CN107137265A - A kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof - Google Patents

A kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof Download PDF

Info

Publication number
CN107137265A
CN107137265A CN201710285333.7A CN201710285333A CN107137265A CN 107137265 A CN107137265 A CN 107137265A CN 201710285333 A CN201710285333 A CN 201710285333A CN 107137265 A CN107137265 A CN 107137265A
Authority
CN
China
Prior art keywords
dragon fruit
parts
coagulant liquid
preparation
skin whitener
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710285333.7A
Other languages
Chinese (zh)
Inventor
陈君
苏远程
韦卓定
梁海平
罗丽丹
郑翱毅
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GUANGXI QINZHOU MASHI FOOD CO Ltd
Original Assignee
GUANGXI QINZHOU MASHI FOOD CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by GUANGXI QINZHOU MASHI FOOD CO Ltd filed Critical GUANGXI QINZHOU MASHI FOOD CO Ltd
Priority to CN201710285333.7A priority Critical patent/CN107137265A/en
Publication of CN107137265A publication Critical patent/CN107137265A/en
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof, comprise the following steps：1) raw material prepares：Prepare following raw material：8 parts of stearic acid, 1 part of single stearic acid glycerine lipoprotein, 3 parts of isopropyl palmitate fat, 8 parts of atoleine, 2 parts of olive oil, 2 parts of solid paraffin, 5 parts of glycerine, 1 part of Tween 80,0.5 part of essence, 0.5 part of Sang Pu LGP, 10 parts of dragon fruit bough coagulant liquid, 59 parts of deionized water；2) preparation of dragon fruit coagulant liquid；3) prepared by oil phase；4) prepared by aqueous phase；5) mix：By step 3) obtained material adds homogeneous reaction pot, and step 4 is added while stirring) obtained material, stirring mixing, cooling, homogeneous after finishing, continue to stir cooling, add step 2) obtained material, continues to stir cooling, discharging, ageing, through dispensing after the assay was approved.

Description

A kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof
Technical field
The invention belongs to skin protection cosmetics technical field, and in particular to a kind of skin whitener of addition dragon fruit coagulant liquid and its Preparation method.
Background technology
Skin whitener has the effect of skin care, can form thin film, and refrangible sunlight on the face, and can make face On color make-up make up evenly, it is more longlasting and difficult for drop-off.Skin whitener, skin cream, face cream, refer to for facial or body Play the white shape cosmetics of skin care effect.Thin film can be formed on skin by being coated in the face cream of face, prevent moisture of skin It is lost in, moisture needed for skin being supplemented rapidly makes skin full, so as to prevent the appearance of microgroove and dry line, effectively releived calm The skin that water shortage is dried.Help skin to keep moistening, maintain the preferable water balance of skin, make skin tender smooth.
Type, quantity and the distribution for the melanin that the colour of skin, hair color and the eye color of people is mainly synthesized with melanocyte It is relevant.Tyrosinase is the first step rate-limiting enzyme and key enzyme of B16 cell.Therefore, junket ammonia is all contained in most of whitening agents Sour enzyme inhibitor.Chromatophore containing 4-5% in the basal layer cell of human epidermal.The color of human skin is not depend on black Chromatophore quantity, but depending on quantity, size, distribution and the melanocyte degree of melanosome.
Dragon fruit (Latin literary fame：Hylocereus undulatus Britt), it is that Cactaceae gage belongs to succulent Fruit uses cultivar, integrates fruit, flowers, vegetables, health care, medicine.Research shows, dragon fruit is a kind of high microsteping, low Fat, the fruit of low sugar degree, in addition to carbohydrate, crude fibre, also containing unrighted acid, polyphenoils, Vc and cyanine Element even also contains the rare vegetable protein of general plant, and heavy metal poisoning has detoxication.Dragon fruit have hypotensive, The effect of reducing blood lipid, removing toxic substances, taste lung, beauty treatment, improving eyesight, also effective in cure to constipation and diabetes, the anthocyanidin that it is rich in has anti- Oxidation, Green Tea Extract, the effect of anti-aging, containing abundant water-soluble dietary fiber, with fat-reducing, hypoglycemic and ease constipation work With；The black seedlet of dragon fruit, containing unrighted acid and polyphenoils, with many health-care efficacies.
