CN108147674A - A kind of preparation method of glare proof glass - Google Patents
A kind of preparation method of glare proof glass Download PDFInfo
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- CN108147674A CN108147674A CN201711473942.1A CN201711473942A CN108147674A CN 108147674 A CN108147674 A CN 108147674A CN 201711473942 A CN201711473942 A CN 201711473942A CN 108147674 A CN108147674 A CN 108147674A
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- 239000011521 glass Substances 0.000 title claims abstract description 60
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 230000004313 glare Effects 0.000 title claims abstract description 17
- 238000005530 etching Methods 0.000 claims abstract description 29
- 239000007788 liquid Substances 0.000 claims abstract description 17
- 238000001035 drying Methods 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
- 239000008139 complexing agent Substances 0.000 claims description 11
- 229910017604 nitric acid Inorganic materials 0.000 claims description 11
- -1 nitric acid Rare-earth salts Chemical class 0.000 claims description 11
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 11
- 239000008367 deionised water Substances 0.000 claims description 10
- 229910021641 deionized water Inorganic materials 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- 239000007800 oxidant agent Substances 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 10
- 239000004094 surface-active agent Substances 0.000 claims description 8
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 6
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 claims description 6
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 claims description 6
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 claims description 6
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 6
- 239000000467 phytic acid Substances 0.000 claims description 6
- 235000002949 phytic acid Nutrition 0.000 claims description 6
- 229940068041 phytic acid Drugs 0.000 claims description 6
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 5
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 5
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 5
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 5
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 5
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 5
- 229940043237 diethanolamine Drugs 0.000 claims description 5
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 5
- 238000007654 immersion Methods 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 5
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical class [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims description 5
- 235000011151 potassium sulphates Nutrition 0.000 claims description 5
- 230000005855 radiation Effects 0.000 claims description 5
- NGDQQLAVJWUYSF-UHFFFAOYSA-N 4-methyl-2-phenyl-1,3-thiazole-5-sulfonyl chloride Chemical compound S1C(S(Cl)(=O)=O)=C(C)N=C1C1=CC=CC=C1 NGDQQLAVJWUYSF-UHFFFAOYSA-N 0.000 claims description 3
- HSJPMRKMPBAUAU-UHFFFAOYSA-N cerium(3+);trinitrate Chemical compound [Ce+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O HSJPMRKMPBAUAU-UHFFFAOYSA-N 0.000 claims description 3
- FYDKNKUEBJQCCN-UHFFFAOYSA-N lanthanum(3+);trinitrate Chemical compound [La+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O FYDKNKUEBJQCCN-UHFFFAOYSA-N 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- JLKDVMWYMMLWTI-UHFFFAOYSA-M potassium iodate Chemical compound [K+].[O-]I(=O)=O JLKDVMWYMMLWTI-UHFFFAOYSA-M 0.000 claims description 3
- 239000001230 potassium iodate Substances 0.000 claims description 3
- 229940093930 potassium iodate Drugs 0.000 claims description 3
- 235000006666 potassium iodate Nutrition 0.000 claims description 3
- JYTNGEWJAZCVAN-UHFFFAOYSA-N 2-hexadecylbenzenesulfonic acid;sodium Chemical compound [Na].CCCCCCCCCCCCCCCCC1=CC=CC=C1S(O)(=O)=O JYTNGEWJAZCVAN-UHFFFAOYSA-N 0.000 claims description 2
- 235000005979 Citrus limon Nutrition 0.000 claims description 2
- 244000131522 Citrus pyriformis Species 0.000 claims description 2
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 2
- 150000002191 fatty alcohols Chemical class 0.000 claims description 2
- 235000002906 tartaric acid Nutrition 0.000 claims description 2
- 239000011975 tartaric acid Substances 0.000 claims description 2
- 230000001795 light effect Effects 0.000 abstract description 3
- 239000002245 particle Substances 0.000 abstract description 3
- 238000003672 processing method Methods 0.000 abstract description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 235000015165 citric acid Nutrition 0.000 description 4
