CN107094775A - A kind of composition for preventing and treating agricultural disease and the spiral shell that goes out - Google Patents
A kind of composition for preventing and treating agricultural disease and the spiral shell that goes out Download PDFInfo
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- CN107094775A CN107094775A CN201710279431.XA CN201710279431A CN107094775A CN 107094775 A CN107094775 A CN 107094775A CN 201710279431 A CN201710279431 A CN 201710279431A CN 107094775 A CN107094775 A CN 107094775A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
- A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of composition for preventing and treating agricultural disease and the spiral shell that goes out.Its active component is benziothiazolinone and niclosamidum.The composition of the present invention carries out binary mixture with other pesticide species such as benziothiazolinone and niclosamidums.The preventing and treating done harm to applied to agricultural bacterial, can greatly improve bacterium prevention and control performance.Two groups of active ingredients show as synergistic effect in composition, it is allowed to amount of application reduction, more longlasting prevention effect, by a small number of applying only once or several times preferably control plant pest bacterium and broadening the possible administration interval time.
Description
Technical field
The invention belongs to agricultural protection technical field, and in particular to the combination of a kind of preventing and treating bacterial diseases of plants and the spiral shell that goes out
Thing.
Background technology
Rapid in plant disease development of drug resistance, chemical control is difficult.Trigger agricultural product to drop in production over a large area, cause serious warp
Ji loss.
The medicament that bacterial disease is prevented and treated in agricultural production is mainly copper agent.This kind of medicament resistance to the action of a drug is serious, preventive effect compared with
It is low, the formation of soil, water body and food is polluted in the environment, triggers environment and food safety risk.Other can be used for agriculture thin
Only a small amount of kind of bacterium treatment, by the dual limitation of resistance and preventive effect in actual production, popularizing area is smaller.
Benziothiazolinone, trade name：Bacterium is vertical to go out, english common name：Benzisothiazolinone, chemical name：1,2
Benzisothiazole-3-ketone, CAS 2634-33-5.It is main most as microbicide and fungus control agent at home and abroad,
For in anti-corrosion, paint, adhesive, detergent, fuel and paper-making industry.Agriculture plant protection industry also has some applications, main to use
In the preventing and treating of agriculture fungi.But, there is presently no report for the preventing and treating in terms of agriculture bacteriosis for benziothiazolinone.
Niclosamidum is that one kind kills eel agent, is also a kind of molluscacide, and it can influence the breathing and carbohydate metabolism activity of polypide,
A variety of snails, tapeworm, beef tapeworm, pork tapeworm and cercaria can be killed.It takes the photograph likely via polypide is suppressed to oxygen
Take to upset its breathing program.Pomacea canaliculata in being agriculturally mainly used in killing rice field.Simultaneously in public health preventing and treating side
Face, for killing snail.Niclosamidum can produce metabolic alterations rapidly in water, and action time is not long.It is also used for business and supported
Fish is half congealed, can fish is half congealed renew water before kill and remove undesired fish.Niclosamidum is very big for toxicity in fish, but in water
In only very short half-life period, using only needing to just be put into new fish in a few days after this piscicide.Due to niclosamidum
Toxicity to human body is big, studies compound synergic medicament, reduces it and use content, and being one is worth the new direction of research.
The content of the invention
It is an object of the invention to provide a preventing and treating agricultural disease and the composition for the spiral shell that goes out.
A kind of composition for preventing and treating agricultural disease and the spiral shell that goes out, its active component is benziothiazolinone and niclosamidum.
The composition also includes insecticides adjuvant, and the content of insecticides adjuvant is 2-98wt%；The insecticides adjuvant be solvent,
One or more in solid carrier, surfactant.
The solvent is toluene, and mixed xylenes thing, trisubstituted benzene, Dibutyl phthalate, phthalandione two is sad, thiacyclohexane,
Gasoline, ethylene glycol, methanol, ethanol, glycol monoethyl ether, the double methyl ethers of ethylene glycol, cyclohexanone, cyclopentanone, 1-METHYLPYRROLIDONE,
Dimethyl sulfoxide (DMSO), dimethylformamide, soybean oil.
The solid carrier be talcum powder, kaolin, montmorillonite, atlapulgite, float stone, bentonite, bentonite, calcite,
One or more in sand.
