CN107010918A - A kind of true mineral varnish of hydrophobic permeable type and preparation method thereof - Google Patents
A kind of true mineral varnish of hydrophobic permeable type and preparation method thereof Download PDFInfo
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- CN107010918A CN107010918A CN201710267986.2A CN201710267986A CN107010918A CN 107010918 A CN107010918 A CN 107010918A CN 201710267986 A CN201710267986 A CN 201710267986A CN 107010918 A CN107010918 A CN 107010918A
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- Prior art keywords
- parts
- mineral varnish
- true mineral
- permeable type
- hydrophobic permeable
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/54—Substitutes for natural stone, artistic materials or the like
- C04B2111/542—Artificial natural stone
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention provides a kind of true mineral varnish of hydrophobic permeable type, includes the raw material of following mass fraction：20 60 parts of 90 110 parts of natural siliceous sand, 10 13 parts of cataloid, 69 parts of pure acrylate emulsion, 0.9 1.5 parts of butyl glycol ether, 29 parts of antiseptic, 6 11 parts of silicone acrylic emulsion, 0.15 0.65 parts of sodium metasilicate, 39 parts of thixotropic agent, 8 19 parts of coalescents, 0.3 0.6 parts of calcium chloride powder, 0.5 3 parts of 5% magnesium chloride solution and water.Additionally provide a kind of preparation method of the true mineral varnish of hydrophobic permeable type.The present invention has the advantages and positive effects of：Water repellency is good, effectively improves the anti-whitening resistance and hardness of paint film；Good air permeability, can solve the hollowing and bubble problem of true mineral varnish coating surface；Initial stage, anti-cracking performance was good, and adhesion strength is high；Preparation technology is simple, suitable for industrialization.
Description
Technical field
The invention belongs to true mineral varnish research and development field, more particularly, to a kind of true mineral varnish of hydrophobic permeable type and preparation method thereof.
Background technology
In recent years, the progress of the coating technologies such as the lifting and emulsion synthesis of health of people environmental protection concept, true stone matter are given the credit to
Sense class coating occupies the larger market share in decoration of exterior wall protection field, gradually replaces stone material, ceramic tile, composited aluminum and plastic decking etc.
External wall decorative material.Compared to stone material, many advantages, such as true mineral varnish has lightweight, cheap, environment protection health, constructs convenient.
But compared to stone surface, true mineral varnish is relatively loose, water-white, the paint film disadvantage such as feel like jelly easily occurs after drenching with rain
Disease, influences attractive in appearance.On the other hand because exterior wall true stone paint film is thicker, it is relatively tight that aggregate surface is wrapped up film forming by polymer emulsion
It is close, cause its gas permeability substantially poorer than the flat emulsion paint that applies, cause exterior wall true stone paint facing coating hollowing and foaming easily occur
Problem.
The content of the invention
The problem to be solved in the present invention is to provide a kind of true mineral varnish of hydrophobic permeable type and preparation method thereof, can solve the problem that above-mentioned
Problem.
In order to solve the above technical problems, the technical solution adopted by the present invention is：A kind of true mineral varnish of hydrophobic permeable type, including such as
The raw material of lower mass fraction：
90-110 parts of natural siliceous sand, 10-13 parts of cataloid, 6-9 parts of pure acrylate emulsion, butyl glycol ether
0.9-1.5 parts, 2-9 parts of antiseptic, 6-11 parts of silicone acrylic emulsion, 0.15-0.65 parts of sodium metasilicate, 3-9 parts of thixotropic agent, coalescents 8-
20-60 parts of 19 parts, 0.3-0.6 parts of calcium chloride powder, 0.5-3 parts of 5% magnesium chloride solution and water.
It is preferred that, the thixotropic agent is polyamide wax and bentonitic mixture.
It is preferred that, described polyamide wax 1-3 parts, 2-6 parts of bentonite.
It is preferred that, the antiseptic is the mixture of chitin, horseradish and theaflavin.
