CN107382599A - A kind of preparation method for the composite humic acid soil conditioner for improving soil activation - Google Patents
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation Download PDFInfo
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- CN107382599A CN107382599A CN201710497693.3A CN201710497693A CN107382599A CN 107382599 A CN107382599 A CN 107382599A CN 201710497693 A CN201710497693 A CN 201710497693A CN 107382599 A CN107382599 A CN 107382599A
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- preparation
- humic acid
- composite
- soil conditioner
- lignite
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B17/00—Other phosphatic fertilisers, e.g. soft rock phosphates, bone meal
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K17/00—Soil-conditioning materials or soil-stabilising materials
- C09K17/40—Soil-conditioning materials or soil-stabilising materials containing mixtures of inorganic and organic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2101/00—Agricultural use
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Soil Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Inorganic Chemistry (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of preparation method for the composite humic acid soil conditioner for improving soil activation,The present invention will be by that will decompose silicate mineral,Soluble phosphorus,Potassium decomposing,The complex micro organism fungicide of the effects such as fixed nitrogen is inoculated into the stalk of pretreatment,In Chinese medicine slag and lignite mixed material,Pretreated stalk,Chinese medicine slag and lignite,Humic acid exposure is more,Dissolution is more,Ferment at constant temperature obtains being rich in humic acid,A large amount of live body beneficial floras,The modifying agent of organic matter,Then pelletized with being chelated in the presence of chelating agent and porous adsorbent flyash,The product stability of preparation is good,It is active high,Various nutriments can slowly be discharged,Improved soil,Increase soil fertility,Reduce the usage amount of fertilizer,Improve utilization rate of fertilizer,Improve the quality and yield of crop,The products material source of the present invention is wide,Cost is low,It is pollution-free,Effect is good,Realize the cyclic utilization of waste,Energy saving economy,It is easy to use that graininess is made,Convenient transport,Have a good application prospect.
Description
Technical field
The present invention relates to soil conditioner technical field, more particularly to a kind of composite humic acid soil for improving soil activation
The preparation method of modifying agent.
Background technology
China is large agricultural country, growing with population, in order to meet people to grain and the need of agricultural byproducts
Ask, it is necessary to improve the yield of grain, traditional mode is to apply chemical fertilizer.Traditional chemical fertilizer has certain yield-increasing efficiency, but by
In with the increase of fertilizer application frequency, chemical fertilizer itself is volatile, loss causes the soil salinization, alkalization, causes the soil organism
Destroyed, microelement deficiencies, soil texture is poor, and ventilating permeable is bad, plant absorption not nutrient, has a strong impact on production
Measure and cause economic loss, also constrain the sustainable development of modern agriculture.The height of humus content in soil, is soil
The important symbol of fertility.Soil humus can directly adjust the water, fertilizer, air and heat process of soil, and supply vitamin grows
Nutrition and energy, meanwhile, the composition containing auxin in humus, there is stimulation to plant growth.Humic acid
Wide material sources, but humic acid is therefrom extracted, the complex process applied to soil, pollution weight, cost is high, uncomfortable
Close large-scale promotion to use, therefore, there is an urgent need to one kind can reduce cost, improves crop yield quality, reduces environmental pollution
The modifying agent of and can improved soil.
The content of the invention
A kind of the defects of the object of the invention is exactly to make up prior art, there is provided composite humic acid for improving soil activation
The preparation method of soil conditioner.