- 238000003756 stirring Methods 0.000 description 3
- 230000003213 activating effect Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- AOJJSUZBOXZQNB-VTZDEGQISA-N 4'-epidoxorubicin Chemical group O([C@H]1C[C@@](O)(CC=2C(O)=C3C(=O)C=4C=CC=C(C=4C(=O)C3=C(O)C=21)OC)C(=O)CO)[C@H]1C[C@H](N)[C@@H](O)[C@H](C)O1 AOJJSUZBOXZQNB-VTZDEGQISA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 125000000373 fatty alcohol group Chemical group 0.000 description 1
- DEQLTFPCJRGSHW-UHFFFAOYSA-N hexadecylbenzene Chemical compound CCCCCCCCCCCCCCCCC1=CC=CC=C1 DEQLTFPCJRGSHW-UHFFFAOYSA-N 0.000 description 1
- SEOVTRFCIGRIMH-UHFFFAOYSA-N indole-3-acetic acid Chemical group C1=CC=C2C(CC(=O)O)=CNC2=C1 SEOVTRFCIGRIMH-UHFFFAOYSA-N 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 235000011007 phosphoric acid Nutrition 0.000 description 1
- 238000006748 scratching Methods 0.000 description 1
- 230000002393 scratching effect Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C03C23/0005—Other surface treatment of glass not in the form of fibres or filaments by irradiation
- C03C23/002—Other surface treatment of glass not in the form of fibres or filaments by irradiation by ultraviolet light
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Surface Treatment Of Glass (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The invention discloses a kind of preparation methods of glare proof glass, include the following steps：（1）Etching liquid preparation,（2）Glass pretreatment,（3）Etching processing.Processing method of the present invention effectively improves the quality of glass, improves the sophistication of glass surface particle, enhances transmitance and anti-dazzle light effect, efficiency, the high yield rate of processing, great popularizing value.
Description
Technical field
The invention belongs to glass processing processing technology fields, and in particular to a kind of preparation method of glare proof glass.
Background technology
The anti-dazzle glas sold on domestic and international market at present is generally realized by two methods：One kind is to glass table
Face carries out plated film to realize, another kind is realized by acid etch glass surface.The antiglare effect of plated film anti-dazzle glas is preferable,
But cost is higher, and plated film easily comes off, surface easily leaves cut etc., affects the transparency of glass.General acid etching
Anti-dazzle glas is first to carry out surface frosting to glass, and then glass frosting face is polished, it is easily de- effectively to overcome plated film
Fall, the easy scratching in surface the defects of.But because existing glass etching processing method is relatively simple, lead to the effect of processing not
It is good, it is inefficient, further improvement is needed to handle.
Invention content
The purpose of the present invention is being directed to the problem of existing, a kind of preparation method of glare proof glass is provided.
The present invention is achieved by the following technical solutions：
A kind of preparation method of glare proof glass, includes the following steps：
（1）Etching liquid is prepared：
A. it is spare to weigh following raw materials according by corresponding parts by weight：16 ~ 19 parts of sulfuric acid, 5 ~ 8 parts of phosphoric acid, 4 ~ 6 parts of phytic acid, 3 ~ 5 portions of lemons
Acid, 2 ~ 4 parts of tartaric acid, 6 ~ 9 parts of ammonium sulfate, 5 ~ 8 parts of potassium sulfates, 3 ~ 5 parts of diethanol amine, 3 ~ 6 parts of calcirm-fluoride, 1 ~ 1.5 part of nitric acid
Rare-earth salts, 2 ~ 3 parts of oxidants, 3 ~ 5 parts of surfactants, 1 ~ 2 part of complexing agent, 65 ~ 70 parts of water；
B. all raw materials that a weighed will be operated to be put into agitator tank jointly, stirred with 2000 ~ 2300 revs/min of rotating speed
Processing 1 ~ 1.5h after take out etching liquid is spare；
（2）Glass pre-processes：
A. one around of glass sparge for processing first being treated with deionized water is managed, spare after then drying；
B. the cleaned glass of a will be operated and do not need to the one side etched shielding, be then placed in ultraviolet irradiation instrument
Radiation treatment is carried out, is taken out after the completion spare；
（3）Etching processing：
A. by step（2）Treated, and glass is immersed in step（1）In etching liquid obtained, taken out after 6 ~ 9min of immersion treatment standby
With；
B. operation a treated one arounds of glass sparge are managed with deionized water, is taken out after then drying.
Further, step（1）It is arbitrary in yttrium nitrate, lanthanum nitrate, cerous nitrate to operate the nitric acid rare earth salt described in a
It is a kind of.