It is preferred that, described chitin 1-5 parts, 0.3-1.5 parts of horseradish, 0.7-2.5 parts of theaflavin.
It is preferred that, the thixotropic agent is bentonite.
It is preferred that, the coalescents are alcohol ether esters.
It is preferred that, include the raw material of following mass fraction：100-110 parts of natural siliceous sand, cataloid 10-12
Part, 6-9 parts of pure acrylate emulsion, 1-1.5 parts of butyl glycol ether, 2-9 parts of antiseptic, 6-9 parts of silicone acrylic emulsion, sodium metasilicate
0.15-0.65 parts, 3-7 parts of thixotropic agent, 10-15 parts of coalescents, 0.3-0.6 parts of calcium chloride powder, 5% magnesium chloride solution 0.5-
3 parts and 20-60 parts of water.
A kind of preparation method of the true mineral varnish of hydrophobic permeable type, comprises the following steps：
Step A, cataloid, pure acrylate emulsion and butyl glycol ether are added in water, is stirred, and are stirred
Rotating speed is 300-350r/min, after stirring 5 minutes, is warming up to 35-40 DEG C, continues to stir 5 minutes；
Step B, sequentially adds antiseptic, silicone acrylic emulsion, sodium metasilicate and calcium chloride powder, stirs, is warming up in heating
45-50 DEG C, it is stirred for 10 minutes, speed of agitator is 350-400r/min；
Step C, sequentially adds thixotropic agent, coalescents, 5% magnesium chloride solution, continues to stir；
Step D, adds natural siliceous sand, stirs 20-30 minute, and whipping temp is controlled at 40-50 DEG C, and speed of agitator is
450-500r/min。
It is preferred that, in the step C, speed of agitator is 400-500r/min, is stirred 10 minutes, and whipping temp control exists
40-50℃。
The present invention has the advantages and positive effects of：
1st, water repellency is good, effectively improves the anti-whitening resistance and hardness of paint film；
2nd, good air permeability, can solve the hollowing and bubble problem of true mineral varnish coating surface；
3rd, initial stage, anti-cracking performance was good, and adhesion strength is high；
4th, preparation technology is simple, suitable for industrialization.
Embodiment
The specific embodiment of the present invention is elaborated below.
Embodiment 1
A kind of true mineral varnish of hydrophobic permeable type, includes the raw material of following mass fraction：
110 parts of natural siliceous sand, 12 parts of cataloid, 6 parts of pure acrylate emulsion, 1 part of butyl glycol ether, crust
5 parts of element, 0.3 part of horseradish, 2.5 parts of theaflavin, 6 parts of silicone acrylic emulsion, 0.65 part of sodium metasilicate, 1 part of polyamide wax, 6 parts of bentonite, alcohol
30 parts of 10 parts of ether-ether class coalescents, 0.3 part of calcium chloride powder, 0.5 part of 5% magnesium chloride solution and water.Coalescents can be
Hexylene glycol monobutyl ether acetate etc..
A kind of preparation method of the true mineral varnish of hydrophobic permeable type, comprises the following steps：
Step A, cataloid, pure acrylate emulsion and butyl glycol ether are added in water, is stirred, and are stirred
Rotating speed is 350r/min, after stirring 5 minutes, is warming up to 35 DEG C, continues to stir 5 minutes；
Step B, sequentially adds antiseptic, silicone acrylic emulsion, sodium metasilicate and calcium chloride powder, stirs, is warming up in heating
45 DEG C, it is stirred for 10 minutes, speed of agitator is 400r/min；
Step C, sequentially adds thixotropic agent, coalescents, 5% magnesium chloride solution, continues to stir, speed of agitator is 500r/
Min, is stirred 10 minutes, and whipping temp is controlled at 40 DEG C；
Step D, adds natural siliceous sand, stirs 30 minutes, and whipping temp is controlled at 40 DEG C, and speed of agitator is 500r/
min。
Embodiment 2
A kind of true mineral varnish of hydrophobic permeable type, includes the raw material of following mass fraction：
100 parts of natural siliceous sand, 10 parts of cataloid, 9 parts of pure acrylate emulsion, 1.5 parts of butyl glycol ether, first
1 part of shell element, 1.5 parts of horseradish, 0.7 part of theaflavin, 9 parts of silicone acrylic emulsion, 0.15 part of sodium metasilicate, 3 parts of polyamide wax, 2 parts of bentonite,
40 parts of 15 parts of alcohol ether esters coalescents, 0.6 part of calcium chloride powder, 3 parts of 5% magnesium chloride solution and water.Coalescents can be
Hexylene glycol monobutyl ether acetate etc..
