CN107382547A - A kind of humic acid Water Soluble Compound fertilizer - Google Patents
A kind of humic acid Water Soluble Compound fertilizer Download PDFInfo
- Publication number
- CN107382547A CN107382547A CN201710817703.7A CN201710817703A CN107382547A CN 107382547 A CN107382547 A CN 107382547A CN 201710817703 A CN201710817703 A CN 201710817703A CN 107382547 A CN107382547 A CN 107382547A
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- China
- Prior art keywords
- parts
- humic acid
- weight
- compound fertilizer
- water soluble
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F11/00—Other organic fertilisers
- C05F11/02—Other organic fertilisers from peat, brown coal, and similar vegetable deposits
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
Abstract
The invention belongs to technical field of fertilizers, especially a kind of humic acid Water Soluble Compound fertilizer, it is made up of the raw material of following parts by weight：31 ~ 33 parts of active humic acid, 11 ~ 12 parts of potassium dihydrogen phosphate, 0.67 ~ 0.69 part of borax, 0.79 ~ 0.81 part of magnesium citrate, 14 ~ 15 parts of urea, 0.56 ~ 0.58 part of methylisothiazolinone, 0.31 ~ 0.33 part of turkey red oil；The present invention, which can rush, to be applied, drip irrigation, pours root, pours and spill, application effect is good, effective culture fertility, infertile field fertile soil, promotees strong plantlets and rootage, improves crop quality, rich in other nutrients such as humic acid, amino acid, effectively solve generally to be easy to run off problem existing for current n p k nutrition element.
Description
Technical field
The invention belongs to technical field of fertilizers, especially a kind of humic acid Water Soluble Compound fertilizer.
Background technology
Crops " high yield is not high-quality, high-quality not high yield ", the problem of this is serious, annoying the agricultural production of China always,
Since reform and opening-up, particularly in recent years, China's agricultural production is scored consecutive bumper harvests, and total grain output has been increased to a new height,
Grain-production becomes total amount by chronic shortage and substantially balanced, with surpluses during good years, structure of agricultural production contradiction, adjustment kind
Structure is planted, develops high performance and fine agriculture, has been a urgent task of the pendulum in face of us.
How crops " high yield not high-quality, high-quality not high yield " the problem of is solved.Channel only has two：First, the choosing of breeding
Educate and promote；Second, balance and the regulation of crop nutrition.The former has caused the attention and concern of government agencies at all levels, and the latter is not yet
Cause enough attention.It was verified that crop will have excellent quality, its nutrition in growth, result stage must be filled
Point, it is excellent balanced.But China, during production estimation, usually due to a variety of causes, excessive applies N P and K
The chemical fertilizer such as composite fertilizer, although obtaining high yield, crops quality declines therewith, and basic reason is that crop nutrition is lost
Weighing apparatus, humic acid are a kind of " plant nutrient regulation fertilizer ", " quality fertilizer ", " health care fertilizer ".In fact, humic acid can improve
The characteristic of crop quality, causing the attention of clay fertilizer educational circles and plant nutrient educational circles in world wide.The agricultural of 21 century, will
It is that the competition of a grain yield type goes to the epoch of quality competition, realizes this transformation, humic acid and wherein trace element exists
Application in fertilizer is just particularly important.
The content of the invention
A kind of in view of the above-mentioned problems, the present invention is intended to provide humic acid Water Soluble Compound fertilizer.
The present invention is achieved through the following technical solutions：
A kind of humic acid Water Soluble Compound fertilizer, is made up of the raw material of following parts by weight：31 ~ 33 parts of active humic acid, di(2-ethylhexyl)phosphate
11 ~ 12 parts of hydrogen potassium, 0.67 ~ 0.69 part of borax, 0.79 ~ 0.81 part of magnesium citrate, 14 ~ 15 parts of urea, methylisothiazolinone
0.56 ~ 0.58 part, 0.31 ~ 0.33 part of turkey red oil.
As the further scheme of invention：The preparation method of described active humic acid, specifically includes following steps：
（1）The paper mulberry bark of the banana skin of 88 ~ 90 parts by weight, the sweet potato stalk of 62 ~ 64 parts by weight and 112 ~ 114 parts by weight is mixed
Crush, insert the constant temperature steam in pot that steams that temperature is 144 ~ 146 DEG C and handle 15 ~ 17min, take out, put into 280 ~ 290 weight
380 ~ 390min of thermal-insulating sealing in part, the water that temperature is 48 ~ 50 DEG C, room temperature natural cooling, obtains single treatment slurry；
（2）The complex enzyme that 1.3 ~ 1.5 parts by weight are added in being starched to single treatment is mixed evenly, and inserts temperature as 36 ~ 38 DEG C
Under conditions of be sealed by fermentation 8 ~ 9 days, add 23 ~ 24 parts by weight, the ethanol solution that mass fraction is 41% ~ 43% mix it is equal
It is even, continue sealing and fermenting 8 ~ 9 days, cross extracting tank and be stripped, take extract, obtain active humic acid.
