CN107033856A - A kind of environment-friendly type antifreeze coolant and preparation method thereof - Google Patents

A kind of environment-friendly type antifreeze coolant and preparation method thereof Download PDF

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Publication number
CN107033856A
CN107033856A CN201710361890.2A CN201710361890A CN107033856A CN 107033856 A CN107033856 A CN 107033856A CN 201710361890 A CN201710361890 A CN 201710361890A CN 107033856 A CN107033856 A CN 107033856A
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parts
coolant
environment
preparation
kathon
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汪建军
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K5/00Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
    • C09K5/20Antifreeze additives therefor, e.g. for radiator liquids

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Thermal Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)

Abstract

The invention discloses a kind of environment-friendly type antifreeze coolant and preparation method thereof, coolant component includes 10 20 parts of octanoic acid, 5 15 parts of citric acid, 8 18 parts of dimethicone, 3 10 parts of ternary polycarboxylic acids, 4 10 parts of triethanolamine, 5 10 parts of hydrogen peroxide, 5 12 parts of pentaerythrite, 3 10 parts of borax, 5 15 parts of isopropanol, 4 10 parts of Kathon CG, 30 50 parts of deionized water by weight, preparation technology of the present invention is simple, preparation process is environment friendly and pollution-free, obtained coolant good cooling results, cool time is long, while also having antifreezing effect.