A kind of preparation method of the true mineral varnish of hydrophobic permeable type, comprises the following steps：
Step A, cataloid, pure acrylate emulsion and butyl glycol ether are added in water, is stirred, and are stirred
Rotating speed is 300r/min, after stirring 5 minutes, is warming up to 40 DEG C, continues to stir 5 minutes；
Step B, sequentially adds antiseptic, silicone acrylic emulsion, sodium metasilicate and calcium chloride powder, stirs, is warming up in heating
50 DEG C, it is stirred for 10 minutes, speed of agitator is 350r/min；
Step C, sequentially adds thixotropic agent, coalescents, 5% magnesium chloride solution, continues to stir, speed of agitator is 400r/
Min, is stirred 10 minutes, and whipping temp is controlled at 50 DEG C；
Step D, adds natural siliceous sand, stirs 20 minutes, and whipping temp is controlled at 50 DEG C, and speed of agitator is 450r/
min。
Embodiment 3
A kind of true mineral varnish of hydrophobic permeable type, includes the raw material of following mass fraction：
105 parts of natural siliceous sand, 11 parts of cataloid, 8 parts of pure acrylate emulsion, 1.2 parts of butyl glycol ether, first
3 parts of shell element, 1 part of horseradish, 2 parts of theaflavin, 7 parts of silicone acrylic emulsion, 0.5 part of sodium metasilicate, 2 parts of polyamide wax, 3 parts of bentonite, alcohol ether
50 parts of 13 parts of esters coalescents, 0.4 part of calcium chloride powder, 2 parts of 5% magnesium chloride solution and water.Coalescents can for oneself two
Alcohol monobutyl ether acetate etc..
A kind of preparation method of the true mineral varnish of hydrophobic permeable type, comprises the following steps：
Step A, cataloid, pure acrylate emulsion and butyl glycol ether are added in water, is stirred, and are stirred
Rotating speed is 350r/min, after stirring 5 minutes, is warming up to 35 DEG C, continues to stir 5 minutes；
Step B, sequentially adds antiseptic, silicone acrylic emulsion, sodium metasilicate and calcium chloride powder, stirs, is warming up in heating
45 DEG C, it is stirred for 10 minutes, speed of agitator is 350r/min；
Step C, sequentially adds thixotropic agent, coalescents, 5% magnesium chloride solution, continues to stir, speed of agitator is 400r/
Min, is stirred 10 minutes, and whipping temp is controlled at 40 DEG C；
Step D, adds natural siliceous sand, stirs 20 minutes, and whipping temp is controlled at 40 DEG C, and speed of agitator is 450r/
min。
Embodiment 4
A kind of true mineral varnish of hydrophobic permeable type, includes the raw material of following mass fraction：
100 parts of natural siliceous sand, 11 parts of cataloid, 8 parts of pure acrylate emulsion, 1 part of butyl glycol ether, crust
5 parts of element, 1.5 parts of horseradish, 0.7 part of theaflavin, 8 parts of silicone acrylic emulsion, 0.6 part of sodium metasilicate, 3 parts of polyamide wax, 2 parts of bentonite, alcohol
60 parts of 11 parts of ether-ether class coalescents, 0.3 part of calcium chloride powder, 0.5 part of 5% magnesium chloride solution and water.Coalescents can be
Hexylene glycol monobutyl ether acetate etc..
