CN107162433A - A kind of glassware etching liquid and its engraving method - Google Patents
A kind of glassware etching liquid and its engraving method Download PDFInfo
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- CN107162433A CN107162433A CN201710444551.0A CN201710444551A CN107162433A CN 107162433 A CN107162433 A CN 107162433A CN 201710444551 A CN201710444551 A CN 201710444551A CN 107162433 A CN107162433 A CN 107162433A
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- glassware
- etching liquid
- acid
- etching
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
Abstract
The invention discloses a kind of glassware etching liquid and its engraving method, including following raw material by weight：30 50 parts of 10 20 parts of ammonium sulfate, 10 20 parts of ammonium acid fluoride, 6 12 parts of potassium sulfate, 5 15 parts of trifluoromethane sulfonic acid, 3 12 parts of four methene Alendronate of ethylene diamine, 2 10 parts of 1,2 ethionic acid, 18 parts of cerous nitrate ammonia, 6 12 parts of oxalic acid, 4 10 parts of sodium benzoate, 26 parts of triethanolamine, 28 parts of methyl benzotriazazole, 15 parts of oxidant, 15 parts of surfactant, 13 parts of complexing agent and water.Its engraving method is raw material first to be mixed into ageing etching liquid is made, and used in glass products organic solvent is cleaned and dried, then the one side that glassware is not required into etching is shielded, and is finally immersed in etching liquid glassware and is soaked, and is taken out cleaning, is dried.This kind of etching liquid is prepared simply, and excellent in stability, recoverable is with low cost, and its engraving method can make glassware obtain good antiglare effect, have the advantages that reliability and durability.
Description
Technical field
The invention belongs to glassware manufacture field, and in particular to a kind of glassware etching liquid and its engraving method.
Background technology
What the anti-dazzle glas sold on current domestic and international market was typically realized by two methods, one kind is to glass table
Face carries out plated film to realize, another to be realized by acid etching glass surface.The antiglare effect of plated film anti-dazzle glas compared with
It is good, but production cost is high, and plated film is easy to come off, and surface easily leaves cut etc., so as to influence transparency.General
Acid etching anti-dazzle glas is first to carry out frosting to glass surface, then glass frosting face is polished, although plated film can be overcome easy
Come off, the defect of the easy scratching in surface, but this production technology is relative complex, and the production cycle is long, and yield rate is low.
In order to improve acid etching anti-dazzle glas production technology, patent publication No. describes for CN101654330 Chinese patent
Anti-dazzle glass is processed with the anti-dazzle etching solution of the glass that composition is hydrofluoric acid, hydrochloric acid, ammonium acid fluoride, gum arabic powder and polyethylene glycol
The production technology of glass, although the simple production process, it is easy to operate, but gum arabic powder is expensive, and cost is higher, and by
In hydrochloric acid high volatility, etching solution stability is poor, is difficult to be recycled；Patent publication No. is special for CN101215097 China
Profit is described to be prepared with the anti-dazzle glas etching solution that composition is hydrochloric acid or sulfuric acid, ammonium acid fluoride, ammonium sulfate, calcirm-fluoride and potassium sulfate
The technique of anti-dazzle glas, also due to hydrochloric acid high volatility, etching solution stability is poor, is difficult to be recycled.
The content of the invention
For problems of the prior art, the invention provides a kind of glassware etching liquid and its engraving method,
This kind of etching liquid is prepared simply, and excellent in stability, recoverable is with low cost, and its engraving method can obtain glassware
Good antiglare effect, has the advantages that reliability and durability.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
A kind of glassware etching liquid, including following raw material by weight：10-20 parts of ammonium sulfate, ammonium acid fluoride 10-
20 parts, 6-12 parts of potassium sulfate, 5-15 parts of trifluoromethane sulfonic acid, 3-12 parts of four methene Alendronate of ethylene diamine, 1, the sulphur of 2- second two
Sour 2-10 parts, 1-8 parts of cerous nitrate ammonia, 6-12 parts of oxalic acid, 4-10 parts of sodium benzoate, 2-6 parts of triethanolamine, methyl benzotriazazole
30-50 parts of 2-8 parts, 1-5 parts of oxidant, 1-5 parts of surfactant, 1-3 parts of complexing agent and water.