Further, step（1）It is any one in hydrogen peroxide, Potassiumiodate, Peracetic acid to operate the oxidant described in a
Kind.
Further, step（1）The surfactant operated described in a is neopelex, cetyl benzene
Any one in sodium sulfonate, fatty alcohol polyoxyethylene ether.
Further, step（1）It is disodium ethylene diamine tetraacetate to operate the complexing agent described in a.
Further, step（2）The temperature for operating the drying process described in a is 65 ~ 70 DEG C.
Further, step（2）The power for operating the ultraviolet irradiation processing described in b is 600 ~ 700W, ultraviolet light
Wavelength is 290 ~ 310nm, when a length of 20 ~ 25min of processing.
Further, step（3）The temperature for operating the drying process described in b is 80 ~ 85 DEG C.
The present invention has the following advantages compared with prior art：
The present invention has carried out glass etching preparation method special Optimal improvements, wherein having prepared a kind of etching liquid, inside adds
After the sulfuric acid that adds, phosphoric acid, phytic acid, citric acid, winestone sour component are used in compounding, the effect and efficiency of etching are effectively guaranteed,
The use of the nitric acid rare earth salt cooperation complexing agent of addition improves anti-dazzle treatment effect, and glass is carried out again before etching processing
Pretreatment, has especially carried out ultraviolet irradiation processing, and treated, and glass surface activity is high, and respond is strong, enhance
The effect and efficiency of subsequent etching processing.Finally under the mating reaction of each step, processing method of the present invention effectively improves glass
The quality of glass improves the sophistication of glass surface particle, enhances transmitance and anti-dazzle light effect, the efficiency of processing, finished product
Rate is high, great popularizing value.
Specific embodiment
Embodiment 1
A kind of preparation method of glare proof glass, includes the following steps：
（1）Etching liquid is prepared：
A. it is spare to weigh following raw materials according by corresponding parts by weight：16 parts of sulfuric acid, 5 parts of phosphoric acid, 4 parts of phytic acid, 3 parts of citric acids, 2 parts of winestones
Acid, 6 parts of ammonium sulfate, 5 parts of potassium sulfates, 3 parts of diethanol amine, 3 parts of calcirm-fluoride, 1 portion of nitric acid rare earth salt, 2 parts of oxidants, 3 parts of surfaces
Activating agent, 1 part of complexing agent, 65 parts of water；
B. all raw materials that a weighed will be operated to be put into agitator tank jointly, with 2000 revs/min of rotating speed stir process 1h
After take out etching liquid is spare；
（2）Glass pre-processes：
A. one around of glass sparge for processing first being treated with deionized water is managed, spare after then drying；
B. the cleaned glass of a will be operated and do not need to the one side etched shielding, be then placed in ultraviolet irradiation instrument
Radiation treatment is carried out, is taken out after the completion spare；
（3）Etching processing：
A. by step（2）Treated, and glass is immersed in step（1）In etching liquid obtained, taken out after immersion treatment 6min standby
With；
B. operation a treated one arounds of glass sparge are managed with deionized water, is taken out after then drying.
Further, step（1）It is yttrium nitrate to operate the nitric acid rare earth salt described in a.
Further, step（1）It is hydrogen peroxide to operate the oxidant described in a.
Further, step（1）It is neopelex to operate the surfactant described in a.
Further, step（1）It is disodium ethylene diamine tetraacetate to operate the complexing agent described in a.
Further, step（2）The temperature for operating the drying process described in a is 65 DEG C.
Further, step（2）The power of the ultraviolet irradiation processing described in b is operated as 600W, the wavelength of ultraviolet light
For 290 ~ 295nm, when a length of 20min of processing.
Further, step（3）The temperature for operating the drying process described in b is 80 DEG C.