Description

A kind of environment-friendly type antifreeze coolant and preparation method thereof
Technical field
The present invention relates to anti-icing fluid preparing technical field, specially a kind of environment-friendly type antifreeze coolant and preparation method thereof.
Background technology
Temperature in the manufacturing works of some large-scale apparatuses is that comparison is high, because these factories have substantial amounts of large-scale Machine, engine will produce substantial amounts of heat when these heavy-duty machines are operated so that the temperature rise in factory.So, I Cooling agent can be used to cool down engine, be minimized its temperature.But if engine temperature drops too low, some are necessary Heat can also be lost in therewith, and such engine cannot normal operation, the manufacturing schedule of Tuo Man factories;Moreover, coolant is once Freeze, it will damage engine.
The content of the invention
It is an object of the invention to provide a kind of environment-friendly type antifreeze coolant and preparation method thereof, to solve above-mentioned background skill The problem of being proposed in art.
To achieve the above object, the present invention provides following technical scheme:A kind of environment-friendly type antifreeze coolant, coolant component Include 10-20 parts of octanoic acid, 5-15 parts of citric acid, 8-18 parts of dimethicone, 3-10 parts of ternary polycarboxylic acids, three second by weight 4-10 parts of hydramine, 5-10 parts of hydrogen peroxide, 5-12 parts of pentaerythrite, 3-10 parts of borax, 5-15 parts of isopropanol, 4-10 parts of Kathon CG, 30-50 parts of deionized water.
It is preferred that, the preferred composition proportion of coolant is:15 parts of octanoic acid, 10 parts of citric acid, 13 parts of dimethicone, ternary 7 parts of polycarboxylic acids, 7 parts of triethanolamine, 8 parts of hydrogen peroxide, 9 parts of pentaerythrite, 7 parts of borax, 10 parts of isopropanol, 7 parts of Kathon CG, go from Sub- 40 parts of water.
It is preferred that, its preparation method comprises the following steps:
A, will octanoic acid, citric acid, dimethicone, ternary polycarboxylic acids and 1/2 deionized water mix after add stirring container in It is sufficiently stirred for, stir speed (S.S.) is 200 revs/min, and mixing time is 10min, standing obtains mixture A;
B, addition triethanolamine, hydrogen peroxide, pentaerythrite, borax, isopropanol, Kathon CG and 1/2 deionization in mixture A Water, adds after mixing and low-temperature heat is carried out in heating container, and heating-up temperature is 30 DEG C, and the heat time is 10min, is cooled to afterwards Room temperature, obtains anti-freeze cooling liquid.
Compared with prior art, the beneficial effects of the invention are as follows:Preparation technology of the present invention is simple, preparation process is environmentally friendly without dirt Dye, obtained coolant good cooling results, cool time is long, while also having antifreezing effect.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment Only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model that the present invention is protected Enclose.
The present invention provides following technical scheme:A kind of environment-friendly type antifreeze coolant, coolant component includes by weight Sad 10-20 parts, 5-15 parts of citric acid, 8-18 parts of dimethicone, 3-10 parts of ternary polycarboxylic acids, 4-10 parts of triethanolamine, mistake 5-10 parts of hydrogen oxide, 5-12 parts of pentaerythrite, 3-10 parts of borax, 5-15 parts of isopropanol, 4-10 parts of Kathon CG, deionized water 30-50 Part.
Embodiment one:
Coolant component includes 10 parts of octanoic acid, 5 parts of citric acid, 8 parts of dimethicone, 3 parts of ternary polycarboxylic acids, three by weight 4 parts of monoethanolamine, 5 parts of hydrogen peroxide, 5 parts of pentaerythrite, 3 parts of borax, 5 parts of isopropanol, 4 parts of Kathon CG, 30 parts of deionized water.
The preparation method of the present embodiment comprises the following steps:
A, will octanoic acid, citric acid, dimethicone, ternary polycarboxylic acids and 1/2 deionized water mix after add stirring container in It is sufficiently stirred for, stir speed (S.S.) is 200 revs/min, and mixing time is 10min, standing obtains mixture A;
B, addition triethanolamine, hydrogen peroxide, pentaerythrite, borax, isopropanol, Kathon CG and 1/2 deionization in mixture A Water, adds after mixing and low-temperature heat is carried out in heating container, and heating-up temperature is 30 DEG C, and the heat time is 10min, is cooled to afterwards Room temperature, obtains anti-freeze cooling liquid.
Embodiment two:
Coolant component includes 20 parts of octanoic acid, 15 parts of citric acid, 18 parts of dimethicone, ternary polycarboxylic acids 10 by weight Part, 10 parts of triethanolamine, 10 parts of hydrogen peroxide, 12 parts of pentaerythrite, 10 parts of borax, 15 parts of isopropanol, 10 parts of Kathon CG, deionization 50 parts of water.
The preparation method of the present embodiment comprises the following steps:
A, will octanoic acid, citric acid, dimethicone, ternary polycarboxylic acids and 1/2 deionized water mix after add stirring container in It is sufficiently stirred for, stir speed (S.S.) is 200 revs/min, and mixing time is 10min, standing obtains mixture A;
B, addition triethanolamine, hydrogen peroxide, pentaerythrite, borax, isopropanol, Kathon CG and 1/2 deionization in mixture A Water, adds after mixing and low-temperature heat is carried out in heating container, and heating-up temperature is 30 DEG C, and the heat time is 10min, is cooled to afterwards Room temperature, obtains anti-freeze cooling liquid.
Embodiment three:
Coolant component by weight include octanoic acid 12 parts, 6 parts of citric acid, 10 parts of dimethicone, 4 parts of ternary polycarboxylic acids, 5 parts of triethanolamine, 6 parts of hydrogen peroxide, 6 parts of pentaerythrite, 4 parts of borax, 6 parts of isopropanol, 5 parts of Kathon CG, 35 parts of deionized water.
The preparation method of the present embodiment comprises the following steps:
A, will octanoic acid, citric acid, dimethicone, ternary polycarboxylic acids and 1/2 deionized water mix after add stirring container in It is sufficiently stirred for, stir speed (S.S.) is 200 revs/min, and mixing time is 10min, standing obtains mixture A;
B, addition triethanolamine, hydrogen peroxide, pentaerythrite, borax, isopropanol, Kathon CG and 1/2 deionization in mixture A Water, adds after mixing and low-temperature heat is carried out in heating container, and heating-up temperature is 30 DEG C, and the heat time is 10min, is cooled to afterwards Room temperature, obtains anti-freeze cooling liquid.
Example IV:
Coolant component by weight include octanoic acid 18 parts, 13 parts of citric acid, 16 parts of dimethicone, 9 parts of ternary polycarboxylic acids, 9 parts of triethanolamine, 9 parts of hydrogen peroxide, 11 parts of pentaerythrite, 9 parts of borax, 13 parts of isopropanol, 9 parts of Kathon CG, 45 parts of deionized water.
The preparation method of the present embodiment comprises the following steps:
A, will octanoic acid, citric acid, dimethicone, ternary polycarboxylic acids and 1/2 deionized water mix after add stirring container in It is sufficiently stirred for, stir speed (S.S.) is 200 revs/min, and mixing time is 10min, standing obtains mixture A;
B, addition triethanolamine, hydrogen peroxide, pentaerythrite, borax, isopropanol, Kathon CG and 1/2 deionization in mixture A Water, adds after mixing and low-temperature heat is carried out in heating container, and heating-up temperature is 30 DEG C, and the heat time is 10min, is cooled to afterwards Room temperature, obtains anti-freeze cooling liquid.
Embodiment five:
Coolant component by weight include octanoic acid 15 parts, 10 parts of citric acid, 13 parts of dimethicone, 7 parts of ternary polycarboxylic acids, 7 parts of triethanolamine, 8 parts of hydrogen peroxide, 9 parts of pentaerythrite, 7 parts of borax, 10 parts of isopropanol, 7 parts of Kathon CG, 40 parts of deionized water.
The preparation method of the present embodiment comprises the following steps:
A, will octanoic acid, citric acid, dimethicone, ternary polycarboxylic acids and 1/2 deionized water mix after add stirring container in It is sufficiently stirred for, stir speed (S.S.) is 200 revs/min, and mixing time is 10min, standing obtains mixture A;
B, addition triethanolamine, hydrogen peroxide, pentaerythrite, borax, isopropanol, Kathon CG and 1/2 deionization in mixture A Water, adds after mixing and low-temperature heat is carried out in heating container, and heating-up temperature is 30 DEG C, and the heat time is 10min, is cooled to afterwards Room temperature, obtains anti-freeze cooling liquid.
Preparation technology of the present invention is simple, preparation process is environment friendly and pollution-free, obtained coolant good cooling results, cool time It is long, while also having antifreezing effect.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (3)

