CN107250123B - 用于将纤维素转化为呋喃产物的方法 - Google Patents
用于将纤维素转化为呋喃产物的方法 Download PDFInfo
- Publication number
- CN107250123B CN107250123B CN201580076596.6A CN201580076596A CN107250123B CN 107250123 B CN107250123 B CN 107250123B CN 201580076596 A CN201580076596 A CN 201580076596A CN 107250123 B CN107250123 B CN 107250123B
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- weight
- glucose
- hydroxymethylfurfural
- ionic liquid
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
- C07D307/50—Preparation from natural products
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
- C07D233/56—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms
- C07D233/58—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
- C07H3/02—Monosaccharides
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
- C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
- C12P7/06—Ethanol, i.e. non-beverage
- C12P7/08—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate
- C12P7/10—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate substrate containing cellulosic material
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
- C13K1/04—Purifying
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/007—Separation of sugars provided for in subclass C13K
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P5/00—Preparation of hydrocarbons or halogenated hydrocarbons
- C12P5/02—Preparation of hydrocarbons or halogenated hydrocarbons acyclic
- C12P5/023—Methane
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Emergency Medicine (AREA)
- Wood Science & Technology (AREA)
- Biotechnology (AREA)
- Genetics & Genomics (AREA)
- Zoology (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Molecular Biology (AREA)
- Furan Compounds (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201462091319P | 2014-12-12 | 2014-12-12 | |
| US62/091,319 | 2014-12-12 | ||
| US201462095673P | 2014-12-22 | 2014-12-22 | |
| US62/095,673 | 2014-12-22 | ||
| PCT/US2015/065403 WO2016094878A1 (en) | 2014-12-12 | 2015-12-11 | Methods for converting cellulose to furanic products |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107250123A CN107250123A (zh) | 2017-10-13 |
| CN107250123B true CN107250123B (zh) | 2021-06-15 |
Family
ID=56108296
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201580076596.6A Expired - Fee Related CN107250123B (zh) | 2014-12-12 | 2015-12-11 | 用于将纤维素转化为呋喃产物的方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10532990B2 (enExample) |
| EP (1) | EP3230270A4 (enExample) |
| JP (1) | JP2017537119A (enExample) |
| CN (1) | CN107250123B (enExample) |
| BR (1) | BR112017011978A2 (enExample) |
| CA (1) | CA2968409A1 (enExample) |
| RU (1) | RU2722487C2 (enExample) |
| WO (1) | WO2016094878A1 (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2015171368A1 (en) * | 2014-05-06 | 2015-11-12 | Iowa State University Research Foundation, Inc. | Method for the isomerization of glucose to fructose |
| WO2016094878A1 (en) | 2014-12-12 | 2016-06-16 | Virdia, Inc. | Methods for converting cellulose to furanic products |
| EP3341520A2 (en) * | 2015-08-27 | 2018-07-04 | Teknologian tutkimuskeskus VTT Oy | Process for converting biomass by using deep eutectic solvents |
| ES2652362B1 (es) * | 2016-07-01 | 2018-11-13 | Universidade De Santiago De Compostela | Mezclas de sales para disolver celulosa |
