CN107227076A - A kind of decoration emulsion paint and preparation method - Google Patents
A kind of decoration emulsion paint and preparation method Download PDFInfo
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- CN107227076A CN107227076A CN201710609859.6A CN201710609859A CN107227076A CN 107227076 A CN107227076 A CN 107227076A CN 201710609859 A CN201710609859 A CN 201710609859A CN 107227076 A CN107227076 A CN 107227076A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/02—Emulsion paints including aerosols
- C09D5/024—Emulsion paints including aerosols characterised by the additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/02—Emulsion paints including aerosols
- C09D5/024—Emulsion paints including aerosols characterised by the additives
- C09D5/025—Preservatives, e.g. antimicrobial agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention provides a kind of decoration emulsion paint and preparation method, the emulsion paint includes following component：Styrene-acrylic emulsion, polyvinyl alcohol, hydroxyethyl cellulose, butanol, antibacterial mildew inhibitor, titanium dioxide, paste attapulgite clay, filler, defoamer, in addition to appropriate water.Preparation method includes：Antibacterial mildew inhibitor is extracted first, extract powder is obtained, it is standby；Then remaining ingredient is well mixed in batches, then adds antibacterial mildew inhibitor extract, be well mixed, you can.Emulsion paint of the present invention is applied to inner wall decoration, not only with preferable waterproof, Corrosion Protection, also with certain anti-soil, the easily performance such as scouring, good permeability, with preferable application prospect.
Description
Technical field
The present invention relates to building material technical field, in particular it relates to a kind of decoration emulsion paint and preparation method.
Background technology
Emulsion paint is built as environment-friendly type coating and repairs profession is approved more and more, emulsion paint using water as
Diluent, is a kind of easy construction, safe, water-fastness, good permeability paint kind of site operation, and it can be mixed according to different schemes of colour
Different color and lusters.And apply the decorative effect in the emulsion paint of interior wall, film feel, flatness and color, texture etc. can be by
People more pay close attention to, and interior wall coating can produce large effect to indoor environment, should have appropriate gas permeability and moisture absorption
Property, complete airtight, nonhygroscopic film can cause the condensation of metope, be unfavorable for improvement and the comfortable for living of indoor environment
Improve.Poisonous and harmful substances can not be contained in interiro wall latex paint, otherwise environment and health can be caused harm；Interiro wall latex paint
Must have preferable water resistance, alkali resistance and scrub resistance.
The content of the invention
For defect of the prior art, it is an object of the invention to provide a kind of decoration emulsion paint and preparation method, institute
Emulsion paint is stated applied to inner wall decoration, not only with preferable waterproof, Corrosion Protection, also cleaned with certain anti-soil, easily,
The performances such as good permeability, with preferable application prospect.
The present invention solves technical problem and adopted the following technical scheme that：
The present invention relates to a kind of decoration emulsion paint, include each component of following parts by weight：17 ~ 23 parts of styrene-acrylic emulsion, polyethylene
9 ~ 16 parts of alcohol, 2.2 ~ 5 parts of hydroxyethyl cellulose, 5 ~ 9 parts of butanol, 3 ~ 8 parts of antibacterial mildew inhibitor, 8 ~ 17 parts of titanium dioxide, paste are concavo-convex
10 ~ 16 parts of rod stone clay, 7 ~ 13 parts of filler, 2.5 ~ 6 parts of defoamer, in addition to appropriate water.
Preferably, 21 parts of the styrene-acrylic emulsion, 13 parts of polyvinyl alcohol, 3.6 parts of hydroxyethyl cellulose, 6 parts of butanol, antibacterial are prevented
Mould dose 5 parts, 12 parts of titanium dioxide, 14 parts of paste attapulgite clay, 10 parts of filler, 5.2 parts of defoamer, in addition to appropriate water.
