CN107300303A - A kind of dried immature fruit of citron orange production method of utilization microwave drying - Google Patents
A kind of dried immature fruit of citron orange production method of utilization microwave drying Download PDFInfo
- Publication number
- CN107300303A CN107300303A CN201710571770.5A CN201710571770A CN107300303A CN 107300303 A CN107300303 A CN 107300303A CN 201710571770 A CN201710571770 A CN 201710571770A CN 107300303 A CN107300303 A CN 107300303A
- Authority
- CN
- China
- Prior art keywords
- immature fruit
- citron orange
- dried immature
- dried
- demulcen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B9/00—Machines or apparatus for drying solid materials or objects at rest or with only local agitation; Domestic airing cupboards
- F26B9/06—Machines or apparatus for drying solid materials or objects at rest or with only local agitation; Domestic airing cupboards in stationary drums or chambers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B1/00—Sieving, screening, sifting, or sorting solid materials using networks, gratings, grids, or the like
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/044—Cleaning involving contact with liquid using agitated containers in which the liquid and articles or material are placed
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B3/00—Drying solid materials or objects by processes involving the application of heat
- F26B3/32—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action
- F26B3/34—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action by using electrical effects
- F26B3/347—Electromagnetic heating, e.g. induction heating or heating using microwave energy
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B2200/00—Drying processes and machines for solid materials characterised by the specific requirements of the drying good
- F26B2200/02—Biomass, e.g. waste vegetative matter, straw
Abstract
A kind of dried immature fruit of citron orange production method of utilization microwave drying, including, 1）Selection；2）Demulcen；3）Section；4）Dry, the dried immature fruit of citron orange after cutting is laid on the circular drip pan of micro-wave oven, temperature is at 50 70 degrees Celsius, until moisture is less than 13%, that is, stop heating；5）Screening；6）Examine.The dried immature fruit of citron orange is dried using microwave in the present invention, its speed dried is fast, and the content of synephrine is high.
Description
Technical field
The present invention relates to a kind of production method of Chinese medicine, more particularly to a kind of dried immature fruit of citron orange production method of utilization microwave drying.
Background technology
In the pharmacy procedure of the prepared slices of Chinese crude drugs, drying is a particularly important ring, and the technology dried has Exposure to Sunlight and electricity at present
It is roasting two kinds, but the efficiency of heating surface of both approaches is not high, and the content of the active ingredient synephrine dried out is not high.
The content of the invention
The technical problem to be solved in the present invention is to overcome the deficiencies in the prior art high there is provided a kind of drying efficiency, and pungent
The not dried immature fruit of citron orange production method of the high utilization microwave drying of woods content.
In order to solve the above technical problems, technical scheme proposed by the present invention is：A kind of dried immature fruit of citron orange production of utilization microwave drying
Method, 1) dried immature fruit of citron orange to be chosen is placed on clean workbench, impurity is picked, the content of selection rear impurity is less than 2%, will picked
The dried immature fruit of citron orange after choosing is put into turnover barrel；
2) demulcen,
2.1) wash, the dried immature fruit of citron orange in turnover barrel is poured into cleaning roller, by cleaning rotating and reverse for roller, will
The dried immature fruit of citron orange is cleaned up；And the dried immature fruit of citron orange cleaned up is encased in stainless steel material frame with holes and drained；2.2) demulcen, by the dried immature fruit of citron orange
It is encased in ventilative material frame, then material frame is put into the cabinet of medicine processing device, first vacuumizes 7-15 minutes so that in cabinet
Air pressure be below -0.06Mpa, open steam valve, logical steam demulcen causes medicinal material to run through in 15-25 minute so that dried immature fruit of citron orange incision
Centre is without the dry heart；
3) dried immature fruit of citron orange for completing demulcen completes section within half an hour, is cut into 1-2mm thin slice, does not complete the trifoliate orange of section
Practical plastic cloth is wrapped up；Prevent the evaporation of dried immature fruit of citron orange moisture, influence section.
4) dry, the dried immature fruit of citron orange after cutting is laid on the circular drip pan of micro-wave oven, temperature is at 50-70 degrees Celsius, always
It is less than 13% to moisture, that is, stops heating；
5) screen, the dried dried immature fruit of citron orange is placed on the screen cloth of screening machine, remove medicine bits, the impurity content after screening is less than
2%；
6) examine,
6.1) need testing solution is prepared, dried dried immature fruit of citron orange 1g is taken, is put into conical flask, methanol 50ml is added, it is weighed
Weight, is heated to reflux 1.5 hours, lets cool, then weighed weight, and the weight of less loss is supplied with methanol, is shaken up, and filtration, precision is measured
Subsequent filtrate 10ml, is evaporated, and the residue 10ml that adds water makes dissolving, by polyamide column, and the polyamide column is 60~90 mesh, 2.5g,
Internal diameter is 1.5cm, and dry column-packing is eluted with water 25ml, collects eluent, be transferred in 25ml measuring bottles, add water to scale, shake
It is even, produce need testing solution；
6.2) take synephrine appropriate, add water and solution of every 1ml containing 30ug is made, be prepared into reference substance solution；
6.3) reference substance solution and each 10-20 μ l of need testing solution are drawn respectively, liquid chromatograph is injected, and determine synephrine
(C9H13NO2) content.