Embodiment 2
A kind of preparation method of glare proof glass, includes the following steps：
（1）Etching liquid is prepared：
A. it is spare to weigh following raw materials according by corresponding parts by weight：18 parts of sulfuric acid, 7 parts of phosphoric acid, 5 parts of phytic acid, 4 parts of citric acids, 3 parts of winestones
Acid, 8 parts of ammonium sulfate, 7 parts of potassium sulfates, 4 parts of diethanol amine, 5 parts of calcirm-fluoride, 1.2 portions of nitric acid rare earth salt, 2.5 parts of oxidants, 4 parts
Surfactant, 1.5 parts of complexing agents, 68 parts of water；
B. all raw materials that a weighed will be operated to be put into agitator tank jointly, with 2200 revs/min of rotating speed stir process
Taken out after 1.2h etching liquid is spare；
（2）Glass pre-processes：
A. one around of glass sparge for processing first being treated with deionized water is managed, spare after then drying；
B. the cleaned glass of a will be operated and do not need to the one side etched shielding, be then placed in ultraviolet irradiation instrument
Radiation treatment is carried out, is taken out after the completion spare；
（3）Etching processing：
A. by step（2）Treated, and glass is immersed in step（1）In etching liquid obtained, taken out after immersion treatment 8min standby
With；
B. operation a treated one arounds of glass sparge are managed with deionized water, is taken out after then drying.
Further, step（1）It is lanthanum nitrate to operate the nitric acid rare earth salt described in a.
Further, step（1）It is Potassiumiodate to operate the oxidant described in a.
Further, step（1）It is cetyl benzenesulfonic acid sodium to operate the surfactant described in a.
Further, step（1）It is disodium ethylene diamine tetraacetate to operate the complexing agent described in a.
Further, step（2）The temperature for operating the drying process described in a is 68 DEG C.
Further, step（2）The power of the ultraviolet irradiation processing described in b is operated as 650W, the wavelength of ultraviolet light
For 295 ~ 300nm, when a length of 23min of processing.
Further, step（3）The temperature for operating the drying process described in b is 82 DEG C.
Embodiment 3
A kind of preparation method of glare proof glass, includes the following steps：
（1）Etching liquid is prepared：
A. it is spare to weigh following raw materials according by corresponding parts by weight：19 parts of sulfuric acid, 8 parts of phosphoric acid, 6 parts of phytic acid, 5 parts of citric acids, 4 parts of winestones
Acid, 9 parts of ammonium sulfate, 8 parts of potassium sulfates, 5 parts of diethanol amine, 6 parts of calcirm-fluoride, 1.5 portions of nitric acid rare earth salt, 3 parts of oxidants, 5 parts of tables
Face activating agent, 2 parts of complexing agents, 70 parts of water；
B. all raw materials that a weighed will be operated to be put into agitator tank jointly, with 2300 revs/min of rotating speed stir process
Taken out after 1.5h etching liquid is spare；
（2）Glass pre-processes：
A. one around of glass sparge for processing first being treated with deionized water is managed, spare after then drying；
B. the cleaned glass of a will be operated and do not need to the one side etched shielding, be then placed in ultraviolet irradiation instrument
Radiation treatment is carried out, is taken out after the completion spare；
（3）Etching processing：
A. by step（2）Treated, and glass is immersed in step（1）In etching liquid obtained, taken out after immersion treatment 9min standby
With；
B. operation a treated one arounds of glass sparge are managed with deionized water, is taken out after then drying.
Further, step（1）It is cerous nitrate to operate the nitric acid rare earth salt described in a.
Further, step（1）It is Peracetic acid to operate the oxidant described in a.
Further, step（1）It is fatty alcohol polyoxyethylene ether to operate the surfactant described in a.
Further, step（1）It is disodium ethylene diamine tetraacetate to operate the complexing agent described in a.
Further, step（2）The temperature for operating the drying process described in a is 70 DEG C.
Further, step（2）The power of the ultraviolet irradiation processing described in b is operated as 700W, the wavelength of ultraviolet light
For 305 ~ 310nm, when a length of 25min of processing.
Further, step（3）The temperature for operating the drying process described in b is 85 DEG C.
The surface particles size of glass made from the method for the present invention is not more than 20 μm, and granularity is small, greater homogeneity.Actual measurement
The glass transmitance ranging from 80 ~ 90% of 4mm has good anti-dazzle light effect.