Preferably, the antibacterial mildew inhibitor includes each component of following parts by weight：
9 ~ 15 parts of peppermint, 10 ~ 18 parts of folium artemisiae argyi, 5 ~ 11 parts of sweet wormwood, 3 ~ 7 parts of capsicum, 3 ~ 5 parts of fennel, 9 ~ 16 parts of cloves, honeysuckle 8 ~
12 parts, 3 ~ 7 parts of calamus.
Preferably, the paste attapulgite clay is that natural attapulgite clay is purified, add water after thermal activation acquisition
Mixture, wherein water content be 30% ~ 50%.
Preferably, the filler is any of superfine talcum powder, superfine light calcium carbonate, ultrafine mica powder.
The invention further relates to a kind of method for preparing decoration emulsion paint, comprise the following steps：
（1）Weigh each component of antibacterial mildew inhibitor respectively according to proportioning, crush and cross 150 mesh sieves, be then well mixed, will mix
Component is placed in apparatus,Soxhlet's, in the mixed solvent 3 ~ 5h of refluxing extraction of ethanol and water, obtains extract solution, then will be extracted
Liquid is concentrated, and is removed solvent, is obtained antibacterial mildew inhibitor extract powder, standby；
（2）Styrene-acrylic emulsion, polyvinyl alcohol, hydroxyethyl cellulose, butanol are weighed according to proportioning to be added in mixer, are sufficiently stirred for
After uniform, add water, then add the paste attapulgite clay and defoamer of proportional quantity, be well mixed, then put mixture
Scattered 30 ~ 40min is sheared in cutter, mixture a1 is obtained；
（3）Mixture a1 is transferred in mixer, the titanium dioxide and filler of proportional quantity is added, 20 ~ 30min is stirred, adds
Step（1）In obtained antibacterial mildew inhibitor extract powder, stir, then mixture be placed under Ultrasonic Conditions ultrasonic
Scattered 20 ~ 30min, produces the emulsion paint.
Preferably, the step（1）The volume of the mixed liquor of middle ethanol and water is the 15 ~ 20 of component of mixture gross mass
Times, wherein the volume ratio of ethanol and water is 1:1~2.
Preferably, the step（2）In the quality that adds water be 5 ~ 10 times of styrene-acrylic emulsion quality.
Preferably, the step（2）The shear rate of middle cutter is 1000 ~ 2000 turns/min.
Preferably, the step（2）The preparation method of middle paste attapulgite clay is：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add water, stirring forms mud in suspension, takes upper suspension
5 ~ 10min of centrifugal treating in 3000 ~ 4000 turns/min centrifuge, vacuum filtration；Filter cake is dried, Muffle furnace is subsequently placed in
In be warming up to 800 DEG C ~ 900 DEG C with 20 DEG C/min speed program, then 3 ~ 4h of constant temperature calcining, adds water after cooling, is placed in ultrasound
It is mixed evenly under the conditions of ripple, you can.
Compared with prior art, the present invention has following beneficial effect：
（1）Decoration emulsion paint of the present invention, applied to inner wall decoration, not only with preferable waterproof, Corrosion Protection,
The characteristics of also there is certain anti-soil, easily clean, in addition, also there is the emulsion paint preferable good permeability to resist with certain
Bacterium anti-mold effect, can effectively prevent indoor mould, the generation of bacterium, and the ring of a safety is provided for the daily life of people
Border, with preferable application prospect.
（2）Antibacterial mildew inhibitor is added with decoration emulsion paint of the present invention, emulsion paint and wall can not only be prevented
Face mould, the growth of bacterium, and the antibacterial mildew inhibitor are pure natural Chinese herbal medicine composition, and safety non-pollution will not be made to human body
Into injury, with preferable environment protecting and safety in utilization.
（3）Added with cream-like attapulgite soil in decoration emulsion paint of the present invention, because attapulgite has preferably
Suspension, levelability and thickening property, and hence it is also possible to instead of original suspending agent, thickener and stabilizer, greatly reduce
Consumption of raw materials and cost of material, meanwhile, the coating uniformity of emulsion paint is improved, moreover it is possible to effectively improve emulsion paint each group
/ and the adhesive property between emulsion paint and building, improve being firmly bonded property.
