CN101928658B - Method for producing acanthopanax bark wine by traditional Chinese medicine steam extraction method - Google Patents

Method for producing acanthopanax bark wine by traditional Chinese medicine steam extraction method Download PDF

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CN101928658B
CN101928658B CN 201010252011 CN201010252011A CN101928658B CN 101928658 B CN101928658 B CN 101928658B CN 201010252011 CN201010252011 CN 201010252011 CN 201010252011 A CN201010252011 A CN 201010252011A CN 101928658 B CN101928658 B CN 101928658B
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wine
acanthopanax bark
medicinal materials
chinese
producing
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CN101928658A (en
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钱建华
方小明
龚景华
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ZHEJIANG ZHIZHONGHE INDUSTRIAL CO., LTD.
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ZHEJIANG ZHIZHONGHE INDUSTRIAL Co Ltd
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Abstract

The invention relates to a method for producing acanthopanax bark wine, in particular to a method for producing the acanthopanax bark wine by improving decoction. The method for producing the acanthopanax bark wine by the traditional Chinese medicine steam extraction method comprises the following steps of: preparing the decoction, preparing semi-finished wine and filling, wherein the step of preparing the decoction is to extract Chinese medicinal materials by adopting the steam extraction method, and the Chinese medicinal materials are at least one of acanthopanax bark, costustoot, clove, amomum fruit, cinnamon and superior cinnamon. The Chinese medicinal materials with strong aromas are extracted by the steam extraction method, and the extract is directly added into the acanthopanax bark wine. Therefore, the acanthopanax bark wine keeps aromatic components of the medicinal materials, overcomes the defects of strong medicinal smell and poor mouthfeel, and has light medicinal smell and pure and good medicinal aroma, so that the quality and sale of acanthopanax bark wine products are improved. Meanwhile, the method for producing the acanthopanax bark wine completely extracts active ingredients of the traditional Chinese medicines, greatly improves the production efficiency, shortens the production cycle of a liquid medicine, and reduces the production cost.