Compared with prior art, the advantage of the invention is that：The dried immature fruit of citron orange is dried using microwave in the present invention, it is dried
Speed it is fast, and the content of synephrine is high.
Embodiment
For the ease of understanding the present invention, present invention work more comprehensively, is meticulously described below in conjunction with preferred embodiment,
But protection scope of the present invention is not limited to embodiment in detail below.
It should be strongly noted that when a certain element, to be described as " be fixed on, be fixed in, be connected to or be communicated in " another
When on element, it can be directly fixed, affixed, connection or connect on another element or by connecting in the middle of other
Fitting is indirectly fixed, affixed, connection or connection are on another element.
Unless otherwise defined, the implication that all technical terms used hereinafter are generally understood that with those skilled in the art
It is identical.Technical term used herein is intended merely to describe the purpose of specific embodiment, is not intended to the limitation present invention
Protection domain.
Embodiment
A kind of dried immature fruit of citron orange production method of utilization microwave drying, 1) dried immature fruit of citron orange to be chosen is placed on clean workbench, pick
Decontamination, the content of selection rear impurity is less than 2%, and the dried immature fruit of citron orange after selection is put into turnover barrel；2) demulcen,
2.1) wash, the dried immature fruit of citron orange in turnover barrel is poured into cleaning roller, by cleaning rotating and reverse for roller, will
The dried immature fruit of citron orange is cleaned up；And the dried immature fruit of citron orange cleaned up is encased in stainless steel material frame with holes and drained；2.2) demulcen, by the dried immature fruit of citron orange
It is encased in ventilative material frame, then material frame is put into the cabinet of medicine processing device, first vacuumizes 7-15 minutes so that in cabinet
Air pressure be below -0.06Mpa, open steam valve, logical steam demulcen causes medicinal material to run through in 15-25 minute so that dried immature fruit of citron orange incision
Centre is without the dry heart；
3) dried immature fruit of citron orange for completing demulcen completes section within half an hour, is cut into 1-2mm thin slice, does not complete the trifoliate orange of section
Practical plastic cloth is wrapped up；
4) dry, the dried immature fruit of citron orange after cutting is laid on the circular drip pan of micro-wave oven, temperature is at 50-70 degrees Celsius, always
It is less than 13% to moisture, that is, stops heating；
5) screen, the dried dried immature fruit of citron orange is placed on the screen cloth of screening machine, remove medicine bits, the impurity content after screening is less than
2%；
6) examine,
6.1) need testing solution is prepared, dried dried immature fruit of citron orange 1g is taken, is put into conical flask, methanol 50ml is added, it is weighed
Weight, is heated to reflux 1.5 hours, lets cool, then weighed weight, and the weight of less loss is supplied with methanol, is shaken up, and filtration, precision is measured
Subsequent filtrate 10ml, is evaporated, and the residue 10ml that adds water makes dissolving, by polyamide column, and the polyamide column is 60~90 mesh, 2.5g,
Internal diameter is 1.5cm, and dry column-packing is eluted with water 25ml, collects eluent, be transferred in 25ml measuring bottles, add water to scale, shake
It is even, produce need testing solution；
6.2) take synephrine appropriate, add water and solution of every 1ml containing 30ug is made, be prepared into reference substance solution；
6.3) reference substance solution and each 10-20 μ l of need testing solution are drawn respectively, liquid chromatograph is injected, and determine synephrine
Content.In the present embodiment, inventor did contrast test twice on June 9th, 2017 and on June 12nd, 2017 respectively, right
The dried immature fruit of citron orange is dried than solarization method, baking and micro-wave drying method in experiment, has been respectively adopted, and by the present embodiment
Method detects the content of its synephrine, and its result is as shown in Table 1.
