CN107212403A - Caulis et Folium Tritici aestivi barley green composition and its preparation process - Google Patents

Caulis et Folium Tritici aestivi barley green composition and its preparation process Download PDF

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Publication number
CN107212403A
CN107212403A CN201710264761.1A CN201710264761A CN107212403A CN 107212403 A CN107212403 A CN 107212403A CN 201710264761 A CN201710264761 A CN 201710264761A CN 107212403 A CN107212403 A CN 107212403A
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caulis
tritici aestivi
wheat
barley
folium tritici
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夏泳
顾守智
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Zhejiang Bei Wo Biological Technology Co Ltd
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Zhejiang Bei Wo Biological Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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Abstract

The present invention provides a kind of Caulis et Folium Tritici aestivi barley green composition and its preparation process, is combined using wheat seedling tender leaf extract with natural xylo-oligosaccharide, and uses advanced preparation process.It is specific to inspect by random samples → pack and be obtained with weighing and burden → dry method mixing and granulation (using the one-step-granulating method with uniform batch mixing function) → tabletting → sterilizing →.The Caulis et Folium Tritici aestivi barley green flake products processed with preparation process are formulated with this, traditional wet granulation, the backwardness technique of oven for drying due to having abandoned, therefore the loss of Barley Greeg active nutrient component is reduced, the useless loss rate of raw material is significantly reduced, and purity is high, mouthfeel is good, and suitable diabetes patient takes.

Description

Caulis et Folium Tritici aestivi barley green composition and its preparation process
Technical field
The present invention relates to a kind of Caulis et Folium Tritici aestivi barley green composition and its preparation process.
Background technology
Current wheat seedling extraction and Barley Greeg piece are mainly what is carried on technical development using barley seedling as raw material.Although being all The wheat section class crop survived the winter, but wheat seedling has many differences with barley seedling:One is the difference of the speed of growth, and barley seedling is than small Faster, the planting experiment according to inventor in 31 ° of regions of Yangtze river basin north latitude for many years shows wheat seedling growth:Same time plantation Barley and wheat (applying same base fertilizer), the former grows into 30cm and about needed 60 days, and the latter then needs 90 days or so;Two be two kinds of wheats The more aobvious stout and strong, softness of the Traits change of seedling, barley seedling vein and straw, and moisture is high, color is partially light green, and wheat seedling leaf Arteries and veins and straw are then partially thin and thin, harder, and color is dark green, and moisture is relatively low;Three be the cold-resistant sex differernce of two kinds of wheat seedings, When appearing above less than -4 DEG C cryogenic freezing weather within continuous 4 days, barley seedling occurs that the yellow leaf of large area (is mainly seedling Point), and wheat seedling is not in then yellow leaf;Four be the difference of nutritional ingredient, and wheat seedling is long because of growth period, chlorophyll, mineral matter, The component contents such as SOD are higher, and the finger of the barley seedling for seeming more stout and strong then in terms of protein, fat, vitamin, Thick many candies Mark is dominant.The extraction that above-mentioned difference has been doomed wheat seedling must be improved and skill on the basis of barley seedling extraction equipment and technique Art is upgraded.Five be that the extracts of two seedlings has obvious Traits change:Wheat seedling extract color is more dark green, and its proportion is than big Wheat seedling extraction goes out greatly a lot (volume of same weight only has 80% or so of barley seedling extract), therefore wheat seedling extract Density it is compacter, stability and mobility are better, compare beneficial to tabletting.
Two kinds of wheat seedling extractions have difference, the combination of Caulis et Folium Tritici aestivi barley green piece on group material formula and preparation process Composition formula and its preparation process must be improved and skill on the basis of the composition and its preparation process of Green -sine of wheat of Herba Hordei Vulgaris piece Art is upgraded.
At home and abroad though in the market has much competitiveness for the Barley Greeg raw material and tablet of prior art production, its technology Following defect is also there is with product:
1st, Barley Greeg purity is relatively low:Because Barley Greeg raw material used in it and cactus powder dispensing are processed with traditional handicraft , added with 10% or so maltodextrin composition, so its purity only has about 90%, and the main component of maltodextrin is just It is starch, starch can be converted into glucose in human body by the effect of enzyme, thereby results in the rise of diabetic population glycemic index.Cause This, the celestial wheat barley green tablet processed with traditional handicraft, unsuitable diabetic population long-term consumption.