A kind of preparation method of the true mineral varnish of hydrophobic permeable type, comprises the following steps：
Step A, cataloid, pure acrylate emulsion and butyl glycol ether are added in water, is stirred, and are stirred
Rotating speed is 350r/min, after stirring 5 minutes, is warming up to 38 DEG C, continues to stir 5 minutes；
Step B, sequentially adds antiseptic, silicone acrylic emulsion, sodium metasilicate and calcium chloride powder, stirs, is warming up in heating
45 DEG C, it is stirred for 10 minutes, speed of agitator is 400r/min；
Step C, sequentially adds thixotropic agent, coalescents, 5% magnesium chloride solution, continues to stir, speed of agitator is 500r/
Min, is stirred 10 minutes, and whipping temp is controlled at 45 DEG C；
Step D, adds natural siliceous sand, stirs 30 minutes, and whipping temp is controlled at 50 DEG C, and speed of agitator is 500r/
min。
Experimental data：
| Detection project | Standard | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Initial stage splitting resistance | Flawless | It is qualified | It is qualified | It is qualified | It is qualified |
| Adhesion strength | ≥0.7MPa | 1.1MPa | 1.3MPa | 1.3MPa | 1.8MPa |
| Adhesion strength after immersion | ≥0.5MPa | 1.4MPa | 1.2MPa | 1.2MPa | 1.5MPa |
Its Plays is JGT24-2000《SAND SLURRY SYNTHETIC EMULSION ARCHITECTURAL COATINGS》W types.
As seen from the above table, the hydrophobic permeable of the true mineral varnish of hydrophobic permeable type of each embodiment is excellent, and hardness is good.Wherein, it is real
Example 4 is applied for most preferred embodiment, hydrophobic permeable is optimal.
Embodiments of the invention are described in detail above, but the content is only presently preferred embodiments of the present invention,
It is not to be regarded as the practical range for limiting the present invention.Any changes and modifications in accordance with the scope of the present application,
Within the patent covering scope that the present invention all should still be belonged to.
Claims (10)
1. a kind of true mineral varnish of hydrophobic permeable type, it is characterised in that：Include the raw material of following mass fraction：
90-110 parts of natural siliceous sand, 10-13 parts of cataloid, 6-9 parts of pure acrylate emulsion, butyl glycol ether 0.9-
1.5 parts, 2-9 parts of antiseptic, 6-11 parts of silicone acrylic emulsion, 0.15-0.65 parts of sodium metasilicate, 3-9 parts of thixotropic agent, coalescents 8-19
Part, 0.3-0.6 parts of calcium chloride powder, 0.5-3 parts of 5% magnesium chloride solution and 20-60 parts of water.
2. the true mineral varnish of hydrophobic permeable type according to claim 1, it is characterised in that：The thixotropic agent is polyamide wax and swollen
Moisten the mixture of soil.
3. the true mineral varnish of hydrophobic permeable type according to claim 2, it is characterised in that：Described polyamide wax 1-3 parts, bentonite
2-6 parts.
4. the true mineral varnish of hydrophobic permeable type according to claim 1, it is characterised in that：The antiseptic is chitin, horseradish
With the mixture of theaflavin.
5. the true mineral varnish of hydrophobic permeable type according to claim 4, it is characterised in that：Described chitin 1-5 parts, horseradish 0.3-
1.5 parts, 0.7-2.5 parts of theaflavin.
6. the true mineral varnish of hydrophobic permeable type according to claim 1, it is characterised in that：The thixotropic agent is bentonite.
7. the true mineral varnish of hydrophobic permeable type according to claim 1, it is characterised in that：The coalescents are alcohol ether esters.
8. the true mineral varnish of hydrophobic permeable type according to claim 1, it is characterised in that：Include the raw material of following mass fraction：
100-110 parts of natural siliceous sand, 10-12 parts of cataloid, 6-9 parts of pure acrylate emulsion, butyl glycol ether 1-1.5
Part, 2-9 parts of antiseptic, 6-9 parts of silicone acrylic emulsion, 0.15-0.65 parts of sodium metasilicate, 3-7 parts of thixotropic agent, 10-15 parts of coalescents, chlorine
Change 20-60 parts of 0.3-0.6 parts of calcium powder, 0.5-3 parts of 5% magnesium chloride solution and water.
