A kind of wolfberry chewable tablet and preparation method thereof
Technical field
The present invention relates to technical field of health care food, more particularly to a kind of wolfberry chewable tablet and preparation method thereof.
Background technology
Qaidam matrimony vine planting base is located at southeastern Caidamu basin, by precipitation is few, sunshine-duration length, day and night temperature
Big to wait climate characteristic influence, the matrimony vine of output is so that particle is big, sugar content is high and famous.Studied through expert, Qaidam matrimony vine is average annual
It is up to 3144 hours during sunshine, 12 DEG C of day and night temperature, has an area of 150 kilometers of ecological environment cleanings, water source, soil are pollution-free, without agriculture
Medicine and heavy-metal residual.
Matrimony vine is Solanaceae Lycium.Matrimony vine is mild-natured, sweet, enter liver kidney two warp.Function filling liver kidney, prison muscles and bones, enrich blood
It is liquid, moistening lung qi-benefitting, supporing yang.Matrimony vine is important " integration of drinking and medicinal herbs " plant of China, is composed oneself with improving eyesight, beautifying face and moistering lotion, nourishes liver
Kidney, the function of strong muscles and bones,
The big vast matrimony vine fruit of promise wood is big, fruit sweet tea, seed are few, color is fresh, rich in various bioactivators, 18 containing needed by human body
The nutritional ingredient such as kind of amino acid, abundant reduced sugar, vitamin and calcium, phosphorus, iron, and germanic, selenium, ketone etc. there is anticancer, it is anti-
The trace element of the effects such as aging, beauty, with high medical value.
Black highland barley is one kind of barley, mainly originates from Tibetan area, is the main food of Tibetan people.Black highland barley dietary fiber has
There is gut purge defaecation, remove the good effects of vivotoxin, be the street cleaner of digestion.Containing beta glucan have gut purge,
Adjust blood glucose, reduction cholesterol, improve the effect such as immunity.
Matrimony vine fiber and barley diet fiber, which coordinate, can treat constipation, detoxify, and prevent and treat enteron aisle diverticulosis, treatment
The effects such as cholelithiasis, reduction blood cholesterol levels and triglycerides, control body weight, reduction blood sugar in diabetic patients.
However, lack in the prior art to the Qinghai Province such as matrimony vine and black highland barley characteristic resources deep development, comprehensive utilization
Product and technology.
The content of the invention
To solve problems of the prior art, it is an object of the invention to provide a kind of wolfberry chewable tablet and its preparation side
Method.
A kind of wolfberry chewable tablet, it is characterised in that its component includes matrimony vine fiber, black highland barley dietary fiber.
Further, the wolfberry chewable tablet, its component includes 1 part of matrimony vine fiber, black highland barley dietary fiber by weight
0.2-3 parts.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 3-8 hours, crushed, granularity is in 40 mesh;
3) wolfberry fruit powder of above-mentioned crushing is added to 50-95% 6-10 times of ethanol refluxing extraction 1-3 times, it is each 1-6 hours,
Extract solution is used for other products, and residue is standby:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby;
5) by above-mentioned residue Aqua pure extract, 4-10 times of amount of water is extracted 2-8 hours every time, is extracted 1-3 times;In merging
Extract solution is stated, being concentrated under reduced pressure into water content is used for other products below 10%, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber;
7) black highland barley is taken, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:10-1:20 add the PH7-10 aqueous solution, heat 1-30 minutes, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 3-8 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, the 50-100% ethanol of same volume is added, 2-24 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 0.2-3 parts of black highland barley dietary fiber weigh step 6 gained matrimony vine fibre by weight ratio
Dimension, adds step 11 gained barley diet fiber, is well mixed, tabletting, you can.
Wolfberry chewable tablet made from the above method is in production food, health food, available for solid pharmaceutical preparation and liquid system
Agent.
The present invention has advantages below compared with prior art:
The present invention in raw material all using the characteristic resources in Qinghai, it is pollution-free;For natural food, containing dietary fiber, nothing
Preservative, without chemical addition agent.
The present invention utilizes the characteristic resources in Qinghai, with the dietary fiber in wolfberry fruit extract fiber compatibility highland barley, fully profit
With different compositions, comprehensive exploitation improves matrimony vine added value.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
Embodiment 1
A kind of wolfberry chewable tablet, it is characterised in that its component includes matrimony vine fiber, black highland barley dietary fiber.
The wolfberry chewable tablet, it is characterised in that its component includes 1 part of matrimony vine fiber, black highland barley dietary fiber 0.2
Part.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 3 hours, crushed, granularity is in 40 mesh;
3) by 6 times of the ethanol refluxing extraction 1 time of the wolfberry fruit powder addition 50% of above-mentioned crushing, 1 hour every time, extract solution was used for
Other products:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby:
5) by above-mentioned residue Aqua pure extract, 4 times of amount of water is extracted 2 hours every time, is extracted 1 time;Merge said extracted liquid,
Water content 10% is concentrated under reduced pressure into, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber.