Further, above-mentioned etching liquid includes following raw material by weight：12-18 parts of ammonium sulfate, ammonium acid fluoride
12-18 parts, 8-10 parts of potassium sulfate, 8-12 parts of trifluoromethane sulfonic acid, 6-9 parts of four methene Alendronate of ethylene diamine, 1,2- second two
5-7 parts of sulfonic acid, 3-5 parts of cerous nitrate ammonia, 8-10 parts of oxalic acid, 6-8 parts of sodium benzoate, 3-5 parts of triethanolamine, methyl benzotriazazole
35-45 parts of 4-6 parts, 2-4 parts of oxidant, 2-4 parts of surfactant, 1-2 parts of complexing agent and water.
Further, above-mentioned etching liquid includes following raw material by weight：15 parts of ammonium sulfate, ammonium acid fluoride 15
Part, 9 parts of potassium sulfate, 10 parts of trifluoromethane sulfonic acid, 8 parts of four methene Alendronate of ethylene diamine, 1,6 parts of 2- ethionic acids, nitric acid
4 parts of cerium ammonia, 9 parts of oxalic acid, 7 parts of sodium benzoate, 4 parts of triethanolamine, 5 parts of methyl benzotriazazole, 3 parts of oxidant, surface-active
40 parts of 3 parts of agent, 1.5 parts of complexing agent and water.
Preferably, the oxidant be hydrogen peroxide, Potassiumiodate, iron chloride or Peracetic acid in it is a kind of or a kind of with
On.
Preferably, the surfactant is AEO or acrylamide.
Preferably, the complexing agent is ethylenediamine tetra-acetic acid or polyhydroxy polyamines.
A kind of glassware engraving method, is followed the steps below：
(1) raw material is weighed by the glassware etching liquid weight, under the conditions of temperature is 42-48 DEG C, stirring
Uniformly, after ageing 12-16h, it is made into etching liquid；
(2) the used in glass products organic solvent of pre-etching is cleaned and carries out drying process；
(3) one side that cleaned glassware is not required into etching is shielded；
(4) glassware is immersed and 15-20min is soaked in the etching liquid prepared, take out used in glass products deionized water
Rinsing, drying.
Preferably, the organic solvent is counted including following component by weight：60-80 parts of absolute ethyl alcohol, isopropanol 15-
1-10 parts of 25 parts, 5-15 parts of acetone and butyl acetate.
Compared with prior art, the present invention has following beneficial effect：
(1) glassware etching liquid raw material sources of the invention are extensively, with low cost, prepare simple, not volatile, stabilization
Property it is excellent, can preserve stand-by for a long time, and this kind of etching liquid uses rear recoverable, reduces raw material output cost, reaches
Recycle the purpose for saving raw material；
(2) using the obtained etching liquid of the present invention and its engraving method, glassware can be made to obtain good antiglare effect, and
And with more reliability and the advantage of durability.
Embodiment
The embodiment of the present invention is further described with reference to embodiment, following examples are only used for more
Technical scheme is clearly demonstrated, and can not be limited the scope of the invention with this.
Embodiment 1
A kind of glassware etching liquid, weighs following raw material：Ammonium sulfate 10kg, ammonium acid fluoride 10kg, potassium sulfate 6kg, three
Methyl fluoride sulfonic acid 5kg, the methene Alendronate 3kg of ethylene diamine four, 1,2- ethionic acids 2kg, cerous nitrate ammonia 1kg, oxalic acid 6kg,
Sodium benzoate 4kg, triethanolamine 2kg, methyl benzotriazazole 2kg, oxidant 1kg, surfactant 1kg, complexing agent 1kg and
Water 30kg.
Wherein, above-mentioned oxidant uses Peracetic acid；Surfactant uses AEO；Complexing agent is adopted
Use ethylenediamine tetra-acetic acid.
A kind of glassware engraving method, is followed the steps below：
(1) raw material is weighed by the glassware etching liquid weight, under the conditions of temperature is 42 DEG C, stirring is equal
It is even, after ageing 12h, it is made into etching liquid；
(2) the used in glass products organic solvent of pre-etching is cleaned and carries out drying process；
(3) one side that cleaned glassware is not required into etching is shielded；
(4) glassware is immersed and 15min is soaked in the etching liquid prepared, take out the punching of used in glass products deionized water
Wash, dry the etching for completing glassware.