（4）Decoration of the present invention is simple and convenient to operate with the preparation method of emulsion paint, and process conditions are gentle, is adapted to
Industrialization promotion is produced.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1：
The present embodiment is related to a kind of decoration emulsion paint and preparation method；
The emulsion paint is prepared from by following component：
21 parts of styrene-acrylic emulsion, 13 parts of polyvinyl alcohol, 3.6 parts of hydroxyethyl cellulose, 6 parts of butanol, 5 parts of antibacterial mildew inhibitor, titanium dioxide
12 parts, 14 parts of paste attapulgite clay, 10 parts of filler, 5.2 parts of defoamer, in addition to appropriate water.
Wherein, the antibacterial mildew inhibitor includes each component of following parts by weight：
11 parts of peppermint, 15 parts of folium artemisiae argyi, 9 parts of sweet wormwood, 4 parts of capsicum, 3 parts of fennel, 12 parts of cloves, 10 parts of honeysuckle, 6 parts of calamus.
The paste attapulgite clay is that natural attapulgite clay is purified, the mixing for the acquisition that adds water after thermal activation
Thing, wherein water content are 40%.
The filler is superfine talcum powder.
The method that the present invention prepares decoration emulsion paint, comprises the following steps：
（1）Weigh each component of antibacterial mildew inhibitor respectively according to proportioning, crush and cross 150 mesh sieves, be then well mixed, will mix
Component is placed in apparatus,Soxhlet's, in the in the mixed solvent refluxing extraction 4h of ethanol and water, extract solution is obtained, then by extract solution
Concentration, removes solvent, obtains antibacterial mildew inhibitor extract powder, standby；
（2）Styrene-acrylic emulsion, polyvinyl alcohol, hydroxyethyl cellulose, butanol are weighed according to proportioning to be added in mixer, are sufficiently stirred for
After uniform, add water, then add the paste attapulgite clay and defoamer of proportional quantity, be well mixed, then put mixture
Scattered 30min is sheared in cutter, mixture a1 is obtained；
（3）Mixture a1 is transferred in mixer, the titanium dioxide and filler of proportional quantity is added, 30min is stirred, adds step
（1）In obtained antibacterial mildew inhibitor extract powder, stir, mixture be then placed in ultrasonic disperse under Ultrasonic Conditions
30min, produces the emulsion paint.
Step（1）The volume of the mixed liquor of middle ethanol and water is 18 times of component of mixture gross mass, wherein ethanol with
The volume ratio of water is 1:1.2.
Step（2）In the quality that adds water be 8 times of styrene-acrylic emulsion quality.
Step（2）The shear rate of middle cutter is 2000 turns/min.
Step（2）The preparation method of middle paste attapulgite clay is：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add water, stirring forms mud in suspension, takes upper suspension
The centrifugal treating 10min in 3000 turns/min centrifuge, vacuum filtration；Filter cake is dried, is subsequently placed in Muffle furnace with 20
DEG C/min speed program is warming up to 900 DEG C, then constant temperature calcining 4h, adds water after cooling, is placed in mixing under Ultrasonic Conditions and stirs
Mix uniform, you can.
Embodiment 2：
The present embodiment is related to a kind of decoration emulsion paint and preparation method；
The emulsion paint is prepared from by following component：
17 parts of styrene-acrylic emulsion, 9 parts of polyvinyl alcohol, 2.2 parts of hydroxyethyl cellulose, 5 parts of butanol, 3 parts of antibacterial mildew inhibitor, titanium dioxide 8
Part, 10 parts of paste attapulgite clay, 7 parts of filler, 2.5 parts of defoamer, in addition to appropriate water.
Wherein, the antibacterial mildew inhibitor includes each component of following parts by weight：
9 parts of peppermint, 10 parts of folium artemisiae argyi, 5 parts of sweet wormwood, 3 parts of capsicum, 3 parts of fennel, 9 parts of cloves, 8 parts of honeysuckle, 3 parts of calamus.