The surfactant be lignin sulfonic acid, naphthalene sulfonic acids, the alkali salt or amine salt of phenolsulfonic acid, sulfonate,
The condensation product of sulfate, aliphatic acid and sulphated fatty alcohol glycol ether, sulfonated naphthalene, naphthalene derivatives and formaldehyde, naphthalene or naphthalene sulfonic acids
With phenol and the condensation product of formaldehyde, NONIN HS 240, ethoxylated isooctyl-phenol, octyl phenol, nonyl phenol, alkyl virtue
Base polyglycol ether, tributyl benzene polyglycol ether, three stearyl phenyl polyglycol ethers, alkyl aryl polyether alcohol, ethyoxyl
Change castor oil, polyoxyethylene alkyl ether, ethylene oxide condensation product, ethoxylation polyoxypropylene, laurate polyglycol ether acetal,
Sorbitol ester, dodecyl benzyl dimethyl ammonium chloride, myristyl benzyl dimethyl ammonium chloride, hexadecyldimethyl benzyl ammonium benzyl
Ammonium chloride, dodecyl dimethyl benzyl ammonium bromide, tetradecyl dimethyl benzyl ammonium, hexadecyldimethyl benzyl ammonium benzyl bromide a-bromotoluene
Change the one or more in ammonium, lignin sulfite waste liquor, methylcellulose.
The plant pathogen is xanthomonas campestris, bacillus subtilis, Bacillus cereus, the raw yellow unit cell of tree
One kind or one in bacterium, blister spot Xanthomonas campestris, the graceful streptomycete of Ah fluorine, clavibacter, pseudomonad, carrot soft rot Erwinia
More than kind.
Above-mentioned composition preventing and treating corps diseases in purposes, particularly prevent and treat angular leaf spot of cucumber, muskmelon fruit blotch,
Bacterial blight of rice, Tomato mottle disease, soft rot of Chinese cabbage, wheat cecospora spot, cucurbita pepo soft rot, pepper bacterial tikka
Purposes in disease, potato scab, ring rot, balck shank, bacterial wilt and soft rot.
Suitable auxiliary agent can be solid or liquid, the material commonly used typically during formulation, such as mineral matter
Filler, Chemical Solvents, dispersant, wetting agent, solvent, adhesive, thickener, film forming agent, adhesive etc..
The application process of above-mentioned composition includes the aerial part or under ground portion for plant growth, including sprays, applies
Smear, soak seed, pouring root, seed dressing and soil disinfection.Above-mentioned composition only can be administered comprising active component, can also be with helping
Agent is mixed together.
Above-mentioned composition can be prepared into acceptable formulation on agricultural chemicals, such as wettable powder, suspending agent, water-dispersible grain
Agent, aqueous emulsion, soluble concentrate, pulvis, microcapsule suspending agent, emulsifiable concentrate, missible oil or microemulsion.According to the property of these compositions with
And the purpose and ambient conditions to be reached using composition, can select composition to spray, atomizing, dust, disseminate or
The method poured or the like is sprinkled to apply.
Compared with prior art, the present invention has the advantages that：The composition of the present invention is with benziothiazolinone and chlorine nitre willow
Other pesticide species such as amine, carry out binary mixture.The preventing and treating done harm to applied to agricultural bacterial, can greatly improve bacterium and prevent
Control performance.Two groups of active ingredients show as synergistic effect in composition, it is allowed to amount of application reduction, more longlasting prevention effect, logical
Cross only once or a small number of apply several times preferably controls plant pest bacterium and broaden the possible administration interval time.
The prevention effect having had to the disease that the bacterium for having produced resistance triggers.
Embodiment
The embodiment to the present invention is described in detail below, it is to be understood that protection scope of the present invention is not
Limited by embodiment.
The preventing and treating of the bacterial diseases such as the muskmelon Acidovorax Avenae Subsp. Citrulli of embodiment 1
Test method：Once sprayed at the initial stage of a disease, each 3 cells of processing, each square meter of cell 20.In before medicine and
10 days investigation statisticses incidences after medicine, each 5 grab sample of cell investigate the lesion area in whole strain per blade and account for leaf
The percentage of piece area, calculates disease index and prevention effect.
Soluble reagents are made into according to following ratio
Benziothiazolinone 20%；
Niclosamidum 0.2%；
Dispersant (lignin sulfonic acid) 10%；
Solvent (dimethylformamide) 87.8%；
The preparation being made into according to the above ratio, 1000-2000 times of dilution is sprayed, and is compareed with 21% benziothiazolinone（Niclosamidum
Without biocidal efficacies, omission is compareed herein）, to muskmelon Acidovorax Avenae Subsp. Citrulli, wheat cecospora spot, cucurbita pepo road soft rot and peppery
The preventive effect of green pepper bacterial leaf spot is more than 85%.Mixed to have obvious synergistic effect, experimental result is as shown in table 1：
Table 1
The preventing and treating of the Tomato mottle of embodiment 2 disease
Test method：Once sprayed at the initial stage of a disease, each 3 cells of processing, each square meter of cell 20.In before medicine and
10 days investigation statisticses incidences after medicine, each 5 grab sample of cell investigate the lesion area in whole strain per blade and account for leaf
The percentage of piece area, calculates disease index and prevention effect.