2nd, the granulation and drying mode fallen behind causes amount of activated nutrition leak:The technical scheme life proposed with above-mentioned patent The celestial wheat Barley Greeg piece of production uses traditional " wet method " granulation, needs to be put into material into 55-60 DEG C of baking oven after granulation Interior to be dried, required time is up to more than 220 minutes.The celestial wheat Barley Greeg product of compression molding is after testing after drying: Its crucial functional component and active nutrient component SOD and ascorbic content are only left 5100U/g and 233mg/ respectively 100g。
3rd, material loss rate is higher:Because Green -sine of wheat of Herba Hordei Vulgaris powder proportion relatively light, Icing Sugar content is higher, easily tacky, cause Mobility is not good enough, therefore material loss rate is relatively higher in granulation and tabletting production process, and powder rate of giving up is up to more than 3%.
The content of the invention
At least one deficiency of the invention in order to overcome prior art is there is provided a kind of Caulis et Folium Tritici aestivi barley green composition, " zero Addition " on the premise of obtain a kind of new Barley Greeg composition and formulation method, with realize reduce Barley Greeg active nutritional into The loss divided, the useless loss rate of raw material is significantly reduced, and purity is high, the good purpose of mouthfeel.
To achieve these goals, the present invention uses following technical scheme:
Caulis et Folium Tritici aestivi barley green composition, its active ingredient is the combination of wheat seedling tender leaf extract and natural xylo-oligosaccharide, Wherein wheat seedling tender leaf extract is extracted using physical method from more Winter Wheat Seedling.
Further, the Caulis et Folium Tritici aestivi barley green composition contains the component of following mass fraction:Wheat seedling tender leaf extract 89~97.5%, natural xylo-oligosaccharide 2.5~11%,
Further, wherein the purity of wheat seedling tender leaf extract is 100%.
Further, the preparation method of wheat seedling tender leaf extract comprises the following steps:
Step a, selects fresh more Winter Wheat Seedling, length is 25-35 centimetres, is cleaned;
Step b, the wheat seedling after cleaning enters the vibrated and dehydrated conveyer with vibration function, is then sent to elevating conveyor In, carry out wind-force by many Fans above elevator and remove water;
Step c, the wheat seedling gone after water is transported to disintegrating machine and crushed;
Step d, the wheat seedling after crushing enters filtering pressure machine, completes screenings separation;
Step e, the wheat slurry after separation is concentrated, and is then dried in vacuo, is obtained wheat seedling tender leaf extract powder.
Further, the vibration frequency of vibrated and dehydrated conveyer is 18~25 times/second in step b, and amplitude range is controlled up and down In 2~4cm;In step b, the blower fan is three, between longitudinal direction is arranged between elevator top, adjacent two Fans side by side Away from for 75cm, the power per Fans is 175W~250W;Conveying direction power of three Fans along wheat seeding is sequentially reduced; In step b, the blower fan is apart from 25 centimetres of wheat seeding;The gradient of elevating conveyor is 60 degree.
Further, in step c, disintegrating machine be provided with the part by weight of tungsten in steel alloy tooth, the steel alloy tooth for 9~ 13%, the part by weight of chromium is 3.8~4.9%, and the part by weight of vanadium is 2%, and the part by weight of cobalt is 4~4.8%.
Further, in step d, filtering pressure machine combines roller completion using band is rolled;In step e, the wheat slurry after separation leads to first After the reciprocating sieve filtering for crossing 120 mesh, buffer tank of the injection with agitating function, then filled by buffer tank into negative pressure of vacuum concentration, Concentrated by 100-120 minutes, finally inject vacuum drier and be dried, obtain wheat seedling tender leaf extract powder.
Further, the natural xylo-oligosaccharide is extracted from corncob obtains.
The present invention also provides a kind of preparation process of Caulis et Folium Tritici aestivi barley green composition, the processing method that tablet is specifically made Using dry method mixing and granulation, then tabletting.
Further, the workshop condition temperature of dry method mixing and granulation is 16~20 DEG C, and humidity is 15~20%.;Tabletting workshop Environment temperature is 18~22 DEG C, and humidity is 18~25%.
