CN107213077A - A kind of preparation method of Chinese herbal medicine ferment shampoo - Google Patents
A kind of preparation method of Chinese herbal medicine ferment shampoo Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The present invention relates to a kind of preparation method of Chinese herbal medicine ferment shampoo, this Chinese herbal medicine ferment shampoo is made up of extracts of Chinese herbal medicine, surfactant, NMF, nourishing agent, thickener, pearling agent, essence and water.The present invention has black hair, effect of relieving itching and removing dandruff.
Description
Technical field
The present invention relates to a kind of preparation method of Chinese herbal medicine ferment shampoo.
Background technology
Head the reason for the increasing with dandruff that itch has a lot, and common is two kinds, and one kind is that fungal infection causes head to be itched to lose hair：Have
Dandruff is also many simultaneously for a little people's scalp pruritus, here it is hair receives fungal infection.Another is that water shortage causes head to be itched to turn around
Hair：Scalp water shortage, which can cause, itches, dry and astringent, or even has pain, and the scalp of long-term water shortage can allow the environment of natural on-off cycles of hair growth to become
It is very poor, easily cause alopecia head itch with white hair grow etc. hair problem.
The many shampoos of in the market are blent using chemokine class and formed, and effect is fine in the short time, but are used for a long time
The hair sex chromosome mosaicism, troublesome such as easily cause hair withered, alopecia, dandruff excessive.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of preparation method of Chinese herbal medicine ferment shampoo, with foster
Effect of hair hair care, relieving itching and removing dandruff and black hair.
In order to solve the above-mentioned technical problem, the present invention uses following technical scheme：
A kind of preparation method of Chinese herbal medicine ferment shampoo, it is characterised in that it is lived by extracts of Chinese herbal medicine containing enzyme, surface
Property agent, NMF, nourishing agent, thickener, pearling agent, essence, bactericide and water are according to mass ratio 5~89:2~89:0~30:0
~50:0.5~15:0~30:0~5:0~5:0~70 composition；
The surfactant includes polyglyceryl fatty acid ester, lauric monoglyceride, methyl glycol fatty acid ester, sorbierite
Acid anhydride monopalmitate, stearoyl lactate, diacetyl tartarate monoglyceride, Cocoamidopropyl betaine, polyoxyethylene nonyl phenyl
Vinethene, polyoxyethylene oleic acid ester, polyoxyethylene stearic acid ester, sorbitan fatty acid ester, two polyglycereol, cetyl three
Methyl quaternary ammonium ammonium bromide, octadecyl dimethyl benzyl quaternary ammonium ammonium chloride, benzyltriethylammoinium chloride, diisooctyl succinate
One or any ratio in sodium sulfonate and aliphatic acid polyethenoxy fat it is two or more；
The NMF is glycerine, fructose, propane diols, sorbierite, polyglutamic acid, niacinamide, polyethylene glycol and xylose
One or any ratio in alcohol it is two or more；
The nourishing agent include honey, sodium salicylate, superoxide dismutase, Alphalin, beta glucan, vitamin e, rely
One or any ratio in propylhomoserin sodium and vitamin E it is two or more；
The thickener include sodium chloride, sodium carboxymethylcellulose, gelatin, sodium alginate and casein in one kind or
Arbitrary proportion it is two or more；
The pearling agent includes one kind in pearl powder, stearic acid diethylene glycol dilaurate, ethylene glycol double stearic acid and mica powder
Or arbitrary proportion is two or more；
The bactericide is included in methylisothiazolinone, methylchloroisothiazandnone, sodium benzoate and potassium sorbate
One or any ratio it is two or more；
The extracts of Chinese herbal medicine containing enzyme, is followed the steps below：
1) product A is prepared：Chinese herbal medicine is added in juice extractor and squeezed the juice, gained juice is product A, residue is residue a；
2) product B is prepared：Residue a is added in stirred tank, and adds solvent, the mass ratio of residue a and solvent is 1:2
