CN106974294A - A kind of Pinolenic acid and or pine-seed oil pine nut polypeptide microcapsule powder and preparation method thereof - Google Patents
A kind of Pinolenic acid and or pine-seed oil pine nut polypeptide microcapsule powder and preparation method thereof Download PDFInfo
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- CN106974294A CN106974294A CN201710345228.8A CN201710345228A CN106974294A CN 106974294 A CN106974294 A CN 106974294A CN 201710345228 A CN201710345228 A CN 201710345228A CN 106974294 A CN106974294 A CN 106974294A
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- HXQHFNIKBKZGRP-URPRIDOGSA-N (5Z,9Z,12Z)-octadecatrienoic acid Chemical compound CCCCC\C=C/C\C=C/CC\C=C/CCCC(O)=O HXQHFNIKBKZGRP-URPRIDOGSA-N 0.000 title claims abstract description 55
- HXQHFNIKBKZGRP-UHFFFAOYSA-N Ranuncelin-saeure-methylester Natural products CCCCCC=CCC=CCCC=CCCCC(O)=O HXQHFNIKBKZGRP-UHFFFAOYSA-N 0.000 title claims abstract description 55
- 108090000765 processed proteins & peptides Proteins 0.000 title claims abstract description 45
- 235000008331 Pinus X rigitaeda Nutrition 0.000 title claims abstract description 44
- 235000011613 Pinus brutia Nutrition 0.000 title claims abstract description 44
- 241000018646 Pinus brutia Species 0.000 title claims abstract description 44
- 102000004196 processed proteins & peptides Human genes 0.000 title claims abstract description 42
- 229920001184 polypeptide Polymers 0.000 title claims abstract description 41
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- 239000003094 microcapsule Substances 0.000 title claims abstract description 23
- 239000000843 powder Substances 0.000 title claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000002156 mixing Methods 0.000 claims abstract description 19
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 18
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 16
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 3
- 239000011162 core material Substances 0.000 claims description 34
- 239000000839 emulsion Substances 0.000 claims description 27
- 238000010008 shearing Methods 0.000 claims description 24
- 239000007864 aqueous solution Substances 0.000 claims description 23
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical group O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 16
- 229920006395 saturated elastomer Polymers 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 14
- -1 diglycerine fatty acid ester Chemical class 0.000 claims description 12
- 229920002774 Maltodextrin Polymers 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 11
- 229930006000 Sucrose Natural products 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 9
- 239000005720 sucrose Substances 0.000 claims description 9
- 239000012153 distilled water Substances 0.000 claims description 8
- 238000012216 screening Methods 0.000 claims description 8
- 239000000377 silicon dioxide Substances 0.000 claims description 8
- 238000001694 spray drying Methods 0.000 claims description 8
- 238000005507 spraying Methods 0.000 claims description 8
- 239000005913 Maltodextrin Substances 0.000 claims description 7
- 239000005018 casein Substances 0.000 claims description 7
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims description 7
- 235000021240 caseins Nutrition 0.000 claims description 7
- 229940035034 maltodextrin Drugs 0.000 claims description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 238000000199 molecular distillation Methods 0.000 claims description 6
- 108010010803 Gelatin Proteins 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- 229920002472 Starch Polymers 0.000 claims description 5
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 5
- 229920000159 gelatin Polymers 0.000 claims description 5
- 239000008273 gelatin Substances 0.000 claims description 5
- 235000019322 gelatine Nutrition 0.000 claims description 5
- 235000011852 gelatine desserts Nutrition 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 239000011734 sodium Substances 0.000 claims description 5
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 5
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 5
- 235000019698 starch Nutrition 0.000 claims description 5
- CODAYFPFZXWNLD-UHFFFAOYSA-N 2-hydroxypropanoyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC(=O)C(C)O CODAYFPFZXWNLD-UHFFFAOYSA-N 0.000 claims description 4
- 235000010469 Glycine max Nutrition 0.000 claims description 4
- 244000068988 Glycine max Species 0.000 claims description 4
- 235000010489 acacia gum Nutrition 0.000 claims description 4
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims description 4
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 4
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 125000005456 glyceride group Chemical group 0.000 claims description 4
- 239000008107 starch Substances 0.000 claims description 4
- 241000196324 Embryophyta Species 0.000 claims description 3
- 108090001060 Lipase Proteins 0.000 claims description 3
- 239000004367 Lipase Substances 0.000 claims description 3
- 102000004882 Lipase Human genes 0.000 claims description 3
- 239000000470 constituent Substances 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 235000019421 lipase Nutrition 0.000 claims description 3
- 235000013826 starch sodium octenyl succinate Nutrition 0.000 claims description 3
- 239000001334 starch sodium octenyl succinate Substances 0.000 claims description 3
- 210000000481 breast Anatomy 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 5
- 238000004945 emulsification Methods 0.000 abstract description 3
- 238000010521 absorption reaction Methods 0.000 abstract description 2
- 230000001804 emulsifying effect Effects 0.000 abstract description 2
- 238000007667 floating Methods 0.000 abstract description 2
- 235000013305 food Nutrition 0.000 abstract description 2
- 238000001556 precipitation Methods 0.000 abstract description 2
- 239000003921 oil Substances 0.000 description 19
- 235000015424 sodium Nutrition 0.000 description 5
- 239000007762 w/o emulsion Substances 0.000 description 5
- 108010048733 Lipozyme Proteins 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- FCCDDURTIIUXBY-UHFFFAOYSA-N lipoamide Chemical compound NC(=O)CCCCC1CCSS1 FCCDDURTIIUXBY-UHFFFAOYSA-N 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 239000005556 hormone Substances 0.000 description 2
- 229940088597 hormone Drugs 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 108010088406 Glucagon-Like Peptides Proteins 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 235000003642 hunger Nutrition 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000007180 physiological regulation Effects 0.000 description 1
- 230000036186 satiety Effects 0.000 description 1
- 235000019627 satiety Nutrition 0.000 description 1
- 230000003248 secreting effect Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000037351 starvation Effects 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Fats And Perfumes (AREA)
- General Preparation And Processing Of Foods (AREA)
- Bakery Products And Manufacturing Methods Therefor (AREA)
Abstract
The present invention relates to a kind of Pinolenic acid and or pine-seed oil pine nut polypeptide microcapsule powder and preparation method thereof, belong to field of food.It is made from the following raw materials in parts by weight：Water-soluble 5 ~ 15 parts of core, 5 ~ 40 parts of mixing oiliness core, 2 ~ 20 parts of emulsifying agent, 50 ~ 90 parts of wall material, 0.5 ~ 10 part of oil-in-water emulsifiers, 0.01 ~ 1 part of anticaking agent.Stability of the present invention, good fluidity; without phenomenons such as floating oil, precipitation, viscous bottles; it is effectively promoted the absorption of pine nut polypeptide; not only protect pine nut polypeptide but also play peculiar effect of two kinds of materials of pine nut polypeptide and Pinolenic acid; the emulsifying agent that the present invention is used simultaneously is Pinolenic acid monoglyceride; the emulsifying agent increases the content of Pinolenic acid while good emulsifying effectiveness is played, and had not only played emulsification but also had played the efficacy effect of Pinolenic acid.