The paste attapulgite clay is that natural attapulgite clay is purified, the mixing for the acquisition that adds water after thermal activation
Thing, wherein water content are 30%.
The filler is ultrafine mica powder.
The method that the present invention prepares decoration emulsion paint, comprises the following steps：
（1）Weigh each component of antibacterial mildew inhibitor respectively according to proportioning, crush and cross 150 mesh sieves, be then well mixed, will mix
Component is placed in apparatus,Soxhlet's, in the in the mixed solvent refluxing extraction 3h of ethanol and water, extract solution is obtained, then by extract solution
Concentration, removes solvent, obtains antibacterial mildew inhibitor extract powder, standby；
（2）Styrene-acrylic emulsion, polyvinyl alcohol, hydroxyethyl cellulose, butanol are weighed according to proportioning to be added in mixer, are sufficiently stirred for
After uniform, add water, then add the paste attapulgite clay and defoamer of proportional quantity, be well mixed, then put mixture
Scattered 30min is sheared in cutter, mixture a1 is obtained；
（3）Mixture a1 is transferred in mixer, the titanium dioxide and filler of proportional quantity is added, 20min is stirred, adds step
（1）In obtained antibacterial mildew inhibitor extract powder, stir, mixture be then placed in ultrasonic disperse under Ultrasonic Conditions
20min, produces the emulsion paint.
Step（1）The volume of the mixed liquor of middle ethanol and water is 15 times of component of mixture gross mass, wherein ethanol with
The volume ratio of water is 1:1.
Step（2）In the quality that adds water be 5 times of styrene-acrylic emulsion quality.
Step（2）The shear rate of middle cutter is 1000 turns/min.
Step（2）The preparation method of middle paste attapulgite clay is：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add water, stirring forms mud in suspension, takes upper suspension
The centrifugal treating 10min in 3000 turns/min centrifuge, vacuum filtration；Filter cake is dried, is subsequently placed in Muffle furnace with 20
DEG C/min speed program is warming up to 800 DEG C, then constant temperature calcining 4h, adds water after cooling, is placed in mixing under Ultrasonic Conditions and stirs
Mix uniform, you can.
Embodiment 3：
The present embodiment is related to a kind of decoration emulsion paint and preparation method；
The emulsion paint is prepared from by following component：
23 parts of styrene-acrylic emulsion, 16 parts of polyvinyl alcohol, 5 parts of hydroxyethyl cellulose, 9 parts of butanol, 8 parts of antibacterial mildew inhibitor, titanium dioxide 17
Part, 16 parts of paste attapulgite clay, 13 parts of filler, 6 parts of defoamer, in addition to appropriate water.
Wherein, the antibacterial mildew inhibitor includes each component of following parts by weight：
15 parts of peppermint, 18 parts of folium artemisiae argyi, 11 parts of sweet wormwood, 7 parts of capsicum, 5 parts of fennel, 16 parts of cloves, 12 parts of honeysuckle, 7 parts of calamus.
The paste attapulgite clay is that natural attapulgite clay is purified, the mixing for the acquisition that adds water after thermal activation
Thing, wherein water content are 50%.
The filler is superfine light calcium carbonate.
The method that the present invention prepares decoration emulsion paint, comprises the following steps：
（1）Weigh each component of antibacterial mildew inhibitor respectively according to proportioning, crush and cross 150 mesh sieves, be then well mixed, will mix
Component is placed in apparatus,Soxhlet's, in the in the mixed solvent refluxing extraction 5h of ethanol and water, extract solution is obtained, then by extract solution
Concentration, removes solvent, obtains antibacterial mildew inhibitor extract powder, standby；
（2）Styrene-acrylic emulsion, polyvinyl alcohol, hydroxyethyl cellulose, butanol are weighed according to proportioning to be added in mixer, are sufficiently stirred for
After uniform, add water, then add the paste attapulgite clay and defoamer of proportional quantity, be well mixed, then put mixture
Scattered 40min is sheared in cutter, mixture a1 is obtained；
（3）Mixture a1 is transferred in mixer, the titanium dioxide and filler of proportional quantity is added, 30min is stirred, adds step
（1）In obtained antibacterial mildew inhibitor extract powder, stir, mixture be then placed in ultrasonic disperse under Ultrasonic Conditions
30min, produces the emulsion paint.
