CN103961613A - Novel preparation method of high-quality loquat syrup - Google Patents

Novel preparation method of high-quality loquat syrup Download PDF

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Publication number
CN103961613A
CN103961613A CN201410189765.4A CN201410189765A CN103961613A CN 103961613 A CN103961613 A CN 103961613A CN 201410189765 A CN201410189765 A CN 201410189765A CN 103961613 A CN103961613 A CN 103961613A
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medicine
decoct
add
time
concentrated
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CN201410189765.4A
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付诚
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JIANGXI BAISHEN PHARMACEUTICAL CO Ltd
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JIANGXI BAISHEN PHARMACEUTICAL CO Ltd
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Abstract

The invention discloses a preparation method of high-quality loquat syrup. The preparation method is characterized in that each 1000 ml of the loquat syrup is prepared from the following raw materials: 68-72 g of loquat leaves, 48-52 g of pericarpium papaveris, 4-6 g of radix stemonae, 8-10 g of cynanchum glaucescens, 5.5-6.5 g of white mulberry root-barks, 5.5-6.5 g of platycodon grandiflorum, 0.14-0.16 g of menthol, 0.45-0.55 g of citric acid, 590-610 g of sucrose, 2.4-2.6 g of sodium benzoate and 1.3-1.5 ml of banana essence. The preparation method comprises the following steps: decocting the raw materials, concentrating, and blending to prepare 1000 ml of the loquat syrup. The loquat syrup product is a light brown clear liquid, is aromatic in smell, sweet in taste and high and stable in quality, is orally taken for three times each day, has the effects of nourishing yin, astringing the lung, relieving a cough and eliminating phlegm, and is used for treating the cough caused by bronchitis; 15 ml of the loquat syrup product is orally taken each time.