Soluble reagents are made into according to following ratio
Benziothiazolinone 10%；
Niclosamidum 10%；
Dispersant (lignin sulfonic acid) 10%；
Solvent (dimethylformamide) 70%；
The preparation being made into according to the above ratio, 1000-2000 times of dilution is sprayed, and is compareed with 20% benziothiazolinone（Niclosamidum
Without biocidal efficacies, omission is compareed herein）, to the sick preventive effect of Tomato mottle more than 95%, the preventive effect of control is only capable of reaching
46%。
The preventing and treating of the bacterial blight of rice of embodiment 3
Test method：Once sprayed at the initial stage of a disease, each 3 cells of processing, each square meter of cell 20.In before medicine and
10 days investigation statisticses incidences after medicine, each 5 grab sample of cell investigate the lesion area in whole strain per blade and account for leaf
The percentage of piece area, calculates disease index and prevention effect.
Soluble reagents are made into according to following ratio
Benziothiazolinone 0.1%；
Niclosamidum 10%；
Dispersant (lignin sulfonic acid) 10%；
Solvent (dimethylformamide) 70%；
The preparation being made into according to the above ratio, 50 times of dilution is sprayed, and is compareed with 11% benziothiazolinone（Niclosamidum does not have
Biocidal efficacies, omission is compareed herein）, to the bacterial leaf-blight preventive effect of paddy rice more than 65%, the preventive effect of control is only capable of reaching 26%.
The preventing and treating of the rice terrace Pomacea canaliculata of embodiment 4
Test method：Perfusion is carried out in Pomacea canaliculata rice terrace occurred frequently, each 3 cells of processing, each square meter of cell 200.In medicine
10 days investigation statisticses incidences after preceding and medicine, each 5 grab sample of cell, the percentage that investigation Pomacea canaliculata is killed,
Calculate disease index and prevention effect.
Soluble reagents are made into according to following ratio
Benziothiazolinone 2.5%；
Niclosamidum 0.5%；
Dispersant (lignin sulfonic acid) 10%；
Solvent (dimethylformamide) 70%；
The preparation being made into according to the above ratio, 1000 times of dilution is irrigated, and is compareed with 5% niclosamidum（Benziothiazolinone does not have
Spiral shell effect is killed, omission is compareed herein）, to Pomacea canaliculata preventive effect more than 68%, the preventive effect of control is only capable of reaching 22%.
The preventing and treating of the Tomato mottle of embodiment 5 disease
Test method：Once sprayed at the initial stage of a disease, each 3 cells of processing, each square meter of cell 20.In before medicine and
10 days investigation statisticses incidences after medicine, each 5 grab sample of cell investigate the lesion area in whole strain per blade and account for leaf
The percentage of piece area, calculates disease index and prevention effect.
Soluble reagents are made into according to following ratio
Benziothiazolinone 10%；
The chloro- 1,1,1- triethoxy ethanes 10% of 2-；
Dispersant (lignin sulfonic acid) 10%；
Solvent (dimethylformamide) 70%；
The preparation being made into according to the above ratio, 1000-2000 times of dilution is sprayed, and is compareed with 20% benziothiazolinone（2- chloro- 1,
1,1- triethoxy ethane does not have biocidal efficacies, and omission is compareed herein）, to the sick preventive effect of Tomato mottle more than 98%, control
Preventive effect be only capable of reaching 46%.
The preventing and treating of the bacterial blight of rice of embodiment 6
Test method：Once sprayed at the initial stage of a disease, each 3 cells of processing, each square meter of cell 20.In before medicine and
10 days investigation statisticses incidences after medicine, each 5 grab sample of cell investigate the lesion area in whole strain per blade and account for leaf
The percentage of piece area, calculates disease index and prevention effect.