Step（1）The volume of the mixed liquor of middle ethanol and water is 20 times of component of mixture gross mass, wherein ethanol with
The volume ratio of water is 1: 2.
Step（2）In the quality that adds water be 10 times of styrene-acrylic emulsion quality.
Step（2）The shear rate of middle cutter is 2000 turns/min.
Step（2）The preparation method of middle paste attapulgite clay is：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add water, stirring forms mud in suspension, takes upper suspension
The centrifugal treating 5min in 4000 turns/min centrifuge, vacuum filtration；Filter cake is dried, is subsequently placed in Muffle furnace with 20
DEG C/min speed program is warming up to 900 DEG C, then constant temperature calcining 3h, adds water after cooling, is placed in mixing under Ultrasonic Conditions and stirs
Mix uniform, you can.
In summary, decoration emulsion paint of the present invention, applied to inner wall decoration, not only with preferable waterproof,
Corrosion Protection, also with certain anti-soil, easily clean the characteristics of, in addition, the emulsion paint also have preferable good permeability
Property and certain antibacterial and mouldproof effect, can effectively prevent indoor mould, the generation of bacterium, one is provided for the daily life of people
Individual safe environment, with preferable application prospect.In addition, the preparation method of described decoration emulsion paint is simple, operation side
Just, process conditions are gentle, are adapted to industrialization promotion production.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (10)
1. a kind of decoration emulsion paint, it is characterised in that include each component of following parts by weight：17 ~ 23 parts of styrene-acrylic emulsion, poly- second
9 ~ 16 parts of enol, 2.2 ~ 5 parts of hydroxyethyl cellulose, 5 ~ 9 parts of butanol, 3 ~ 8 parts of antibacterial mildew inhibitor, 8 ~ 17 parts of titanium dioxide, paste are recessed
Convex 10 ~ 16 parts of rod stone clay, 7 ~ 13 parts of filler, 2.5 ~ 6 parts of defoamer, in addition to appropriate water.
2. decoration emulsion paint according to claim 1, it is characterised in that 21 parts of the styrene-acrylic emulsion, polyvinyl alcohol 13
Part, 3.6 parts of hydroxyethyl cellulose, 6 parts of butanol, 5 parts of antibacterial mildew inhibitor, 12 parts of titanium dioxide, 14 parts of paste attapulgite clay, fill out
Expect 10 parts, 5.2 parts of defoamer, in addition to appropriate water.
3. decoration emulsion paint according to claim 1, it is characterised in that the antibacterial mildew inhibitor includes following parts by weight
Each component：
9 ~ 15 parts of peppermint, 10 ~ 18 parts of folium artemisiae argyi, 5 ~ 11 parts of sweet wormwood, 3 ~ 7 parts of capsicum, 3 ~ 5 parts of fennel, 9 ~ 16 parts of cloves, honeysuckle 8 ~
12 parts, 3 ~ 7 parts of calamus.
4. decoration emulsion paint according to claim 1, it is characterised in that the paste attapulgite clay is natural recessed
Convex rod stone clay is purified, the mixture for the acquisition that adds water after thermal activation, and wherein water content is 30% ~ 50%.
5. decoration emulsion paint according to claim 1, it is characterised in that the filler is superfine talcum powder, ultra-fine light
Any of matter calcium carbonate, ultrafine mica powder.