The main material of the present invention:More Winter Wheat Seedling extract (Barley Greeg) accounting about 89~97.5% of 100% purity;Match somebody with somebody Material:The natural xylo-oligosaccharide accounting about 2.5~11% extracted from corncob.Because the mouthfeel of Barley Greeg is partially bitter, salty, puckery, suitably Addition xylo-oligosaccharide can improve the mouthfeel of Barley Greeg piece so that Barley Greeg piece can directly chew edible, thus reach more preferably Assimilation effect.Xylo-oligosaccharide stability is super good, acidproof, heat-resisting, the difficult moisture absorption, not easy to ferment, will not be as some carbohydrate tablettings after Easily in the tablet surface formation crystallization water, while xylo-oligosaccharide is described as " super bifidus factor ", the numerous of beneficial bacteria of intestinal tract can be promoted Grow, suppress harmful bacteria growing, reaching improves the effect of constipation, diarrhoea and chronic enteritis.In addition, the energy value of xylo-oligosaccharide is almost It is zero, blood glucose concentration is also had no effect.In summary, the dispensing using xylo-oligosaccharide as Caulis et Folium Tritici aestivi barley green piece exists It is beneficial to compression molding in technique, then has in terms of nutritional health function preferably complementary.
Preparation process:1) pelletize:Dehumidifier and air-conditioning are opened in advance, and the PELLET MILL PLANT air humidity control after sterilization is existed 15~20%, temperature control is at 16~20 DEG C.Then wheat Barley Greeg powder and xylo-oligosaccharide are weighed in proportion, first by wheat seedling wheat Green plain powder raw material pours into granulator batch mixing pot, then with appropriate purified water xylo-oligosaccharide is dissolved into the thick of liquid, afterwards In batch mixing by the xylo-oligosaccharide of the shower nozzle of granulator uniform sprinkling liquid into pot, it is because of the white low of solid-state to do so Xylan powder can cause the Barley Greeg slice, thin piece surface pressed some white dots occur, and the same Barley Greeg of the xylo-oligosaccharide of liquid After powder is fully chelated, it not only avoid slice, thin piece surface and white dot occur, and preferable adhesive effect can also be played.When oligomeric Xylose material feeding is finished and two kinds of material are obtained after full and uniform mixing, and granulator opens hot blast (55~60 DEG C) and blows Matter Transfer Rolling is pelletized, while a small amount of moisture contained by the xylo-oligosaccharide of liquid is also removed whereby, after about 90 minutes, program knot of pelletizing Beam.2) tabletting:Tabletting workshop after sterilization requires 18~22 DEG C of temperature, and humidity is 18~25%.The material for making grain is sent into Tablet press machine hopper, machine rotational speed is adjusted to 18 revs/min, and punch die pressure is adjusted to 40kg.The wheat extruded by above-mentioned technical parameter Green plain piece, color is emerald green, wheat seeding aromatic flavour, and surface is smooth, uniform color, hardness are moderate, and raw material give up loss rate about 1%, passes through Slaking test:Disintegration time limited be 39 points 20 seconds.
Compared with prior art, the present invention has advantages below:
Technical scheme proposed by the present invention is, using a kind of Caulis et Folium Tritici aestivi barley green extract of 100% purity as main material, to add Plus natural xylo-oligosaccharide carries out preparation, concrete technology flow process is:Weighing and burden → dry method mixing and granulation is (using with uniform batch mixing The one-step-granulating method of function) → tabletting → sterilizing → inspects by random samples → packs.The wheat seedling processed with preparation process is formulated with this Barley Greeg flake products, due to abandoned wet granulation, oven for drying backwardness technique, therefore reduce Barley Greeg active nutritional into The loss divided, the useless loss rate of raw material is significantly reduced, and purity is high, and mouthfeel is good.This Caulis et Folium Tritici aestivi barley green piece is because without malt paste Essence, its dispensing xylo-oligosaccharide will not be converted into glucose in body in addition, therefore suitable population (is especially suitable for glycosuria more extensively Patient group is edible).
Specifically, including following aspect:
1st, purity is higher, and without maltodextrin, suitable population is more extensive:The technical scheme processing provided with the present invention The Caulis et Folium Tritici aestivi barley green extract of the main material that Caulis et Folium Tritici aestivi barley green piece is used --- 100% purity compares conventional formulation and work The yong barley leaves of the compositions such as maltodextrin, the brown rice of addition 5-20% that the Barley Greeg piece of skill processing is used extract raw material (being not suitable for diabetic population), purity is higher, and greatly reduces the content of starch of product so that the suitable population of product is more Extensively.