Description

The method of producing acanthopanax bark wine by Chinese medicine steam extraction method
Technical field
The present invention relates to a kind of production method of slender acanthopanax bark spirit, relate in particular to a kind of production method of improving concoction preparation method's slender acanthopanax bark spirit.
Background technology
Slender acanthopanax bark spirit is the traditional product in Zhejiang, is a traditional famous brand of wine that long history is arranged.Slender acanthopanax bark spirit adopts China's traditional medicine and modern nutriology knowledge, select the 20 kinds of traditional Chinese medicines materials such as Wu Chia Pee, Radix Angelicae Sinensis, fructus amomi, cape jasmine, radix polygonati officinalis, behind the special vintage soaking in Chinese liquor, add glutinous rice-honey wine, white sugar, honey, adopt unique " fermentation of nine wines, four degree leachings " making method and Thousand-Island Lake crystal's system to form.In slender acanthopanax bark spirit's production process, need to make liquid, the effective constituent in namely extracting.The technology of making at present liquid can be divided into pickling process, circumfluence method and percolation.
(1) pickling process: be divided into cold pickling process, hot pickling process and pump circulation dipping
1. cold pickling process is at room temperature to flood Chinese medicinal materials, claims again the normal temperature dipping method.Be operating as get it filled material meal or fragment, be equipped with in the lid container, add quantitative basic wine, generally flood more than 14 days, in the steeping process, often stir or jolting.
2. hot pickling process, traditional method places container with lid with after the medicinal material chopping or pulverizing, and adds the wine of prescription specified amount, with after boiling certain hour, then lets cool storage.Industry in producing greatly binds up with gauze the Chinese medicinal materials after the coarse crushing, is suspended from the liquor, puts into the container of sealing again, puts in the water-bath to flood 3-7 days with 40-50 ℃, also can flood twice and merge immersion liquid, filters after the placement a few days and collects medicinal liquor.
3. pump circulation is flooded: will extract with the disposable preparation of wine liquid full dose complete, utilize at normal temperatures pump to circulate and contact extraction with medicinal material extracting circulation fluid, on extractor, the outlet of circulation fluid pipe should have spray equipment, evenly places in the hope of liquid stream and produces spice kind slag or channeling.
(2) percolation
Percolation is that the medicinal material coarse grain is put in the percolator, and basic wine adds from the top of percolator continuously, and percolate constantly flows out from the bottom, thereby lixiviate goes out the method for contained soluble components in the medicinal material.
(3) circumfluence method: be divided into backflow hot dipping method and reflow cold dip method
1. backflow hot dipping method: the processing of crude drugs process of preparing Chinese medicine is placed in the leacher, connect condenser on the leacher, volume (basic wine) is added in the leacher, heated solvent, solvent evaporation makes molten gas cooling become liquid by condenser, this liquid is back in the leacher again, so repeatedly, until leach fully.
2. reflow cold dip method: the copper wire basket that pharmaceutical decocting piece is placed leacher.Add basic wine by liquid storage cylinder through valve, when treating that leach liquor is full of siphon pipe, then automatically flow in the evaporating pan through valve, be heated evaporation in evaporating pan, steam enters condenser along conduit, flows into again in the liquid storage cylinder after condensation, flow into leacher, repeatedly lixiviate by valve again.
The producer of present most of production slender acanthopanax bark spirit is most to adopt and all uses pickling process and percolation to extract Chinese medicinal materials to make liquid.The advantage of pickling process is the flavour ingredient in the Chinese medicinal materials fully to be extracted, but complicated component fails effective constituent and other invalid components are carried out effective separation, and the speed of extracting is slow, production cycle is long, extracts active ingredients is incomplete, production efficiency is low, and flavour of a drug were denseer when preparation was produced in the slender acanthopanax bark spirit.The advantage that percolation extracts Chinese medicinal materials be can accelerate the Chinese medicinal materials extraction rate, extracts active ingredients is more complete, it is higher to give birth to tea efficient, but the liquid of making preparation when producing in the slender acanthopanax bark spirit flavour of a drug denseer.According to present human consumer, generally believe that slender acanthopanax bark spirit's flavour of a drug are dense, be not easy entrance, seriously restricted the sale of slender acanthopanax bark spirit.
Summary of the invention
Solved the defective that slender acanthopanax bark spirit's flavour of a drug are dense, be difficult for entrance, the method that the purpose of this invention is to provide a kind of producing acanthopanax bark wine by Chinese medicine steam extraction method, the method adopts the vapor extraction Chinese medicinal materials directly to be formulated in the slender acanthopanax bark spirit, the flavour ingredient that has kept medicinal material, thus slender acanthopanax bark spirit's product quality and sale improved.
In order to realize above-mentioned purpose, the present invention adopts following technical scheme:
The method of producing acanthopanax bark wine by Chinese medicine steam extraction method, the method comprises concoction preparation, the preparation of work in-process wine and can step, wherein: adopt described hydrodistillation method to extract Chinese medicinal materials in the preparation of described concoction, adopt the Chinese medicinal materials of hydrodistillation method to be at least a kind of in Wu Chia Pee, the banksia rose, cloves, fructus amomi, Chinese cassia tree and the official osmanthus.
As preferably, the Chinese medicinal materials of above-mentioned employing hydrodistillation method is Wu Chia Pee, the banksia rose, cloves, fructus amomi, Chinese cassia tree and official osmanthus.
As preferably, the weight ratio of Chinese medicinal materials weight and water was at 1: 1.5~1: 3 during above-mentioned hydrodistillation.
As preferably, adopting the add-on of the concoction of every flavor Chinese medicine that the hydrodistillation method extracts in the above-mentioned work in-process wine preparation is 0.1%~0.3% of slender acanthopanax bark spirit's total amount.
As preferably, also adopt traditional pickling process to extract Chinese medicinal materials in the above-mentioned concoction preparation, the Chinese medicinal materials that adopts traditional pickling process to extract is wolfberry fruit, Herba Epimedii, wolfberry fruit, cassia twig, Mountain Spicy Tree Fruit, red colouring agent for food, also used as a Chinese medicine, cape jasmine, Radix Angelicae Sinensis, Radix Codonopsis, kaempferia galamga, dried orange peel, Buddha's hand and peppermint.
As preferred again, Chinese medicinal materials weight and basic wine weight ratio were at 1: 3~1: 6 when Chinese medicinal materials flooded when above-mentioned traditional pickling process was extracted.
Add-on as the concoction of every flavor Chinese medicine of the traditional pickling process extraction of employing in preferred again, the above-mentioned work in-process wine preparation is 0.5%~2% of slender acanthopanax bark spirit's total amount.
The present invention is owing to adopted above-mentioned technical scheme, employing is the denseer Chinese medicinal materials of hydrodistillation fragrance, extract directly preparation joins in the slender acanthopanax bark spirit, the flavour ingredient that has kept medicinal material, solved the defective that slender acanthopanax bark spirit's flavour of a drug are dense, be difficult for entrance, slender acanthopanax bark spirit's flavour of a drug of producing are light refreshing, and medicine is fragrant pure good, thereby improve slender acanthopanax bark spirit's product quality and sale.Simultaneously, the extracts active ingredients of Chinese medicine of the present invention is complete, has greatly improved the efficient of producing, and has shortened the liquid fabrication cycle, has reduced production cost.In addition, the present invention extracts by the traditional cold pickling process for the Chinese medicinal materials that other are not suitable for vapor extraction, can not destroy the effective ingredient of other Chinese medicinal materialss.
Embodiment
The method of producing acanthopanax bark wine by Chinese medicine steam extraction method, the method comprise concoction preparation, liquid glucose preparation, the preparation of work in-process wine and can step.
Test in concoction preparation, the liquid that floods with liquid and the tradition of vapor extraction is mixed to join in the wine to be tested.Adopt the Chinese medicinal materials of hydrodistillation to have: Wu Chia Pee, the banksia rose, cloves, fructus amomi, Chinese cassia tree, official osmanthus, the weight ratio of Chinese medicinal materials weight and water was at 1: 2 during hydrodistillation.Adopt the medicinal material of traditional pickling process to have: wolfberry fruit, Herba Epimedii, wolfberry fruit, cassia twig, Mountain Spicy Tree Fruit, red colouring agent for food, also used as a Chinese medicine, cape jasmine, Radix Angelicae Sinensis, Radix Codonopsis, kaempferia galamga, dried orange peel, Buddha's hand, peppermint, Chinese medicinal materials weight and basic wine weight ratio were at 1: 5 during the Chinese medicinal materials dipping.
The processing condition of hydrodistillation method: take by weighing a certain amount of herbal medicine, pack into equably in the Erlenmeyer flask, by passing into flatly water vapor, another outlet connects prolong, prolong connects water-and-oil separator, distills 20-40 minute, collect volatile oil after oily water separation, (below 20 ℃) are preserved at normal temperatures.
Usage quantity: operate by slender acanthopanax bark spirit's proportioning, tested number is that Wu Chia Pee, the banksia rose, cloves, fructus amomi, Chinese cassia tree, each hydrodistillation liquid of official osmanthus add preparation by 0.2% of slender acanthopanax bark spirit's total amount, and wolfberry fruit, Herba Epimedii, wolfberry fruit, cassia twig, Mountain Spicy Tree Fruit, red colouring agent for food, also used as a Chinese medicine, cape jasmine, Radix Angelicae Sinensis, Radix Codonopsis, kaempferia galamga, dried orange peel, Buddha's hand, each Chinese medicinal materials dipping extracting solution of peppermint add preparation by 1% of slender acanthopanax bark spirit's total amount.
The Chinese medicinal materials liquid extracts the comparison of liquid