The present invention is achieved by the following technical solutions：
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, is made up of step in detail below：
（1）It will be added to after stalk, Chinese medicine slag co-grinding in 10wt% phosphoric acid solution and be stirred premix processing, every 100 grams mixed
Compound adds 0.05-0.2 milliliters 10wt% phosphoric acid solution, is then transferred into microwave irradiation 8-10min in microwave treater；
（2）Lignite be crushed into 200 mesh sieves, be added in reactor, add the 3-5 times of distilled water measured, rise temperature to 60-90
DEG C when add ferrous sulfate, sodium fluoride reaction 30-50min, now no longer heat, add ammoniacal liquor continue react 40-60min；
（3）By step（1）Irradiated mixed material and step（2）Lignite after activation, which is added in batch mixer, to be stirred, control
Moisture processed is 55-65%, then adds composite bacteria agent and is placed in fermentation tank and ferment, it is 25-35 to control fermentation temperature
DEG C, ferment 24-48h；
（4）After fermentation ends, disodium ethylene diamine tetraacetate, citric acid, lactic acid and flyash are added, with 400-600 revs/min turn
Speed stirring is granulated to being uniformly dispersed, drying, screening packaging.
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, step（1）Described in stalk,
Chinese medicine slag is according to mass ratio 1：1 mixing, particle size is not more than 2mm after crushing.
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, step（1）Described in premix
Processing is to soak, time 4-6h.
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, step（1）Described in microwave
The power of processor is 800W, and irradiation temperature is controlled at 125-150 DEG C.
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, step（2）Described in sulfuric acid
Ferrous addition is the 1-3% of lignite, and the addition of sodium fluoride is the 0.5-2% of lignite, and the addition of ammoniacal liquor is the 10- of lignite
15%。
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, step（3）Described in be added to
Stirred in batch mixer, rotating speed is 800-1200 revs/min.
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, the step（3）In compound life
Thing microbial inoculum is pressed by colloid bacillus cereus agent, bacillus megaterium agent, bacillus laterosporus agent, bacillus subtilis microbial inoculum, actinomyces
According to weight than 3：2：2：1：1 mixing composition, living bacteria count >=10,000,000,000/g, the addition of composite bacteria agent is step（2）
And step（3）Mixed material 8-12%.
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, step（4）Described in granulation
Refer to use extruder extruder grain, particle diameter 2-5mm, round as a ball drying after extruding, moisture is below 15%.
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, a kind of described soil that improves are lived
Mixture, lignite, the ethylenediamine tetra-acetic acid two of the preparation method of the composite humic acid soil conditioner of property, Chinese medicine slag and stalk
Sodium, citric acid, the quality proportioning of lactic acid and flyash are 250-350：100-120：12-18：7-10：15-20：55-65.
It is an advantage of the invention that：Complex micro organism fungicide directly acts on lignite, Chinese medicine slag and the rotten plant of stalk fermentation production
Acid, with the characteristics of cycle length, product is unstable, the present invention is placed in microwave treater by phosphoric acid activation stalk and Chinese medicine slag
Middle radiation treatment, obtains the Chinese medicine slag and stalk containing humic-acid kind, and lignite is handled by high-temperature activation respectively, makes humic acid
Dissolution, then using the complex micro organism fungicide for decomposing the effects such as silicate mineral, Soluble phosphorus, potassium decomposing, fixed nitrogen, be inoculated into lignite,
In the mixed material of Chinese medicine slag and stalk, ferment at constant temperature obtains the improvement rich in humic acid, a large amount of live body beneficial floras, organic matter
Agent, then with being pelletized in the presence of chelating agent disodium ethylene diamine tetraacetate, citric acid and porous adsorbent flyash, preparation
Product stability is good, and activity is high, is chelated mutually between composition, can slowly discharge various nutriments, reach slow release effect,
Can improved soil, increase soil fertility, reduce the usage amount of fertilizer, improve utilization rate of fertilizer, improve quality and the production of crop
Amount, products material source of the invention is wide, and cost is low, pollution-free, and effect is good, realizes the cyclic utilization of waste, energy saving economy, is made
Graininess is easy to use, convenient transport, has a good application prospect.