2nd, unique formula improves the mouthfeel of Barley Greeg piece, enhances effect to enteron aisle:There is provided due to the present invention The Caulis et Folium Tritici aestivi barley green piece of technical scheme processing contains a certain proportion of xylo-oligosaccharide formula so that the Caulis et Folium Tritici aestivi barley green piece is produced Product have a strand light sweet taste, and it is edible that the improvement of mouthfeel allows Caulis et Folium Tritici aestivi barley green piece directly to chew, so as to reach more preferable suction Produce effects really.Xylo-oligosaccharide is described as " super bifidus factor ", can promote the breeding of beneficial bacteria of intestinal tract, suppresses harmful bacteria growing, reaches To the effect of improvement constipation, diarrhoea and chronic enteritis.In addition, the energy value of xylo-oligosaccharide is almost nil, to diabetic population Blood sugar concentration is also had no effect.
3rd, the proportion of goods damageds of material are substantially reduced:By the Caulis et Folium Tritici aestivi barley green piece institute for the technical scheme processing that the present invention is provided The Caulis et Folium Tritici aestivi barley green powder raw material of use is more great than the ratio of Green -sine of wheat of Herba Hordei Vulgaris powder, and density is higher, and mobility is more preferably, in addition oligomeric The adhesive effect that xylose uniqueness mixing method is produced, therefore, the material for the Caulis et Folium Tritici aestivi barley green piece processed with the technology of the present invention is damaged Consumption rate only has 1%, the proportion of goods damageds for the Green -sine of wheat of Herba Hordei Vulgaris piece 3% processed compared to conventional formulation and technique, hence it is evident that reduced.
4th, advanced granulation mode reduces the loss of Barley Greeg active nutrient component:Traditional wet granulation needs nearly four The drying course of hour, the drying mode of this vapo(u)rability easily causes the loss of Barley Greeg active nutritional, and the present invention is carried The technical scheme of confession is the dry granulation for only needing to complete for 90 minutes or so, and the hot air circulation employed in it is compared to the height under static state Temperature evaporation, the active component influence on material is much smaller.By detecting contrast:The celestial wheat board processed with conventional formulation and technique Barley Greeg piece and green fingers board Barley Greeg piece (being bought respectively at hundred Cheng Tang brand shops of Chengdu market and Suzhou dealer), its SOD and ascorbic content only have 5100U/g, 5000U/g and 233mg/100g, 220mg/100g respectively;And carried with the present invention The Caulis et Folium Tritici aestivi barley green piece of the technical scheme processing of confession, its SOD and ascorbic content respectively reached 24900U/g and 570mg/100g。
Embodiment
For above and other objects of the present invention, feature and advantage can be become apparent, preferred embodiment cited below particularly, It is described in detail below.
Embodiment 1:
A kind of formula and its preparation process of Caulis et Folium Tritici aestivi barley green piece:Change without adhesive, preservative, stabilizer etc. In the case of learning additive, by weight than xylo-oligosaccharide that Caulis et Folium Tritici aestivi barley green powder and the weight ratio for 97.5% are 2.5% (this Invent the core source health board xylo-oligosaccharide that the xylo-oligosaccharide used in each embodiment is produced by the imperial power biology in listed company Shandong) carry out Dispensing.
Procedure of processing is as follows:1) pelletize:Dehumidifier and air-conditioning are opened in advance, by the PELLET MILL PLANT air humidity control after sterilization System is 15~20%, and temperature control is at 16~20 DEG C.Then the oligomeric of 58.5 kilograms of Caulis et Folium Tritici aestivi barley green powder and 1.5 kilograms is weighed Xylose, first pours into granulator batch mixing pot, then xylo-oligosaccharide is dissolved into appropriate purified water by Caulis et Folium Tritici aestivi barley green powder raw material Liquid it is thick, back batch mixing side by the xylo-oligosaccharide of the shower nozzle of granulator from uniform sprinkling liquid to pot, when oligomeric Xylose material feeding is finished and two kinds of material are obtained after full and uniform mixing, and granulator opens hot blast (55~60 DEG C) and blows Matter Transfer Rolling is pelletized, while a small amount of moisture contained by the xylo-oligosaccharide of liquid is also removed whereby, after about 90 minutes, program knot of pelletizing Beam.2) tabletting:Tabletting workshop after sterilization requires that temperature is 18~22 DEG C, and humidity is 18~25%, and the material for making grain is sent Enter tablet press machine hopper, machine rotational speed is adjusted to 18 revs/min, and punch die pressure is adjusted to 40kg.It is per minute by above-mentioned technical parameter Can slice 558, about 215 minutes complete 60kg materials tabletting, can obtain specification be 500mg/ pieces emerald green barley green tablet About 119000.3) sterilize, inspect by random samples, encapsulate:After product after sterilizing determines that microbiological indicator meets company standard through sampling observation, enter Enter packet assembler, it is desirable to using thicken PET is medical, food grade plastic bottle, aluminium foil sealing, specification is:0.5g × 200 piece/bottle, The silica gel particle drier of the built-in bag 4g specifications of bottle.