Containing abundant pectin in dragon fruit, prior art to the pectin processing method in dragon fruit or Dragonfruit Juice, Or extracting method has boiling water extraction process, classical acid formulation, ammonium oxalate extraction method, microwave assisting method, ultrasonic extraction etc..1) Boiling water extraction process is earliest, operates simplest method, is only capable of extracting the water soluble pectin in plant tissue, yield is low, production Cycle is long, and a variety of impurityes are contained in finished product, so general without the method in industrial production；2) acid extraction method is very conventional, day Right pectin is insoluble in water, but it has a characteristic to be exactly to be soluble in diluted acid, therefore the first step is just during acidity extraction pectin It is protopectin to be changed into the pectin for being dissolved in water using this characteristic, it is exactly to add a class material (ratio that the method, which extracts the-step, Such as say ethanol or part metals salts substances), enable pectin Precipitation, the method feature is exactly that technique is simple, and power consumption is few, Cost is cheap, and quality is more stable, because second step is introduced into a class material (lower-molecular substance, multivalence in some plant pericarps Metal ion and pigment), such material is still residued in pectin solution so that poor in terms of its gelling performance, color and luster, is passed The sour formulation of system, technological operation is easy, with low cost, but is readily incorporated impurity in alcohol precipitation pectin step so that pectin characteristic becomes Difference, although extraction pectin content is more, but extraction time length etc.；3) the extraction principle of ammonium oxalate extraction method causes non-for ammonium oxalate Water soluble pectin acid calcium becomes soluble, and calcium is removed in the form of calcium oxalate precipitation, can also use chelating agent calgon, make non- The dissolubility increase of water soluble pectin.Concrete operations are in 90 DEG C of processing by pericarp or pomace with 0.25% ammonium oxalate solution After 24h, produced after filtering according to the follow-up fourth skill of acid system, the pectin yield that this method is extracted extracts production than hydrochloric acid, sulfuric acid Amount is high, and product quality can also be up to state standards.It is small with corrosivity, pollute small, be a kind of more green extracting method, but It is the presence of activity time；4) microwave abstracting is to penetrate spe medium by frequency electromagnetic waves, finally reaches extract, Extract is because absorbing microwave energy temperature rapid increase, so that material internal pressure increases and ruptured, cytoplasm pectin exists It is dissolved at relatively low temperature in spe medium, the advantage of multistage microwave amplifier pectin：Microwave abstracting can greatly speed up tissue hydrolysis, And it is heated than more uniform, the backbone of pectin, reduction energy consumption, easily-controlled operation, reduction labor intensity, gelation will not be destroyed Can, color and luster and solubility property improve, with short production cycle, yield is relative to be improved, and alcohol consumption is reduced, have the disadvantage technique less into Ripe, firing rate is too fast, the more difficult control of temperature, when microwave condition (such as wavelength, power etc.) is different, causes product form each Different, microwave leakage can be damaged to organism；Microwave―assisted extraction, technological operation is easy to control, with short production cycle, gelation Can be good, but temperature hardly possible control, and large-scale industrial production can not be realized；5) ultrasonic extraction is because ultrasonic wave is in medium transmittance process In there is normal pressure and negative pressure, both alternate conversion.At ultrasonic wave ten only pressure when, to medium molecule produce extruding Effect, when ultrasonic wave is in negative pressure, medium molecule is mutually discrete, and cavitation is produced when alternating frequency increase, instant Liquid formation bubble, bubble volume increase, finally rupture, so that extract is loosely organized, to increase extract and extract solution Contact area, improves dissolving of the material into extract solution.Compared with traditional acidity extraction, the advantage of ultrasonic extraction is to carry Take the time short, yield is high, without heating, and the pectin of ultrasonic wave extraction is of light color, and ash content is low, purity is high, good product quality.Lack Point is that Study of operational conditions is still immature, and equipment control condition requires higher, to reach that industrialized requirement is also needed to further Process conditions are explored.Dragon fruit is applied into cosmetics has good market prospects.
The content of the invention
It is an object of the invention to provide a kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof, fire is made full use of The physical property and nutritional characteristic of imperial fruit, reduce the precipitation of gel, and the nutritional ingredient of dragon fruit is kept to the full extent.
The present invention is achieved by the following technical solution：
A kind of preparation method for the skin whitener for adding dragon fruit coagulant liquid, comprises the following steps：
1) raw material prepares：Prepare following raw material：8 parts of stearic acid, 1 part of single stearic acid glycerine lipoprotein, palmitic acid isopropyl 3 parts of fat, 8 parts of atoleine, 2 parts of olive oil, 2 parts of solid paraffin, 5 parts of glycerine, 1 part of Tween-80,0.5 part of essence, Sang Pu LGP 0.5 part, 10 parts of dragon fruit bough coagulant liquid, 59 parts of deionized water；
2) preparation of dragon fruit coagulant liquid：
1. dragon fruit bough is chosen；
1. 2. step obtained to dragon fruit bough cleaning, stripping, mashing；
2. 3. step obtained to material progress activated carbon decolorizing and obtains supernatant；
4. heating is decolourized：The supernatant that 3. step is obtained is incorporated into steam blasting tank, and pressure 3.5MPa keeps 3min, Abrupt release, ebuillition of heated to color fade, filtering obtains coagulant liquid standby；
3) prepared by oil phase：By stearic acid, single stearic acid glycerine lipoprotein, isopropyl palmitate fat, atoleine, olive oil, solid Paraffin, glycerine are added in oil phase ingredients pot, heating, are stirred；
4) prepared by aqueous phase：Tween-80, essence, Sang Pu LGP, deionized water are added in aqueous phase ingredients pot, heated, stirring Uniformly；
5) mix：By step 3) obtained material adds homogeneous reaction pot, and step 4 is added while stirring) obtained material, Stirring mixing, cooling, homogeneous after finishing continue to stir cooling, add step 2) obtained material, continue to stir cooling, discharging, Ageing, through dispensing after the assay was approved.