Description

A kind of preparation method of new intensified loquet distillate
Technical field
The invention belongs to field of traditional Chinese medicine pharmacy, be specifically related to a kind of preparation method of new intensified loquet distillate.
Background technology
Intensified loquet distillate is light brown supernatant liquid; Gas is fragrant, taste is sweet.Yin nourishing is astringed the lung, eliminating phlegm and stopping cough.For bronchitic cough.Main component is Folium Eriobotryae, Pericarpium Papaveris, the Radix Stemonae, Rhizoma Cynanchi Stauntonii, Cortex Mori, Radix Platycodonis, Mentholum.Folium Eriobotryae, Cortex Mori lung heat clearing, Radix Stemonae lung moistening, Pericarpium Papaveris is astringed the lung, Radix Platycodonis lung qi dispersing, lung falls in Rhizoma Cynanchi Stauntonii.Function cures mainly: yin nourishing is astringed the lung, relieving cough and expelling phlegm.For chronic cough due to asthenia of viscera, bronchitis etc.
Prior art as, < < intensified loquet distillate and preparation method thereof > > CN200510010324.4, the present invention relates to a kind of intensified loquet distillate and preparation method thereof, seven tastes such as Folium Eriobotryae, except Mentholum, the Six-element Chinese medicines such as all the other Folium Eriobotryaes decoct with water secondary, each 2 hours, collecting decoction, filter, be concentrated into relative density of medicine liquid 1.13-1.15, adding steviosin 2g dissolves, add citric acid 0.5g, appropriate and the Mentholum with dissolve with ethanol essence, stir, mix, standing, filter, add water to 1000ml, be mixed, obtain.The present invention has the following advantages: 1. the weight that can reduce medicine excipient.2. dissolution velocity is fast, stable to heat and acid.3. the shortcomings such as made medicine is difficult for fermentation, expanded, and overcoming syrup only could anti-bacteria when high concentration and easily cause bacterial growth during the reduction of sugared concentration, expanded.4. steviosin can be used as that health promoting candy is for a long time edible to have no adverse effects to human body, is specially adapted to cardiovascular diseases, obesity, diabetics.And for example: < < intensified loquet distillate and preparation method thereof > > CN201110111681.5, weight ratio part of intensified loquet distillate of the present invention is: Folium Eriobotryae 50g, Pericarpium Papaveris 45g, Radix Stemonae 10g, Rhizoma Cynanchi Stauntonii 6g Cortex Mori 4g, Radix Platycodonis 4g, Mentholum 0.09g; Its preparation method is except Mentholum, and the Six-elements such as all the other Folium Eriobotryaes decoct with water secondary, each 2.5 hours, collecting decoction, filters, and is concentrated into 700ml, add sodium benzoate 2.6g, be stirred to dissolving, with sucrose 700g, continue to be heated to boiling, be incubated 30 minutes, standing, filter, add water to 1200ml, mix, obtain.Intensified loquet distillate of the present invention has yin nourishing astringes the lung, relieving cough and expelling phlegm effect, cough-relieving better function.
Summary of the invention
The preparation method that the object of this invention is to provide a kind of new intensified loquet distillate
The object of the invention is to implement by following technical proposal:
A preparation method for new intensified loquet distillate, every 1000ml intensified loquet distillate is prepared from by following raw material and weight portion: Folium Eriobotryae 68-72g, Pericarpium Papaveris 48-52g, Radix Stemonae 4-6g, Rhizoma Cynanchi Stauntonii 8-10g, Cortex Mori 5.5-6.5g, Radix Platycodonis 5.5-6.5g, Mentholum 0.14-0.16g, citric acid 0.45-0.55g, sucrose 590-610g, sodium benzoate 2.4-2.6g, flavoring banana essence 1.3-1.5ml, makes 1000ml
(1), decoct
Decoct for the first time, get Folium Eriobotryae, Pericarpium Papaveris, the Radix Stemonae, Rhizoma Cynanchi Stauntonii, Cortex Mori, Radix Platycodonis and successively 6 taste decoction pieces are added to extraction pot, add the water of 6 ± 0.6 times of decoction pieces amounts, be heated to micro-boiling, decoct 2 ± 0.2 hours, emit decoction liquor.