Embodiment
A kind of preparation method for the composite humic acid soil conditioner for improving soil activation, is made up of step in detail below：
（1）By 150Kg stalks, 150Kg Chinese medicine slags co-grinding into the micro mist that particle size is 2mm, it is then added to 150L10wt%'s
5h is soaked in phosphoric acid solution, is then transferred into 800W microwave treater with 135 DEG C of temperature microwave irradiation 8min；
（2）100Kg lignite crushed into 200 mesh sieves to be added in reactor, add 300Kg distilled water, rise temperature to 60
DEG C when add 1Kg ferrous sulfate, 0.5Kg sodium fluoride reaction 30min, now no longer heat, add 11L ammoniacal liquor continue it is anti-
Answer 40min；
（3）By step（1）Irradiated mixed material and step（2）Lignite after activation is added in batch mixer with 800 revs/min
Rotating speed is stirred, and it is 55% to control moisture, then adds the agent of 10.6Kg colloid bacillus cereus, 7.2Kg bacillus megateriums
Agent, the agent of 7.2Kg bacillus laterosporuses, 3.5Kg bacillus subtilis microbial inoculum and 3.5Kg actinomyces are placed in fermentation tank and fermented, control
Fermentation temperature is 28 DEG C, and ferment 30h；
（4）After fermentation ends, 13Kg disodium ethylene diamine tetraacetates, 7Kg citric acids, 16Kg lactic acid and 60Kg flyash are added, with
600 revs/min of rotating speed is stirred to being uniformly dispersed, and goes to extruder extruder grain, particle diameter 2-5mm, round as a ball drying, water after extruding
Sub-control system is below 15%, screening packaging.
Claims (9)
1. a kind of preparation method for the composite humic acid soil conditioner for improving soil activation, it is characterised in that by detail below
Step is made：
（1）It will be added to after stalk, Chinese medicine slag co-grinding in 10wt% phosphoric acid solution and be stirred premix processing, every 100 grams mixed
Compound adds the 10wt% of 0.05-0.2 milliliters phosphoric acid solution, is then transferred into microwave irradiation 8-10min in microwave treater；
（2）Lignite be crushed into 200 mesh sieves, be added in reactor, add the 3-5 times of distilled water measured, rise temperature to 60-90
DEG C when add ferrous sulfate, sodium fluoride reaction 30-50min, now no longer heat, add ammoniacal liquor continue react 40-60min；
（3）By step（1）Irradiated mixed material and step（2）Lignite after activation, which is added in batch mixer, to be stirred, control
Moisture processed is 55-65%, then adds composite bacteria agent and is placed in fermentation tank and ferment, it is 25-35 to control fermentation temperature
DEG C, ferment 24-48h；
（4）After fermentation ends, disodium ethylene diamine tetraacetate, citric acid, lactic acid and flyash are added, with 400-600 revs/min turn
Speed stirring is granulated to being uniformly dispersed, drying, screening packaging.
2. a kind of preparation method of composite humic acid soil conditioner for improving soil activation according to claim 1, its
It is characterised by, step（1）Described in stalk, Chinese medicine slag is according to mass ratio 1：1 mixing, particle size is not more than 2mm after crushing.
3. a kind of preparation method of composite humic acid soil conditioner for improving soil activation according to claim 1, its
It is characterised by, step（1）Described in premix processing be immersion, time 4-6h.
4. a kind of preparation method of composite humic acid soil conditioner for improving soil activation according to claim 1, its
It is characterised by, step（1）Described in the power of microwave treater be 800W, irradiation temperature is controlled at 125-150 DEG C.
5. a kind of preparation method of composite humic acid soil conditioner for improving soil activation according to claim 1, its
It is characterised by, step（2）Described in ferrous sulfate addition be lignite 1-3%, the addition of sodium fluoride is the 0.5- of lignite
2%, the addition of ammoniacal liquor is the 10-15% of lignite.
6. a kind of preparation method of composite humic acid soil conditioner for improving soil activation according to claim 1, its
It is characterised by, step（3）Described in be added in batch mixer and stir, rotating speed is 800-1200 revs/min.