The present invention
Step 2) described in selection dragon fruit bough, preferably remove the branch that rots, have a stain or defect, such as small holes caused by worms, small The branch of scab spot, profile mechanical damage etc., the quality of branch directly affects the quality of coagulant liquid, and decayed portion will be cut out more A bit；
Step 2) described in cleaning, stripping, mashing, 1. step is preferably obtained to dragon fruit bough and pours into conveyer belt, it is defeated Bubble washer is sent to, scavenging period is short, it is cleaned to be air-dried afterwards with putting with washing, branch surface is then peelled off with pocket knife A tunic, be put into shredding machine and cut into pieces, mashing in hole diameter of sieve (perforated) plate 0.7-1.0 millimeter of beater is sent into by elevator；
Step 2) described in activated carbon decolorizing, 2. step is preferably obtained to material and is diluted with water 5 times, with 100 mesh filter clothes After filtering twice, the activated carbon for adding 1% (w/w) stirs, and is precipitated to clarification, filters 150 mesh filter clothes, takes supernatant；
Step 2) described in ebuillition of heated to color fade, filtering, preferably ebuillition of heated uses 200 mesh to color fade Filter-cloth filtering.
Step 3) described in heating, be preferably heated to 70-75 DEG C.
Step 4) described in heating, be preferably heated to 75 DEG C.
Step 5) described in mixing, preferably by step 3) obtained material adds homogeneous reaction pot, and step is added while stirring The rapid material 4) obtained, 70-75 DEG C of stirring, rotating speed 1500r/min mixes 15 minutes, is cooled to 60-65 DEG C, homogeneous 5 minutes, Rotating speed 1500r/min, continues to stir, rotating speed 1500r/min is cooled to after 40 DEG C, adds step 2) obtained material, continues to stir Mix, rotating speed 1500r/min, be cooled to 35 DEG C of dischargings, be aged 24 hours, through dispensing after the assay was approved.
Present invention additionally comprises the skin whitener of the addition dragon fruit coagulant liquid obtained using method made above, dragon fruit is added Branch extract (gel), is a kind of new and with anti-oxidant, whitening, the product of moisture-keeping function, belongs to oil-in-water (O/W), Lotion is fine and smooth, uniformity, pH4-8.5,40+1 DEG C of holding 24h, recovers after room temperature, no water-oil separating phenomenon；(- 8+2) DEG C is protected 24h is held, recovers preceding without obvious character difference with experiment after room temperature.
Compared with prior art, the invention has the advantages that：
1st, containing abundant pectin in dragon fruit bough, and pectin is used as a kind of natural polymer, prior art There are boiling water extraction process, classical acid formulation, oxalic acid to the pectin processing method or extracting method in dragon fruit or Dragonfruit Juice Ammonium extraction method, microwave―assisted extraction, ultrasonic extraction etc., above method all comes with some shortcomings.During processing, During particularly heating is decolourized, with the increase of concentration of pectin, the viscosity of dragon fruit bough material is also increased, pectin category In long-chain macromolecule material, intermolecular have a stronger intermolecular force, and hydrogen bond and hydrophobic effect incidence are big and add fluid The resistance of flowing, is integrally formed baroque polymer, causes viscosity increase, gel to separate out, while producing precipitation, influence is most The quality of finished product.The present invention is by steam blasting, and material by continuous warming, increases in HTHP, the environment of high-moisture Pressure and suddenly decompression, cooling, make the backbone of pectin be changed into the degree increase of short-chain structure, destroy intermolecular force, Reduce hydrogen bond and hydrophobic effect incidence and reduce the resistance of flow of fluid, prevent gel from separating out.
2nd, present invention applicant is had found by studying, can be because if slurries are directly come out to beater carries out steam blasting For mixing for water soluble pectin and water-insoluble pectin, causing the viscosity of dragon fruit bough material increases, and is formed on liquid level top layer Film, is unfavorable for the volatilization of moisture, can produce a large amount of supernatants and gel precipitation, cause active ingredient loss, final influenceization The whitening of cosmetic, moistening effect.
Embodiment
With embodiment, the invention will be further described below, but the invention is not limited in these embodiments.