~40, it is 60 DEG C~100 DEG C in temperature, pressure adjusts pH value extremely under the conditions of 0~5MPa, stirring decocts 20min~120min
5.5~8.5, filtering, gained filtrate is product B, and residue is residue b；
3) products C is prepared：Residue b, water and enzyme are added in stirred tank, residue b, water and enzyme mass ratio are 10:20
~200:0.1~2, at 25 DEG C~60 DEG C, 24h~120h is extracted, is filtered, gained filtrate is products C；
4) extracts of Chinese herbal medicine containing enzyme is prepared：By product A, product B, products C and natural gum according to mass ratio 0~98:1~
98:1~98:0~60 mixes, and produces extracts of Chinese herbal medicine；
The Chinese herbal medicine be weigh 1~7 part of orange peel according to parts by weight, it is 1~5 part of banana skin, 1~5 part of pine and cypress, black
1~6 part of 1~5 part of beans, 1~5 part of aloe and dandelion；
During the solvent is ethanol, water, ethyl acetate, ether, acetic acid, sodium acetate, phosphoric acid, potassium dihydrogen phosphate and hydrochloric acid
It is a kind of or arbitrary proportion two or more；
The enzyme be cellulase, phytase, sea snail enzymes I, sea snail enzymes II, sea snail enzymes III, sea urchin enzyme, sea hare enzyme, Bao enzyme,
One kind or arbitrary proportion in glusulase, beta galactosidase, beta-glucosidase, chitinase, agarase and alginase
It is two or more；
The natural gum be guar gum, Arabic gum, peach gum, agar-agar, algin, polyacrylamide, Sodium Polyacrylate and
One kind or arbitrary proportion in sodium carboxymethylcellulose it is two or more.
Step 1) described weigh 2 parts of orange peel, 2 parts of banana skin, 1 part of pine and cypress, 3 parts of black soya bean, aloe 2 according to parts by weight
2 parts of part and dandelion.
Step 2) solvent be 0.2mol/L aqueous acetic acid and 0.2mol/L sodium acetate aqueous solution according to volume
Than 14.8:35.2, pH be 5.0 cushioning liquid.
Step 3) described in enzyme be cellulase and phytase according to mass ratio 1:2 composition.
Step 4) described in natural gum be peach gum.
The surfactant is polyglyceryl fatty acid ester, lauric monoglyceride and cetyl trimethyl quaternary ammonium bromination
Ammonium is according to mass ratio 3:2:1 composition；The NMF be glycerine, fructose, propane diols, sorbierite and polyglutamic acid according to
Mass ratio 1:1:2:1:1 composition；The nourishing agent is honey, superoxide dismutase, Alphalin, vitamin e and Wei Sheng
Plain E is according to mass ratio 1:3:2:1:1 composition；The thickener is sodium alginate and sodium chloride according to mass ratio 1:2 group
Compound；The pearling agent is the double stearic acid of ethylene glycol and stearic acid diethylene glycol dilaurate according to mass ratio 1:2 composition；It is described to kill
Microbial inoculum is methylisothiazolinone and potassium sorbate according to mass ratio 1:1 composition；Extracts of Chinese herbal medicine, surfactant,
NMF, nourishing agent, thickener, pearling agent, essence, the mass ratio of bactericide and water are 35:5:8:10:0.5:3:0.5:0.5:
37.5。
Orange peel, also known as dried orange peel.With refreshing oneself, ventilate, regulating qi-flowing for eliminating phlegm, stomach invigorating dehumidify, reduced blood pressure, the work(of toxin-expelling and face nourishing
Effect.Fresh orange peel juice, with very strong permeability, can puncture balloon.
Aloe (scientific name：Aloe vera) Aloe, it is Liliaceae perennial evergreen herbaceous plant, it is leafage life, big and fertile
Thickness, in seat shape or is born in stem top, the normal lanceolar of leaf or the short width of leaf, and there is sharp tooth thorn at edge.With purging intense heat；Removing toxic substances；Stagnation resolvation；Kill
Worm.Argument is red；Constipation；Gonorrhoea；Hematuria；Pediatric epilepsy scared；Infantile malnutrition due to digestive disturbances or intestinalparasites；Burn and scald；Women's amenorrhoea；Hemorrhoid；Scabies；Carbuncle furuncle poison；Fall
Play damage；Bactericidal action, antiinflammatory action moistens beautification function, and the effect of letting out under stomach invigorating, cardiac stimulant promoting blood circulation effect is immunized and regeneration work
With immune and antitumor action, detoxication, anti-aging effects, analgesia, sedation, anti-sunlight function.
