CN107267286A - Emulate rose spray and preparation method thereof - Google Patents
Emulate rose spray and preparation method thereof Download PDFInfo
- Publication number
- CN107267286A CN107267286A CN201710530131.4A CN201710530131A CN107267286A CN 107267286 A CN107267286 A CN 107267286A CN 201710530131 A CN201710530131 A CN 201710530131A CN 107267286 A CN107267286 A CN 107267286A
- Authority
- CN
- China
- Prior art keywords
- rose
- spray
- parts
- attar
- berry extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41G—ARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
- A41G1/00—Artificial flowers, fruit, leaves, or trees; Garlands
- A41G1/001—Artificial flowers, fruit, leaves, or trees; Garlands characterised by their special functions
- A41G1/006—Diffusing perfume or the like
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
Abstract
One kind emulation rose spray and preparation method thereof, the spray is composed of the following raw materials by weight：2~3 parts of acrylic acid, 8~12 parts of ethanol, 3~5 parts of Bordeaux mixture, 5~10 parts of Flos Rosae Rugosas pollen, 0.5~0.8 part of alkylnaphthalene sulfonate, 0.2~0.6 part of styrax, 1~2 part of Vanillin, 2~4 parts of rose berry extract, 0.1~0.3 part of Tea Polyphenols, 0.5~0.7 part of attar of rose.The sprayer formulation that the present invention is provided is sprayed on emulation rose surface, the fragrance of a flower is lasting specifically designed for emulation rose design, it is pollution-free there is provided preparation method, attar of rose, rose berry extract extraction efficiency are high, the impurity contained is few, does not destroy active ingredient, and uniformity is good.
Description
Technical field
The present invention relates to artificial flowers technical field, and in particular to one kind emulation rose spray and preparation method thereof.
Background technology
In very long a period of time, high-grade artificial flowers have beautified our living environment.With the improvement of living standards,
Fresh flower progresses into family.Beautify the important colored material of family and PE it should be noted that artificial flower is still for we.It, which has, holds
Long property, convenience and the big characteristic of intention three.
Fresh flower is pretty and dazzling, but the flowers are in blossom that blossom fall is pitiable, and artificial flower meets people's love flower and cherishs colored love knot.Artificial flower is made
Product can be disposed at the occasion that fresh flower works can not be put and inconvenience is often managed, and such as rather dark place, decoration cabinet is medium.It is daily
Eliminated in decoration and change the operation such as water, wash bottle, as long as removing the dust on surface in time, durable in use, nursing is convenient.
Huge be also manifested by flower arrangement exhibition both domestic and external and match of artificial flowers market potential has high-grade emulation floriculture to make
Product, this also illustrates that artificial flowers are increasingly praised highly and paid close attention to, and gives artificial flowers market potential great space, hotel lobby
In large-scale flower arrangement also mixed and be inserted into fresh flower by high-grade artificial flowers or high-grade artificial flowers mostly, the light such as bar, amusement hall, bathing pool
Line is dark or high humidity local suitably with high-grade artificial flowers works.In the middle of the escalator in market, all kinds of commodity and large-scale cupboard
In window, for the ease of arrangement, waterproof and conveniently manage and view and admire lasting, it is all a large amount of to be arranged flowers using high-grade artificial flowers.
But existing artificial flowers can only be simulated by color and profile to true flowers, reach the effect mixed the spurious with the genuine
Really, how to allow artificial flowers to give out the due fragrance of true fresh flower institute, be always problem of the pendulum in face of people, it is main at present logical
Cross the mode of perfumes or artificial flowers material is improved, but common perfume is not suitable for artificial flowers and used, it is necessary to specially
Door is designed for artificial flowers.
The content of the invention
It is an object of the invention to solve above-mentioned technical problem, there is provided one kind emulation rose spray and its preparation side
Method.