Above-mentioned organic solvent includes following component：Absolute ethyl alcohol 60kg, isopropanol 15kg, acetone 5kg and butyl acetate
1kg。
Embodiment 2
A kind of glassware etching liquid, weighs following raw material：Ammonium sulfate 12kg, ammonium acid fluoride 12kg, potassium sulfate 8kg, three
Methyl fluoride sulfonic acid 8kg, the methene Alendronate 6kg of ethylene diamine four, 1,2- ethionic acids 5kg, cerous nitrate ammonia 3kg, oxalic acid 8kg,
Sodium benzoate 6kg, triethanolamine 3kg, methyl benzotriazazole 4kg, oxidant 2kg, surfactant 2kg, complexing agent 1kg and
Water 35kg.
Wherein, above-mentioned oxidant uses two kinds of mixtures of hydrogen peroxide and Potassiumiodate, and both mass ratioes are 2:1；Table
Face activating agent uses acrylamide；Complexing agent uses polyhydroxy polyamines.
A kind of glassware engraving method, is followed the steps below：
(1) raw material is weighed by the glassware etching liquid weight, under the conditions of temperature is 43 DEG C, stirring is equal
It is even, after ageing 13h, it is made into etching liquid；
(2) the used in glass products organic solvent of pre-etching is cleaned and carries out drying process；
(3) one side that cleaned glassware is not required into etching is shielded；
(4) glassware is immersed and 16min is soaked in the etching liquid prepared, take out the punching of used in glass products deionized water
Wash, dry the etching for completing glassware.
Above-mentioned organic solvent includes following component：Absolute ethyl alcohol 65kg, isopropanol 18kg, acetone 8kg and butyl acetate
3kg。
Embodiment 3
A kind of glassware etching liquid, weighs following raw material：Ammonium sulfate 15kg, ammonium acid fluoride 15kg, potassium sulfate 9kg, three
Methyl fluoride sulfonic acid 10kg, the methene Alendronate 8kg of ethylene diamine four, 1,2- ethionic acids 6kg, cerous nitrate ammonia 4kg, oxalic acid 9kg,
Sodium benzoate 7kg, triethanolamine 4kg, methyl benzotriazazole 5kg, oxidant 3kg, surfactant 3kg, complexing agent 1.5kg
With water 40kg.
Wherein, above-mentioned oxidant uses hydrogen peroxide, three kinds of quality between mixture, and three of Potassiumiodate and iron chloride
Than for 3:1:1；Surfactant uses AEO；Complexing agent uses ethylenediamine tetra-acetic acid.
A kind of glassware engraving method, is followed the steps below：
(1) raw material is weighed by the glassware etching liquid weight, under the conditions of temperature is 45 DEG C, stirring is equal
It is even, after ageing 14h, it is made into etching liquid；
(2) the used in glass products organic solvent of pre-etching is cleaned and carries out drying process；
(3) one side that cleaned glassware is not required into etching is shielded；
(4) glassware is immersed and 18min is soaked in the etching liquid prepared, take out the punching of used in glass products deionized water
Wash, dry the etching for completing glassware.
Above-mentioned organic solvent includes following component：Absolute ethyl alcohol 70kg, isopropanol 20kg, acetone 10kg and butyl acetate
5kg。
Embodiment 4
A kind of glassware etching liquid, weighs following raw material：Ammonium sulfate 18kg, ammonium acid fluoride 18kg, potassium sulfate 10kg, three
Methyl fluoride sulfonic acid 12kg, the methene Alendronate 9kg of ethylene diamine four, 1,2- ethionic acids 7kg, cerous nitrate ammonia 5kg, oxalic acid
10kg, sodium benzoate 8kg, triethanolamine 5kg, methyl benzotriazazole 6kg, oxidant 4kg, surfactant 4kg, complexing agent
2kg and water 45kg.
Wherein, above-mentioned oxidant uses two kinds of mixtures of iron chloride and Peracetic acid, and mass ratio between the two is
1:2；Surfactant uses acrylamide；Complexing agent uses polyhydroxy polyamines.
A kind of glassware engraving method, is followed the steps below：
(1) raw material is weighed by the glassware etching liquid weight, under the conditions of temperature is 47 DEG C, stirring is equal
It is even, after ageing 15h, it is made into etching liquid；
(2) the used in glass products organic solvent of pre-etching is cleaned and carries out drying process；
(3) one side that cleaned glassware is not required into etching is shielded；
(4) glassware is immersed and 19min is soaked in the etching liquid prepared, take out the punching of used in glass products deionized water
Wash, dry the etching for completing glassware.
