CN107338654A - 一种阻燃隔热涤纶窗帘及其制备方法 - Google Patents

一种阻燃隔热涤纶窗帘及其制备方法 Download PDF

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CN107338654A
CN107338654A CN201710396847.XA CN201710396847A CN107338654A CN 107338654 A CN107338654 A CN 107338654A CN 201710396847 A CN201710396847 A CN 201710396847A CN 107338654 A CN107338654 A CN 107338654A
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王岳来
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Abstract

本发明提供了一种阻燃隔热涤纶窗帘及其制备方法，该窗帘包括涤纶基布和阻燃涂层，所述阻燃涂层由以下原料制成：水性聚氨酯乳液、聚乙烯醇、磷酸三丁酯、阴离子表面活性剂、偶联剂、紫外线吸收剂、三乙醇胺、玻璃纤维、填料、消泡剂、磷酸铵和水。其制备方法是先将水性聚氨酯乳液、聚乙烯醇、磷酸三丁酯、阴离子表面活性剂、偶联剂、紫外线吸收剂、三乙醇胺、玻璃纤维、填料、消泡剂、磷酸铵加至水中，超声分散，研磨，然后对涤纶面料进行涂层，喷淋胶液，烘干，即得。本发明的涤纶窗帘具有良好的阻燃隔热性能，手感舒适、柔软。