The technical problems to be solved by the invention are realized using following technical scheme：
One kind emulation rose spray, is composed of the following raw materials by weight：
2~3 parts of acrylic acid, 8~12 parts of ethanol, 3~5 parts of Bordeaux mixture, 5~10 parts of Flos Rosae Rugosas pollen, alkylnaphthalene sulfonate
0.5~0.8 part, 0.2~0.6 part of styrax, 1~2 part of Vanillin, 2~4 parts of rose berry extract, Tea Polyphenols 0.1~0.3
Part, 0.5~0.7 part of attar of rose.
It is preferred that, the spray is composed of the following raw materials by weight：
2.5 parts of acrylic acid, 10 parts of ethanol, 0.4 part of Bordeaux mixture, 7.5 parts of Flos Rosae Rugosas pollen, 0.6 part of alkylnaphthalene sulfonate, peace
Breath is fragrant 0.4 part, 1.5 parts of Vanillin, 0.3 part of rose berry extract, 0.2 part of Tea Polyphenols, 0.6 part of attar of rose.
It is preferred that, the Bordeaux mixture is formulated by 3 grams of copper sulphate, 2.5 grams of white lime and 0.5 kilogram of water.
It is preferred that, the alkylnaphthalene sulfonate is Negel.
One kind emulation rose spray preparation method, including following steps：
(1) attar of rose is prepared
The rose 100g of natural drying is taken, it is finely ground, it is placed in 1000ml round-bottomed flasks, adds 700ml distilled water, cold soaking
Pressed after 2h after steam distillation heating extraction, backflow 4h, separate attar of rose, add a small amount of anhydrous sodium sulfate drying, produce rose
Rare oil；
(2) rose berry extract is prepared
Fructus rosae is smashed to pieces and is put into pressure pan, ethanol is added, pressurizes and keep pressure for a period of time, then pressure release and is carried out
Filtering, filtrate is placed in refrigerating chamber and refrigerated, and the filtrate after refrigeration terminates is centrifuged, and collects supernatant, and rose is made
Rare berry extract；
(3) spray is prepared
Acrylic acid, ethanol, Bordeaux mixture, Flos Rosae Rugosas pollen, alkylnaphthalene sulfonate, styrax, vanilla are weighed by formula ratio
Element, rose berry extract, Tea Polyphenols and attar of rose, warm water dissolve and stirred to being completely dissolved, and then carry out ultrasonically treated, cooling
To room temperature, the spray is made.
It is preferred that, water temperature is controlled in the step (1), during cold soaking at 2~5 DEG C.
It is preferred that, in the step (2), amount of alcohol added is 2~3 times of fructus rosae weight.
It is preferred that, in the step (2), moulding pressure is 250~300Mpa, and pressure hold time is 10~20min.
It is preferred that, in the step (2), refrigerated storage temperature is 3~5 DEG C, and cold preservation time is 2~3h.
It is preferred that, in the step (2), the rotating speed of centrifugation is 1000~1200r/min, disengaging time is 10~
15min。
Compared with prior art, beneficial effects of the present invention are as follows：
Rose berry extract, Tea Polyphenols are mixed with other components in formula, can effectively prevent spray in atmosphere by
Quickly oxidation, extends scent duration；On the one hand attar of rose can distribute Rose Essentielle, and on the other hand Flos Rosae Rugosas pollen is carried out
Absorption prevents the quick diffusion of fragrance, reaches effect of lasting delicate fragrance；Bordeaux mixture, alkylnaphthalene sulfonate are added in formula to spray
Mist agent viscosity is controlled, and improves spray stability, while the cleaning health on artificial flowers surface can be kept, prevents bacterium from growing
It is raw；The spray preparation method that the present invention is provided, attar of rose, rose berry extract extraction efficiency are high, and the impurity contained is few, does not break
Bad active ingredient, uniformity is good, and obtained spray, which is sprinkled upon on emulation roseleaf, can keep lasting delicate fragrance, will not be right
Surrounding environment is polluted.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Embodiment is closed, the present invention is expanded on further.