Banana skin, rich in tryptophan, vitamin B6, abundant thrombocytin, can produce comfortable, satisfaction, happy, satisfied and pleasure
The mood of sight.Verified by external research, the value of banana and banana skin extraction has surmounted the value of a variety of vegetables and fruits extractions, into
For the optimal leading role in plant extraction.With the effect for suppressing bacterium and fungi growth.
Black soya bean is legume soybean (scientific name：Glycinemax (L.) merr) black seeds.It is black soya bean also known as big shield beans, black
Soybean etc..Black soya bean has high protein, characteristic low in calories, and crust is black, the inside yellow or green.Black soya bean has norcholesterol, benefit
Kidney, beneficial spleen, eliminating the phlegm Zhichuan, beautifying and anti-aging, toxin expelling, effect of fat-reducing and improvement anaemia.
Pine and cypress seed is the fruit of pine tree, also known as korean pine seed.Pine nut is fatty, protein, carbohydrate etc..Pine nut is both
Important Chinese medicine, eats the body-building heart long, and skin care is promoted longevity.Cure mainly joint wind, it is dizzy, go dead flesh, bleach, aproll gas, profit
The five internal organs, by wandering arthritis cold air, empty thin few gas tonifying for the deficiency, fertile the five internal organs dissipate all wind, wet stomach, and long term usage body is light, and macrobiosis is not old.
Dandelion (Classification system：Taraxacum mongolicum Hand.-Mazz.) dandelion, Po Poding, Hua Hua
Youth etc..Composite family, Dandelion herbaceos perennial.Root is coniform, and surface sepia, shrinkage, limb edge has wave-formed mouth sometimes
Or pinniform drastic crack, base portion is gradually narrow into petiole, and the normal band reddish violet of petiole and master pulse, scape top aubergine is close by spider's thread shape white
Long pubescence；Capitulum, involucre mitriform, achene crineous, long pappus white, 4~October of flowering fruit bearing stage.Dandelion Injectable Solution test tube
It is interior to have stronger bactericidal action to staphylococcus aureus resistance bacterial strain, hemolytic streptococcus.To Diplococcus pneumopniae, meningitis ball
Bacterium, corynebacterium diphtheriae, Pseudomonas aeruginosa, shigella dysenteriae, typhoid bacillus etc. and micrococcus catarrhalis also have certain bactericidal action.Dandelion alcohol extracting
Liquid 1：400 can suppress tulase, but decoction 1：100 is invalid.It 1：80 water decoction can delay ECHO11 viral cytopathics, alcohol
Extract (31mg/kg) can kill Leptospira, also have inhibitory action to some fungies.There is good kill to campylobacter pylori
The effect of going out.Folium Taraxacum has the obstruction of dredging newborn vascular, promotes the effect of lactation.Polysaccharide (the Tof mono- extracted in taraxacum
CFr), the C3H mouse of inoculation MM46 tumour cells is awarded with 40,2,600mg/kg ip, early stage administration has no effect, but 11~
The administration of the later stage of 20 days and 2~20 days next day is then effective.Type allergic reaction (DHR of T mono-) is delayed to tumour cell, in ddy mono-
In Ehrlich (same tumor) systems and C3H mono- MM46 (syngeneic tumor) system, its footpad reaction is administered with compareing in the CFr later stages of Tof mono-
Group is compared to substantially rising.In ADMC systems, the CFr of Tof mono- are compared with the glycogen for being known to activated macrophage, with stronger
Activation capability.Foreign study, dandelion has choleretic effect, and clinical treatment chronic gallbladder spasmolytic and calculosis are effective.In addition Pu
Public English still has diuresis stomach invigorating, and hypocatharsis etc. is acted on.
Peach gum, is the resin being secreted in the barks such as rosaceous plant peach or mountain peach, also known as peach oil, peach fat, peach blossom tear,
Peach gum, peach coagulates.With blood QI invigorating, diarrhea is controlled, is relieved pain.
Invention has following advantageous effects：
1st, the present invention uses orange peel for primary raw material, and a large amount of volatile oil are contained in fresh orange peel juice, and it has very
Strong permeability, is conducive to the absorption of the rapid osmotic and hair of nutriment to nutriment.
2nd, aloe and peach gum have very strong repair in the present invention, can repair impaired hair.
3rd, dandelion and banana skin have good bactericidal and bacteriostatic effect in the present invention, can prevent the growth of hair mushroom.