7) black highland barley is weighed by formula, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:10 add the PH7 aqueous solution, heat 1 minute, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 3 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, 50% ethanol of same volume is added, 2 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 0.2 part of black highland barley dietary fiber weigh step 6 gained matrimony vine fiber by weight ratio,
Step 11 gained barley diet fiber is added, is well mixed, tabletting, you can.
Embodiment 2
A kind of wolfberry chewable tablet composition, it is characterised in that its component of the composition includes matrimony vine fiber, black highland barley
Dietary fiber.
The wolfberry chewable tablet composition, it is characterised in that including 1 part of matrimony vine fiber, 3 parts of black highland barley dietary fiber.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 8 hours, crushed, granularity is in 40 mesh;
3) by 10 times of the ethanol refluxing extraction 2 times of the wolfberry fruit powder addition 95% of above-mentioned crushing, 6 hours every time, extract solution was used
In other products:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby:
5) by above-mentioned residue Aqua pure extract, 10 times of amount of water is extracted 8 hours every time, is extracted 3 times;Merge said extracted liquid,
Water content 8% is concentrated under reduced pressure into, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber;
7) black highland barley is weighed by formula, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:20 add the PH10 aqueous solution, heat 30 minutes, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 8 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, the absolute ethyl alcohol of same volume is added, 24 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 3 parts of black highland barley dietary fiber weigh step 6 gained matrimony vine fiber by weight ratio, plus
Enter step 11 gained barley diet fiber, be well mixed, tabletting, you can.
Embodiment 3
A kind of wolfberry chewable tablet composition, it is characterised in that its component of the composition includes matrimony vine fiber, black highland barley
Dietary fiber.
The wolfberry chewable tablet composition, it is characterised in that including 1 part of matrimony vine fiber, 2 parts of black highland barley dietary fiber.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 6 hours, crushed, granularity is in 40 mesh;
3) by 8 times of the ethanol refluxing extraction 3 times of the wolfberry fruit powder addition 65% of above-mentioned crushing, 2 hours every time, extract solution was used for
Other products:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby:
5) by above-mentioned residue Aqua pure extract, 6 times of amount of water is extracted 4 hours every time, is extracted 2 times;Merge said extracted liquid,
Water content 6% is concentrated under reduced pressure into, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber;
7) black highland barley is weighed by formula, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:5 add the PH8 aqueous solution, heat 20 minutes, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 4 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, 75% ethanol of same volume is added, 12 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 2 parts of black highland barley dietary fiber weigh step 6 gained matrimony vine fiber by weight ratio, plus
Enter step 11 gained barley diet fiber, be well mixed, tabletting, you can.
Embodiment 4
A kind of wolfberry chewable tablet composition, it is characterised in that its component of the composition includes matrimony vine fiber, black highland barley
Dietary fiber.
The wolfberry chewable tablet composition, it is characterised in that including 1 part of matrimony vine fiber, 1.8 parts of black highland barley dietary fiber.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 7 hours, crushed, granularity is in 40 mesh;
3) by 9 times of the ethanol refluxing extraction 2 times of the wolfberry fruit powder addition 75% of above-mentioned crushing, 3 hours every time, extract solution was used for
Other products:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby:
5) by above-mentioned residue Aqua pure extract, 5 times of amount of water is extracted 5 hours every time, is extracted 1 time;Merge said extracted liquid,
Water content 9% is concentrated under reduced pressure into, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber;
7) black highland barley is weighed by formula, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:13 add the PH9 aqueous solution, heat 15 minutes, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 5.5 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, 80% ethanol of same volume is added, 6 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 1.8 parts of black highland barley dietary fiber weigh step 6 gained matrimony vine fiber by weight ratio,
Step 11 gained barley diet fiber is added, is well mixed, tabletting, you can.
Embodiment 5
A kind of wolfberry chewable tablet composition, it is characterised in that its component of the composition includes matrimony vine fiber, black highland barley
Dietary fiber.
The wolfberry chewable tablet composition, it is characterised in that including 1 part of matrimony vine fiber, 1.5 parts of black highland barley dietary fiber.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 5.5 hours, crushed, granularity is in 40 mesh;
3) by 7 times of the ethanol refluxing extraction 2 times of the wolfberry fruit powder addition 70% of above-mentioned crushing, 2 hours every time, extract solution was used for
Other products:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby:
5) by above-mentioned residue Aqua pure extract, 5 times of amount of water is extracted 3.5 hours every time, is extracted 1 time;Merge said extracted
Liquid, is concentrated under reduced pressure into water content 10%, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber;
7) black highland barley is weighed by formula, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:18 add PH 9 aqueous solution, heat 5 minutes, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 7 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, 90% ethanol of same volume is added, 8 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 1.5 parts of black highland barley dietary fiber weigh step 6 gained matrimony vine fiber by weight ratio,
Step 11 gained barley diet fiber is added, is well mixed, tabletting, you can.