Embodiment 1：
A kind of preparation method for the skin whitener for adding dragon fruit coagulant liquid, comprises the following steps：
1) raw material prepares：Prepare following raw material：8 parts of stearic acid, 1 part of single stearic acid glycerine lipoprotein, palmitic acid isopropyl 3 parts of fat, 8 parts of atoleine, 2 parts of olive oil, 2 parts of solid paraffin, 5 parts of glycerine, 1 part of Tween-80,0.5 part of essence, Sang Pu LGP 0.5 part, 10 parts of dragon fruit bough coagulant liquid, 59 parts of deionized water；
2) preparation of dragon fruit coagulant liquid：
1. dragon fruit bough is chosen：Remove the branch that rots, have a stain or defect, such as small holes caused by worms, small scab spot, profile machinery are damaged The branch of wound etc., the quality of branch directly affects the quality of coagulant liquid, and decayed portion will be cut out more；
2. 1. step is obtained to dragon fruit bough and pours into conveyer belt, be transported to bubble washer, scavenging period is short, with putting It is cleaned to be air-dried afterwards with washing, a tunic on branch surface is then peelled off with pocket knife, shredding machine is put into and cuts into pieces, pass through It is beaten in the beater of 0.7 millimeter of hole diameter of sieve (perforated) plate of elevator feeding；
3. 2. step is obtained to material and is diluted with water 5 times, with 100 mesh filter-cloth filterings twice after, add 1% (w/w) work Property charcoal stir, be precipitated to clarification, filter 150 mesh filter clothes, take supernatant；
4. heating is decolourized：The supernatant that 3. step is obtained is incorporated into steam blasting tank, and pressure 3.5MPa keeps 3min, Abrupt release, ebuillition of heated to color fade, with 200 mesh filter-cloth filterings, obtains coagulant liquid standby；
3) prepared by oil phase：By stearic acid, single stearic acid glycerine lipoprotein, isopropyl palmitate fat, atoleine, olive oil, solid Paraffin, glycerine are added in oil phase ingredients pot, are heated to 70 DEG C, are stirred；
4) prepared by aqueous phase：Tween-80, essence, Sang Pu LGP, deionized water are added in aqueous phase ingredients pot, 70 are heated to DEG C, stir；
5) mix：By step 3) obtained material adds homogeneous reaction pot, and step 4 is added while stirring) obtained material, 70-75 DEG C of stirring, rotating speed 1500r/min mixes 15 minutes, is cooled to 60-65 DEG C, homogeneous 5 minutes, rotating speed 1500r/min, after Continuous stirring, rotating speed 1500r/min is cooled to after 40 DEG C, adds step 2) obtained material, continues to stir, rotating speed 1500r/ Min, is cooled to 35 DEG C of dischargings, is aged 24 hours, through dispensing after the assay was approved.
Embodiment 2：
A kind of preparation method for the skin whitener for adding dragon fruit coagulant liquid, comprises the following steps：
1) raw material prepares：Prepare following raw material：8 parts of stearic acid, 1 part of single stearic acid glycerine lipoprotein, palmitic acid isopropyl 3 parts of fat, 8 parts of atoleine, 2 parts of olive oil, 2 parts of solid paraffin, 5 parts of glycerine, 1 part of Tween-80,0.5 part of essence, Sang Pu LGP 0.5 part, 10 parts of dragon fruit bough coagulant liquid, 59 parts of deionized water；
2) preparation of dragon fruit coagulant liquid：
1. dragon fruit bough is chosen：Remove the branch that rots, have a stain or defect, such as small holes caused by worms, small scab spot, profile machinery are damaged The branch of wound etc., the quality of branch directly affects the quality of coagulant liquid, and decayed portion will be cut out more；
2. 1. step is obtained to dragon fruit bough and pours into conveyer belt, be transported to bubble washer, scavenging period is short, with putting It is cleaned to be air-dried afterwards with washing, a tunic on branch surface is then peelled off with pocket knife, shredding machine is put into and cuts into pieces, pass through It is beaten in the beater of 1.0 millimeters of hole diameter of sieve (perforated) plate of elevator feeding；
3. 2. step is obtained to material and is diluted with water 5 times, with 100 mesh filter-cloth filterings twice after, add 1% (w/w) work Property charcoal stir, be precipitated to clarification, filter 150 mesh filter clothes, take supernatant；
4. heating is decolourized：The supernatant that 3. step is obtained is incorporated into steam blasting tank, and pressure 3.5MPa keeps 3min, Abrupt release, ebuillition of heated to color fade, with 200 mesh filter-cloth filterings, obtains coagulant liquid standby；
3) prepared by oil phase：By stearic acid, single stearic acid glycerine lipoprotein, isopropyl palmitate fat, atoleine, olive oil, solid Paraffin, glycerine are added in oil phase ingredients pot, are heated to 72 DEG C, are stirred；
4) prepared by aqueous phase：Tween-80, essence, Sang Pu LGP, deionized water are added in aqueous phase ingredients pot, 70 are heated to DEG C, stir；
5) mix：By step 3) obtained material adds homogeneous reaction pot, and step 4 is added while stirring) obtained material, 70-75 DEG C of stirring, rotating speed 1500r/min mixes 15 minutes, is cooled to 60-65 DEG C, homogeneous 5 minutes, rotating speed 1500r/min, after Continuous stirring, rotating speed 1500r/min is cooled to after 40 DEG C, adds step 2) obtained material, continues to stir, rotating speed 1500r/ Min, is cooled to 35 DEG C of dischargings, is aged 24 hours, through dispensing after the assay was approved.