4th, the present invention combines the natural Chinese medicinal herb with different efficacies, is extracted using squeezing, cushioning liquid and enzyme is extracted
Three kinds of extracting modes are combined, and extract will not be damaged.
5th, the present invention is extracted using cushioning liquid, pH narrow fluctuation ranges, and extract is stable；Model is fluctuated using highly basic strong acid pH
Enclose big, extract is unstable, and easily extract is damaged.
6th, the present invention is without chemokine, safety and environmental protection.
Embodiment
The present invention is further illustrated with reference to instantiation.
Embodiment 1
Chinese herbal medicine ferment shampoo is by extracts of Chinese herbal medicine, surfactant, NMF, nourishing agent, thickener, pearly-lustre
Agent, essence, bactericide and water are according to mass ratio 35:5:8:10:0.5:3:0.5:0.5:37.5 compositions.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) product A is prepared：2 parts of orange peel, 2 parts of banana skin, 1 part of pine and cypress, 3 parts of black soya bean, reed are weighed according to parts by weight
2 parts of 2 parts of luxuriant growth and dandelion, which are added in juice extractor, squeezes the juice, and gained juice is product A, and residue is residue a；
2) product B is prepared：Residue a is added in stirred tank, and adds solvent, solvent is that 0.2mol/L acetic acid is water-soluble
Liquid and 0.2mol/L sodium acetate aqueous solution are according to volume ratio 14.8:35.2, pH be 5.0 cushioning liquid.Residue a and solvent
Mass ratio is 1:12, it is 85 DEG C in temperature, pressure adjusts pH value to 6.0~7.5, mistake under the conditions of 1MPa, stirring decocts 40min
Filter, gained filtrate is product B, and residue is residue b；
3) products C is prepared：Residue b, water and enzyme are added in stirred tank, the enzyme be cellulase and phytase according to
Mass ratio 1:2 composition, residue b, water and enzyme mass ratio are 10:120:0.2, at 40 DEG C, 48h is extracted, in 85 DEG C, pressure
Go out enzyme 20min under the conditions of 2MPa, filtering, and gained filtrate is products C；
4) extracts of Chinese herbal medicine is prepared：By product A, product B, products C and peach gum according to mass ratio 5:75:19.5:0.5 mixes
It is even, produce extracts of Chinese herbal medicine.
Embodiment 2
Chinese herbal medicine ferment shampoo is by extracts of Chinese herbal medicine, surfactant, NMF, nourishing agent, thickener, pearly-lustre
Agent, essence, bactericide and water are according to mass ratio 35:5:8:10:0.5:3:0.5:0.5:37.5 compositions.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) product A is prepared：6 parts of orange peel, 5 parts of banana skin, 5 parts of pine and cypress, 4 parts of black soya bean, reed are weighed according to parts by weight
6 parts of 5 parts of luxuriant growth and dandelion, which are added in juice extractor, squeezes the juice, and gained juice is product A, and residue is residue a；
2) product B is prepared：Residue a is added in stirred tank, and adds solvent, solvent is that 0.2mol/L acetic acid is water-soluble
Liquid and 0.2mol/L sodium acetate aqueous solution are according to volume ratio 14.8:35.2, pH be 5.0 cushioning liquid.Residue a and solvent
Mass ratio is 1:12, it is 85 DEG C in temperature, pressure adjusts pH value to 6.0~7.5, mistake under the conditions of 1MPa, stirring decocts 40min
Filter, gained filtrate is product B, and residue is residue b；
3) products C is prepared：Residue b, water and enzyme are added in stirred tank, the enzyme be cellulase and phytase according to
Mass ratio 1:2 composition, residue b, water and enzyme mass ratio are 10:120:0.2, at 40 DEG C, 48h is extracted, in 85 DEG C, pressure
Go out enzyme 20min under the conditions of 2MPa, filtering, and gained filtrate is products C；
4) extracts of Chinese herbal medicine is prepared：By product A, product B, products C and peach gum according to mass ratio 5:75:19.5:0.5 mixes
It is even, produce extracts of Chinese herbal medicine.
