CN107281086A

CN107281086A - A kind of repair latex and preparation method thereof

Info

Publication number: CN107281086A
Application number: CN201710534770.8A
Authority: CN
Inventors: 智佳
Original assignee: Individual
Current assignee: Individual
Priority date: 2017-07-03
Filing date: 2017-07-03
Publication date: 2017-10-24

Abstract

The invention discloses a kind of repair latex and preparation method thereof, the repair latex is prepared from by the raw material of following mass percent：Fructus Fici extract 5%, polyquaternium 4%, squalene 3%, Gotu Kola P.E 6%, extractive of usnea 4%, orange peel oil 4.3%, placental hormone 2%, salmon ovary peptide 5%, epithelical cell growth factor 2%, jojoba seed oil 3%, vitamin E 2%, Sodium Hyaluronate 0.2%, sesame seed oil 6%, the lemon seed oil 4.5%, tussol 1%, deionized water surplus.Emulsion obtained by the present invention has the function of the significant newborn and reconstruction tissue for promoting cell, and with preferable moisturizing, anti-aging function.

Description

A kind of repair latex and preparation method thereof

Technical field

The present invention relates to skin care field, and in particular to a kind of repair latex and preparation method thereof.

Background technology

Sensitive skin has following characteristics mostly；

1st, epiderm skin is thin, and capilary is obvious；

2nd, skin lacks the easily congested redness of gloss, cheek；

3rd, cause skin that unsure state is easily presented because of seasonal variations；Situation, it may appear that itch, play fash；

4th, easily by cold wind, food, water quality, ultraviolet, synthetic fibers, fragrance；Or the influence of material.The life of healthy skin The reason cycle is 28 days, and the compact texture that marshalling is formed from basalis to cuticula is sufficiently protected and moisturizing there is provided skin Function.Skin possesses normal physiological period, and the cuticula horn cell of the skin the superiors can arrange very neat, and lines is extremely thin Cause, oil-water balance.The skin metabolism period staggering of sensitive skin, epidermal structure arrangement is mixed and disorderly, Skin Cell also prematurity, natural When moisturizing factor and intercellular lipid are also manufactured without complete, cuticula is just peeled off, and keratoderma cell arrangement is irregular, and And can up roll up crowded, the moisture content inside skin is easily lost in, and the protection without sebum film, excitor substance or allergin are easily invaded Enter, cause inflammation inside skin.

At present, the product that most of antiallergic senses are repaired on the market, anti-inflammatory of only calming, this has side to immediate allergic skin Help, but to the conditioning of sensitive in fact use less, and also can not be truly the reparative regeneration for realizing skin.

The content of the invention

To solve the above problems, the invention provides a kind of repair latex, the new life and reconstruction group of cell can be promoted Knit.

To achieve the above object, the technical scheme taken of the present invention is：

A kind of repair latex, is prepared from by the raw material of following mass percent：

Fructus Fici extract 5%, polyquaternium 4%, squalene 3%, Gotu Kola P.E 6%, extractive of usnea 4%, Orange (CITRUS SPP.) peel oil 4.3%, placental hormone 2%, salmon ovary peptide 5%, epithelical cell growth factor 2%, Jojoba (SIMMONDSIA CHINENSIS) seed oil 3%, vitamin E 2%, Sodium Hyaluronate 0.2%, sesame (SESAMUM INDICUM) seed oil 6%, lemon (CITRUS LIMON) seed oil 4.5%, tussol 1%, deionized water surplus.

Wherein, the Fructus Fici extract is as obtained by prepared by following steps：

It S1, will clean after the fig fruit that drains is placed in and crushed in micronizer, 3-8 times of water added, by quality hundred Divide to add at neutral proteinase, 30-50 DEG C than the ratio for 0.5-2% and digest 0.5-2h, filter, obtain enzymolysis liquid；

S2, by naturally to thaw again after the zymotic fluid quick freeze of gained, precipitate age of starch in extract；Collect supernatant Liquid, remainder centrifugation is collected centrifugal liquid and is incorporated in supernatant；