Embodiment 3：
A kind of preparation method for the skin whitener for adding dragon fruit coagulant liquid, comprises the following steps：
1) raw material prepares：Prepare following raw material：8 parts of stearic acid, 1 part of single stearic acid glycerine lipoprotein, palmitic acid isopropyl 3 parts of fat, 8 parts of atoleine, 2 parts of olive oil, 2 parts of solid paraffin, 5 parts of glycerine, 1 part of Tween-80,0.5 part of essence, Sang Pu LGP 0.5 part, 10 parts of dragon fruit bough coagulant liquid, 59 parts of deionized water；
2) preparation of dragon fruit coagulant liquid：
1. dragon fruit bough is chosen：Remove the branch that rots, have a stain or defect, such as small holes caused by worms, small scab spot, profile machinery are damaged The branch of wound etc., the quality of branch directly affects the quality of coagulant liquid, and decayed portion will be cut out more；
2. 1. step is obtained to dragon fruit bough and pours into conveyer belt, be transported to bubble washer, scavenging period is short, with putting It is cleaned to be air-dried afterwards with washing, a tunic on branch surface is then peelled off with pocket knife, shredding machine is put into and cuts into pieces, pass through It is beaten in the beater of 0.7 millimeter of hole diameter of sieve (perforated) plate of elevator feeding；
3. 2. step is obtained to material and is diluted with water 5 times, with 100 mesh filter-cloth filterings twice after, add 1% (w/w) work Property charcoal stir, be precipitated to clarification, filter 150 mesh filter clothes, take supernatant；
4. heating is decolourized：The supernatant that 3. step is obtained is incorporated into steam blasting tank, and pressure 3.5MPa keeps 3min, Abrupt release, ebuillition of heated to color fade, with 200 mesh filter-cloth filterings, obtains coagulant liquid standby；
3) prepared by oil phase：By stearic acid, single stearic acid glycerine lipoprotein, isopropyl palmitate fat, atoleine, olive oil, solid Paraffin, glycerine are added in oil phase ingredients pot, are heated to 75 DEG C, are stirred；
4) prepared by aqueous phase：Tween-80, essence, Sang Pu LGP, deionized water are added in aqueous phase ingredients pot, 70 are heated to DEG C, stir；
5) mix：By step 3) obtained material adds homogeneous reaction pot, and step 4 is added while stirring) obtained material, 70-75 DEG C of stirring, rotating speed 1500r/min mixes 15 minutes, is cooled to 60-65 DEG C, homogeneous 5 minutes, rotating speed 1500r/min, after Continuous stirring, rotating speed 1500r/min is cooled to after 40 DEG C, adds step 2) obtained material, continues to stir, rotating speed 1500r/ Min, is cooled to 35 DEG C of dischargings, is aged 24 hours, through dispensing after the assay was approved.
Comparative example 1：
Step be the same as Example 3, the preparation of dragon fruit coagulant liquid is adopted with the following method：
1. dragon fruit bough is chosen：Remove the branch that rots, have a stain or defect, such as small holes caused by worms, small scab spot, profile machinery are damaged The branch of wound etc., the quality of branch directly affects the quality of coagulant liquid, and decayed portion will be cut out more；
2. 1. step is obtained to dragon fruit bough and pours into conveyer belt, be transported to bubble washer, scavenging period is short, with putting It is cleaned to be air-dried afterwards with washing, a tunic on branch surface is then peelled off with pocket knife, shredding machine is put into and cuts into pieces, pass through It is beaten in the beater of 0.7 millimeter of hole diameter of sieve (perforated) plate of elevator feeding；
3. 2. step is obtained to material and is diluted with water 5 times, with 100 mesh filter-cloth filterings twice after, add 1% (w/w) work Property charcoal stir, be precipitated to clarification, filter 150 mesh filter clothes, take supernatant；
4. heating is decolourized：The supernatant that 3. step is obtained, ebuillition of heated to color fade, with 200 mesh filter-cloth filterings, is obtained Coagulant liquid is standby.