Embodiment 3
Chinese herbal medicine ferment shampoo is by extracts of Chinese herbal medicine, surfactant, NMF, nourishing agent, thickener, pearly-lustre
Agent, essence, bactericide and water are according to mass ratio 35:5:8:10:0.5:3:0.5:0.5:37.5 compositions.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) product A is prepared：4 parts of orange peel, 3 parts of banana skin, 3 parts of pine and cypress, 4 parts of black soya bean, reed are weighed according to parts by weight
3 parts of 5 parts of luxuriant growth and dandelion, which are added in juice extractor, squeezes the juice, and gained juice is product A, and residue is residue a；
2) product B is prepared：Residue a is added in stirred tank, and adds solvent, solvent is that 0.2mol/L acetic acid is water-soluble
Liquid and 0.2mol/L sodium acetate aqueous solution are according to volume ratio 14.8:35.2, pH be 5.0 cushioning liquid.Residue a and solvent
Mass ratio is 1:12, it is 85 DEG C in temperature, pressure adjusts pH value to 6.0~7.5, mistake under the conditions of 1MPa, stirring decocts 40min
Filter, gained filtrate is product B, and residue is residue b；
3) products C is prepared：Residue b, water and enzyme are added in stirred tank, the enzyme be cellulase and phytase according to
Mass ratio 1:2 composition, residue b, water and enzyme mass ratio are 10:120:0.2, at 40 DEG C, 48h is extracted, in 85 DEG C, pressure
Go out enzyme 20min under the conditions of 2MPa, filtering, and gained filtrate is products C；
4) extracts of Chinese herbal medicine is prepared：By product A, product B, products C and peach gum according to mass ratio 5:75:19.5:0.5 mixes
It is even, produce extracts of Chinese herbal medicine.
Embodiment 4
Chinese herbal medicine ferment shampoo is by extracts of Chinese herbal medicine, surfactant, NMF, nourishing agent, thickener, pearly-lustre
Agent, essence, bactericide and water are according to mass ratio 35:5:8:10:0.5:3:0.5:0.5:37.5 compositions.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) product A is prepared：1 part of orange peel, 5 parts of banana skin, 2 parts of pine and cypress, 4 parts of black soya bean, reed are weighed according to parts by weight
1 part of 5 parts of luxuriant growth and dandelion, which are added in juice extractor, squeezes the juice, and gained juice is product A, and residue is residue a；
2) product B is prepared：Residue a is added in stirred tank, and adds solvent, solvent is that 0.2mol/L acetic acid is water-soluble
Liquid and 0.2mol/L sodium acetate aqueous solution are according to volume ratio 14.8:35.2, pH be 5.0 cushioning liquid.Residue a and solvent
Mass ratio is 1:12, it is 85 DEG C in temperature, pressure adjusts pH value to 6.0~7.5, mistake under the conditions of 1MPa, stirring decocts 40min
Filter, gained filtrate is product B, and residue is residue b；
3) products C is prepared：Residue b, water and enzyme are added in stirred tank, the enzyme be cellulase and phytase according to
Mass ratio 1:2 composition, residue b, water and enzyme mass ratio are 10:120:0.2, at 40 DEG C, 48h is extracted, in 85 DEG C, pressure
Go out enzyme 20min under the conditions of 2MPa, filtering, and gained filtrate is products C；
4) extracts of Chinese herbal medicine is prepared：By product A, product B, products C and peach gum according to mass ratio 5:75:19.5:0.5 mixes
It is even, produce extracts of Chinese herbal medicine.
Embodiment 5
Chinese herbal medicine ferment shampoo is by extracts of Chinese herbal medicine, surfactant and thickener according to mass ratio 80:19.5:
0.5 composition.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) product A is prepared：2 parts of orange peel, 2 parts of banana skin, 1 part of pine and cypress, 3 parts of black soya bean, reed are weighed according to parts by weight
2 parts of 2 parts of luxuriant growth and dandelion, which are added in juice extractor, squeezes the juice, and gained juice is product A, and residue is residue a；
2) product B is prepared：Residue a is added in stirred tank, and adds solvent, solvent is 60% ethanol water.
The mass ratio of residue a and solvent is 1:12, under the conditions of temperature is 85 DEG C, stirring decocts 40min, adjusts pH value to 6.0~7.5,
Filtering, gained filtrate is product B, and residue is residue b；
3) products C is prepared：Residue b, water and enzyme are added in stirred tank, the enzyme be cellulase and chitinase by
According to mass ratio 1:2 composition, residue b, water and enzyme mass ratio are 10:120:0.2, at 40 DEG C, 48h is extracted, in 85 DEG C of bars
Go out enzyme 20min under part, filtering, and gained filtrate is products C；
4) extracts of Chinese herbal medicine is prepared：By product A, product B, products C and peach gum according to mass ratio 5:75:19.5:0.5 mixes
It is even, produce extracts of Chinese herbal medicine.