Claims (3)

1. the method for producing acanthopanax bark wine by Chinese medicine steam extraction method, the method comprises the concoction preparation, the preparation of work in-process wine and can step, the Chinese medicinal materials of concoction preparation is by Wu Chia Pee, the banksia rose, cloves, fructus amomi, Chinese cassia tree, official osmanthus, wolfberry fruit, Herba Epimedii, cassia twig, Mountain Spicy Tree Fruit, red colouring agent for food, also used as a Chinese medicine, cape jasmine, Radix Angelicae Sinensis, Radix Codonopsis, kaempferia galamga, dried orange peel, Buddha's hand and peppermint form, it is characterized in that: adopt the hydrodistillation method to extract Chinese medicinal materials in the concoction preparation, adopting the Chinese medicinal materials of hydrodistillation method is Wu Chia Pee, the banksia rose, cloves, fructus amomi, Chinese cassia tree and official osmanthus, the add-on of the concoction of every flavor Chinese medicine that employing hydrodistillation method is extracted in the preparation of work in-process wine is 0.1%~0.3% of slender acanthopanax bark spirit's total amount; Also adopt traditional pickling process to extract Chinese medicinal materials in the concoction preparation, the Chinese medicinal materials that adopts traditional pickling process to extract is wolfberry fruit, Herba Epimedii, cassia twig, Mountain Spicy Tree Fruit, red colouring agent for food, also used as a Chinese medicine, cape jasmine, Radix Angelicae Sinensis, Radix Codonopsis, kaempferia galamga, dried orange peel, Buddha's hand and peppermint, and the add-on of the concoction of every flavor Chinese medicine that the traditional pickling process of employing is extracted in the preparation of work in-process wine is 0.5%~2% of slender acanthopanax bark spirit's total amount.
2. the method for producing acanthopanax bark wine by Chinese medicine steam extraction method according to claim 1, it is characterized in that: the weight ratio of Chinese medicinal materials weight and water is 1:1.5~1:3 during hydrodistillation.
3. the method for producing acanthopanax bark wine by Chinese medicine steam extraction method according to claim 1 is characterized in that: when traditional pickling process is extracted during the Chinese medicinal materials dipping Chinese medicinal materials weight and basic wine weight ratio be 1:3~1:6.
CN 201010252011 2010-08-12 2010-08-12 Method for producing acanthopanax bark wine by traditional Chinese medicine steam extraction method Active CN101928658B (en)

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CN106929355A (en) * 2017-03-21 2017-07-07 广州五加皮酒业有限公司 Health preserving wine production system and method

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1371977A (en) * 2001-02-22 2002-10-02 陈列 Method for preparing ginseng cortex acanthopanacis health care wine

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1371977A (en) * 2001-02-22 2002-10-02 陈列 Method for preparing ginseng cortex acanthopanacis health care wine

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
汪建国."五加皮酒各时期组方、制法、功效和历史渊源".《中国酿造》.2008,(第18期),第103-104,110页.
汪建国."五加皮酒各时期组方、制法、功效和历史渊源".《中国酿造》.2008,(第18期),第103-104,110页. *
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