As the further scheme of invention：Described complex enzyme, by following weight than enzyme be made：Cellulase：Phytic acid
Enzyme：Dextranase=8.7 ~ 8.9:3.2~3.4:5.2~5.4.
As the further scheme of invention：A kind of preparation method of humic acid Water Soluble Compound fertilizer, is specifically included following
Step：
A. active humic acid is heated to 85 ~ 87 DEG C, adds potassium dihydrogen phosphate, borax, magnesium citrate and urea, be 70 with rotating speed
~ 80r/min agitator 28 ~ 30min of insulated and stirred, is warming up to 168 ~ 170 DEG C with 4.6 ~ 4.8 DEG C/min heating rate, obtains
Solution；
B. methylisothiazolinone and turkey red oil are added into solution, is stirred with the agitator that rotating speed is 120 ~ 130r/min
9 ~ 10min, 37 ~ 39min of homogeneous under conditions of temperature is 40 ~ 42 DEG C, rotating speed is 90 ~ 100r/min, it is granulated, obtains humic sour water
Dissolubility compound fertilizer；
C. it is packed, sterilize, labelling, obtain finished product.
As the further scheme of invention：The particle diameter of described granulation is 1.5 ~ 1.7mm.
Beneficial effects of the present invention：A kind of humic acid Water Soluble Compound fertilizer provided by the invention, it can rush and apply, drip irrigation, pour
Root, pour and spill, application effect is good, effective culture fertility, infertile field fertile soil, promote strong plantlets and rootage, improve crop quality, rich in humic acid,
Other nutrients such as amino acid, effectively solve generally to be easy to run off problem existing for current n p k nutrition element.
（1）Fat-reducing synergy：Can reduce fixation of the N P and K in soil, the N P and K in activating soil, in micro member
Element balance, nutrition is comprehensive, promotes crop growth, crop anti-adversity ability is improved, so as to improve utilization rate of fertilizer.
（2）Activating soil：Humic acid makes the good crumb structure of Zinc fractions, promotes the growth of indigenous microorganism so that
Loosing soil, increase soil fertility, degrading pesticide residues toxicity, chelate harmful heavy metal ions, reduce pollution, soil is more strong
Health.
（3）Top dressing formulaization：Top dressing suitably supplements potash fertilizer typically based on nitrogenous fertilizer, adds trace element in boron, magnesium etc. and applies
Fertilizer is more scientific rationally, not only improves the quality of product, and lift the quality of agricultural product.
（4）Applicable crops are wide：Suitable for crops such as wheat, rice, corn and soybean, rapes, wheat, rice can be promoted to return
Green grass or young crops is fast, tiller is more, resistant to lodging, the ability of enhancing cold-resistant, drought resisting and disease and insect resistance；Energy reinforcing fiber is used on cotton crudefiber crop
Pulling force and intensity, significantly improve yield and quality.
Embodiment
Illustrate the present invention with specific embodiment below, but be not limitation of the present invention.
Embodiment 1
In the embodiment of the present invention, a kind of humic acid Water Soluble Compound fertilizer, it is made up of the raw material of following parts by weight：Active humic acid
31 parts, 11 parts of potassium dihydrogen phosphate, 0.67 part of borax, 0.79 part of magnesium citrate, 14 parts of urea, 0.56 part of methylisothiazolinone,
0.31 part of turkey red oil.
As the further scheme of invention：The preparation method of described active humic acid, specifically includes following steps：
（1）By the paper mulberry bark co-grinding of the banana skin of 88 parts by weight, the sweet potato stalk of 62 parts by weight and 112 parts by weight, insert
The constant temperature steam in pot that steams that temperature is 144 DEG C handles 15min, takes out, and is protected in 280 parts by weight of input, the water that temperature is 48 DEG C
Temperature sealing 380min, room temperature natural cooling, obtains single treatment slurry；
（2）The complex enzymes of 1.3 parts by weight is added in starching to single treatment to be mixed evenly, and inserts temperature as under conditions of 36 DEG C
Be sealed by fermentation 8 ~ 9 days, add 23 parts by weight, mass fraction be 41% ethanol solution be mixed evenly, continue sealing and fermenting 8 ~
9 days, cross extracting tank and be stripped, take extract, obtain active humic acid.