Embodiment 1
One kind emulation rose spray, is composed of the following raw materials by weight：
2 parts of acrylic acid, 8 parts of ethanol, 3 parts of Bordeaux mixture, 5 parts of Flos Rosae Rugosas pollen, 0.5 part of alkylnaphthalene sulfonate, styrax 0.2
Part, 1 part of Vanillin, 2 parts of rose berry extract, 0.1 part of Tea Polyphenols, 0.5 part of attar of rose.
The Bordeaux mixture is formulated by 3 grams of copper sulphate, 2.5 grams of white lime and 0.5 kilogram of water.
The alkylnaphthalene sulfonate is Negel.
One kind emulation rose spray preparation method, including following steps：
(1) attar of rose is prepared
The rose 100g of natural drying is taken, it is finely ground, it is placed in 1000ml round-bottomed flasks, 700ml distilled water is added, 2
Pressed at~5 DEG C after cold soaking 2h after steam distillation heating extraction, backflow 4h, separate attar of rose, add a small amount of anhydrous sodium sulfate
Dry, produce attar of rose；
(2) rose berry extract is prepared
Fructus rosae is smashed to pieces and is put into pressure pan, ethanol is added, amount of alcohol added is 2~3 times of fructus rosae weight, and pressurization is simultaneously
Keep pressure for a period of time, moulding pressure is 250~300Mpa, pressure hold time is 10~20min, then pressure release and is carried out
Filtering, filtrate is placed in refrigerating chamber and refrigerated, and refrigerated storage temperature is 3~5 DEG C, and cold preservation time is 2~3h, refrigerates the filter after terminating
Liquid is centrifuged, and the rotating speed of centrifugation is 1000~1200r/min, and disengaging time is 10~15min, collects supernatant
Liquid, is made rose berry extract；
(3) spray is prepared
Acrylic acid, ethanol, Bordeaux mixture, Flos Rosae Rugosas pollen, alkylnaphthalene sulfonate, styrax, vanilla are weighed by formula ratio
Element, rose berry extract, Tea Polyphenols and attar of rose, warm water dissolve and stirred to being completely dissolved, and then carry out ultrasonically treated, cooling
To room temperature, the spray is made.
Embodiment 2
One kind emulation rose spray, is composed of the following raw materials by weight：
2.5 parts of acrylic acid, 10 parts of ethanol, 0.4 part of Bordeaux mixture, 7.5 parts of Flos Rosae Rugosas pollen, 0.6 part of alkylnaphthalene sulfonate, peace
Breath is fragrant 0.4 part, 1.5 parts of Vanillin, 0.3 part of rose berry extract, 0.2 part of Tea Polyphenols, 0.6 part of attar of rose.
The Bordeaux mixture is formulated by 3 grams of copper sulphate, 2.5 grams of white lime and 0.5 kilogram of water.
The alkylnaphthalene sulfonate is Negel.
One kind emulation rose spray preparation method, including following steps：
(1) attar of rose is prepared
The rose 100g of natural drying is taken, it is finely ground, it is placed in 1000ml round-bottomed flasks, 700ml distilled water is added, 2
Pressed at~5 DEG C after cold soaking 2h after steam distillation heating extraction, backflow 4h, separate attar of rose, add a small amount of anhydrous sodium sulfate
Dry, produce attar of rose；
(2) rose berry extract is prepared
Fructus rosae is smashed to pieces and is put into pressure pan, ethanol is added, amount of alcohol added is 2~3 times of fructus rosae weight, and pressurization is simultaneously
Keep pressure for a period of time, moulding pressure is 250~300Mpa, pressure hold time is 10~20min, then pressure release and is carried out
Filtering, filtrate is placed in refrigerating chamber and refrigerated, and refrigerated storage temperature is 3~5 DEG C, and cold preservation time is 2~3h, refrigerates the filter after terminating
Liquid is centrifuged, and the rotating speed of centrifugation is 1000~1200r/min, and disengaging time is 10~15min, collects supernatant
Liquid, is made rose berry extract；
(3) spray is prepared
Acrylic acid, ethanol, Bordeaux mixture, Flos Rosae Rugosas pollen, alkylnaphthalene sulfonate, styrax, vanilla are weighed by formula ratio
Element, rose berry extract, Tea Polyphenols and attar of rose, warm water dissolve and stirred to being completely dissolved, and then carry out ultrasonically treated, cooling
To room temperature, the spray is made.
