will increase subsequent concentration process burden, and the method for prioritizing selection is continuous flow upstream
Extraction, has been commercialized mechanized equipment at present.
Beneficial effects of the present invention：
The problem of present invention easily scatters and disappears for chrysanthemum-flavored, it is proposed that two-step extraction, be to carry out Flavor volatiles first
The extraction of matter, is stripped using ethanol, and its alcohol extract uses directly as formula；Then water extraction is carried out again, is preferably selected inverse
Concentration gradient, and combine vacuum concentration process and obtain the water extracted immersing paste, as one of formula material；Work is extracted using above-mentioned two step
Skill, two kinds of extracts of chrysanthemum alcohol extract and water extract can be obtained, wherein water extract mainly provides main body flavour and the battalion of drink
Material is supported, alcohol extract mainly provides the main body flavor of chrysanthemum.
Embodiment
Embodiment 1：The preparation method of chrysanthemum concrete, including alcohol extracting, filtering, filter residue water extraction, filtering, concentrated extract again,
Specifically include herein below：
（1）Chrysanthemum is crushed to 10-20 mesh, is put into the extraction equipment with reflux cooler, adds volume ratio 50%-95%'s
Ethanol water, addition are 10-30 times of volume of chrysanthemum quality, are warming up to 35 DEG C -80 DEG C, refluxing extraction 0.2h-2.0h；Carry
After taking end, first of chrysanthemum alcohol extract is filtered out；For alcohol extract through being concentrated under reduced pressure into 1-2 times of volume of chrysanthemum quality, it concentrates temperature
40 DEG C -50 DEG C of degree；
（2）In above-mentioned steps（1）Water is added in chrysanthemum filter residue and carries out second extraction, amount of water is the 10- of raw material chrysanthemum quality
30 times of volumes, 50 DEG C -100 DEG C are warming up to, extract 0.2h-2.0h；After extraction terminates, second extract solution is filtered out；Extract solution passes through
Vacuum filter or plate-frame filtering, are concentrated in vacuo, 50 DEG C -70 DEG C of its thickening temperature, concentration volume to raw material chrysanthemum quality
0.3-1.0 times, obtain chrysanthemum concrete.
Claims (3)
1. a kind of preparation method of chrysanthemum concrete, it is characterised in that including water extraction, filtering, the concentration again of alcohol extracting, filtering, filter residue
Medicinal extract, specifically include herein below：
（1）Chrysanthemum is crushed to 10-20 mesh, is put into the extraction equipment with reflux cooler, adds volume ratio 50%-95%'s
Ethanol water, addition are 10-30 times of volume of chrysanthemum quality, are warming up to 35 DEG C -80 DEG C, refluxing extraction 0.2h-2.0h；Carry
After taking end, first of chrysanthemum alcohol extract is filtered out；For alcohol extract through being concentrated under reduced pressure into 1-2 times of volume of chrysanthemum quality, it concentrates temperature
40 DEG C -50 DEG C of degree；
（2）In above-mentioned steps（1）Water is added in chrysanthemum filter residue and carries out second extraction, amount of water is the 10- of raw material chrysanthemum quality
30 times of volumes, 50 DEG C -100 DEG C are warming up to, extract 0.2h-2.0h；After extraction terminates, second extract solution is filtered out；Extract solution passes through
Vacuum filter or plate-frame filtering, are concentrated in vacuo, 50 DEG C -70 DEG C of its thickening temperature, concentration volume to raw material chrysanthemum quality
0.3-1.0 times, obtain chrysanthemum concrete.
2. the preparation method of chrysanthemum concrete according to claim 1, it is characterised in that described chrysanthemum can arbitrarily select Bo
Feverfew, tribute chrysanthemum, chrysanthemum indicum, chu chrysanthemum, FLOS CHRYSANTHEMI ALBA from Haizhou of China.