As the further scheme of invention：Described complex enzyme, by following weight than enzyme be made：Cellulase：Phytic acid
Enzyme：Dextranase=8.7:3.2:5.2.
As the further scheme of invention：A kind of preparation method of humic acid Water Soluble Compound fertilizer, is specifically included following
Step：
A. active humic acid is heated to 85 DEG C, adds potassium dihydrogen phosphate, borax, magnesium citrate and urea, be 70r/ with rotating speed
Min agitator insulated and stirred 28min, 168 are warming up to 4.6 DEG C/min heating rate ~ DEG C, obtain solution；
B. methylisothiazolinone and turkey red oil are added into solution, the agitator for being 120r/min with rotating speed stirs
9min, the homogeneous 37min under conditions of temperature is 40 DEG C, rotating speed is 90r/min, it is granulated, obtains humic acid Water Soluble Compound fertilizer；
C. it is packed, sterilize, labelling, obtain finished product.
As the further scheme of invention：The particle diameter of described granulation is 1.5mm.
Embodiment 2
In the embodiment of the present invention, a kind of humic acid Water Soluble Compound fertilizer, it is made up of the raw material of following parts by weight：Active humic acid
32 parts, 11.5 parts of potassium dihydrogen phosphate, 0.68 part of borax, 0.8 part of magnesium citrate, 14.5 parts of urea, methylisothiazolinone 0.57
Part, 0.31 ~ 0.33 part of turkey red oil.
As the further scheme of invention：The preparation method of described active humic acid, specifically includes following steps：
（1）By the paper mulberry bark co-grinding of the banana skin of 89 parts by weight, the sweet potato stalk of 63 parts by weight and 113 parts by weight, insert
The constant temperature steam in pot that steams that temperature is 145 DEG C handles 16min, takes out, and is protected in 285 parts by weight of input, the water that temperature is 49 DEG C
Temperature sealing 385min, room temperature natural cooling, obtains single treatment slurry；
（2）The complex enzymes of 1.4 parts by weight is added in starching to single treatment to be mixed evenly, and inserts temperature as under conditions of 37 DEG C
It is sealed by fermentation 8 ~ 9 days, 23.5 parts by weight of addition, the ethanol solution that mass fraction is 42% are mixed evenly, and continue to be sealed by fermentation
8 ~ 9 days, cross extracting tank and be stripped, take extract, obtain active humic acid.
As the further scheme of invention：Described complex enzyme, by following weight than enzyme be made：Cellulase：Phytic acid
Enzyme：Dextranase=8.8:3.3:5.3.
As the further scheme of invention：A kind of preparation method of humic acid Water Soluble Compound fertilizer, is specifically included following
Step：
A. active humic acid is heated to 86 DEG C, adds potassium dihydrogen phosphate, borax, magnesium citrate and urea, be 75r/ with rotating speed
Min agitator insulated and stirred 29min, is warming up to 169 DEG C with 4.7 DEG C/min heating rate, obtains solution；
B. methylisothiazolinone and turkey red oil are added into solution, the agitator for being 125r/min with rotating speed stirs
9.5min, the homogeneous 38min under conditions of temperature is 41 DEG C, rotating speed is 95r/min, it is granulated, obtains humic acid water soluble composite fertilizer
Material；
C. it is packed, sterilize, labelling, obtain finished product.
As the further scheme of invention：The particle diameter of described granulation is 1.6mm.
Embodiment 3
In the embodiment of the present invention, a kind of humic acid Water Soluble Compound fertilizer, it is made up of the raw material of following parts by weight：Active humic acid
33 parts, 12 parts of potassium dihydrogen phosphate, 0.69 part of borax, 0.81 part of magnesium citrate, 15 parts of urea, 0.58 part of methylisothiazolinone,
0.33 part of turkey red oil.
As the further scheme of invention：The preparation method of described active humic acid, specifically includes following steps：
（1）By the paper mulberry bark co-grinding of the banana skin of 90 parts by weight, the sweet potato stalk of 64 parts by weight and 114 parts by weight, insert
The constant temperature steam in pot that steams that temperature is 146 DEG C handles 17min, takes out, and is protected in 290 parts by weight of input, the water that temperature is 50 DEG C
Temperature sealing 390min, room temperature natural cooling, obtains single treatment slurry；
（2）The complex enzymes of 1.5 parts by weight is added in starching to single treatment to be mixed evenly, and inserts temperature as under conditions of 38 DEG C
Be sealed by fermentation 8 ~ 9 days, add 24 parts by weight, mass fraction be 43% ethanol solution be mixed evenly, continue sealing and fermenting 8 ~
9 days, cross extracting tank and be stripped, take extract, obtain active humic acid.