Claims (8)
1. a kind of preparation method of glare proof glass, which is characterized in that include the following steps：
（1）Etching liquid is prepared：
A. it is spare to weigh following raw materials according by corresponding parts by weight：16 ~ 19 parts of sulfuric acid, 5 ~ 8 parts of phosphoric acid, 4 ~ 6 parts of phytic acid, 3 ~ 5 portions of lemons
Acid, 2 ~ 4 parts of tartaric acid, 6 ~ 9 parts of ammonium sulfate, 5 ~ 8 parts of potassium sulfates, 3 ~ 5 parts of diethanol amine, 3 ~ 6 parts of calcirm-fluoride, 1 ~ 1.5 part of nitric acid
Rare-earth salts, 2 ~ 3 parts of oxidants, 3 ~ 5 parts of surfactants, 1 ~ 2 part of complexing agent, 65 ~ 70 parts of water；
B. all raw materials that a weighed will be operated to be put into agitator tank jointly, stirred with 2000 ~ 2300 revs/min of rotating speed
Processing 1 ~ 1.5h after take out etching liquid is spare；
（2）Glass pre-processes：
A. one around of glass sparge for processing first being treated with deionized water is managed, spare after then drying；
B. the cleaned glass of a will be operated and do not need to the one side etched shielding, be then placed in ultraviolet irradiation instrument
Radiation treatment is carried out, is taken out after the completion spare；
（3）Etching processing：
A. by step（2）Treated, and glass is immersed in step（1）In etching liquid obtained, taken out after 6 ~ 9min of immersion treatment standby
With；
B. operation a treated one arounds of glass sparge are managed with deionized water, is taken out after then drying.
A kind of 2. preparation method of glare proof glass according to claim 1, which is characterized in that step（1）Operate institute in a
The nitric acid rare earth salt stated is any one in yttrium nitrate, lanthanum nitrate, cerous nitrate.
A kind of 3. preparation method of glare proof glass according to claim 1, which is characterized in that step（1）Operate institute in a
The oxidant stated is any one in hydrogen peroxide, Potassiumiodate, Peracetic acid.
A kind of 4. preparation method of glare proof glass according to claim 1, which is characterized in that step（1）Operate institute in a
The surfactant stated is neopelex, any one in cetyl benzenesulfonic acid sodium, fatty alcohol polyoxyethylene ether
Kind.
A kind of 5. preparation method of glare proof glass according to claim 1, which is characterized in that step（1）Operate institute in a
The complexing agent stated is disodium ethylene diamine tetraacetate.
A kind of 6. preparation method of glare proof glass according to claim 1, which is characterized in that step（2）Operate institute in a
The temperature for the drying process stated is 65 ~ 70 DEG C.
A kind of 7. preparation method of glare proof glass according to claim 1, which is characterized in that step（2）Operate institute in b
For the power of ultraviolet irradiation processing stated for 600 ~ 700W, the wavelength of ultraviolet light is 290 ~ 310nm, processing when a length of 20 ~
25min。
A kind of 8. preparation method of glare proof glass according to claim 1, which is characterized in that step（3）Operate institute in b
The temperature for the drying process stated is 80 ~ 85 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711473942.1A CN108147674A (en) | 2017-12-29 | 2017-12-29 | A kind of preparation method of glare proof glass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711473942.1A CN108147674A (en) | 2017-12-29 | 2017-12-29 | A kind of preparation method of glare proof glass |
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| Publication Number | Publication Date |
|---|---|
| CN108147674A true CN108147674A (en) | 2018-06-12 |
Family
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|---|---|---|---|
| CN201711473942.1A Pending CN108147674A (en) | 2017-12-29 | 2017-12-29 | A kind of preparation method of glare proof glass |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110981207A (en) * | 2019-12-17 | 2020-04-10 | 安徽凤阳玻璃有限公司 | Preparation method of plate glass with anti-dazzle and anti-reflection functions |
Citations (7)
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|---|---|---|---|---|
| CN101215097A (en) * | 2008-01-03 | 2008-07-09 | 东华大学 | Formulation of anti-dazzle glass product etching liquid and etching technique |
| CN104609736A (en) * | 2015-02-11 | 2015-05-13 | 陕西科技大学 | Anti-dazzle liquid for glass, preparation method of anti-dazzle liquid and method for preparing anti-dazzle glass by using anti-dazzle liquid |
| CN104944790A (en) * | 2014-03-31 | 2015-09-30 | 东友精细化工有限公司 | Glass-reinforcing composition and method of manufacturing touchscreen glass using the same |
| CN105152542A (en) * | 2015-10-19 | 2015-12-16 | 上海光和光学制造股份有限公司 | Preparation method of anti-dazzle glass |
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