Soluble reagents are made into according to following ratio
Benziothiazolinone 0.1%；
Nipecotic acid methyl esters 10%；
Dispersant (lignin sulfonic acid) 10%；
Solvent (dimethylformamide) 70%；
The preparation being made into according to the above ratio, 50 times of dilution is sprayed, and is compareed with 11% benziothiazolinone（Nipecotic acid methyl esters
Without biocidal efficacies, omission is compareed herein）, to the bacterial leaf-blight preventive effect of paddy rice more than 85%, the preventive effect of control is only capable of reaching
26%。
The preventing and treating of the rice terrace Pomacea canaliculata of embodiment 7
Test method：Perfusion is carried out in Pomacea canaliculata rice terrace occurred frequently, each 3 cells of processing, each square meter of cell 200.In medicine
10 days investigation statisticses incidences after preceding and medicine, each 5 grab sample of cell, the percentage that investigation Pomacea canaliculata is killed,
Calculate disease index and prevention effect.
Soluble reagents are made into according to following ratio
Foscarnet sodium hexahydrate 2.5%；
Niclosamidum 0.5%；
Dispersant (lignin sulfonic acid) 10%；
Solvent (dimethylformamide) 70%；
The preparation being made into according to the above ratio, 1000 times of dilution is irrigated, and is compareed with 5% niclosamidum（The water of Foscarnet sodium six
Compound is compareed herein without spiral shell effect, omission is killed）, to Pomacea canaliculata preventive effect more than 88%, the preventive effect of control is only capable of reaching 22%.
Disclosed above is only the specific embodiment of the present invention, and still, the present invention is not limited to this, any this area
What technical staff can think change should all fall into protection scope of the present invention.
Claims (6)
1. a kind of composition for preventing and treating agricultural disease and the spiral shell that goes out, it is characterised in that its active component is benziothiazolinone and niclosamidum.
2. the composition of preventing and treating agricultural disease according to claim 1 and the spiral shell that goes out, it is characterised in that the composition is also wrapped
Containing insecticides adjuvant, the content of insecticides adjuvant is 2-98wt%；The insecticides adjuvant is in solvent, solid carrier, surfactant
It is one or more kinds of.
3. the composition of preventing and treating agricultural disease according to claim 2 and the spiral shell that goes out, it is characterised in that the solvent is first
Benzene, mixed xylenes thing, trisubstituted benzene, Dibutyl phthalate, the octanoic acid of phthalandione two, thiacyclohexane, gasoline, ethylene glycol, methanol, second
Alcohol, glycol monoethyl ether, the double methyl ethers of ethylene glycol, cyclohexanone, cyclopentanone, 1-METHYLPYRROLIDONE, dimethyl sulfoxide (DMSO), dimethyl methyl
Acid amides, soybean oil.
4. preventing and treating agricultural disease according to claim 2 and the composition of spiral shell of going out, it is characterised in that the solid carrier is
One or more in talcum powder, kaolin, montmorillonite, atlapulgite, float stone, bentonite, bentonite, calcite, sand.
5. the composition of preventing and treating agricultural disease according to claim 2 and the spiral shell that goes out, it is characterised in that the surfactant
For lignin sulfonic acid, naphthalene sulfonic acids, the alkali salt or amine salt of phenolsulfonic acid, sulfonate, sulfate, aliphatic acid and sulphation fat
The condensation product of fat alcohol glycol ether, sulfonated naphthalene, naphthalene derivatives and formaldehyde, naphthalene or naphthalene sulfonic acids and phenol and the condensation product of formaldehyde, gather
Oxygen ethene octyl phenyl ether, ethoxylated isooctyl-phenol, octyl phenol, nonyl phenol, alkylaryl polyglycol ether, tributyl benzene gathers
Glycol ether, three stearyl phenyl polyglycol ethers, alkyl aryl polyether alcohol, ethoxylated castor oil, polyoxyethylene alkyl ether,
Ethylene oxide condensation product, ethoxylation polyoxypropylene, laurate polyglycol ether acetal, sorbitol ester, dodecyl dimethyl
Benzyl ammonium chloride, myristyl benzyl dimethyl ammonium chloride, cetalkonium chloride, dodecyl dimethyl benzyl
Base ammonium bromide, tetradecyl dimethyl benzyl ammonium, cetyl dimethyl benzyl ammonium bromide, lignin sulfite gives up
One or more in liquid, methylcellulose.
6. application of the composition in plant pathogen is killed described in claim 1, it is characterised in that the plant pathogen
For xanthomonas campestris, bacillus subtilis, Bacillus cereus sets raw Xanthomonas campestris, blister spot Xanthomonas campestris, the graceful chain of Ah fluorine
One or more in mould, clavibacter, pseudomonad, carrot soft rot Erwinia.
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Application publication date: 20170829 |