Embodiment 3
One kind emulation rose spray, is composed of the following raw materials by weight：
3 parts of acrylic acid, 12 parts of ethanol, 5 parts of Bordeaux mixture, 10 parts of Flos Rosae Rugosas pollen, 0.8 part of alkylnaphthalene sulfonate, styrax
0.6 part, 2 parts of Vanillin, 4 parts of rose berry extract, 0.3 part of Tea Polyphenols, 0.7 part of attar of rose.
The Bordeaux mixture is formulated by 3 grams of copper sulphate, 2.5 grams of white lime and 0.5 kilogram of water.
The alkylnaphthalene sulfonate is Negel.
One kind emulation rose spray preparation method, including following steps：
(1) attar of rose is prepared
The rose 100g of natural drying is taken, it is finely ground, it is placed in 1000ml round-bottomed flasks, 700ml distilled water is added, 2
Pressed at~5 DEG C after cold soaking 2h after steam distillation heating extraction, backflow 4h, separate attar of rose, add a small amount of anhydrous sodium sulfate
Dry, produce attar of rose；
(2) rose berry extract is prepared
Fructus rosae is smashed to pieces and is put into pressure pan, ethanol is added, amount of alcohol added is 2~3 times of fructus rosae weight, and pressurization is simultaneously
Keep pressure for a period of time, moulding pressure is 250~300Mpa, pressure hold time is 10~20min, then pressure release and is carried out
Filtering, filtrate is placed in refrigerating chamber and refrigerated, and refrigerated storage temperature is 3~5 DEG C, and cold preservation time is 2~3h, refrigerates the filter after terminating
Liquid is centrifuged, and the rotating speed of centrifugation is 1000~1200r/min, and disengaging time is 10~15min, collects supernatant
Liquid, is made rose berry extract；
(3) spray is prepared
Acrylic acid, ethanol, Bordeaux mixture, Flos Rosae Rugosas pollen, alkylnaphthalene sulfonate, styrax, vanilla are weighed by formula ratio
Element, rose berry extract, Tea Polyphenols and attar of rose, warm water dissolve and stirred to being completely dissolved, and then carry out ultrasonically treated, cooling
To room temperature, the spray is made.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and that described in above-described embodiment and specification is only the present invention
Preference, be not intended to limit the present invention, without departing from the spirit and scope of the present invention, the present invention also have it is various
Changes and improvements, these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by institute
Attached claims and its equivalent thereof.
Claims (10)
1. one kind emulation rose spray, it is characterised in that the spray is composed of the following raw materials by weight：
2~3 parts of acrylic acid, 8~12 parts of ethanol, 3~5 parts of Bordeaux mixture, 5~10 parts of Flos Rosae Rugosas pollen, alkylnaphthalene sulfonate 0.5~
0.8 part, 0.2~0.6 part of styrax, 1~2 part of Vanillin, 2~4 parts of rose berry extract, 0.1~0.3 part of Tea Polyphenols, rose
Rare oily 0.5~0.7 part.
2. rose spray is emulated as claimed in claim 1, it is characterised in that the spray is by following raw material
Composition：
2.5 parts of acrylic acid, 10 parts of ethanol, 0.4 part of Bordeaux mixture, 7.5 parts of Flos Rosae Rugosas pollen, 0.6 part of alkylnaphthalene sulfonate, styrax
0.4 part, 1.5 parts of Vanillin, 0.3 part of rose berry extract, 0.2 part of Tea Polyphenols, 0.6 part of attar of rose.
3. emulation rose spray as claimed in claim 1 or 2, it is characterised in that the Bordeaux mixture is by 3 grams of sulfuric acid
Copper, 2.5 grams of white lime and 0.5 kilogram of water are formulated.