Embodiment 6
A kind of wolfberry chewable tablet composition, it is characterised in that its component of the composition includes matrimony vine fiber, black highland barley
Dietary fiber.
The wolfberry chewable tablet composition, it is characterised in that including 1 part of matrimony vine fiber, 2.5 parts of black highland barley dietary fiber.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 6.5 hours, crushed, granularity is in 40 mesh;
3) by 9 times of the ethanol refluxing extraction 3 times of the wolfberry fruit powder addition 85% of above-mentioned crushing, 4 hours every time, extract solution was used for
Other products:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby:
5) by above-mentioned residue Aqua pure extract, 7 times of amount of water is extracted 7.5 hours every time, is extracted 2 times;Merge said extracted
Liquid, is concentrated under reduced pressure into water content 8%, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber;
7) black highland barley is weighed by formula, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:10 add PH 10 aqueous solution, heat 14 minutes, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 6 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, 95% ethanol of same volume is added, 10 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 2.5 parts of black highland barley dietary fiber weigh step 6 gained matrimony vine fiber by weight ratio,
Step 11 gained barley diet fiber is added, is well mixed, tabletting, you can.
Embodiment 7
A kind of wolfberry chewable tablet composition, it is characterised in that its component of the composition includes matrimony vine fiber, black highland barley
Dietary fiber.
The wolfberry chewable tablet composition, it is characterised in that including 1 part of matrimony vine fiber, 1 part of black highland barley dietary fiber.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 4.5 hours, crushed, granularity is in 40 mesh;
3) by 7 times of the ethanol refluxing extraction 1 time of the wolfberry fruit powder addition 55% of above-mentioned crushing, 6 hours every time, extract solution was used for
Other products:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby:
5) by above-mentioned residue Aqua pure extract, 10 times of amount of water is extracted 7 hours every time, is extracted 1 time;Merge said extracted liquid,
Water content 7% is concentrated under reduced pressure into, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber;
7) black highland barley is weighed by formula, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:11 add the PH7 aqueous solution, heat 25 minutes, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 8 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, 70% ethanol of same volume is added, 8 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 1 part of black highland barley dietary fiber weigh step 6 gained matrimony vine fiber by weight ratio, plus
Enter step 11 gained barley diet fiber, be well mixed, tabletting, you can.
Embodiment 8
A kind of wolfberry chewable tablet composition, it is characterised in that its component of the composition includes matrimony vine fiber, black highland barley
Dietary fiber.
The wolfberry chewable tablet composition, it is characterised in that including 1 part of matrimony vine fiber, 1.6 parts of black highland barley dietary fiber.
A kind of preparation method of wolfberry chewable tablet, it is characterised in that:Comprise the following steps:
1) dried wolfberry of Qinghai Province Haixi Mongolian-Tibetan Autonomous Prefecture Dulan County promise wood flood is taken, the removal of impurity is gone in screening;
2) matrimony vine after screening is cleaned up, puts -80 DEG C of snap frozens 8 hours, crushed, granularity is in 40 mesh;
3) by 8 times of the ethanol refluxing extraction 1 time of the wolfberry fruit powder addition 95% of above-mentioned crushing, 6 hours every time, extract solution was used for
Other products:
4) above-mentioned residue is dried, supercritical extract, extract is used for other products, residue is standby:
5) by above-mentioned residue Aqua pure extract, 8 times of amount of water is extracted 5.5 hours every time, is extracted 3 times;Merge said extracted
Liquid, is concentrated under reduced pressure into water content 9%, residue is standby;
6) above-mentioned residue is taken, is freeze-dried, produces matrimony vine fiber;
7) black highland barley is weighed by formula, dry milling processes prepare highland barley bran;
8) wheat bran is taken by 1:20 add the PH8 aqueous solution, heat 5 minutes, centrifugation;
9) supernatant after above-mentioned centrifugation is taken, pH value 8 is adjusted, stirs, is centrifuged;
10) supernatant after above-mentioned centrifugation is taken, 80% ethanol of same volume is added, 24 hours are stood;
11) above-mentioned standing liquid is taken, is centrifuged, abandoning supernatant, lower floor is dried, and produces black highland barley dietary fiber;
12) 1 part of matrimony vine fiber, 1.6 parts of black highland barley dietary fiber weigh step 6 gained matrimony vine fiber by weight ratio,
Step 11 gained barley diet fiber is added, is well mixed, tabletting, you can.