As a result identify:The Caulis et Folium Tritici aestivi barley green tablet surface smoothness processed by said ratio and technical parameter partially in Deng color is emerald green, uniform color, hardness are moderate, fragment accounting about 0.3%, and raw material gives up loss rate about 1%, through slaking test:Disintegration When be limited to 38 points 30 seconds.Mouthfeel:Wheat seeding is strong and brisk in taste, but without obvious sweet taste, it is slightly biased bitter, puckery, salty.
Embodiment 2:
A kind of formula and its preparation process of Caulis et Folium Tritici aestivi barley green piece:Change without adhesive, preservative, stabilizer etc. In the case of learning additive, weight is matched somebody with somebody than the xylo-oligosaccharide that Caulis et Folium Tritici aestivi barley green powder and the weight ratio for 96% are 4% Material.
Procedure of processing is as follows:1) pelletize:Dehumidifier and air-conditioning are opened in advance, by the PELLET MILL PLANT air humidity control after sterilization System is 15~20%, and temperature control is at 16~20 DEG C.Then the oligomeric of 62.4 kilograms of Caulis et Folium Tritici aestivi barley green powder and 2.6 kilograms is weighed Xylose, first pours into granulator batch mixing pot, then xylo-oligosaccharide is dissolved into appropriate purified water by Caulis et Folium Tritici aestivi barley green powder raw material Liquid it is thick, back batch mixing side by the xylo-oligosaccharide of the shower nozzle of granulator from uniform sprinkling liquid to pot, when oligomeric Xylose material feeding is finished and two kinds of material are obtained after full and uniform mixing, and granulator opens hot blast (55~60 DEG C) and blows Matter Transfer Rolling is pelletized, while a small amount of moisture contained by the xylo-oligosaccharide of liquid is also removed whereby, after about 90 minutes, program knot of pelletizing Beam.2) tabletting:Tabletting workshop after sterilization requires that temperature is 18~22 DEG C, and humidity is 18~25%, and the material for making grain is sent Enter tablet press machine hopper, machine rotational speed is adjusted to 18 revs/min, and punch die pressure is adjusted to 40kg.It is per minute by above-mentioned technical parameter Can slice 558, about 230 minutes complete 65kg materials tabletting, can obtain specification be 500mg/ pieces emerald green barley green tablet About 128700.3) sterilize, inspect by random samples, encapsulate:After product after sterilizing determines that microbiological indicator meets company standard through sampling observation, enter Enter packet assembler, it is desirable to using thicken PET is medical, food grade plastic bottle, aluminium foil sealing, specification is:0.5g × 200 piece/bottle, The silica gel particle drier of the built-in bag 4g specifications of bottle.
As a result identify:The Caulis et Folium Tritici aestivi barley green tablet surface smoothness processed by said ratio and technical parameter partially in First-class, color is emerald green, uniform color, hardness are moderate, fragment accounting about 0.26%, and raw material gives up loss rate about 1%, through slaking test: Disintegration time limited be 39 points 10 seconds.Mouthfeel:Wheat seeding is strong and brisk in taste, but sweet taste is still not obvious enough, and bitter, puckery, saline taste road is compared to " implementation Example 1 " slightly weakens.