9. a kind of preparation method of the true mineral varnish of hydrophobic permeable type as claimed in claim 1, it is characterised in that：Including following step
Suddenly：
Step A, cataloid, pure acrylate emulsion and butyl glycol ether are added in water, is stirred, speed of agitator
For 300-350r/min, after stirring 5 minutes, 35-40 DEG C is warming up to, continues to stir 5 minutes；
Step B, sequentially adds antiseptic, silicone acrylic emulsion, sodium metasilicate and calcium chloride powder, is stirred in heating, is warming up to 45-50
DEG C, it is stirred for 10 minutes, speed of agitator is 350-400r/min；
Step C, sequentially adds thixotropic agent, coalescents, 5% magnesium chloride solution, continues to stir；
Step D, adds natural siliceous sand, stirs 20-30 minutes, and whipping temp is controlled at 40-50 DEG C, and speed of agitator is 450-
500r/min。
10. the preparation method of the true mineral varnish of hydrophobic permeable type according to claim 9, it is characterised in that：In the step C,
Speed of agitator is 400-500r/min, is stirred 10 minutes, and whipping temp is controlled at 40-50 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710267986.2A CN107010918A (en) | 2017-04-22 | 2017-04-22 | A kind of true mineral varnish of hydrophobic permeable type and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710267986.2A CN107010918A (en) | 2017-04-22 | 2017-04-22 | A kind of true mineral varnish of hydrophobic permeable type and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN107010918A true CN107010918A (en) | 2017-08-04 |
Family
ID=59447887
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710267986.2A Pending CN107010918A (en) | 2017-04-22 | 2017-04-22 | A kind of true mineral varnish of hydrophobic permeable type and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107384087A (en) * | 2017-09-22 | 2017-11-24 | 苏州振振好新型建材科技有限公司 | A kind of nontoxic durable true mineral varnish of fire-resistant waterproof and preparation method thereof |
| CN114436616A (en) * | 2020-11-03 | 2022-05-06 | 湖南梨树园涂料有限公司 | Inorganic exterior wall mildew-proof stone-like paint |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103468082A (en) * | 2013-08-14 | 2013-12-25 | 青岛益群漆业集团有限公司 | Nanometer anti pollution self-cleaning stone paint |
| CN105255292A (en) * | 2015-09-15 | 2016-01-20 | 李茂英 | Nanometer modified real stone paint base material |
| CN105505071A (en) * | 2015-12-18 | 2016-04-20 | 三棵树涂料股份有限公司 | Water-repellent breathable type stone-like paint and preparation method thereof |
-
2017
- 2017-04-22 CN CN201710267986.2A patent/CN107010918A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103468082A (en) * | 2013-08-14 | 2013-12-25 | 青岛益群漆业集团有限公司 | Nanometer anti pollution self-cleaning stone paint |
| CN105255292A (en) * | 2015-09-15 | 2016-01-20 | 李茂英 | Nanometer modified real stone paint base material |
| CN105505071A (en) * | 2015-12-18 | 2016-04-20 | 三棵树涂料股份有限公司 | Water-repellent breathable type stone-like paint and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107384087A (en) * | 2017-09-22 | 2017-11-24 | 苏州振振好新型建材科技有限公司 | A kind of nontoxic durable true mineral varnish of fire-resistant waterproof and preparation method thereof |
| CN114436616A (en) * | 2020-11-03 | 2022-05-06 | 湖南梨树园涂料有限公司 | Inorganic exterior wall mildew-proof stone-like paint |
| CN114436616B (en) * | 2020-11-03 | 2023-03-24 | 湖南梨树园涂料有限公司 | Inorganic exterior wall mildew-proof stone-like paint |
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Application publication date: 20170804 |