As the further scheme of invention：Described complex enzyme, by following weight than enzyme be made：Cellulase：Phytic acid
Enzyme：Dextranase=8.9:3.4:5.4.
As the further scheme of invention：A kind of preparation method of humic acid Water Soluble Compound fertilizer, is specifically included following
Step：
A. active humic acid is heated to 87 DEG C, adds potassium dihydrogen phosphate, borax, magnesium citrate and urea, be 80r/ with rotating speed
Min agitator insulated and stirred 30min, is warming up to 170 DEG C with 4.8 DEG C/min heating rate, obtains solution；
B. methylisothiazolinone and turkey red oil are added into solution, the agitator for being 130r/min with rotating speed stirs
10min, the homogeneous 39min under conditions of temperature is 42 DEG C, rotating speed is 100r/min, it is granulated, obtains humic acid water soluble composite fertilizer
Material；
C. it is packed, sterilize, labelling, obtain finished product.
As the further scheme of invention：The particle diameter of described granulation is 1.7mm.
Comparative example
Commercially available Common compound fertilizer material
12 mu of " Jimian 298 " cotton is planted using the fertilizer of the present embodiment and the fertilizer of comparative example, is equally divided into 4 groups, every group 3
Mu, in addition to different using fertilizer type, other conditions all same, count the average yield per mu unginned cotton amount of cotton：
The cotton comparing result of the embodiment of table 1 and comparative example
| Average yield per mu unginned cotton amount（kg） | With respect to rate of growth（%） | |
| Embodiment 1 | 348.03 | 14.60 |
| Embodiment 2 | 348.76 | 14.84 |
| Embodiment 3 | 349.96 | 15.24 |
| Comparative example | 303.68 | —— |
As known from Table 1, the per mu yield of cotton can be effectively improved using the fertilizer of the present invention.
Plant that " complete 12 mu of 1233 " corn of jade, is equally divided into 4 groups, often using the fertilizer of the present embodiment and the fertilizer of comparative example
3 mu of group, in addition to different using fertilizer type, other conditions all same, count the average 100-grain weight and per mu yield of corn：
The corn comparing result of the embodiment of table 2 and comparative example
| Average 100-grain weight（g） | Per mu yield（kg） | With respect to rate of growth（%） | |
| Embodiment 1 | 37.61 | 740.02 | 16.58 |
| Embodiment 2 | 37.75 | 743.57 | 17.14 |
| Embodiment 3 | 37.66 | 741.35 | 16.79 |
| Comparative example | 32.65 | 634.76 | —— |
As known from Table 2, the 100-grain weight and per mu yield of corn can be effectively improved using the fertilizer of the present invention.
Claims (5)
1. a kind of humic acid Water Soluble Compound fertilizer, it is characterised in that be made up of the raw material of following parts by weight：Active humic acid 31
~ 33 parts, 11 ~ 12 parts of potassium dihydrogen phosphate, 0.67 ~ 0.69 part of borax, 0.79 ~ 0.81 part of magnesium citrate, 14 ~ 15 parts of urea, methyl
0.56 ~ 0.58 part of OIT, 0.31 ~ 0.33 part of turkey red oil.
2. humic acid Water Soluble Compound fertilizer according to claim 1, it is characterised in that the system of described active humic acid
Preparation Method, specifically include following steps：
（1）The paper mulberry bark of the banana skin of 88 ~ 90 parts by weight, the sweet potato stalk of 62 ~ 64 parts by weight and 112 ~ 114 parts by weight is mixed
Crush, insert the constant temperature steam in pot that steams that temperature is 144 ~ 146 DEG C and handle 15 ~ 17min, take out, put into 280 ~ 290 weight
380 ~ 390min of thermal-insulating sealing in part, the water that temperature is 48 ~ 50 DEG C, room temperature natural cooling, obtains single treatment slurry；
（2）The complex enzyme that 1.3 ~ 1.5 parts by weight are added in being starched to single treatment is mixed evenly, and inserts temperature as 36 ~ 38 DEG C
Under conditions of be sealed by fermentation 8 ~ 9 days, add 23 ~ 24 parts by weight, the ethanol solution that mass fraction is 41% ~ 43% mix it is equal
It is even, continue sealing and fermenting 8 ~ 9 days, cross extracting tank and be stripped, take extract, obtain active humic acid.