Embodiment 3:
A kind of formula and its preparation process of Caulis et Folium Tritici aestivi barley green piece:Change without adhesive, preservative, stabilizer etc. In the case of learning additive, weight is matched somebody with somebody than the xylo-oligosaccharide that Caulis et Folium Tritici aestivi barley green powder and the weight ratio for 94% are 6% Expect
Procedure of processing is as follows:1) pelletize:Dehumidifier and air-conditioning are opened in advance, by the PELLET MILL PLANT air humidity control after sterilization System is 15~20%, and temperature control is at 16~20 DEG C.Then the oligomeric wood of 47 kilograms of Caulis et Folium Tritici aestivi barley green powder and 3 kilograms is weighed Sugar, first pours into granulator batch mixing pot by Caulis et Folium Tritici aestivi barley green powder raw material, then with appropriate purified water xylo-oligosaccharide is dissolved into liquid State it is thick, back batch mixing side by the xylo-oligosaccharide of the shower nozzle of granulator from uniform sprinkling liquid to pot, when oligomeric wood Sugared material feeding is finished and two kinds of material are obtained after full and uniform mixing, and granulator unlatching hot blast (55~60 DEG C) blows Matter Transfer and turned over Capable granulation is rolled into, while a small amount of moisture contained by the xylo-oligosaccharide of liquid is also removed whereby, after about 90 minutes, program knot of pelletizing Beam.2) tabletting:Tabletting workshop after sterilization requires that temperature is 18~22 DEG C, and humidity is 18~25%, and the material for making grain is sent Enter tablet press machine hopper, machine rotational speed is adjusted to 18 revs/min, and punch die pressure is adjusted to 40kg.It is per minute by above-mentioned technical parameter Can slice 558, about 178 minutes complete 50kg materials tabletting, can obtain specification be 500mg/ pieces emerald green barley green tablet About 99000.3) sterilize, inspect by random samples, encapsulate:After product after sterilizing determines that microbiological indicator meets company standard through sampling observation, enter Enter packet assembler, it is desirable to using thicken PET is medical, food grade plastic bottle, aluminium foil sealing, specification is:0.5g × 200 piece/bottle, The silica gel particle drier of the built-in bag 4g specifications of bottle.
As a result identify:The Caulis et Folium Tritici aestivi barley green tablet surface smoothness processed by said ratio and technical parameter is excellent Good, color is emerald green, uniform color, hardness are moderate, fragment accounting about 0.22%, and raw material gives up loss rate about 1%, through slaking test:Collapse 39 points are limited to during solution 40 seconds.Mouthfeel:Wheat seeding is strong and brisk in taste, salty sweet tea mixing taste (sweet taste therein is partially lighter), and bitter, astringent taste is also obvious It is thin out.
Embodiment 4:
A kind of formula and its preparation process of Caulis et Folium Tritici aestivi barley green piece:Change without adhesive, preservative, stabilizer etc. In the case of learning additive, weight is entered than the xylo-oligosaccharide that Caulis et Folium Tritici aestivi barley green powder and the weight ratio for 92.5% are 7.5% Row dispensing
Procedure of processing is as follows:1) pelletize:Dehumidifier and air-conditioning are opened in advance, by the PELLET MILL PLANT air humidity control after sterilization System is 15~20%, and temperature control is at 16~20 DEG C.Then the low of 64.75 kilograms of Caulis et Folium Tritici aestivi barley green powder and 5.25 kilograms is weighed Xylan, first pours into granulator batch mixing pot, then xylo-oligosaccharide is dissolved with appropriate purified water by Caulis et Folium Tritici aestivi barley green powder raw material Into the thick of liquid, back batch mixing side by the xylo-oligosaccharide of the shower nozzle of granulator from uniform sprinkling liquid to pot, when low Xylan material feeding is finished and two kinds of material are obtained after full and uniform mixing, and granulator unlatching hot blast (55~60 DEG C) blows material and followed Ring rolling is pelletized, while a small amount of moisture contained by the xylo-oligosaccharide of liquid is also removed whereby, after about 96 minutes, program of pelletizing Terminate.2) tabletting:Tabletting workshop after sterilization requires that temperature is 18~22 DEG C, and humidity is 18~25%, will make the material of grain Tablet press machine hopper is sent into, machine rotational speed is adjusted to 18 revs/min, and punch die pressure is adjusted to 40kg.By above-mentioned every point of technical parameter Clock can slice 558, about 248 minutes complete 70kg materials tabletting, can obtain specification be 500mg/ pieces emerald green Barley Greeg piece Agent about 138600.3) sterilize, inspect by random samples, encapsulate:After product after sterilizing determines that microbiological indicator meets company standard through sampling observation, Into packet assembler, it is desirable to using thicken PET is medical, food grade plastic bottle, aluminium foil sealing, specification is:0.5g × 200 piece/ Bottle, the silica gel particle drier of a bag 4g specifications built in bottle.