Claims (1)
1. a kind of dried immature fruit of citron orange production method of utilization microwave drying, it is characterised in that：1) dried immature fruit of citron orange to be chosen is placed in clean work
Make on platform, pick impurity, the content of selection rear impurity is less than 2%, the dried immature fruit of citron orange after selection is put into turnover barrel；
2）Demulcen,
2.1）Wash, the dried immature fruit of citron orange in turnover barrel is poured into cleaning roller, by cleaning rotating and reverse for roller, by the dried immature fruit of citron orange
Clean up；And the dried immature fruit of citron orange cleaned up is encased in stainless steel material frame with holes and drained；2.2）Demulcen, the dried immature fruit of citron orange is encased in
In ventilative material frame, then material frame is put into the cabinet of medicine processing device, first vacuumized 7-15 minutes so that the air pressure in cabinet
Below -0.06Mpa, to open steam valve, logical steam demulcen causes medicinal material to run through in 15-25 minutes so that do not have in the middle of dried immature fruit of citron orange incision
There is the dry heart；
3）The dried immature fruit of citron orange that demulcen is completed completes section within half an hour, is cut into 1-2mm thin slice, and the dried immature fruit of citron orange for not completing section is used
Plastic cloth is wrapped up；
4）Dry, the dried immature fruit of citron orange after cutting is laid on the circular drip pan of micro-wave oven, temperature is at 50-70 degrees Celsius, until water
Divide and be less than 13%, that is, stop heating；
5）Screening, the dried dried immature fruit of citron orange is placed on the screen cloth of screening machine, removes medicine bits, and the impurity content after screening is less than 2%；
6）Examine,
6.1）Need testing solution is prepared, dried dried immature fruit of citron orange 1g is taken, is put into conical flask, addition methanol 50ml, weighed weight,
It is heated to reflux 1.5 hours, lets cool, then weighed weight, the weight of less loss is supplied with methanol, is shaken up, is filtered, precision measures subsequent filtrate
10ml, is evaporated, and the residue 10ml that adds water makes dissolving, by polyamide column, and the polyamide column is 60~90 mesh, 2.5g, and internal diameter is
1.5cm, dry column-packing is eluted with water 25ml, is collected eluent, is transferred in 25ml measuring bottles, adds water to scale, shake up, produce
Need testing solution；
6.2）Take synephrine appropriate, add water and solution of every 1ml containing 30ug is made, be prepared into reference substance solution；
6.3）Reference substance solution and each 10-20 μ l of need testing solution are drawn respectively, liquid chromatograph is injected, and are determined synephrine and are contained
Amount.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710571770.5A CN107300303A (en) | 2017-07-13 | 2017-07-13 | A kind of dried immature fruit of citron orange production method of utilization microwave drying |
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| CN201710571770.5A CN107300303A (en) | 2017-07-13 | 2017-07-13 | A kind of dried immature fruit of citron orange production method of utilization microwave drying |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114470051A (en) * | 2022-01-20 | 2022-05-13 | 北京橘井健康科技集团有限公司 | Preparation method of roasted immature bitter orange for DACHAIHU decoction |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101366849A (en) * | 2007-08-15 | 2009-02-18 | 未名天人中药有限公司 | Quality control method for traditional Chinese medicine citrus aurantium |
| CN101805267A (en) * | 2010-04-27 | 2010-08-18 | 南京泽朗医药科技有限公司 | Method for preparing synephrine through continuous intermediate-pressure column chromatography |
| CN102068573A (en) * | 2009-11-20 | 2011-05-25 | 天津中新药业集团股份有限公司乐仁堂制药厂 | Quality control method for stomach reinforcing and digestion promoting tangerine peel, pinellia, immature bitter orange and atractylodes macrocephala pill |
| CN103432326A (en) * | 2013-08-10 | 2013-12-11 | 田克力 | Preparation method for rhizoma cyperi decoction pieces |
| CN105902620A (en) * | 2016-03-18 | 2016-08-31 | 内蒙古王爷地苁蓉生物有限公司 | Fresh cistanche decoction piece and preparation method thereof |
-
2017
- 2017-07-13 CN CN201710571770.5A patent/CN107300303A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101366849A (en) * | 2007-08-15 | 2009-02-18 | 未名天人中药有限公司 | Quality control method for traditional Chinese medicine citrus aurantium |
| CN102068573A (en) * | 2009-11-20 | 2011-05-25 | 天津中新药业集团股份有限公司乐仁堂制药厂 | Quality control method for stomach reinforcing and digestion promoting tangerine peel, pinellia, immature bitter orange and atractylodes macrocephala pill |
| CN101805267A (en) * | 2010-04-27 | 2010-08-18 | 南京泽朗医药科技有限公司 | Method for preparing synephrine through continuous intermediate-pressure column chromatography |
| CN103432326A (en) * | 2013-08-10 | 2013-12-11 | 田克力 | Preparation method for rhizoma cyperi decoction pieces |
| CN105902620A (en) * | 2016-03-18 | 2016-08-31 | 内蒙古王爷地苁蓉生物有限公司 | Fresh cistanche decoction piece and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114470051A (en) * | 2022-01-20 | 2022-05-13 | 北京橘井健康科技集团有限公司 | Preparation method of roasted immature bitter orange for DACHAIHU decoction |
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Application publication date: 20171027 |