| EP3481939A4 (en) | 2016-07-06 | 2020-02-26 | Virdia, Inc. | METHODS FOR REFINING A LIGNOCELLULOSIC HYDROLYSAT |
| CN108408714A (zh) * | 2018-05-09 | 2018-08-17 | 东莞理工学院 | 一种以胡敏素制备层状结构介孔碳材料的方法 |
| FI129866B (fi) * | 2019-05-15 | 2022-10-14 | Lappeenrannan Lahden Teknillinen Yliopisto Lut | Menetelmä lignoselluloosamateriaalin fraktioimiseksi ja mainitulla menetelmällä saadut tuotteet |
| JP7677951B2 (ja) * | 2020-04-08 | 2025-05-15 | 日揮ホールディングス株式会社 | 糖を回収する方法 |
| CN113070103A (zh) * | 2021-04-26 | 2021-07-06 | 上海邢东化工科技有限公司 | 一种弱酸阳离子交换树脂的提纯工艺及提纯设备 |
| WO2023166122A1 (en) * | 2022-03-04 | 2023-09-07 | Avantium Knowledge Centre B.V. | Method of extracting 5-chloromethylfurfural with an organic solvent from cellulosic fibers and man-made non-cellulosic fibers hydrolysed together with hydrochloric acid |
| CN115160267B (zh) * | 2022-08-04 | 2024-01-16 | 安阳工学院 | 一种离子液体型复合介质及采用其制备糠醛类化合物的方法 |
| CN116987051B (zh) * | 2023-08-04 | 2025-08-26 | 安徽理工大学 | 一种水解法制备5-羟甲基糠醛的方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101720320A (zh) * | 2007-06-18 | 2010-06-02 | 阿彻丹尼尔斯-米德兰公司 | 使用非功能性聚合树脂提纯羟甲基糠醛的方法 |
| CN102066304A (zh) * | 2008-06-17 | 2011-05-18 | 威斯康星校友研究基金会 | 木素纤维素生物质到燃料和化学品的化学转变方法 |
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| US3684574A (en) | 1970-04-20 | 1972-08-15 | Anheuser Busch | Method of producing sweet syrup by resin isomerization of dextrose syrup |
| US4618579A (en) * | 1984-09-28 | 1986-10-21 | Genencor, Inc. | Raw starch saccharification |
| US4764596A (en) * | 1985-11-05 | 1988-08-16 | Repap Technologies Inc. | Recovery of lignin |
| SU1432121A1 (ru) * | 1986-05-26 | 1988-10-23 | Ioffe Iosif | Способ регенерации варочной жидкости |
| JPH07165781A (ja) * | 1993-12-07 | 1995-06-27 | Asai Gerumaniumu Kenkyusho:Kk | グルコースの異性化方法及び異性化或いはその促進剤 |
| JP2996875B2 (ja) * | 1994-07-04 | 2000-01-11 | 新日本製鐵株式会社 | ステーブクーラーの耐火煉瓦鋳ぐるみ方法 |
| US6177575B1 (en) | 1998-06-12 | 2001-01-23 | E. I. Du Pont De Nemours And Company | Process for manufacture of imidazoles |
| RU2165708C2 (ru) * | 1998-07-31 | 2001-04-27 | Валентина Андреевна Васькина | Состав для производства мучного кондитерского изделия |
| US6518440B2 (en) | 2001-03-05 | 2003-02-11 | Gene E. Lightner | Hydroxymethylfurfural derived from cellulose contained in lignocellulose solids |
| US20060081637A1 (en) * | 2004-10-14 | 2006-04-20 | Lundy Michael J | Bucket |
| WO2007111605A1 (en) * | 2006-03-29 | 2007-10-04 | Virginia Tech Intellectual Properties, Inc. | Cellulose-solvent-based lignocellulose fractionation with modest reaction conditions and reagent cycling |
| EP2049458B1 (en) * | 2007-01-26 | 2013-12-25 | Probelte Pharma, S.A. | Process for the production of hydroxytyrosol containing extract from olives and solids containing residues of olive oil extraction |
| US8968811B2 (en) * | 2007-01-26 | 2015-03-03 | Probelte Pharma, S.A. | Hydroxytrosol containing extract obtained from olives and solids containing residues of olive oil extraction |
| EP2118362A4 (en) | 2007-02-07 | 2012-03-21 | Univ Queensland | FRACTIONATION OF A LIGNOCELLULOSIC FABRIC |
| CN101354468B (zh) * | 2007-07-23 | 2010-06-23 | 鸿富锦精密工业(深圳)有限公司 | 变焦装置 |
| US8110667B2 (en) | 2008-04-28 | 2012-02-07 | Battelle Memorial Institute | Method for conversion of carbohydrate polymers to value-added chemical products |
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| EP2448951B1 (en) * | 2009-07-01 | 2016-06-01 | Wisconsin Alumni Research Foundation | Biomass hydrolysis |