3. the preparation method of chrysanthemum concrete according to claim 1, it is characterised in that it is complete that chrysanthemum can include each kind condition
Whole chrysanthemum or inferior flower.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710271005.1A CN107410808A (en) | 2017-04-24 | 2017-04-24 | A kind of preparation method of chrysanthemum concrete |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710271005.1A CN107410808A (en) | 2017-04-24 | 2017-04-24 | A kind of preparation method of chrysanthemum concrete |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107410808A true CN107410808A (en) | 2017-12-01 |
Family
ID=60424220
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710271005.1A Pending CN107410808A (en) | 2017-04-24 | 2017-04-24 | A kind of preparation method of chrysanthemum concrete |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107410808A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001245629A (en) * | 2000-03-07 | 2001-09-11 | Api Co Ltd | Material for medicament or health food and method for producing the same |
| CN101530445A (en) * | 2008-03-11 | 2009-09-16 | 凌如文 | Dry extract of chrysanthemum |
| CN104232313A (en) * | 2014-09-25 | 2014-12-24 | 秦富英 | Flowery extract |
| CN104523994A (en) * | 2014-12-24 | 2015-04-22 | 朵海林 | Wolfberry and sanvitalia compound composition and preparation method thereof |
| CN104856921A (en) * | 2015-06-01 | 2015-08-26 | 新疆生命核力高科股份有限公司 | Chrysanthemum lip-moistening balm and preparation method thereof |
-
2017
- 2017-04-24 CN CN201710271005.1A patent/CN107410808A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001245629A (en) * | 2000-03-07 | 2001-09-11 | Api Co Ltd | Material for medicament or health food and method for producing the same |
| CN101530445A (en) * | 2008-03-11 | 2009-09-16 | 凌如文 | Dry extract of chrysanthemum |
| CN104232313A (en) * | 2014-09-25 | 2014-12-24 | 秦富英 | Flowery extract |
| CN104523994A (en) * | 2014-12-24 | 2015-04-22 | 朵海林 | Wolfberry and sanvitalia compound composition and preparation method thereof |
| CN104856921A (en) * | 2015-06-01 | 2015-08-26 | 新疆生命核力高科股份有限公司 | Chrysanthemum lip-moistening balm and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103642592B (en) | Full utilization technology of rose flower | |
| CN103349110B (en) | Active tea cream high in extraction rate and complete in beneficial component preservation and preparation method thereof | |
| CN104970147B (en) | A kind of preparation method of high fluorine high chlorophyll tea extract | |
| CN106433986A (en) | Chinese prickly ash essential oil and preparation method thereof | |
| CN102533433A (en) | Method for supercritical extraction of sea buckthorn oil | |
| CN110447889A (en) | A kind of preparation method of Ganodenna Lucidum P.E | |
| CN105969527A (en) | Comprehensive utilization method of ginger leaves | |
| CN107568548B (en) | Sophora flower bud solid beverage and preparation method thereof | |
| CN106433985B (en) | A kind of ginger essential oil and preparation method thereof | |
| CN106962530A (en) | A kind of Yellow Fructus Gardeniae leaf black tea and its processing method | |
| CN102461954A (en) | Deodorization allicin composite beverage | |
| CN104397291A (en) | Preparation method of concentrated juice of herbal tea | |
| CN104974194B (en) | A kind of extraction process of grape skin polyphenol | |
| CN104224867B (en) | A kind of desmodium sugar-free particle and preparation method thereof | |
| CN105875935A (en) | Pearl barley effervescent tea tablets capable of eliminating dampness | |
| CN107410808A (en) | A kind of preparation method of chrysanthemum concrete | |
| CN107232469A (en) | It is a kind of to retain natural color, smell and taste and the chrysanthemum solid beverage processing method of nutritive value | |
| CN101928658B (en) | Method for producing acanthopanax bark wine by traditional Chinese medicine steam extraction method | |
| CN115769882A (en) | Roselle dried orange peel concentrated essence and preparation method thereof | |
| CN104371891B (en) | A kind of preparation method avenging chrysanthemum bitter-buckwheat nutritive wine | |
| CN109568373A (en) | A method of pulp of dogwood fruit or wine-prepared fructus corni granule are prepared using continuous dynamic countercurrent extraction process | |
| CN114366796A (en) | Preparation method of ginger oil with dampness eliminating effect | |
| CN101928660B (en) | Method for producing cortex acanthopanacis spirits by Chinese medicinal material fluid extract method | |
| CN104186872B (en) | Borneol leaves extracting solution and borneol leaves green tea beverage and preparation method | |
| CN105981835A (en) | Cooling instant green tea with herba menthae |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171201 |
|
| RJ01 | Rejection of invention patent application after publication |