4. rose spray is emulated as claimed in claim 1 or 2, it is characterised in that the alkylnaphthalene sulfonate is alkyl
Sodium naphthalene sulfonate.
5. one kind emulation rose spray preparation method, it is characterised in that including following steps：
(1) attar of rose is prepared
The rose 100g of natural drying is taken, it is finely ground, it is placed in 1000ml round-bottomed flasks, adds after 700ml distilled water, cold soaking 2h
By steam distillation heating extraction, after the 4h that flows back, attar of rose is separated, a small amount of anhydrous sodium sulfate drying is added, produces attar of rose；
(2) rose berry extract is prepared
Fructus rosae is smashed to pieces and is put into pressure pan, ethanol is added, pressurizes and keep pressure for a period of time, then pressure release and was carried out
Filter, filtrate is placed in refrigerating chamber and refrigerated, and the filtrate after refrigeration terminates is centrifuged, and collects supernatant, and rose is made
Berry extract；
(3) spray is prepared
Acrylic acid, ethanol, Bordeaux mixture, Flos Rosae Rugosas pollen, alkylnaphthalene sulfonate, styrax, Vanillin, rose are weighed by formula ratio
Rare berry extract, Tea Polyphenols and attar of rose, warm water dissolve and stirred to being completely dissolved, and then carry out ultrasonically treated, are cooled to room
Temperature, is made the spray.
6. rose spray preparation method is emulated as claimed in claim 5, it is characterised in that in the step (1), cold soaking
When control water temperature at 2~5 DEG C.
7. rose spray preparation method is emulated as claimed in claim 5, it is characterised in that in the step (2), ethanol
Addition is 2~3 times of fructus rosae weight.
8. rose spray preparation method is emulated as claimed in claim 5, it is characterised in that in the step (2), pressurization
Pressure is 250~300Mpa, and pressure hold time is 10~20min.
9. rose spray preparation method is emulated as claimed in claim 5, it is characterised in that in the step (2), refrigeration
Temperature is 3~5 DEG C, and cold preservation time is 2~3h.
10. rose spray preparation method is emulated as claimed in claim 5, it is characterised in that in the step (2), from
The rotating speed of heart separation is 1000~1200r/min, and disengaging time is 10~15min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710530131.4A CN107267286A (en) | 2017-07-03 | 2017-07-03 | Emulate rose spray and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710530131.4A CN107267286A (en) | 2017-07-03 | 2017-07-03 | Emulate rose spray and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107267286A true CN107267286A (en) | 2017-10-20 |
Family
ID=60070732
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710530131.4A Pending CN107267286A (en) | 2017-07-03 | 2017-07-03 | Emulate rose spray and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107267286A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040229770A1 (en) * | 2003-02-13 | 2004-11-18 | Clark David G. | Enhancing the fragrance of an article |
| CN1572163A (en) * | 2003-05-26 | 2005-02-02 | 安昞玉 | Spraying scent and fragrance producing sheets for artificial flowers |
| CN105031701A (en) * | 2015-09-17 | 2015-11-11 | 天峨县平昌生态农业有限公司 | Environmentally-friendly plant source deodorant |
-
2017
- 2017-07-03 CN CN201710530131.4A patent/CN107267286A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040229770A1 (en) * | 2003-02-13 | 2004-11-18 | Clark David G. | Enhancing the fragrance of an article |
| CN1572163A (en) * | 2003-05-26 | 2005-02-02 | 安昞玉 | Spraying scent and fragrance producing sheets for artificial flowers |
| CN105031701A (en) * | 2015-09-17 | 2015-11-11 | 天峨县平昌生态农业有限公司 | Environmentally-friendly plant source deodorant |
Non-Patent Citations (2)
| Title |
|---|
| 利生: "《科学使用农药知识》", 31 May 2011, 西安地图出版社 * |
| 马希汉，等: "玫瑰精油提取工艺研究", 《林产化学与工业》 * |
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Application publication date: 20171020 |