As a result identify:The Caulis et Folium Tritici aestivi barley green tablet surface smoothness processed by said ratio and technical parameter is excellent It is good, in green in color, uniform color, hardness on, fragment accounting about 0.18%, raw material gives up loss rate about 1%, through slaking test:Collapse 39 points are limited to during solution 50 seconds.Mouthfeel:Wheat seeding is strong and brisk in taste, light sweet taste, and saline taste is compared to " embodiment 3 " has weakened, bitter, puckery Taste is pressed substantially.
Eating effect is tested:
1) 55~70 years old person in middle and old age group enterogastritis people group:12 people (each 6 of men and women), are eaten, often by the formula of embodiment 2 Its morning and afternoon 3~4 point are respectively edible 6 on an empty stomach, may be selected to chew clothes or less than 70 DEG C warm water take.After continuously eating one week, 8 People feedback stool is molded;After continuously eating 10 days, stomach rises 5 people feedback, sour regurgitation phenomenon substantially mitigates;After continuously eating 15 days, 12 people all feed back body energetically, spirit and energy be obviously improved, meanwhile, the frequency of the 4 symptom's feedback pain that often occurs having a stomach-ache Rate is significantly reduced, and pain also slightly mitigates.
2) 30~45 years old young and middle-aged constipation people group:12 people (male 4 female 8), are eaten, every morning by the formula of embodiment 4 It is respectively edible 6 on an empty stomach with afternoon 3~4 point, it may be selected to chew clothes or less than 70 DEG C warm water take.After continuously eating one week, 3 people feedback The phenomenon that can not pull of defecating substantially mitigates;After continuously eating 10 days, 7 people feedback once (can defecate universal by normal defecation daily It is black, smelly);After continuous edible 15 days, have 10 people feedback constipation situation be improved significantly, wherein 2 people reflection occurred it is whole strong The diarrhoea phenomenon of property, all not medicine self-healing after 2 days.
3) the people group often having a sleepless night for 35~50 years old:12 people (male 3 female 9), are eaten, every morning by the formula of embodiment 3 It is respectively edible 6 on an empty stomach with afternoon 3~4 point, it may be selected to chew clothes or less than 70 DEG C warm water take.After continuously eating 10 days, 6 people feedback Sleep quality is made moderate progress, and energy has been lifted;After continuously eating 15 days, 10 people feedback time for falling asleep substantially shortens, matter of sleeping Amount is obviously improved, and the required length of one's sleep has shortened;After continuously eating 25 days, only people feedback improvement sleep is not obvious, but Tired sense substantially mitigates when get up in the morning, and the brain dizziness phenomenon on daytime has weakened, wherein 7 women represent skin complexion Substantially improve.
4) 40~55 years old people with high uric acid group:12 people (all males), are eaten, every morning by the formula of embodiment 1 It is respectively edible 10 on an empty stomach with afternoon 3~4 point, it may be selected to chew clothes or less than 70 DEG C warm water take.After continuously eating 10 days, 6 people are anti- Feedback uric acid index is changed into normal or substantially close to normal;After continuously eating 2 weeks, 5 people feedback uric acid index is completely normal, and 4 people are anti- Feedback substantially reduction;After continuously eating 3 weeks, have 10 people feedback uric acid index and obtain stability contorting or basic control, wherein 3 legs Pin has edema pain phenomenon, and person reflects that the symptom that swells and ache has mitigated.
Described above is the preferred embodiment of the present invention, it is noted that for the those of ordinary skill of this technology neighborhood For, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications are also considered as Protection scope of the present invention.

Claims (10)

1. Caulis et Folium Tritici aestivi barley green composition, it is characterised in that the active ingredient of the composition be wheat seedling tender leaf extract and The combination of natural xylo-oligosaccharide, wherein wheat seedling tender leaf extract is extracted using physical method from more Winter Wheat Seedling.
2. Caulis et Folium Tritici aestivi barley green composition according to claim 1, it is characterised in that the Caulis et Folium Tritici aestivi barley green composition Component containing following mass fraction:Wheat seedling tender leaf extract 89~97.5%, natural xylo-oligosaccharide 2.5~11%.
3. Caulis et Folium Tritici aestivi barley green composition according to claim 1, it is characterised in that wherein wheat seedling tender leaf extract Purity is 100%.