Decoct for the second time, get the water that the medicinal residues that decoct for the first time add 4 ± 0.4 times of decoction pieces amounts, be heated to micro-boiling, decoct 2 ± 0.2 hours, emit decoction liquor.
Filter: with 200 order filter clothes will be for the first time, decoction liquor filtration for the second time, merging filtrate.
Wherein: Steam Pressure Control of Circulated in 0.33Mpa, steam pressure should take maintain medicinal liquid micro-boil as degree.
(2) concentrated
Open steam valve pressure < 0.1Mpa, an effect keeps vacuum at-0.02～-0.08Mpa, and two effects keep vacuums at-0.02～-0.08Mpa, concentrate, and is concentrated into and supplements in time medicinal liquid when a certain amount of.
Be concentrated into relative density and be not less than 1.01, steam off and vacuum.
Wherein: filtrate is sucked to concentrator approximately 2/3 place by vacuum intake method, close material inlet valve.
Thickening temperature is controlled at below 90 ℃.
(3) concentrated solution is collected
With clean container, collect concentrated solution.
(4) preparation
Get sucrose, sodium benzoate, citric acid, Mentholum, measure essence.
In material-compound tank, add concentrated solution, heating, open and stir, add sodium benzoate, sucrose to make it to be uniformly dissolved, continue heated and boiled to 110 ± 5 ℃, stop stirring constant temperature 120 ± 5 minutes, open to stir and to be cooled to 55 ℃ when following, add citric acid, essence and with the Mentholum of dissolve with ethanol, stop stirring and add purified water and be settled to instruction amount of preparation (1000L), at stirring and evenly mixing.Static, filter censorship.
Boil sugared controlled pressure at 0.15～0.20Mpa.
Sampling and measuring relative density, should be not less than 1.195(26 ℃).
(5) embedding
Temperature is at 18～26 ℃, relative humidity 45～65%.
Temperature during liquid medicine filling should be lower than 55 ℃, and institute's vehicle should have been filled with in 12 hours.
Content uniformity: average loading amount is not less than 200 ml, single bottled amount is no less than 194 ml.
The processing of Chinese crude drug is concocted:
The Radix Stemonae: by the medicine cutter cutting of the cleaned Radix Stemonae, cut into 2-5cm short; Rhizoma Cynanchi Stauntonii: by the medicine cutter cutting of cleaned Rhizoma Cynanchi Stauntonii, cut into 2-5cm short; Cortex Mori: by the medicine cutter cutting of cleaned Cortex Mori, cut into 1-3cm short; Undesirablely should sort out cutting again.
By the cutting good Radix Stemonae, Rhizoma Cynanchi Stauntonii, Cortex Mori, be respectively charged in drip pan, charge depth≤3cm, puts into baking oven.80 ℃ of baking temperatures, are dried to 3 hours and turn over medicine once, until medicine is dried to rear receipts medicine, let cool.
Radix Platycodonis: by the medicine cutter cutting of the Radix Platycodonis of select.Cut into 1-3cm section, undesirable should sorting out heavily cut.
Product of the present invention is light brown supernatant liquid; Gas is fragrant, and taste is sweet, and quality is high, steady quality.Oral.One time 15 milliliters, 3 times on the one.Yin nourishing is astringed the lung, eliminating phlegm and stopping cough.For bronchitic cough.
The specific embodiment:
Below in conjunction with embodiment, the present invention is described further.Following examples are only several specific embodiment of the present invention, but design concept of the present invention is not limited to this, allly utilize this design to carry out the change of unsubstantiality to the present invention, all should belong to the behavior of invading protection domain of the present invention.
Embodiment 1
Name of material consumption
Folium Eriobotryae 69g
Pericarpium Papaveris 50g
Radix Stemonae 15g
Rhizoma Cynanchi Stauntonii 9g
Cortex Mori 6g
Radix Platycodonis 6g
