CN107334678A - A kind of method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract - Google Patents
A kind of method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract Download PDFInfo
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- CN107334678A CN107334678A CN201710585033.0A CN201710585033A CN107334678A CN 107334678 A CN107334678 A CN 107334678A CN 201710585033 A CN201710585033 A CN 201710585033A CN 107334678 A CN107334678 A CN 107334678A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
It is the degradable nonwoven fabric formed by chitin fiber, chitin fiber, cellulose fibre compound weave the invention discloses a kind of method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract；The described solution being supported on base material is prepared by camellia essential oil, camellia seed dregs of rice extract, chitosan, citric acid, grape-kernel oil, antibacterial peptide, D-sorbite, purified water.Woven using composite fibre spun lacing and base material is made, face matter is smooth submissive, non-stimulated, part-time antibiotic effect, also compounding is added with camellia seed dregs of rice extract component, antibacterial peptide isoreactivity functional component, antibiotic effect is further improved, it is natural safe, non-stimulated, there is the pleasant smell of natural tea perfume, can relieving restlessness, refresh oneself, be made antibacterial wet tissue skin can be played cleaning, moisturizing, sterilization and sterilize the effect of.
Description
Technical field
The present invention relates to the method for preparing antibacterial wet tissue, more particularly to one kind to prepare moist antibacterial using camellia seed dregs of rice extract
The method of towel.
Background technology
Wet tissue is from wet strong soft fine high osmosis base material, through folding, humidifying, pack disposable cleaning health use is made
Product, because its have the characteristics that cleaning, moisturizing skin basic function and be easy to carry as must can not in people's daily life
Few cleaning supplies.It was used for such as civil aviaton, hotel, restaurant, exhibition commercial affairs and reception place in the past, in recent years with people
Growth in the living standard, the personal consumption amount of wet tissue gradually increase, and are mainly used in the outdoor such as travelling, tourism water inconvenience
Occasion, also cleaning-nursing of family infant etc..The wet tissue product more categories of forward direction and the development of applicable multipath.
The yield of wet tissue has faster growth in recent years, there is the wet tissue product of individual brands up to a hundred, year consumption on domestic market
Measure about 500-600 tons.There is family more than 50 in the more regular manufacturing enterprise in the whole nation, separately there is workshop-based small enterprise several hundred.Middle height
Shelves products export is more, and foreign brand name is also constantly increasing in the quantity of China's fixed point processing.
Wet tissue is typically made up of two parts：Base material and decoction.
Base material one kind is wet-strength paper, and one kind is non-woven fabrics.Currently the majority wet tissue is all to use non-woven fabrics in the market, and
Non-woven fabrics is again based on spunlace non-woven cloth.Spunlace non-woven cloth：Be by the fine water flow jet of high pressure to one or more layers web,
Make fiber mutually entangled, so that fibre web is able to reinforce and possesses certain strength, and moisture can be pinned.
All kinds of tea seed aboundresources in China, the current national hm2 of tea oil resource raw material area 366. 6 ten thousand, it is woody to account for the whole nation
More than the 80% of edible oil materials area, produce the t of Seed of Camellia oleifera 6.45 × 106 per year.Cake of camellia oleifera seeds is after tea seed extracts oil
Resultant product, wherein in addition to containing Residual oil, also containing protein, polysaccharose substance, Tea Saponin, polyphenol, alkaloid and tannin etc.
Composition.Tea Saponin is a kind of oleanane type triterpene saponins mixture extracted from cake of camellia oleifera seeds, is a kind of function admirable
Nonionic natural surfactant, and with the multiple biological activities such as hemolytic, antibacterial.Utilize camellia seed dregs of rice extract
Antibacterial wet tissue is prepared, improves camellia seed dregs of rice utilization rate and use range.
The content of the invention
The defects of the object of the invention is exactly to make up prior art, there is provided one kind is prepared anti-using camellia seed dregs of rice extract
The method of bacterium wet tissue.
The present invention is achieved by the following technical solutions：
A kind of method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, it is to be added with base material and load with the solution on the base material
Work is made, described base material be formed by chitin fiber, chitin fiber, cellulose fibre compound weave it is degradable non-
Woven cloths；The described solution being supported on base material is by camellia essential oil, camellia seed dregs of rice extract, chitosan, citric acid, grape
Seed oil, antibacterial peptide, D-sorbite, purified water are prepared.
The described method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, described base material is by 20-30% chitosans
Fiber, 20-30% chitin fibers, the blending spun lacing braiding of 40-60% cellulose fibres form.
The described method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, the described solution being supported on base material are
It is made by following raw materials in part by weight：Camellia essential oil 15-20, camellia seed dregs of rice extract 5-25, chitosan 5-10, citric acid 4-6, Portugal
Grape seed oil 16-18, antibacterial peptide 2-3, D-sorbite 8-12, purified water 400-500.