Comparative example 2：
Step be the same as Example 3, the preparation of dragon fruit coagulant liquid is adopted with the following method：
1. dragon fruit bough is chosen：Remove the branch that rots, have a stain or defect, such as small holes caused by worms, small scab spot, profile machinery are damaged The branch of wound etc., the quality of branch directly affects the quality of coagulant liquid, and decayed portion will be cut out more；
2. 1. step is obtained to dragon fruit bough and pours into conveyer belt, be transported to bubble washer, scavenging period is short, with putting It is cleaned to be air-dried afterwards with washing, a tunic on branch surface is then peelled off with pocket knife, shredding machine is put into and cuts into pieces, pass through It is beaten in the beater of 0.7 millimeter of hole diameter of sieve (perforated) plate of elevator feeding, is incorporated into steam blasting tank, pressure 3.5MPa keeps 3min, Abrupt release；
3. 2. step is obtained to material and is diluted with water 5 times, with 100 mesh filter-cloth filterings twice after, add 1% (w/w) work Property charcoal stir, be precipitated to clarification, filter 150 mesh filter clothes, take supernatant；
4. heating is decolourized：The supernatant that 3. step is obtained, ebuillition of heated to color fade, with 200 mesh filter-cloth filterings, is obtained Coagulant liquid is standby.
Comparative example 3：
Butanediol 6%, propane diols 5%, glycerine 5%, yeast extract 5%, caprylic/capric triglyceride 3%, spermaceti are hard Lipidol/cetearyl glucoside 2.5%, ring five dimethyl silicone polymer/cyclohexasiloxane 2%, dimethyl silicone polymer 2%th, cetostearyl alcohol 1.2%, stearine/PEG-100 stearates 1.2%%, Laurocapram 1%%, poly- third Acrylamide/C13-14 isoparaffins/laureth -70.7%, tocopherol 0.5%, Phenoxyethanol 0.45%, 12_ hexylene glycols 0.3%th, licoflavone 0.2%, xanthans 0.1%%, Butylated Hydroxytoluene 0.05%, Sodium Hyaluronate 0.02%, surplus for go from Sub- water.
Experimentation：
1st, replenishing water and preserving moisture effect assessment
According to cosmetic composition moisture absorption, the difference of performance of keeping humidity, different moisturizing agent molecule to the active force of hydrone not Together, moisture is absorbed different with the ability of moisture is kept.Oil content has sealing process to moisture, can prevent scattering and disappearing for moisture.Moisture absorption is made It is firmly big, it is strong to water molecules power, absorb and keep the amount of moisture also than larger, closure is good, moisture loss It is few.The biomaterial of cuticula, epidermis etc. is imitated using adhesive tape, cosmetics are coated with adhesive tape, answering for actual cosmetics is simulated Use situation.It is of poor quality before and after weighing sample placement after certain time under conditions of constant temperature and humidity, obtain the damage of sample size Lose, the effect of moisturizing ingredient moisturizing can be calculated.By contrast, product made from assay embodiment 3 and comparative example 1-3 Replenishing water and preserving moisture effect.
Experiment material
Some pieces of the clean glass plates of 7.5X7.5cm, 3M adhesive plasters, 50-500 μ L liquid-transfering guns, assay balance, potassium acetate saturation is molten Liquid relative humidity about 60%, a ten thousandth balance.
Experimental method and testing procedure
(1) 6 pieces of glass plate weight (M for posting 3M adhesive plasters are weighed0), record respectively, 3 pieces are blank control, and 3 pieces are sample Experiment.
(2) take 200 μ L samples to be added dropwise on the glass plate for posting 3M adhesive plasters with liquid-transfering gun, the weight is weighed with assay balance (M1) (being accurate to 0.OOOlg), sample is smoothened, glass plate is put into the drier of the constant humidity of requirement, is repeated 3 times.Will Remaining 3 pieces of blank control glass plate is put into the drier of constant humidity together.
(3) after 4h, 8h is placed, glass plate is taken out, the glass plate weight (M is weighed2), test its moisturizing rate and relatively wet The drier of constant humidity is immediately placed into after degree rate, weighing.
(4) points for attention of this experiment：Smear as far as possible uniform during sample, it is impossible to have carry-over on applicator.Will Sample, which takes out, to be weighed and is put into, and a drier control is within 15min, average 1 piece of glass plate 1min.Control time is Due to sample, exposed to external environment, its moisture loss is very fast, can have a strong impact on test result.Glass plate is inverted immediately after taking out The container in balance is also upside down on preprepared blank glass plate, during weighing.
(5) moisturizing rate calculation formula：
Moisturizing rate=(M2-M0)/(M1-M0) X100%
M0：Hollow plate quality/g
M1：Glass sheet quality/g after sample-adding
M2：Quality/g after some hours is placed in drier
Test its relative humidity be 60% when 4h and 8h in moisturizing rate.
Experimental result
As a result show that embodiment effect is substantially better than comparative example.