Embodiment 6
Chinese herbal medicine ferment shampoo is by extracts of Chinese herbal medicine, surfactant, NMF, nourishing agent, thickener, pearly-lustre
Agent, essence, bactericide and water are according to mass ratio 35:5:8:10:0.5:3:0.5:0.5:37.5 compositions.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) product A is prepared：2 parts of orange peel, 2 parts of banana skin, 1 part of pine and cypress, 3 parts of black soya bean, reed are weighed according to parts by weight
2 parts of 2 parts of luxuriant growth and dandelion, which are added in juice extractor, squeezes the juice, and gained juice is product A, and residue is residue a；
2) product B is prepared：Residue a is added in stirred tank, and adds solvent, solvent is that the hydrochloric acid that pH is 2.5 is water-soluble
Liquid.The mass ratio of residue a and solvent is 1:12, it is 85 DEG C in temperature, pressure adjusts pH under the conditions of 1MPa, stirring decocts 40min
Value is to 6.0~7.5, and filtering, gained filtrate is product B, and residue is residue b；
3) products C is prepared：Residue b, water and enzyme are added in stirred tank, the enzyme be cellulase and phytase according to
Mass ratio 1:2 composition, residue b, water and enzyme mass ratio are 10:120:0.2, at 40 DEG C, 48h is extracted, in 85 DEG C, pressure
Go out enzyme 20min under the conditions of 2MPa, filtering, and gained filtrate is products C；
4) extracts of Chinese herbal medicine is prepared：By product A, product B, products C and peach gum according to mass ratio 5:75:19.5:0.5 mixes
It is even, produce extracts of Chinese herbal medicine.
Embodiment 7
Chinese herbal medicine ferment shampoo is by extracts of Chinese herbal medicine, surfactant, NMF, nourishing agent, thickener, pearly-lustre
Agent, essence, bactericide and water are according to mass ratio 35:5:8:10:0.5:3:0.5:0.5:37.5 compositions.
The preparation technology of extracts of Chinese herbal medicine, is followed the steps below：
1) product A is prepared：2 parts of orange peel, 2 parts of banana skin, 1 part of pine and cypress, 3 parts of black soya bean, reed are weighed according to parts by weight
2 parts of 2 parts of luxuriant growth and dandelion, which are added in juice extractor, squeezes the juice, and gained juice is product A, and residue is residue a；
2) product B is prepared：Residue a is added in stirred tank, and adds solvent, solvent is that 0.2mol/L acetic acid is water-soluble
Liquid and 0.2mol/L sodium acetate aqueous solution are according to volume ratio 14.8:35.2, pH be 5.0 cushioning liquid.Residue a and solvent
Mass ratio is 1:12, it is 85 DEG C in temperature, pressure adjusts pH value to 6.0~7.5, mistake under the conditions of 1MPa, stirring decocts 40min
Filter, gained filtrate is product B, and residue is residue b；
3) products C is prepared：Residue b, water and enzyme are added in stirred tank, the enzyme be cellulase and phytase according to
Mass ratio 1:2 composition, residue b, water and enzyme mass ratio are 10:120:0.2, at 40 DEG C, 48h is extracted, in 85 DEG C, pressure
Go out enzyme 20min under the conditions of 2MPa, filtering, and gained filtrate is products C；
4) extracts of Chinese herbal medicine is prepared：By product A, product B and products C according to mass ratio 5:75:20 mix, and produce medium-height grass
Medicament extracting solution.
In embodiment 1 to 7, the surfactant is polyglyceryl fatty acid ester, lauric monoglyceride and cetyl
Trimethyl quaternary ammonium ammonium bromide is according to mass ratio 3:2:1 composition；The NMF is glycerine, fructose, propane diols, sorbierite
With polyglutamic acid according to mass ratio 1:1:2:1:1 composition；The nourishing agent is honey, superoxide dismutase, vitamin
A, vitamin e and vitamin E are according to mass ratio 1:3:2:1:1 composition；The thickener be sodium alginate and sodium chloride by
According to mass ratio 1:2 composition；The pearling agent is the double stearic acid of ethylene glycol and stearic acid diethylene glycol dilaurate according to mass ratio 1:2
Composition；The bactericide is methylisothiazolinone and potassium sorbate according to mass ratio 1:1 composition.