S3, by supernatant with 3-7BV/h flow velocity by macroporous resin column, after Dynamic Adsorption saturation, with deionized water with The 5-8BV/h above-mentioned macroporous resin column of flow velocity elution is colourless to efflux, then the organic solvent for being 50%-60% with volume fraction Eluted with 8-12BV/h flow velocity, collect eluent, be concentrated under reduced pressure, obtain medicinal extract；

S4, medicinal extract water is dissolved after with 4-6BV/h flow velocity by polyamide column, after Dynamic Adsorption saturation, use 4-5BV Deionized water elutes above-mentioned polyamide column with 3-9BV/h flow velocity, then the aqueous solution for being 40%-50% with volume fraction is with 5- 10BV/h flow velocity is eluted, and collection has eluent, is spray-dried, is obtained Fructus Fici extract.

Wherein, the Gotu Kola P.E is as obtained by prepared by following steps：

After fresh centella saline sook 0.5~1 hour, after being placed in flash extracter processing processing 2-5 seconds, plus Enter 90% methanol or ethanol solution of 6 times of volumes, handle 1-3 minutes, after separation of solid and liquid, reclaim methanol or ethanol solution, concentrate, So that extract is in paste, then is extracted 3 times with water-saturated n-butanol to extract, it is after recycling design, extract vacuum is dense Contracting drying, obtains Gotu Kola P.E.

Wherein, the extractive of usnea is as obtained by prepared by following steps：

Sunglo is cleaned after draining, ultramicro grinding processing is carried out, then with solid-liquid ratio 1g:10mL, adding mass fraction is 70% ethanol, is placed in Ultrasonic cell smash, 35 DEG C of extraction 30min；Top extract solution is drawn after the completion of extraction to be put into Rotary Evaporators carry out vacuum distillation, collect Extraction solvent, and spray drying obtains extractive of usnea.

Present invention also offers the preparation method of above-mentioned repair latex, comprise the following steps：

S1, by above-mentioned formula weigh each raw material：

S2, by the polyquaternium weighed, squalene and water mix after, be warming up to 80-85 DEG C, it is ensured that material is completely dissolved, Obtain A phases；

S3, by the orange peel oil weighed, jojoba seed oil, vitamin E, sesame seed oil, the lemon seed oil mix after, be warming up to 80-85 DEG C, stir, obtain B phases；

S4, the Fructus Fici extract weighed, Gotu Kola P.E, extractive of usnea, Sodium Hyaluronate mixed it is equal After even, C phases are obtained；

S5, the tussol weighed, placental hormone, salmon ovary peptide, epithelical cell growth factor are mixed evenly after, obtain D phases；

S6, B phases are pumped into A phases homogeneous stir and be incubated after 30 minutes within 5 minutes, slow cooling to 45 degree addition C phases continues Cooling, 25 DEG C add D phases and stir, and discharge, and sterilization is filling to produce.

The invention has the advantages that：

By the way that Fructus Fici extract, squalene, placental hormone and salmon ovary peptide, collaboration extractive of usnea and product is used in combination The use of the careless extract of snow so that the emulsion of gained has the anti-oxidant, crease-resistant of highly significant, promotes promoting epidermization effect；It is logical The addition of epithelical cell growth factor is crossed, excellent skin repair function is made it have；The addition of tussol can be avoided and subtracted Light problem of being remained silent caused by skin care item overnutrition.In summary, the preparation obtained by the present invention has highly significant Promote skin regeneration and delay the effect of cell senescence.

Embodiment

In order that objects and advantages of the present invention are more clearly understood, the present invention is carried out with reference to embodiments further Describe in detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit this hair It is bright.

In following examples, used Fructus Fici extract is as obtained by prepared by following steps：

The Gotu Kola P.E is as obtained by prepared by following steps：

The extractive of usnea is as obtained by prepared by following steps：

Used organic solvent is the turpentine derivatives of natural origin, and the turpentine derivatives are different for firpene Structure, disproportionation products.Other materials is commercially available.

Embodiment 1

Embodiment 2

A kind of preparation method of repair latex, comprises the following steps：

S1, the formula as described in embodiment 1 weigh each raw material：

Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should It is considered as protection scope of the present invention.