Above-mentioned organic solvent includes following component：Absolute ethyl alcohol 75kg, isopropanol 22kg, acetone 12kg and butyl acetate
8kg。
Embodiment 5
A kind of glassware etching liquid, weighs following raw material：Ammonium sulfate 20kg, ammonium acid fluoride 20kg, potassium sulfate 12kg, three
Methyl fluoride sulfonic acid 15kg, the methene Alendronate 12kg of ethylene diamine four, 1,2- ethionic acids 10kg, cerous nitrate ammonia 8kg, oxalic acid
12kg, sodium benzoate 10kg, triethanolamine 6kg, methyl benzotriazazole 8kg, oxidant 5kg, surfactant 5kg, complexing
Agent 3kg and water 50kg.
Wherein, above-mentioned oxidant uses hydrogen peroxide；Surfactant uses AEO；Complexing agent is used
Ethylenediamine tetra-acetic acid.
A kind of glassware engraving method, is followed the steps below：
(1) raw material is weighed by the glassware etching liquid weight, under the conditions of temperature is 48 DEG C, stirring is equal
It is even, after ageing 16h, it is made into etching liquid；
(2) the used in glass products organic solvent of pre-etching is cleaned and carries out drying process；
(3) one side that cleaned glassware is not required into etching is shielded；
(4) glassware is immersed and 20min is soaked in the etching liquid prepared, take out the punching of used in glass products deionized water
Wash, dry the etching for completing glassware.
Above-mentioned organic solvent includes following component：Absolute ethyl alcohol 80kg, isopropanol 25kg, acetone 15kg and butyl acetate
10kg。
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to foregoing reality
Apply example the present invention is described in detail, for those skilled in the art, it still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic.All essences in the present invention
God is with principle, and any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (8)
1. a kind of glassware etching liquid, it is characterised in that including following raw material by weight：10-20 parts of ammonium sulfate, fluorine
Change 10-20 parts of hydrogen ammonium, 6-12 parts of potassium sulfate, 5-15 parts of trifluoromethane sulfonic acid, 3-12 parts of four methene Alendronate of ethylene diamine, 1,
2-10 parts of 2- ethionic acids, 1-8 parts of cerous nitrate ammonia, 6-12 parts of oxalic acid, 4-10 parts of sodium benzoate, 2-6 parts of triethanolamine, methylbenzene
And 30-50 parts of 2-8 parts of triazole, 1-5 parts of oxidant, 1-5 parts of surfactant, 1-3 parts of complexing agent and water.
2. a kind of glassware etching liquid according to claim 1, it is characterised in that including following original by weight
Material：12-18 parts of ammonium sulfate, 12-18 parts of ammonium acid fluoride, 8-10 parts of potassium sulfate, 8-12 parts of trifluoromethane sulfonic acid, ethylene diamine four
6-9 parts of methylenephosphonic acid sodium, 1,5-7 parts of 2- ethionic acids, 3-5 parts of cerous nitrate ammonia, 8-10 parts of oxalic acid, 6-8 parts of sodium benzoate, three second
3-5 parts of hydramine, 4-6 parts of methyl benzotriazazole, 2-4 parts of oxidant, 2-4 parts of surfactant, 1-2 parts of complexing agent and water 35-
45 parts.
3. a kind of glassware etching liquid according to claim 2, it is characterised in that including following original by weight
Material：15 parts of ammonium sulfate, 15 parts of ammonium acid fluoride, 9 parts of potassium sulfate, 10 parts of trifluoromethane sulfonic acid, the methene Alendronate 8 of ethylene diamine four
Part, 1,6 parts of 2- ethionic acids, 4 parts of cerous nitrate ammonia, 9 parts of oxalic acid, 7 parts of sodium benzoate, 4 parts of triethanolamine, methyl benzotriazazole
40 parts of 5 parts, 3 parts of oxidant, 3 parts of surfactant, 1.5 parts of complexing agent and water.
4. a kind of glassware etching liquid according to claim 1, it is characterised in that the oxidant is hydrogen peroxide, iodine
It is one or more than one kinds of in sour potassium, iron chloride or Peracetic acid.