Beneficial effects of the present invention are further illustrated with reference to experimental data：
1st, general information
Inventor is between in August, 2013~2016 year November, and 1400 volunteers of selection use products of the present invention, wherein male
Property, each 700 of women, the range of age be 35~55 years old.Universal symptom is that hair dries up, scalp itch, dandruff do not come out, white hair
It is more.This 1400 experimenters are divided into 7 groups immediately, every group of 200 people test common shampoo and (remove and do not add Chinese herbal medicine respectively
Outside extract solution, other preparation methods are consistent with embodiment 1), embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 6 and
Embodiment 7.
2nd, test method
During hair washing using experiment provide common shampoo (in addition to extracts of Chinese herbal medicine is not added, other preparation methods with
Embodiment 1 is consistent), embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 6 and embodiment 7, use 6 months.
3rd, judgment criteria and evaluation result
3.1 judgment criteria
Recovery from illness：Clinical symptoms all disappear.Take a turn for the better：Clinical symptoms substantially mitigate.It is invalid：Clinical symptoms without being clearly better,
There is exacerbation trend.
3.2 evaluation results statistics such as table 1.
17 groups of shampoo Comparison of therapeutic of table
It can be seen that the present invention is significantly better than common shampoo in terms of relieving itching and removing dandruff and black hair by the data of table 1, wherein in fact
Apply that the effect of example 1 is optimal, residue a embodiment 6 is extracted using aqueous hydrochloric acid solution, can not show a candle to use cushioning liquid in using effect
Embodiment 1 to 4；It also not can not show a candle to, using the embodiment 1 to 4 for adding peach gum, say using the using effect of the embodiment 7 of peach gum
The bright technical scheme of the embodiment of the present invention 1 is optimal.
Claims (6)
1. a kind of preparation method of Chinese herbal medicine ferment shampoo, it is characterised in that it is by extracts of Chinese herbal medicine containing enzyme, surface-active
Agent, NMF, nourishing agent, thickener, pearling agent, essence, bactericide and water are according to mass ratio 5~89:2~89:0~30:0~
50:0.5~15:0~30:0~5:0~5:0~70 composition；
The surfactant includes polyglyceryl fatty acid ester, lauric monoglyceride, methyl glycol fatty acid ester, sorbitol anhydride list
Palmitate, stearoyl lactate, diacetyl tartarate monoglyceride, Cocoamidopropyl betaine, Nonyl pheno
Ether, polyoxyethylene oleic acid ester, polyoxyethylene stearic acid ester, sorbitan fatty acid ester, two polyglycereol, cetyl trimethyl
Quaternary ammonium ammonium bromide, octadecyl dimethyl benzyl quaternary ammonium ammonium chloride, benzyltriethylammoinium chloride, diisooctyl succinate sulfonic acid
One or any ratio in sodium and aliphatic acid polyethenoxy fat it is two or more；
During the NMF is glycerine, fructose, propane diols, sorbierite, polyglutamic acid, niacinamide, polyethylene glycol and xylitol
One or any ratio it is two or more；
The nourishing agent includes honey, sodium salicylate, superoxide dismutase, Alphalin, beta glucan, vitamin e, lysine
One or any ratio in sodium and vitamin E it is two or more；
The thickener includes one or any in sodium chloride, sodium carboxymethylcellulose, gelatin, sodium alginate and casein
Ratio it is two or more；
The pearling agent include one kind in pearl powder, stearic acid diethylene glycol dilaurate, ethylene glycol double stearic acid and mica powder or
Arbitrary proportion it is two or more；
The bactericide includes one kind in methylisothiazolinone, methylchloroisothiazandnone, sodium benzoate and potassium sorbate
Or arbitrary proportion is two or more；
The extracts of Chinese herbal medicine containing enzyme, is followed the steps below：
1）Prepare product A：Chinese herbal medicine is added in juice extractor and squeezed the juice, gained juice is product A, residue is residue a；
2）Prepare product B：Residue a is added in stirred tank, and adds solvent, the mass ratio of residue a and solvent is 1:2~