1. a kind of environment-friendly type antifreeze coolant, it is characterised in that:Coolant component includes 10-20 parts of octanoic acid, lemon by weight 5-15 parts of lemon acid, 8-18 parts of dimethicone, 3-10 parts of ternary polycarboxylic acids, 4-10 parts of triethanolamine, 5-10 parts of hydrogen peroxide, season Penta 5-12 parts of tetrol, 3-10 parts of borax, 5-15 parts of isopropanol, 4-10 parts of Kathon CG, 30-50 parts of deionized water.
2. a kind of environment-friendly type antifreeze coolant according to claim 1, it is characterised in that:The preferred composition proportion of coolant For:Octanoic acid 15 parts, 10 parts of citric acid, 13 parts of dimethicone, 7 parts of ternary polycarboxylic acids, 7 parts of triethanolamine, 8 parts of hydrogen peroxide, 9 parts of pentaerythrite, 7 parts of borax, 10 parts of isopropanol, 7 parts of Kathon CG, 40 parts of deionized water.
3. realize a kind of preparation method of environment-friendly type antifreeze coolant described in claim 1, it is characterised in that:Its preparation method Comprise the following steps:
A, will octanoic acid, citric acid, dimethicone, ternary polycarboxylic acids and 1/2 deionized water mix after add stirring container in It is sufficiently stirred for, stir speed (S.S.) is 200 revs/min, and mixing time is 10min, standing obtains mixture A;
B, addition triethanolamine, hydrogen peroxide, pentaerythrite, borax, isopropanol, Kathon CG and 1/2 deionization in mixture A Water, adds after mixing and low-temperature heat is carried out in heating container, and heating-up temperature is 30 DEG C, and the heat time is 10min, is cooled to afterwards Room temperature, obtains anti-freeze cooling liquid.
CN201710361890.2A 2017-05-22 2017-05-22 A kind of environment-friendly type antifreeze coolant and preparation method thereof Pending CN107033856A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102321456A (en) * 2011-07-27 2012-01-18 上海电力学院 Cooling liquid for automobile with all-aluminum engine and preparation method of cooling liquid
CN105482782A (en) * 2015-11-27 2016-04-13 蚌埠海明压铸机有限公司 Pitting-prevention engine liquid coolant
CN105670573A (en) * 2016-03-18 2016-06-15 杭州哈尔斯实业有限公司 Environment-friendly antifreezing anti-boiling heat conducting medium and application thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102321456A (en) * 2011-07-27 2012-01-18 上海电力学院 Cooling liquid for automobile with all-aluminum engine and preparation method of cooling liquid
CN105482782A (en) * 2015-11-27 2016-04-13 蚌埠海明压铸机有限公司 Pitting-prevention engine liquid coolant
CN105670573A (en) * 2016-03-18 2016-06-15 杭州哈尔斯实业有限公司 Environment-friendly antifreezing anti-boiling heat conducting medium and application thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
周艳梅等: "一种新型发动机冷却液缓蚀剂配方的研究", 《清洗世界》 *

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