5. a kind of glassware etching liquid according to claim 1, it is characterised in that the surfactant is fatty alcohol
APEO or acrylamide.
6. a kind of glassware etching liquid according to claim 1, it is characterised in that the complexing agent is ethylenediamine tetrem
Acid or polyhydroxy polyamines.
7. a kind of glassware engraving method, it is characterised in that comprise the following steps：
(1) raw material is weighed by the glassware etching liquid weight, under the conditions of temperature is 42-48 DEG C, stirred,
It is aged after 12-16h, is made into etching liquid；
(2) the used in glass products organic solvent of pre-etching is cleaned and carries out drying process；
(3) one side that cleaned glassware is not required into etching is shielded；
(4) glassware is immersed and 15-20min is soaked in the etching liquid prepared, taking-up used in glass products deionized water rinsing,
Drying.
8. a kind of glassware engraving method according to claim 7, it is characterised in that the organic solvent is by weight
Number meter includes following component：1-10 parts of 60-80 parts of absolute ethyl alcohol, 15-25 parts of isopropanol, 5-15 parts of acetone and butyl acetate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710444551.0A CN107162433A (en) | 2017-06-13 | 2017-06-13 | A kind of glassware etching liquid and its engraving method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710444551.0A CN107162433A (en) | 2017-06-13 | 2017-06-13 | A kind of glassware etching liquid and its engraving method |
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| CN107162433A true CN107162433A (en) | 2017-09-15 |
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| CN201710444551.0A Withdrawn CN107162433A (en) | 2017-06-13 | 2017-06-13 | A kind of glassware etching liquid and its engraving method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108147674A (en) * | 2017-12-29 | 2018-06-12 | 安徽凤阳亚欧玻璃工艺品有限公司 | A kind of preparation method of glare proof glass |
| CN112521021A (en) * | 2020-12-08 | 2021-03-19 | 广东山之风环保科技有限公司 | Sodium-calcium glass frosting liquid and preparation method thereof |
| CN113087403A (en) * | 2021-03-31 | 2021-07-09 | 佛山犀马精细化工有限公司 | Forming process for glass substrate etching effect with fingerprint printing resistance, scraping resistance and wear resistance |
| CN113173710A (en) * | 2021-06-03 | 2021-07-27 | 江苏亿豪新材料科技有限公司 | Formula and etching process of etching liquid for glass product |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101215097A (en) * | 2008-01-03 | 2008-07-09 | 东华大学 | Formulation of anti-dazzle glass product etching liquid and etching technique |
| CN101531463A (en) * | 2009-04-01 | 2009-09-16 | 上海多林化工科技有限公司 | Aqueous glass frosting powder chemical composition and preparation method thereof |
| CN103194318A (en) * | 2013-04-28 | 2013-07-10 | 赵新凤 | Environment-friendly cleaning agent |
-
2017
- 2017-06-13 CN CN201710444551.0A patent/CN107162433A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101215097A (en) * | 2008-01-03 | 2008-07-09 | 东华大学 | Formulation of anti-dazzle glass product etching liquid and etching technique |
| CN101531463A (en) * | 2009-04-01 | 2009-09-16 | 上海多林化工科技有限公司 | Aqueous glass frosting powder chemical composition and preparation method thereof |
| CN103194318A (en) * | 2013-04-28 | 2013-07-10 | 赵新凤 | Environment-friendly cleaning agent |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108147674A (en) * | 2017-12-29 | 2018-06-12 | 安徽凤阳亚欧玻璃工艺品有限公司 | A kind of preparation method of glare proof glass |
| CN112521021A (en) * | 2020-12-08 | 2021-03-19 | 广东山之风环保科技有限公司 | Sodium-calcium glass frosting liquid and preparation method thereof |
| CN113087403A (en) * | 2021-03-31 | 2021-07-09 | 佛山犀马精细化工有限公司 | Forming process for glass substrate etching effect with fingerprint printing resistance, scraping resistance and wear resistance |
| CN113087403B (en) * | 2021-03-31 | 2023-07-21 | 佛山犀马精细化工有限公司 | Forming process for glass substrate with fingerprint resistance and scratch resistance and wear resistance |
| CN113173710A (en) * | 2021-06-03 | 2021-07-27 | 江苏亿豪新材料科技有限公司 | Formula and etching process of etching liquid for glass product |
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Application publication date: 20170915 |