7. a kind of preparation method of composite humic acid soil conditioner for improving soil activation according to claim 1, its
It is characterised by, the step（3）Middle composite bacteria agent is by colloid bacillus cereus agent, bacillus megaterium agent, side spore gemma bar
Microbial inoculum, bacillus subtilis microbial inoculum, actinomyces are according to weight than 3：2：2：1：1 mixing composition, living bacteria count >=10,000,000,000/g,
The addition of composite bacteria agent is step（2）And step（3）Mixed material 8-12%.
8. a kind of preparation method of composite humic acid soil conditioner for improving soil activation according to claim 1, its
It is characterised by, step（4）Described in granulation refer to use extruder extruder grain, particle diameter 2-5mm, round as a ball drying after extruding,
Below moisture 15%.
9. a kind of preparation method of composite humic acid soil conditioner for improving soil activation according to claim 1, its
It is characterised by, a kind of preparation method of the composite humic acid soil conditioner of described raising soil activation, Chinese medicine slag and stalk
Mixture, lignite, disodium ethylene diamine tetraacetate, citric acid, the quality proportioning of lactic acid and flyash be 250-350：100-
120：12-18：7-10：15-20：55-65.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710497693.3A CN107382599A (en) | 2017-06-27 | 2017-06-27 | A kind of preparation method for the composite humic acid soil conditioner for improving soil activation |
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| CN201710497693.3A CN107382599A (en) | 2017-06-27 | 2017-06-27 | A kind of preparation method for the composite humic acid soil conditioner for improving soil activation |
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| CN107382599A true CN107382599A (en) | 2017-11-24 |
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| CN201710497693.3A Pending CN107382599A (en) | 2017-06-27 | 2017-06-27 | A kind of preparation method for the composite humic acid soil conditioner for improving soil activation |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107986908A (en) * | 2017-12-06 | 2018-05-04 | 云南云天化股份有限公司 | A kind of microbial manure matrix of suitable bacillus growth |
| CN112154895A (en) * | 2020-09-21 | 2021-01-01 | 安徽小溪生态科技发展有限公司 | High-humic acid water rice seedling raising substrate based on livestock and poultry manure and straw as well as preparation method and application thereof |
| CN113337292A (en) * | 2021-06-21 | 2021-09-03 | 中国科学院东北地理与农业生态研究所 | Preparation method of lignite-straw-based degraded saline-alkali wetland restoration agent |
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| US20120047974A1 (en) * | 2010-08-31 | 2012-03-01 | Qian Huang | Biochemical Humic Acid Product Prepared from Kitchen Waste and the Method of Preparing the Same |
| CN104312589A (en) * | 2014-09-03 | 2015-01-28 | 云南尚呈生物科技有限公司 | Fermented brown coal residue soil conditioner and processing method thereof |
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2017
- 2017-06-27 CN CN201710497693.3A patent/CN107382599A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120047974A1 (en) * | 2010-08-31 | 2012-03-01 | Qian Huang | Biochemical Humic Acid Product Prepared from Kitchen Waste and the Method of Preparing the Same |
| CN104312589A (en) * | 2014-09-03 | 2015-01-28 | 云南尚呈生物科技有限公司 | Fermented brown coal residue soil conditioner and processing method thereof |
Non-Patent Citations (2)
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| 侯勇: "秸秆发酵制取生化腐殖酸过程中的理化特性及微生物学特性研究", 《中国博士学位论文全文数据库 农业科技辑》 * |
| 李翠英: "腐殖酸肥料的种类与使用方法", 《农村百事通》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107986908A (en) * | 2017-12-06 | 2018-05-04 | 云南云天化股份有限公司 | A kind of microbial manure matrix of suitable bacillus growth |
| CN112154895A (en) * | 2020-09-21 | 2021-01-01 | 安徽小溪生态科技发展有限公司 | High-humic acid water rice seedling raising substrate based on livestock and poultry manure and straw as well as preparation method and application thereof |
| CN113337292A (en) * | 2021-06-21 | 2021-09-03 | 中国科学院东北地理与农业生态研究所 | Preparation method of lignite-straw-based degraded saline-alkali wetland restoration agent |
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Application publication date: 20171124 |