| WO2011041455A1 (en) | 2009-09-29 | 2011-04-07 | The Regents Of The University Of California | Recovery of sugars from ionic liquid biomass liquor by solvent extraction |
| US8790542B2 (en) | 2009-09-30 | 2014-07-29 | Sandia Corporation | Compositions and methods useful for ionic liquid treatment of biomass |
| CN102249869A (zh) | 2010-05-18 | 2011-11-23 | 中国科学院兰州化学物理研究所 | 离子液体催化合成聚甲氧基二甲醚的工艺过程 |
| US9174909B2 (en) * | 2012-02-02 | 2015-11-03 | Wisconsin Alumni Research Foundation | Two-stage, acid-catalyzed conversion of carbohydrates into levulinic acid |
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| WO2013166237A1 (en) | 2012-05-02 | 2013-11-07 | The Regents Of The University Of California | Sugar extraction and ionic liquid recycling using alkaline solutions |
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| WO2016094878A1 (en) | 2014-12-12 | 2016-06-16 | Virdia, Inc. | Methods for converting cellulose to furanic products |
-
2015
- 2015-12-11 WO PCT/US2015/065403 patent/WO2016094878A1/en not_active Ceased
- 2015-12-11 US US15/527,597 patent/US10532990B2/en not_active Expired - Fee Related
- 2015-12-11 BR BR112017011978A patent/BR112017011978A2/pt not_active Application Discontinuation
- 2015-12-11 CA CA2968409A patent/CA2968409A1/en active Pending
- 2015-12-11 EP EP15867656.9A patent/EP3230270A4/en not_active Withdrawn
- 2015-12-11 JP JP2017530586A patent/JP2017537119A/ja active Pending
- 2015-12-11 RU RU2017124242A patent/RU2722487C2/ru active
- 2015-12-11 CN CN201580076596.6A patent/CN107250123B/zh not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101720320A (zh) * | 2007-06-18 | 2010-06-02 | 阿彻丹尼尔斯-米德兰公司 | 使用非功能性聚合树脂提纯羟甲基糠醛的方法 |
| CN102066304A (zh) * | 2008-06-17 | 2011-05-18 | 威斯康星校友研究基金会 | 木素纤维素生物质到燃料和化学品的化学转变方法 |
Non-Patent Citations (5)
| Title |
|---|
| Catalytic conversion of cellulose into 5-hydroxymethylfurfural in high yields via a two-step process;Xinhua Qi等;《Cellulose》;20110619;第18卷;参见第1328页图1,第1329页第1栏第13-16行 * |
| Xinhua Qi等.Catalytic conversion of cellulose into 5-hydroxymethylfurfural in high yields via a two-step process.《Cellulose》.2011,第18卷参见第1328页图1,第1329页第1栏第13-16行. * |
| Yuriy Roma'n-Leshkov等.Solvent Effects on Fructose Dehydrationto 5-Hydroxymethylfurfural in Biphasic Systems Saturated with Inorganic Salts.《Top Catal》.2009,第52卷参见第298页图1,第300页表1. * |
| 木质素的制备;张晓阳等;《纤维素生物质水解与应用》;郑州:郑州大学出版社;20121231;参见第224页 * |
| 果葡糖浆的生产;赵萍;《粮油食品工艺》;兰州:甘肃科学技术出版社;20041130;参见第156页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2016094878A8 (en) | 2016-07-21 |
| US20170362194A1 (en) | 2017-12-21 |
| RU2017124242A (ru) | 2019-01-14 |
| US10532990B2 (en) | 2020-01-14 |
| EP3230270A1 (en) | 2017-10-18 |
| WO2016094878A1 (en) | 2016-06-16 |
| CA2968409A1 (en) | 2016-06-16 |
| RU2722487C2 (ru) | 2020-06-01 |
| EP3230270A4 (en) | 2018-07-04 |
| RU2017124242A3 (enExample) | 2019-12-05 |
| BR112017011978A2 (pt) | 2017-12-26 |
| CN107250123A (zh) | 2017-10-13 |
| JP2017537119A (ja) | 2017-12-14 |
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Address after: Virginia Applicant after: Verdia Ltd. Address before: louisiana Applicant before: VIRDIA, Inc. |
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| CF01 | Termination of patent right due to non-payment of annual fee |
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