40, it is 60 DEG C~100 DEG C in temperature, pressure adjusts pH value to 5.5 under the conditions of 0~5MPa, stirring decocts 20min~120min
~8.5, filtering, gained filtrate is product B, and residue is residue b；
3）Prepare products C：Residue b, water and enzyme are added in stirred tank, residue b, water and enzyme mass ratio are 10:20~
200:0.1~2, at 25 DEG C~60 DEG C, 24h~120h is extracted, is filtered, gained filtrate is products C；
4）Prepare extracts of Chinese herbal medicine containing enzyme：By product A, product B, products C and natural gum according to mass ratio 0~98:1~98:1~
98:0~60 mixes, and produces extracts of Chinese herbal medicine；
The Chinese herbal medicine is to weigh 1~7 part of orange peel, 1~5 part of banana skin, 1~5 part of pine and cypress, black soya bean 1 according to parts by weight
1~6 part of~5 parts, 1~5 part of aloe and dandelion；
The solvent is one kind in ethanol, water, ethyl acetate, ether, acetic acid, sodium acetate, phosphoric acid, potassium dihydrogen phosphate and hydrochloric acid
Or arbitrary proportion is two or more；
The enzyme is cellulase, phytase, sea snail enzymes I, sea snail enzymes II, sea snail enzymes III, sea urchin enzyme, sea hare enzyme, Bao enzyme, snail
Two of one kind or arbitrary proportion in enzyme, beta galactosidase, beta-glucosidase, chitinase, agarase and alginase
More than kind；
The natural gum is guar gum, Arabic gum, peach gum, agar-agar, algin, polyacrylamide, Sodium Polyacrylate and carboxylic first
One kind or arbitrary proportion in base sodium cellulosate it is two or more.
2. the preparation method of Chinese herbal medicine ferment shampoo as claimed in claim 1, it is characterised in that：Step 1）It is described according to weight
Amount number weighs 2 parts of 2 parts of orange peel, 2 parts of banana skin, 1 part of pine and cypress, 3 parts of black soya bean, 2 parts of aloe and dandelion.
3. the preparation method of the Chinese herbal medicine ferment shampoo as described in claims 1 to 3, it is characterised in that：Step 2）It is described molten
Agent is 0.2mol/L aqueous acetic acid and 0.2mol/L sodium acetate aqueous solution according to volume ratio 14.8:35.2, pH be 5.0
Cushioning liquid.
4. the preparation method of the Chinese herbal medicine ferment shampoo as described in Claims 1-4, it is characterised in that：Step 3）Described in
Enzyme is cellulase and phytase according to mass ratio 1:2 composition.
5. the preparation method of the Chinese herbal medicine ferment shampoo as described in claim 1 to 5, it is characterised in that：Step 4）Described in
Natural gum is peach gum.
6. the preparation method of Chinese herbal medicine ferment shampoo as claimed in claim 1, it is characterised in that：The surfactant is
Polyglyceryl fatty acid ester, lauric monoglyceride and cetyl trimethyl quaternary ammonium ammonium bromide are according to mass ratio 3:2:1 combination
Thing；The NMF is glycerine, fructose, propane diols, sorbierite and polyglutamic acid according to mass ratio 1:1:2:1:1 combination
Thing；The nourishing agent is honey, superoxide dismutase, Alphalin, vitamin e and vitamin E according to mass ratio 1:3:2:1:
1 composition；The thickener is sodium alginate and sodium chloride according to mass ratio 1:2 composition；The pearling agent is second two
The double stearic acid of alcohol and stearic acid diethylene glycol dilaurate are according to mass ratio 1:2 composition；The bactericide is methylisothiazolinone
With potassium sorbate according to mass ratio 1:1 composition；Extracts of Chinese herbal medicine, surfactant, NMF, nourishing agent, thickener,
Pearling agent, essence, the mass ratio of bactericide and water are 35:5:8:10:0.5:3:0.5:0.5:37.5.
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| CN110882193A (en) * | 2019-12-18 | 2020-03-17 | 佛山科学技术学院 | Anti-hair loss shampoo and preparation method thereof |
| CN115089538A (en) * | 2022-07-26 | 2022-09-23 | 吴流俊 | Shampoo with Chinese honeylocust fruit rice as main formula |
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| CN115089538A (en) * | 2022-07-26 | 2022-09-23 | 吴流俊 | Shampoo with Chinese honeylocust fruit rice as main formula |
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