The described method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, the processing of described camellia seed dregs of rice extract
Method comprises the following steps：
（1）, by camellia seed dregs of rice ungrease treatment, drying fine grinding to 40-100 mesh, be 1 by solid-liquid ratio：It is 80- that 4-6, which is added to concentration,
In 85% ethanol solution, heating water bath handles 40-60 minutes in the case where ultrasonic power is 200-400W, filters separation to 40-55 DEG C,
Filtrate low temperature at 50-65 DEG C concentrates, and concentrate vacuum drying, obtains Tea Saponin；
（2）, by filter residue by solid-liquid ratio be 1:15-20 is added in distilled water, ultrasonic dissolution 28-35 minutes, with 0.5mol/L hydrochloric acid
Solution adjusts pH value to 5.0-5.5, adds the 0.2-0.4% of solution weight composite plant hydrolase, in 40-45 DEG C of thermostatted water
Bathe and 115-125 minutes are digested in oscillator, 90-100 DEG C of water-bath enzyme deactivation 15-20 minute is heated to, with 0.5mol/L sodium hydroxides
Solution adjusts pH values to 8-8.5, adds alkali protease, addition is 4500-4700U/g filter residues, in 50-55 DEG C of thermostatted water
Bathe and 90-100 minutes are digested in oscillator, be heated to 95-100 DEG C of water-bath enzyme deactivation 10-15 minute, under the conditions of 15-20 DEG C, with
4500-5000r/min centrifuges 10-15 minutes, obtains supernatant and is freezed in freeze drier, then is well mixed with Tea Saponin,
Produce；
Described composite plant hydrolase is to be in mass ratio by cellulase, amylase, protease, carbohydrase, zytase
1:1-2:2-4:2-3:1-2 is made.
It is an advantage of the invention that：
The method provided by the invention that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, woven and be made using composite fibre spun lacing
Base material, face matter is smooth submissive, non-stimulated, part-time antibiotic effect, and also compounding is living added with camellia seed dregs of rice extract component, antibacterial peptide etc.
Sexual function composition, further improves antibiotic effect, natural safe, non-stimulated, has the pleasant smell of natural tea perfume, can relieving restlessness,
Refresh oneself, the effect of antibacterial wet tissue can play cleaning, moisturizing, sterilization and sterilization to skin is made.
Embodiment
It is a kind of using camellia seed dregs of rice extract prepare antibacterial wet tissue method, be with base material and load with it is molten on the base material
Liquid is processed into, and described base material is dropped by what chitin fiber, chitin fiber, cellulose fibre compound weave formed
Solve non-woven cloth；The described solution being supported on base material be by camellia essential oil, camellia seed dregs of rice extract, chitosan, citric acid,
Grape-kernel oil, antibacterial peptide, D-sorbite, purified water are prepared.
The described method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, described base material are that 25% chitosan is fine
Dimension, the blending spun lacing braiding of 22% chitin fiber, 53% cellulose fibre form.
The described method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, the described solution being supported on base material are
It is made by following raw materials in part by weight：Camellia essential oil 20, camellia seed dregs of rice extract 25, chitosan 10, citric acid 6, grape-kernel oil 18,
Antibacterial peptide 3, D-sorbite 12, purified water 500.
The described method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, the processing of described camellia seed dregs of rice extract
Method comprises the following steps：
（1）, by camellia seed dregs of rice ungrease treatment, drying fine grinding to 100 mesh, be 1 by solid-liquid ratio：6 be added to concentration for 85% ethanol it is molten
In liquid, heating water bath handles 40 minutes in the case where ultrasonic power is 300W to 55 DEG C, filters separation, filtrate low temperature at 55 DEG C is dense
Contracting, concentrate vacuum drying, obtains Tea Saponin；
（2）, by filter residue by solid-liquid ratio be 1:20 add in distilled water, ultrasonic dissolution 35 minutes, are adjusted with 0.5mol/L hydrochloric acid solutions
PH value is saved to 5.5,0.4% composite plant hydrolase of solution weight is added, 125 is digested in 45 DEG C of thermostatic control oscillator vibrations
Minute, 100 DEG C of water-bath enzyme deactivations 20 minutes are heated to, pH values is adjusted to 8.5 with 0.5mol/L sodium hydroxide solutions, adds alkalescence
Protease, addition are 4700U/g filter residues, are digested 100 minutes in 55 DEG C of thermostatic control oscillator vibrations, are heated to 100 DEG C of water-baths
Enzyme deactivation 15 minutes, under the conditions of 20 DEG C, centrifuged 15 minutes with 4500r/min, obtain supernatant and freezed in freeze drier, then
It is well mixed, produces with Tea Saponin；
Described composite plant hydrolase is to be in mass ratio by cellulase, amylase, protease, carbohydrase, zytase
1:1:3:2:2 are made.