3. humic acid Water Soluble Compound fertilizer according to claim 1, it is characterised in that described complex enzyme, by following
Weight than enzyme be made：Cellulase：Phytase：Dextranase=8.7 ~ 8.9:3.2~3.4:5.2~5.4.
4. the preparation method of humic acid Water Soluble Compound fertilizer according to claim 1, it is characterised in that specifically include with
Lower step：
A. active humic acid is heated to 85 ~ 87 DEG C, adds potassium dihydrogen phosphate, borax, magnesium citrate and urea, be 70 with rotating speed
~ 80r/min agitator 28 ~ 30min of insulated and stirred, is warming up to 168 ~ 170 DEG C with 4.6 ~ 4.8 DEG C/min heating rate, obtains
Solution；
B. methylisothiazolinone and turkey red oil are added into solution, is stirred with the agitator that rotating speed is 120 ~ 130r/min
9 ~ 10min, 37 ~ 39min of homogeneous under conditions of temperature is 40 ~ 42 DEG C, rotating speed is 90 ~ 100r/min, it is granulated, obtains humic sour water
Dissolubility compound fertilizer；
C. it is packed, sterilize, labelling, obtain finished product.
5. the preparation method of humic acid Water Soluble Compound fertilizer according to claim 4, it is characterised in that described granulation
Particle diameter be 1.5 ~ 1.7mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710817703.7A CN107382547A (en) | 2017-09-12 | 2017-09-12 | A kind of humic acid Water Soluble Compound fertilizer |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710817703.7A CN107382547A (en) | 2017-09-12 | 2017-09-12 | A kind of humic acid Water Soluble Compound fertilizer |
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| Publication Number | Publication Date |
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| CN107382547A true CN107382547A (en) | 2017-11-24 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710817703.7A Pending CN107382547A (en) | 2017-09-12 | 2017-09-12 | A kind of humic acid Water Soluble Compound fertilizer |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108117460A (en) * | 2018-01-31 | 2018-06-05 | 河南博联农业研究院有限公司 | A kind of water soluble fertilizer for synergy of losing weight and preparation method thereof |
| CN108191491A (en) * | 2018-01-31 | 2018-06-22 | 河南博联农业研究院有限公司 | A kind of water soluble fertilizer of a great number of elements and preparation method thereof |
| CN111513062A (en) * | 2020-04-30 | 2020-08-11 | 珠海市润农科技有限公司 | Emulsion in water for preventing and treating citrus fruit tree yellow dragon disease, preparation method and use method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105000983A (en) * | 2015-07-16 | 2015-10-28 | 高洪斌 | Biological humic acid compound fertilizer, and preparation and using methods thereof |
| CN106748361A (en) * | 2016-11-29 | 2017-05-31 | 青岛海之星生物科技有限公司 | A kind of humic acid water soluble fertilizer and preparation method thereof |
| CN106905084A (en) * | 2015-12-22 | 2017-06-30 | 吕良强 | A kind of composite biological humic acid fertilizer material |
-
2017
- 2017-09-12 CN CN201710817703.7A patent/CN107382547A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105000983A (en) * | 2015-07-16 | 2015-10-28 | 高洪斌 | Biological humic acid compound fertilizer, and preparation and using methods thereof |
| CN106905084A (en) * | 2015-12-22 | 2017-06-30 | 吕良强 | A kind of composite biological humic acid fertilizer material |
| CN106748361A (en) * | 2016-11-29 | 2017-05-31 | 青岛海之星生物科技有限公司 | A kind of humic acid water soluble fertilizer and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108117460A (en) * | 2018-01-31 | 2018-06-05 | 河南博联农业研究院有限公司 | A kind of water soluble fertilizer for synergy of losing weight and preparation method thereof |
| CN108191491A (en) * | 2018-01-31 | 2018-06-22 | 河南博联农业研究院有限公司 | A kind of water soluble fertilizer of a great number of elements and preparation method thereof |
| CN111513062A (en) * | 2020-04-30 | 2020-08-11 | 珠海市润农科技有限公司 | Emulsion in water for preventing and treating citrus fruit tree yellow dragon disease, preparation method and use method |
| CN111513062B (en) * | 2020-04-30 | 2023-08-25 | 珠海市润农科技有限公司 | Aqueous emulsion for preventing and treating citrus fruit tree yellow dragon disease, and preparation method and application method thereof |
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