2nd, whitening anti-wrinkling measure of merit
Object on probation：Skin whitener prepared by each embodiment tries out the women 50 that object is age 25-35 Sui.
Application method：Usage cycles are 2 months, take after daily morning and evening face cleaning and are uniformly applied to face in right amount, are gently massaged into Absorb.
Experimental result
As a result show that embodiment effect is substantially better than comparative example.

Claims (10)

1. a kind of preparation method for the skin whitener for adding dragon fruit coagulant liquid, it is characterised in that comprise the following steps：
1) raw material prepares：Prepare following raw material：8 parts of stearic acid, 1 part of single stearic acid glycerine lipoprotein, isopropyl palmitate fat 3 Part, 8 parts of atoleine, 2 parts of olive oil, 2 parts of solid paraffin, 5 parts of glycerine, 1 part of Tween-80,0.5 part of essence, Sang Pu LGP 0.5 part, 10 parts of dragon fruit bough coagulant liquid, 59 parts of deionized water；
2) preparation of dragon fruit coagulant liquid：
1. dragon fruit bough is chosen；
1. 2. step obtained to dragon fruit bough cleaning, stripping, mashing；
2. 3. step obtained to material progress activated carbon decolorizing and obtains supernatant；
4. heating is decolourized：The supernatant that 3. step is obtained is incorporated into steam blasting tank, and pressure 3.5MPa keeps 3min, moment Release, ebuillition of heated to color fade, filtering obtains coagulant liquid standby；
3) prepared by oil phase：By stearic acid, single stearic acid glycerine lipoprotein, isopropyl palmitate fat, atoleine, olive oil, solid paraffin, Glycerine is added in oil phase ingredients pot, heating, is stirred；
4) prepared by aqueous phase：Tween-80, essence, Sang Pu LGP, deionized water are added in aqueous phase ingredients pot, heating stirs；
5) mix：By step 3) obtained material adds homogeneous reaction pot, and step 4 is added while stirring) obtained material, stirring Mixing, cooling, homogeneous after finishing continue to stir cooling, add step 2) obtained material, continue to stir cooling, discharging is old Change, through dispensing after the assay was approved.
2. a kind of preparation method of skin whitener for adding dragon fruit coagulant liquid according to claim 1, it is characterised in that：Step It is rapid 2) described in selection dragon fruit bough, be remove rot branch, have a stain or defect, such as small holes caused by worms, small scab spot, profile machine The branch of tool damage etc..
3. a kind of preparation method of skin whitener for adding dragon fruit coagulant liquid according to claim 1, it is characterised in that：Step It is rapid 2) described in mashing separation, be that cleaned fruit by elevator is entered millerator, by pericarp, pulp, fruit stone point From the pulp adjustment refractive power got is 9%.
4. a kind of preparation method of skin whitener for adding dragon fruit coagulant liquid according to claim 1, it is characterised in that：Step It is rapid 2) described in cleaning, stripping, mashing, be that 1. step is obtained to dragon fruit bough to pour into conveyer belt, be transported to bubble flushing Machine, with putting with washing, it is cleaned after air-dried, a tunic on branch surface is then peelled off with pocket knife, be put into shredding machine be cut into it is broken It is beaten in piece, the beater that hole diameter of sieve (perforated) plate 0.7-1.0 millimeters is sent into by elevator.
5. a kind of preparation method of skin whitener for adding dragon fruit coagulant liquid according to claim 1, it is characterised in that：Step It is rapid 2) described in activated carbon decolorizing, be that 2. step is obtained to material to be diluted with water 5 times, with 100 mesh filter-cloth filterings twice after, plus The activated carbon for entering 1% stirs, and is precipitated to clarification, filters 150 mesh filter clothes, takes supernatant.
6. a kind of preparation method of skin whitener for adding dragon fruit coagulant liquid according to claim 1, it is characterised in that：Step It is rapid 2) described in ebuillition of heated to color fade, filtering refers to ebuillition of heated to color fade, with 200 mesh filter-cloth filterings.
7. a kind of preparation method of skin whitener for adding dragon fruit coagulant liquid according to claim 1, it is characterised in that：Step It is rapid 3) described in heating, be heated to 70-75 DEG C.
8. a kind of preparation method of skin whitener for adding dragon fruit coagulant liquid according to claim 1, it is characterised in that：Step It is rapid 4) described in heating, be heated to 75 DEG C.
9. a kind of preparation method of skin whitener for adding dragon fruit coagulant liquid according to claim 1, it is characterised in that：Step It is rapid 5) described in mixing, be by step 3) obtained material adds homogeneous reaction pot, and step 4 is added while stirring) obtained thing Material, 70-75 DEG C of stirring, rotating speed 1500r/min mixes 15 minutes, is cooled to 60-65 DEG C, homogeneous 5 minutes, rotating speed 1500r/ Min, continues to stir, rotating speed 1500r/min is cooled to after 40 DEG C, adds step 2) obtained material, continues to stir, rotating speed 1500r/min, is cooled to 35 DEG C of dischargings, is aged 24 hours, through dispensing after the assay was approved.