Claims (4)
1. a kind of method that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, it is with base material and load and the solution on the base material
It is processed into, it is characterised in that：Described base material is by chitin fiber, chitin fiber, cellulose fibre compound weave
The degradable nonwoven fabric formed；The described solution being supported on base material is gathered by camellia essential oil, camellia seed dregs of rice extract, shell
Sugar, citric acid, grape-kernel oil, antibacterial peptide, D-sorbite, purified water are prepared.
2. the method according to claim 1 that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, it is characterised in that described
Base material be by 20-30% chitin fibers, 20-30% chitin fibers, 40-60% cellulose fibres blending spun lacing braiding form.
3. the method according to claim 1 that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, it is characterised in that described
The solution being supported on base material be made of by following raw materials in part by weight：Camellia essential oil 15-20, camellia seed dregs of rice extract 5-25,
Chitosan 5-10, citric acid 4-6, grape-kernel oil 16-18, antibacterial peptide 2-3, D-sorbite 8-12, purified water 400-500.
4. the method according to claim 1 that antibacterial wet tissue is prepared using camellia seed dregs of rice extract, it is characterised in that described
The processing method of camellia seed dregs of rice extract comprise the following steps：
（1）, by camellia seed dregs of rice ungrease treatment, drying fine grinding to 40-100 mesh, be 1 by solid-liquid ratio：It is 80- that 4-6, which is added to concentration,
In 85% ethanol solution, heating water bath handles 40-60 minutes in the case where ultrasonic power is 200-400W, filters separation to 40-55 DEG C,
Filtrate low temperature at 50-65 DEG C concentrates, and concentrate vacuum drying, obtains Tea Saponin；
（2）, by filter residue by solid-liquid ratio be 1:15-20 is added in distilled water, ultrasonic dissolution 28-35 minutes, with 0.5mol/L hydrochloric acid
Solution adjusts pH value to 5.0-5.5, adds the 0.2-0.4% of solution weight composite plant hydrolase, in 40-45 DEG C of thermostatted water
Bathe and 115-125 minutes are digested in oscillator, 90-100 DEG C of water-bath enzyme deactivation 15-20 minute is heated to, with 0.5mol/L sodium hydroxides
Solution adjusts pH values to 8-8.5, adds alkali protease, addition is 4500-4700U/g filter residues, in 50-55 DEG C of thermostatted water
Bathe and 90-100 minutes are digested in oscillator, be heated to 95-100 DEG C of water-bath enzyme deactivation 10-15 minute, under the conditions of 15-20 DEG C, with
4500-5000r/min centrifuges 10-15 minutes, obtains supernatant and is freezed in freeze drier, then is well mixed with Tea Saponin,
Produce；
Described composite plant hydrolase is to be in mass ratio by cellulase, amylase, protease, carbohydrase, zytase
1:1-2:2-4:2-3:1-2 is made.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107980819A (en) * | 2018-01-15 | 2018-05-04 | 中鸿纳米纤维技术丹阳有限公司 | A kind of pure natural nanoscale thimerosal |
| CN108653713A (en) * | 2018-06-12 | 2018-10-16 | 广西庆翠堂生物科技有限责任公司 | A kind of natural composite antibacterial composition and preparation method thereof containing Tea Saponin |
| CN110522654A (en) * | 2019-09-06 | 2019-12-03 | 王文概 | Safe and non-stimulating Baby Care wet tissue containing camellia seed oil and preparation method thereof |
| CN111593566A (en) * | 2020-05-28 | 2020-08-28 | 安徽省天助纺织科技集团股份有限公司 | Degradable functional wet tissue and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107980819A (en) * | 2018-01-15 | 2018-05-04 | 中鸿纳米纤维技术丹阳有限公司 | A kind of pure natural nanoscale thimerosal |
| CN108653713A (en) * | 2018-06-12 | 2018-10-16 | 广西庆翠堂生物科技有限责任公司 | A kind of natural composite antibacterial composition and preparation method thereof containing Tea Saponin |
| CN108653713B (en) * | 2018-06-12 | 2022-01-07 | 广西庆翠堂生物科技有限责任公司 | Natural composite antibacterial composition containing tea saponin and preparation method thereof |
| CN110522654A (en) * | 2019-09-06 | 2019-12-03 | 王文概 | Safe and non-stimulating Baby Care wet tissue containing camellia seed oil and preparation method thereof |
| CN111593566A (en) * | 2020-05-28 | 2020-08-28 | 安徽省天助纺织科技集团股份有限公司 | Degradable functional wet tissue and preparation method thereof |
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Application publication date: 20171110 |