Description

一种阻燃隔热涤纶窗帘及其制备方法
技术领域
本发明属于窗帘面料技术领域，具体涉及一种阻燃隔热涤纶窗帘及其制备方法。
背景技术
近年来，随着人们生活水平的不断提高，以及消防法规和纺织品阻燃标准的建立和不断完善，需进行阻燃整理的装饰用纺织品和产业用纺织品数量不断增加。建筑物内装饰材料等的防火安全问题日益受到政府和公众的关注。在家用纺织品中，用于窗帘的纺织品占很大比例，其中使用最多的是涤纶纤维。
涤纶的使用渗透到家庭、民用、军用各个方面，它是目前产量最高、发展最快的化学纤维，在化纤产量中占首位。但合成纤维的易燃性限制了其更广泛的使用，同时给使用者带来不安全隐患。据统计，在火灾事故中，以床上用品、家具、装饰物和衣着占很大比例，而在火灾造成的死亡中，属于纺织品火灾死亡的占50％。近年来，由于纺织品引燃而引起的火灾事故日益增多，严重危及人们的生命，造成巨大的经济损失。国内外除军需外，工业、交通、旅游、消防等部门对阻燃纺织品的需求亦日益迫切。为此，对涤纶织物进行阻燃整理，具有极其重大的意义。
发明内容
解决的技术问题：本发明的目的是提供一种阻燃隔热涤纶窗帘及其制备方法，该涤纶窗帘具有良好的阻燃隔热性能，手感舒适、柔软。
技术方案：一种阻燃隔热涤纶窗帘，包括涤纶基布和阻燃涂层，所述阻燃涂层由以下重量份计的原料制成：水性聚氨酯乳液10-20份，聚乙烯醇3-7份，磷酸三丁酯0.8-2.4份，阴离子表面活性剂0.5-1.2份，偶联剂0.2-0.7份，紫外线吸收剂0.3-0.8份，三乙醇胺0.2-0.5份，玻璃纤维0.1-0.3份，填料2-5份，消泡剂0.4-1.2份，磷酸铵1.2-2.5份，水5-10份。
进一步地，所述阴离子表面活性剂为十二烷基苯磺酸钠。
进一步地，所述紫外线吸收剂为金红石型氧化钛。
进一步地，所述玻璃纤维的直径为5-10μm。
进一步地，所述填料为海泡石、石棉纤维粉、硅藻土、羧甲基纤维素钠的混合物，海泡石、石棉纤维粉、硅藻土、羧甲基纤维素钠的重量比为1：1：1：1。
上述阻燃隔热涤纶窗帘的制备方法，包括以下步骤：
步骤1，将水性聚氨酯乳液、聚乙烯醇、磷酸三丁酯、阴离子表面活性剂、偶联剂、紫外线吸收剂、三乙醇胺、玻璃纤维、填料、消泡剂、磷酸铵加至水中，超声分散，研磨，得到阻燃涂层剂；
步骤2，以步骤1所得阻燃涂层剂对涤纶面料进行涂层，然后喷淋胶液，烘干，即得。
进一步地，所述胶液是10-20wt.％CU-620A纯丙乳液。
有益效果：本发明的涤纶窗帘具有良好的阻燃隔热性能，手感舒适、柔软。
具体实施方式
实施例1
一种阻燃隔热涤纶窗帘，包括涤纶基布和阻燃涂层，所述阻燃涂层由以下重量份计的原料制成：水性聚氨酯乳液10份，聚乙烯醇3份，磷酸三丁酯0.8份，阴离子表面活性剂0.5份，偶联剂0.2份，紫外线吸收剂0.3份，三乙醇胺0.2份，玻璃纤维0.1份，填料2份，消泡剂0.4份，磷酸铵1.2份，水5份。
其中，所述阴离子表面活性剂为十二烷基苯磺酸钠；所述紫外线吸收剂为金红石型氧化钛；所述玻璃纤维的直径为5-10μm；所述填料为海石、石棉纤维粉、硅藻土、羧甲基纤维素钠的混合物，海泡石、石棉纤维粉、硅藻土、羧甲基纤维素钠的重量比为1：1：1：1。
上述阻燃隔热涤纶窗帘的制备方法，包括以下步骤：
步骤1，将水性聚氨酯乳液、聚乙烯醇、磷酸三丁酯、阴离子表面活性剂、偶联剂、紫外线吸收剂、三乙醇胺、玻璃纤维、填料、消泡剂、磷酸铵加至水中，超声分散，研磨，得到阻燃涂层剂；
步骤2，以步骤1所得阻燃涂层剂对涤纶面料进行涂层，然后喷淋胶液，烘干，即得。
其中，所述胶液是10-20wt.％CU-620A纯丙乳液。
所得涤纶窗帘极限氧指数为35％，防火等级可达B级，续燃时间为0s，损毁长度为37mm。
实施例2
一种阻燃隔热涤纶窗帘，包括涤纶基布和阻燃涂层，所述阻燃涂层由以下重量份计的原料制成：水性聚氨酯乳液13份，聚乙烯醇4份，磷酸三丁酯1.3份，阴离子表面活性剂0.7份，偶联剂0.4份，紫外线吸收剂0.4份，三乙醇胺0.3份，玻璃纤维0.2份，填料3份，消泡剂0.6份，磷酸铵1.7份，水7份。
其中，所述阴离子表面活性剂为十二烷基苯磺酸钠；所述紫外线吸收剂为金红石型氧化钛；所述玻璃纤维的直径为5-10μm；所述填料为海石、石棉纤维粉、硅藻土、羧甲基纤维素钠的混合物，海泡石、石棉纤维粉、硅藻土、羧甲基纤维素钠的重量比为1：1：1：1。
上述阻燃隔热涤纶窗帘的制备方法，包括以下步骤：
步骤1，将水性聚氨酯乳液、聚乙烯醇、磷酸三丁酯、阴离子表面活性剂、偶联剂、紫外线吸收剂、三乙醇胺、玻璃纤维、填料、消泡剂、磷酸铵加至水中，超声分散，研磨，得到阻燃涂层剂；
步骤2，以步骤1所得阻燃涂层剂对涤纶面料进行涂层，然后喷淋胶液，烘干，即得。
其中，所述胶液是10-20wt.％CU-620A纯丙乳液。
所得涤纶窗帘极限氧指数为38％，防火等级可达B级，续燃时间为0s，损毁长度为42mm。
实施例3
一种阻燃隔热涤纶窗帘，包括涤纶基布和阻燃涂层，所述阻燃涂层由以下重量份计的原料制成：水性聚氨酯乳液18份，聚乙烯醇6份，磷酸三丁酯1.8份，阴离子表面活性剂0.9份，偶联剂0.6份，紫外线吸收剂0.6份，三乙醇胺0.4份，玻璃纤维0.2份，填料4份，消泡剂0.9份，磷酸铵2.1份，水8份。
其中，所述阴离子表面活性剂为十二烷基苯磺酸钠；所述紫外线吸收剂为金红石型氧化钛；所述玻璃纤维的直径为5-10μm；所述填料为海石、石棉纤维粉、硅藻土、羧甲基纤维素钠的混合物，海泡石、石棉纤维粉、硅藻土、羧甲基纤维素钠的重量比为1：1：1：1。
上述阻燃隔热涤纶窗帘的制备方法，包括以下步骤：
步骤1，将水性聚氨酯乳液、聚乙烯醇、磷酸三丁酯、阴离子表面活性剂、偶联剂、紫外线吸收剂、三乙醇胺、玻璃纤维、填料、消泡剂、磷酸铵加至水中，超声分散，研磨，得到阻燃涂层剂；
步骤2，以步骤1所得阻燃涂层剂对涤纶面料进行涂层，然后喷淋胶液，烘干，即得。
其中，所述胶液是10-20wt.％CU-620A纯丙乳液。
所得涤纶窗帘极限氧指数为36％，防火等级可达B级，续燃时间为0s，损毁长度为40mm。
实施例4
一种阻燃隔热涤纶窗帘，包括涤纶基布和阻燃涂层，所述阻燃涂层由以下重量份计的原料制成：水性聚氨酯乳液20份，聚乙烯醇7份，磷酸三丁酯2.4份，阴离子表面活性剂1.2份，偶联剂0.7份，紫外线吸收剂0.8份，三乙醇胺0.5份，玻璃纤维0.3份，填料5份，消泡剂1.2份，磷酸铵2.5份，水10份。
其中，所述阴离子表面活性剂为十二烷基苯磺酸钠；所述紫外线吸收剂为金红石型氧化钛；所述玻璃纤维的直径为5-10μm；所述填料为海石、石棉纤维粉、硅藻土、羧甲基纤维素钠的混合物，海泡石、石棉纤维粉、硅藻土、羧甲基纤维素钠的重量比为1：1：1：1。
上述阻燃隔热涤纶窗帘的制备方法，包括以下步骤：
步骤1，将水性聚氨酯乳液、聚乙烯醇、磷酸三丁酯、阴离子表面活性剂、偶联剂、紫外线吸收剂、三乙醇胺、玻璃纤维、填料、消泡剂、磷酸铵加至水中，超声分散，研磨，得到阻燃涂层剂；
步骤2，以步骤1所得阻燃涂层剂对涤纶面料进行涂层，然后喷淋胶液，烘干，即得。
其中，所述胶液是10-20wt.％CU-620A纯丙乳液。
所得涤纶窗帘极限氧指数为39％，防火等级可达B级，续燃时间为0s，损毁长度为37mm。