10. the skin whitener for the addition dragon fruit coagulant liquid that the preparation method any one of claim 1-9 is obtained.
CN201710285333.7A 2017-04-27 2017-04-27 A kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof Pending CN107137265A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710285333.7A CN107137265A (en) 2017-04-27 2017-04-27 A kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710285333.7A CN107137265A (en) 2017-04-27 2017-04-27 A kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107137265A true CN107137265A (en) 2017-09-08

Family

ID=59775010

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710285333.7A Pending CN107137265A (en) 2017-04-27 2017-04-27 A kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof

Country Status (1)

Country Link
CN (1) CN107137265A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103417418A (en) * 2012-05-23 2013-12-04 孙莹 Pitaya essence whitening face cream
CN104473828A (en) * 2014-12-17 2015-04-01 广西壮族自治区农业科学院农产品加工研究所 Dragon fruit stem moisturizing lotion and preparation method thereof
CN105832578A (en) * 2016-04-12 2016-08-10 天津大学 Ginsenoside whitening and moisturizing cream and preparation method thereof
CN106071552A (en) * 2016-06-23 2016-11-09 曾凡跃 A kind of Pitaya Flower, Flos Rosae Rugosae composite beverage and preparation method thereof
CN106070431A (en) * 2016-06-23 2016-11-09 广西玛氏农业科技股份有限公司 A kind of Hylocereus undatus battercake and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103417418A (en) * 2012-05-23 2013-12-04 孙莹 Pitaya essence whitening face cream
CN104473828A (en) * 2014-12-17 2015-04-01 广西壮族自治区农业科学院农产品加工研究所 Dragon fruit stem moisturizing lotion and preparation method thereof
CN105832578A (en) * 2016-04-12 2016-08-10 天津大学 Ginsenoside whitening and moisturizing cream and preparation method thereof
CN106071552A (en) * 2016-06-23 2016-11-09 曾凡跃 A kind of Pitaya Flower, Flos Rosae Rugosae composite beverage and preparation method thereof
CN106070431A (en) * 2016-06-23 2016-11-09 广西玛氏农业科技股份有限公司 A kind of Hylocereus undatus battercake and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李鹏: "火龙果茎凝胶汁、多糖的初步研究", 《中国优秀硕士学位论文全文数据库 农业科技辑》 *

Similar Documents

Publication Publication Date Title
CN108451851B (en) A kind of long-acting replenishing water and preserving moisture facial mask and preparation method thereof
CN104473828B (en) A kind of dragon fruit stem end moisture retention liquid and preparation method thereof
CN105832622B (en) Tremella extract and its preparation method and application
CN110464682B (en) Peach gum composition, preparation method and application
CN105287340B (en) A kind of skin whitening, moisturizing eye cream and preparation method thereof
CN102274141B (en) Herba selaginellae revival moisturizing cream and preparation method thereof
CN105287292A (en) Whitening moisture-retention face cream and preparation method thereof
CN109330965B (en) A cosmetic composition containing plant extract
CN106580837A (en) Whitening and moisture supplementing mask
CN106727042A (en) A kind of tender white MASQUE APAISANT HYDRATANT containing Margarita extract
CN106902033A (en) A kind of scrub cosmetics and preparation method thereof
CN106619177A (en) Whitening and moisturizing cosmetic of white yak bone collagen protein peptide and preparation method of whitening and moisturizing cosmetic
CN106667845A (en) Mask with anti-photoaging effect
CN107412073A (en) A kind of composition containing peach gum hydrolysate and its preparation method and application
CN109535269A (en) A kind of preparation process and its application of dendrobium nobile micromolecular polysaccharide extracting solution
WO2018112857A1 (en) Moisturizing skin-care lotion
CN106726757B (en) Peony seed oil microemulsion gel and preparation method thereof
CN109125177A (en) A kind of petal water and preparation method thereof of anti-ageing firm skin
CN106913491A (en) Add skin whitener of dragon fruit coagulant liquid and preparation method thereof
CN108619028A (en) A kind of multiple-effect moisturizing daily renewal cream and preparation method thereof
CN107320357A (en) A kind of cosmetics containing polysaccharide
CN109512734A (en) Have effects that restore exterior-applied plant extract, cosmetics of elasticity of skin and gloss and preparation method thereof
CN107616938A (en) A kind of preparation method of agalloch eaglewood stoste
CN107137265A (en) A kind of skin whitener for adding dragon fruit coagulant liquid and preparation method thereof
CN113288823B (en) Pomelo peel pectin mask essence and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170908