Claims

1. a kind of repair latex, it is characterised in that be prepared from by the raw material of following mass percent：

Fructus Fici extract 5%, polyquaternium 4%, squalene 3%, Gotu Kola P.E 6%, extractive of usnea 4%, orange fruit Skin oil 4.3%, placental hormone 2%, salmon ovary peptide 5%, epithelical cell growth factor 2%, jojoba seed oil 3%, vitamin E 2%th, Sodium Hyaluronate 0.2%, sesame seed oil 6%, the lemon seed oil 4.5%, tussol 1%, deionized water surplus.

2. a kind of repair latex as claimed in claim 1, it is characterised in that the Fructus Fici extract passes through following steps system Standby gained：

It S1, will clean after the fig fruit that drains is placed in and crushed in micronizer, add 3-8 times of water, by mass percentage Neutral proteinase is added for 0.5-2% ratio, 0.5-2h is digested at 30-50 DEG C, filters, obtain enzymolysis liquid；

S2, by naturally to thaw again after the zymotic fluid quick freeze of gained, precipitate age of starch in extract；Collect supernatant, Remainder is centrifuged, and is collected centrifugal liquid and is incorporated in supernatant；

S3, by supernatant with 3-7BV/h flow velocity by macroporous resin column, after Dynamic Adsorption saturation, with deionized water with 5- It is colourless to efflux that 8BV/h flow velocity elutes above-mentioned macroporous resin column, then the organic solvent for being 50%-60% with volume fraction with 8-12BV/h flow velocity is eluted, and is collected eluent, is concentrated under reduced pressure, obtains medicinal extract；

S4, medicinal extract water is dissolved after with 4-6BV/h flow velocity by polyamide column, after Dynamic Adsorption saturation, gone with 4-5BV from Sub- water elutes above-mentioned polyamide column with 3-9BV/h flow velocity, then the aqueous solution for being 40%-50% with volume fraction is with 5-10BV/h Flow velocity eluted, collection have eluent, be spray-dried, obtain Fructus Fici extract.

3. a kind of repair latex as claimed in claim 1, it is characterised in that the Gotu Kola P.E passes through following steps system Standby gained：

After fresh centella saline sook 0.5~1 hour, after being placed in flash extracter processing processing 2-5 second, addition 6 90% methanol or ethanol solution of times volume, are handled 1-3 minute, after separation of solid and liquid, reclaim methanol or ethanol solution, are concentrated, are made It is in paste to obtain extract, then extract is extracted 3 times with water-saturated n-butanol, and after recycling design, extract is concentrated in vacuo Dry, obtain Gotu Kola P.E.

4. a kind of repair latex as claimed in claim 1, it is characterised in that the extractive of usnea is prepared by following steps Gained：

Sunglo is cleaned after draining, ultramicro grinding processing is carried out, then with solid-liquid ratio 1g:10mL, it is 70% to add mass fraction Ethanol, be placed in Ultrasonic cell smash, 35 DEG C extraction 30min；Top extract solution is drawn after the completion of extraction and is put into rotation Evaporimeter carries out vacuum distillation, collects Extraction solvent, and spray drying obtains extractive of usnea.

5. a kind of preparation method of repair latex, it is characterised in that comprise the following steps：

S1, the formula as described in claim any one of 1-4 weigh each raw material：

S2, by the polyquaternium weighed, squalene and water mix after, be warming up to 80-85 DEG C, it is ensured that material is completely dissolved, obtain A Phase；

S3, by the orange peel oil weighed, jojoba seed oil, vitamin E, sesame seed oil, the lemon seed oil mix after, be warming up to 80- 85 DEG C, stir, obtain B phases；

S4, the Fructus Fici extract weighed, Gotu Kola P.E, extractive of usnea, Sodium Hyaluronate are mixed evenly after, Obtain C phases；

S6, B phases are pumped into A phases homogeneous stir and be incubated after 30 minutes within 5 minutes, slow cooling adds C phases to 45 degree to be continued to cool, 25 DEG C add D phases and stir, and discharge, and sterilization is filling to produce.