6. the method that one kind prepares the decoration emulsion paint as described in any one of claim 1 ~ 5, it is characterised in that including as follows
Step：
（1）Weigh each component of antibacterial mildew inhibitor respectively according to proportioning, crush and cross 150 mesh sieves, be then well mixed, will mix
Component is placed in apparatus,Soxhlet's, in the mixed solvent 3 ~ 5h of refluxing extraction of ethanol and water, obtains extract solution, then will be extracted
Liquid is concentrated, and is removed solvent, is obtained antibacterial mildew inhibitor extract powder, standby；
（2）Styrene-acrylic emulsion, polyvinyl alcohol, hydroxyethyl cellulose, butanol are weighed according to proportioning to be added in mixer, are sufficiently stirred for
After uniform, add water, then add the paste attapulgite clay and defoamer of proportional quantity, be well mixed, then put mixture
Scattered 30 ~ 40min is sheared in cutter, mixture a1 is obtained；
（3）Mixture a1 is transferred in mixer, the titanium dioxide and filler of proportional quantity is added, 20 ~ 30min is stirred, adds
Step（1）In obtained antibacterial mildew inhibitor extract powder, stir, then mixture be placed under Ultrasonic Conditions ultrasonic
Scattered 20 ~ 30min, produces the emulsion paint.
7. the preparation method of decoration emulsion paint according to claim 6, it is characterised in that the step（1）Middle ethanol
Volume with the mixed liquor of water is 15 ~ 20 times of component of mixture gross mass, and the wherein volume ratio of ethanol and water is 1:1~2.
8. the preparation method of decoration emulsion paint according to claim 6, it is characterised in that the step（2）In add water
Quality be 5 ~ 10 times of styrene-acrylic emulsion quality.
9. the preparation method of decoration emulsion paint according to claim 6, it is characterised in that the step（2）Middle shearing
The shear rate of machine is 1000 ~ 2000 turns/min.
10. the preparation method of decoration emulsion paint according to claim 6, it is characterised in that the step（2）Middle paste
The preparation method of Concave-convex clay rod is：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add water, stirring forms mud in suspension, takes upper suspension
5 ~ 10min of centrifugal treating in 3000 ~ 4000 turns/min centrifuge, vacuum filtration；Filter cake is dried, Muffle furnace is subsequently placed in
In be warming up to 800 DEG C ~ 900 DEG C with 20 DEG C/min speed program, then 3 ~ 4h of constant temperature calcining, adds water after cooling, is placed in ultrasound
It is mixed evenly under the conditions of ripple, you can.
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| CN201710609859.6A CN107227076A (en) | 2017-07-25 | 2017-07-25 | A kind of decoration emulsion paint and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710609859.6A CN107227076A (en) | 2017-07-25 | 2017-07-25 | A kind of decoration emulsion paint and preparation method |
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| CN107227076A true CN107227076A (en) | 2017-10-03 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111534159A (en) * | 2020-04-17 | 2020-08-14 | 郑州市创意装饰设计有限公司 | Anticorrosive material for sculpture and preparation method thereof |
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| CN102391731A (en) * | 2011-10-24 | 2012-03-28 | 沈阳建筑大学 | Preparation method of rare earth anti-bacteria tilelike coating |
-
2017
- 2017-07-25 CN CN201710609859.6A patent/CN107227076A/en not_active Withdrawn
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1083084A (en) * | 1993-05-31 | 1994-03-02 | 大连市风彩涂料厂 | Waterproof paint |
| CN1456610A (en) * | 2003-02-18 | 2003-11-19 | 杨光忠 | Environmental protective latex paint |
| CN101153152A (en) * | 2006-09-25 | 2008-04-02 | 中宏（天津）实业有限公司 | Method of producing environment protection type heat insulating waterproof coating material for building |
| CN102391731A (en) * | 2011-10-24 | 2012-03-28 | 沈阳建筑大学 | Preparation method of rare earth anti-bacteria tilelike coating |
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| CN111534159A (en) * | 2020-04-17 | 2020-08-14 | 郑州市创意装饰设计有限公司 | Anticorrosive material for sculpture and preparation method thereof |
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