Claims (7)

1.一种阻燃隔热涤纶窗帘，其特征在于：包括涤纶基布和阻燃涂层，所述阻燃涂层由以下重量份计的原料制成：水性聚氨酯乳液10-20份，聚乙烯醇3-7份，磷酸三丁酯0.8-2.4份，阴离子表面活性剂0.5-1.2份，偶联剂0.2-0.7份，紫外线吸收剂0.3-0.8份，三乙醇胺0.2-0.5份，玻璃纤维0.1-0.3份，填料2-5份，消泡剂0.4-1.2份，磷酸铵1.2-2.5份，水5-10份。
2.根据权利要求1所述的阻燃隔热涤纶窗帘，其特征在于：所述阴离子表面活性剂为十二烷基苯磺酸钠。
3.根据权利要求1所述的阻燃隔热涤纶窗帘，其特征在于：所述紫外线吸收剂为金红石型氧化钛。
4.根据权利要求1所述的阻燃隔热涤纶窗帘，其特征在于：所述玻璃纤维的直径为5-10μm。
5.根据权利要求1所述的阻燃隔热涤纶窗帘，其特征在于：所述填料为海泡石、石棉纤维粉、硅藻土、羧甲基纤维素钠的混合物，海泡石、石棉纤维粉、硅藻土、羧甲基纤维素钠的重量比为1：1：1：1。
6.权利要求1所述的阻燃隔热涤纶窗帘的制备方法，其特征在于：包括以下步骤：
步骤1，将水性聚氨酯乳液、聚乙烯醇、磷酸三丁酯、阴离子表面活性剂、偶联剂、紫外线吸收剂、三乙醇胺、玻璃纤维、填料、消泡剂、磷酸铵加至水中，超声分散，研磨，得到阻燃涂层剂；
步骤2，以步骤1所得阻燃涂层剂对涤纶面料进行涂层，然后喷淋胶液，烘干，即得。
7.根据权利要求6所述的阻燃隔热涤纶窗帘的制备方法，其特征在于：所述胶液是10-20wt.%CU-620A纯丙乳液。
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