4. Caulis et Folium Tritici aestivi barley green composition according to claim 1, it is characterised in that the preparation of wheat seedling tender leaf extract Method comprises the following steps:
Step a, selects fresh more Winter Wheat Seedling, length is 25-35 centimetres, is cleaned;
Step b, the wheat seedling after cleaning enters the vibrated and dehydrated conveyer with vibration function, is then sent in elevating conveyor, Wind-force, which is carried out, by many Fans above elevator removes water;
Step c, the wheat seedling gone after water is transported to disintegrating machine and crushed;
Step d, the wheat seedling after crushing enters filtering pressure machine, completes screenings separation;
Step e, the wheat slurry after separation is concentrated, and is then dried in vacuo, is obtained wheat seedling tender leaf extract powder.
5. Caulis et Folium Tritici aestivi barley green composition according to claim 4, it is characterised in that vibrated and dehydrated conveyer in step b Vibration frequency be 18~25 times/second, up and down amplitude range control in 2~4cm;In step b, the blower fan is three, longitudinal direction It is arranged on side by side above elevator, the spacing between adjacent two Fans is 75cm, the power per Fans is 175W~250W; Conveying direction power of three Fans along wheat seeding is sequentially reduced;In step b, the blower fan is apart from 25 centimetres of wheat seeding;Lifting The gradient of conveyer is 60 degree.
6. Caulis et Folium Tritici aestivi barley green composition according to claim 4, it is characterised in that in step c, disintegrating machine is provided with conjunction The part by weight of tungsten is 9~13% in golden steel tooth, the steel alloy tooth, and the part by weight of chromium is 3.8~4.9%, the weight of vanadium Ratio is 2%, and the part by weight of cobalt is 4~4.8%.
7. Caulis et Folium Tritici aestivi barley green composition according to claim 4, it is characterised in that in step d, filtering pressure machine, which is used, rolls band Completed with reference to roller;In step e, after the wheat slurry after separation is filtered by the reciprocating sieve of 120 mesh first, injection carries agitating function Buffer tank, then by buffer tank enter negative pressure of vacuum concentrate fill, by 100-120 minute concentration, finally inject vacuum drier It is dried, obtains wheat seedling tender leaf extract powder.
8. Caulis et Folium Tritici aestivi barley green composition according to claim 1, it is characterised in that the natural xylo-oligosaccharide is from corn Extract and obtain in core.
9. a kind of preparation process of Caulis et Folium Tritici aestivi barley green composition as claimed in claim 1, it is characterised in that wheat seedling wheat is green The processing method that tablet is made in promotor composition uses dry method mixing and granulation, then tabletting.
10. the preparation process of Caulis et Folium Tritici aestivi barley green composition according to claim 9, it is characterised in that dry method batch mixing system The workshop condition temperature of grain is 16~20 DEG C, and humidity is 15~20%.;Tabletting workshop condition temperature is 18~22 DEG C, and humidity is 18~25%.
CN201710264761.1A 2017-04-21 2017-04-21 Caulis et Folium Tritici aestivi barley green composition and its preparation process Pending CN107212403A (en)

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Publication number Priority date Publication date Assignee Title
CN109953335A (en) * 2017-12-26 2019-07-02 杭州博可生物科技股份有限公司 The new application of Barley Greeg and its alimentation composition with probiotics

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CN1584026A (en) * 2004-06-01 2005-02-23 中国农业大学 Production of oligomeric xylose and special immobilized xylanase therefor
CN101012466A (en) * 2007-02-09 2007-08-08 河南工业大学 Method for preparing low-polyxylose by microwave treatment corn core enzymatical process
CN105211858A (en) * 2015-10-12 2016-01-06 兴化市绿禾食品有限公司 One has the full powder of bioactive Barley Greeg and production technology thereof

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CN1243747A (en) * 1997-08-15 2000-02-09 北京建昊高科技股份有限公司 Growth-promoting composition for bacteria useful to microecology of intestine
CN1403591A (en) * 2001-09-05 2003-03-19 中国农业大学 Prepn of oligoxylose
CN1584026A (en) * 2004-06-01 2005-02-23 中国农业大学 Production of oligomeric xylose and special immobilized xylanase therefor
CN101012466A (en) * 2007-02-09 2007-08-08 河南工业大学 Method for preparing low-polyxylose by microwave treatment corn core enzymatical process
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* Cited by examiner, † Cited by third party
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CN109953335A (en) * 2017-12-26 2019-07-02 杭州博可生物科技股份有限公司 The new application of Barley Greeg and its alimentation composition with probiotics

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