Mentholum 0.15g
Citric acid 0.5g
Sucrose 600g
Sodium benzoate 2.5g
Flavoring banana essence 1.4ml
Make 1000ml
The processing of Chinese crude drug is concocted:
The Radix Stemonae: by the medicine cutter cutting of the cleaned Radix Stemonae.Cut into 2-5cm short, undesirablely should sort out cutting again.By the good Radix Stemonae of cutting, pack in drip pan, charge depth≤3cm, puts into baking oven.80 ℃ of baking temperatures, are dried to 3 hours and turn over medicine once, until medicine is dried to rear receipts medicine, let cool.
Rhizoma Cynanchi Stauntonii: by the medicine cutter cutting of cleaned Rhizoma Cynanchi Stauntonii.Cut into 2-5cm short, undesirablely should sort out cutting again.By the good Rhizoma Cynanchi Stauntonii of cutting, pack in drip pan, charge depth≤3cm, puts into baking oven.80 ℃ of baking temperatures, are dried to 3 hours and turn over medicine once, until medicine is dried to rear receipts medicine, let cool.
Cortex Mori: by the medicine cutter cutting of cleaned Cortex Mori.Cut into 1-3cm short, undesirablely should sort out cutting again.By the good Cortex Mori of cutting, pack in drip pan, charge depth≤3cm, puts into baking oven.80 ℃ of baking temperatures, are dried to 3 hours and turn over medicine once, until medicine is dried to rear receipts medicine, let cool.
Radix Platycodonis: by the medicine cutter cutting of the Radix Platycodonis of select.Cut into 1-3cm section, undesirable should sorting out heavily cut.
(1), decoct
Decoct for the first time, get Folium Eriobotryae, Pericarpium Papaveris, the Radix Stemonae, Rhizoma Cynanchi Stauntonii, Cortex Mori, Radix Platycodonis and successively 6 taste decoction pieces are added to extraction pot, add the water of 6 times of decoction pieces amounts, be heated to micro-boiling, decoct 2 hours, emit decoction liquor.
Decoct for the second time, get the water that the medicinal residues that decoct for the first time add 4 times of decoction pieces amounts, be heated to micro-boiling, decoct 2 hours, emit decoction liquor.
Filter: with 200 order filter clothes will be for the first time, decoction liquor filtration for the second time, merging filtrate.
Wherein: Steam Pressure Control of Circulated in 0.33Mpa, steam pressure should take maintain medicinal liquid micro-boil as degree.
(2) concentrated
Filtrate is sucked to concentrator approximately 2/3 place by vacuum intake method, close material inlet valve.
Open steam valve pressure < 0.1Mpa, an effect keeps vacuum at-0.02～-0.08Mpa, and two effects keep vacuums at-0.02～-0.08Mpa, concentrate, and is concentrated into and supplements in time medicinal liquid when a certain amount of.
Be concentrated into relative density and be not less than 1.01, collect the inventory that concentrated solution is about 1687.5L(2250L) time, steam off and vacuum.
Wherein: thickening temperature is controlled at below 90 ℃.
(3) concentrated solution is collected
With clean container, collect concentrated solution.
(4) preparation
Get sucrose, sodium benzoate, citric acid, Mentholum, measure essence.
In material-compound tank, add concentrated solution, heating, open and stir, add sodium benzoate, sucrose to make it to be uniformly dissolved, continue heated and boiled to 110 ℃, stop stirring constant temperature 120 minutes, open to stir and to be cooled to 55 ℃ when following, add citric acid, essence and with the Mentholum of dissolve with ethanol, stop stirring and add purified water and be settled to instruction amount of preparation (3000L), at stirring and evenly mixing.Static, filter censorship.
Boil sugared controlled pressure at 0.15～0.20Mpa.
Sampling and measuring relative density, should be not less than 1.195(26 ℃).
(5) embedding
Temperature is at 18～26 ℃, relative humidity 45～65%,
Temperature during liquid medicine filling should be lower than 55 ℃, and institute's vehicle should have been filled with in 12 hours.
Content uniformity: average loading amount is not less than 200 ml, single bottled amount is no less than 194 ml.
Other embodiment:

Claims (6)

1. a preparation method for new intensified loquet distillate, is characterized in that preparation method is as follows: every 1000ml intensified loquet distillate is prepared from by following raw material and weight portion: Folium Eriobotryae 68-72g, Pericarpium Papaveris 48-52g, Radix Stemonae 4-6g, Rhizoma Cynanchi Stauntonii 8-10g, Cortex Mori 5.5-6.5g, Radix Platycodonis 5.5-6.5g, Mentholum 0.14-0.16g, citric acid 0.45-0.55g, sucrose 590-610g, sodium benzoate 2.4-2.6g, flavoring banana essence 1.3-1.5ml, makes 1000ml;
(1), decoct
Decoct for the first time, get Folium Eriobotryae, Pericarpium Papaveris, the Radix Stemonae, Rhizoma Cynanchi Stauntonii, Cortex Mori, Radix Platycodonis and successively 6 taste decoction pieces are added to extraction pot, add the water of 6 ± 0.6 times of decoction pieces amounts, be heated to micro-boiling, decoct 2 ± 0.2 hours, emit decoction liquor;
Decoct for the second time, get the water that the medicinal residues that decoct for the first time add 4 ± 0.4 times of decoction pieces amounts, be heated to micro-boiling, decoct 2 ± 0.2 hours, emit decoction liquor;
Filter: with 200 order filter clothes will be for the first time, decoction liquor filtration for the second time, merging filtrate;
(2) concentrated
Open steam valve pressure < 0.1Mpa, an effect keeps vacuum at-0.02～-0.08Mpa, and two effects keep vacuums at-0.02～-0.08Mpa, concentrate, and is concentrated into and supplements in time medicinal liquid when a certain amount of;
Be concentrated into relative density and be not less than 1.01, steam off and vacuum;
(3) concentrated solution is collected
With clean container, collect concentrated solution;
(4) preparation
Get sucrose, sodium benzoate, citric acid, Mentholum, measure essence;
In material-compound tank, add concentrated solution, heating, open and stir, add sodium benzoate, sucrose to make it to be uniformly dissolved, continue heated and boiled to 110 ± 5 ℃, stop stirring constant temperature 120 ± 5 minutes, open to stir and to be cooled to 55 ℃ when following, add citric acid, essence and with the Mentholum of dissolve with ethanol, stop stirring and add purified water and be settled to instruction amount of preparation (1000L), at stirring and evenly mixing; Static, filter censorship;
(5) fill.
2. the preparation method of a kind of new intensified loquet distillate according to claim 1, is characterized in that, during decoction, Steam Pressure Control of Circulated in 0.33Mpa, steam pressure should take maintain medicinal liquid micro-boil as degree.
3. the preparation method of a kind of new intensified loquet distillate according to claim 1, is characterized in that, when concentrated, filtrate is sucked to concentrator approximately 2/3 place by vacuum intake method, closes material inlet valve, and thickening temperature is controlled at below 90 ℃.
4. the preparation method of a kind of new intensified loquet distillate according to claim 1, is characterized in that, during preparation, boils sugared controlled pressure at 0.15～0.20Mpa, and sampling and measuring relative density, should be not less than 1.195(26 ℃).
5. the preparation method of a kind of new intensified loquet distillate according to claim 1, is characterized in that, during fill, embedding condition is: temperature is at 18～26 ℃, relative humidity 45～65%; Temperature during liquid medicine filling should be lower than 55 ℃, and institute's vehicle should have been filled with in 12 hours; Content uniformity: average loading amount is not less than 200 ml, single bottled amount is no less than 194 ml.
6. the preparation method of a kind of new intensified loquet distillate according to claim 1, it is characterized in that to the processing of Part of Chinese Medicinal concoct require be:
The Radix Stemonae: by the medicine cutter cutting of the cleaned Radix Stemonae, cut into 2-5cm short; Rhizoma Cynanchi Stauntonii: by the medicine cutter cutting of cleaned Rhizoma Cynanchi Stauntonii, cut into 2-5cm short; Cortex Mori: by the medicine cutter cutting of cleaned Cortex Mori, cut into 1-3cm short; Undesirablely should sort out cutting again;
By the cutting good Radix Stemonae, Rhizoma Cynanchi Stauntonii, Cortex Mori, be respectively charged in drip pan, charge depth≤3cm, puts into baking oven; 80 ℃ of baking temperatures, are dried to 3 hours and turn over medicine once, until medicine is dried to rear receipts medicine, let cool.
CN201410189765.4A 2014-05-07 2014-05-07 Novel preparation method of high-quality loquat syrup Pending CN103961613A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104225397A (en) * 2014-08-28 2014-12-24 桐城市永锦建筑工程有限公司 Loquat solution and preparation method thereof
CN106465821A (en) * 2016-08-31 2017-03-01 范健身 A kind of method that lung moistening Distillate Folium Eriobotryae is prepared based on Folium Eriobotryae
CN109125258A (en) * 2018-10-25 2019-01-04 华润三九（南昌）药业有限公司 A kind of preparation method of intensified loquet distillate
CN113456770A (en) * 2021-08-12 2021-10-01 海南葫芦娃药业集团股份有限公司 Strong loquat syrup and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102764397A (en) * 2011-04-30 2012-11-07 顾建光 Intensified loquet distillate and its preparation method
US20130323351A1 (en) * 2012-05-30 2013-12-05 Odin Carrillo Loquat Tea Composition

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102764397A (en) * 2011-04-30 2012-11-07 顾建光 Intensified loquet distillate and its preparation method
US20130323351A1 (en) * 2012-05-30 2013-12-05 Odin Carrillo Loquat Tea Composition

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104225397A (en) * 2014-08-28 2014-12-24 桐城市永锦建筑工程有限公司 Loquat solution and preparation method thereof
CN106465821A (en) * 2016-08-31 2017-03-01 范健身 A kind of method that lung moistening Distillate Folium Eriobotryae is prepared based on Folium Eriobotryae
CN109125258A (en) * 2018-10-25 2019-01-04 华润三九（南昌）药业有限公司 A kind of preparation method of intensified loquet distillate
CN109125258B (en) * 2018-10-25 2020-09-18 华润三九（南昌）药业有限公司 Preparation method of strong loquat syrup
CN113456770A (en) * 2021-08-12 2021-10-01 海南葫芦娃药业集团股份有限公司 Strong loquat syrup and preparation method thereof

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