Description
Technical field
The invention belongs to field of food, and in particular to a kind of Pinolenic acid and or pine-seed oil pine nut polypeptide microcapsule powder and its
Preparation method.
Background technology
Biologically active peptide is by amino acid with the different general names for constituting the different peptides constituted with arrangement mode.Active peptide has
There are a variety of body metabolisms and physiological regulation function, such as promote immune, regulation hormone, lowering blood pressure and blood fat, anti-oxidant effect.
Amino acid contained species is more complete in pine nut, but the molecular structure of pine nut albumen is complicated, and relative molecular mass is big, directly eats
Digestibility and biological value do not reach the set goal far afterwards.Pine nut polypeptide can overcome weakness of the pine nut albumen in terms of nutrition,
The polypeptide compound easily digested and assimilated is provided.Pine nut polypeptide easily influenceed by factors such as air oxidation, humid environments and
Degraded, the lifetime is limited.To solve this problem, present invention spy is embedded pine nut polypeptide by microcapsule technology, and pine nut
Polypeptide belongs to water-soluble, therefore the present invention first passes through Pinolenic acid and/or pine-seed oil and pine nut polypeptide is prepared into water-in-oil type breast
Liquid, is then embedded by water-soluble wall material, finally gives the microcapsule powder of W/O/W.So both protect pine nut many
Peptide has played peculiar effect of two kinds of materials of pine nut polypeptide and pine-seed oil simultaneously again.
Pinolenic acid is exclusive a kind of unrighted acid in pine-seed oil, and it can stimulate two kinds of starvation of human secretory
Feel inhibitory hormone（CCK and glucagon-like peptide）, they not only assist in body and preferably digest fat, moreover it is possible to
" satiety " signal is transmitted to brain, appetite is reduced, helps to control the intake of heat.Pinolenic acid can reduce cholesterol simultaneously
With reduction triglycerides, suppress vessel retraction, eliminate other unrighted acids and harmful effect of body etc. is acted on.
The content of the invention
The present invention provide a kind of Pinolenic acid and or pine-seed oil pine nut polypeptide microcapsule powder and preparation method thereof, to solve pine
Sub- polypeptide is easily influenceed and degraded by factors such as air oxidation, humid environments, the problem of lifetime is limited.
The present invention takes the technical scheme to be：It is made from the following raw materials in parts by weight：Water-soluble 5 ~ 15 parts of core, mixing
5 ~ 40 parts of oiliness core, 2 ~ 20 parts of emulsifying agent, 50 ~ 90 parts of wall material, 0.5 ~ 10 part of oil-in-water emulsifiers, anticaking agent 0.01 ~ 1
Part.
The water-soluble core is pine nut polypeptide；
The mixing oiliness core is one or both of Pinolenic acid and pine-seed oil；
The emulsifying agent is Pinolenic acid monoglyceride；
The wall material is one kind or two in maltodextrin, converted starch, gelatin, Arabic gum, sodium carboxymethylcellulose, sucrose
Plant the mixture of any of the above ratio composition；
The oil-in-water emulsifiers are casein sodium, single diglycerine fatty acid ester, stearoyl lactate, diacetyl tartarate
One or both of single double glyceride, sucrose fatty ester, modified soy bean lipoid, starch Sodium Octenyl Succinate any of the above
The mixture of ratio composition；
The anticaking agent is silica；
A kind of Pinolenic acid and or pine-seed oil pine nut polypeptide microcapsule powder preparation method, comprise the following steps：
（One）Prepare core：
（1）The water-soluble core of 5 ~ 15 parts by weight is configured to saturated aqueous solution；
（2）Water-soluble core material solution is added in 5 ~ 40 parts of mixing oiliness core；
（3）The emulsifying agent of 2 ~ 20 parts of addition into mixing oiliness core, in disperseing 5 minutes at a high speed under 10000r/min, is made oil
Water-in type emulsion；
（Two）The preparation of microcapsule powder：
（1）Wall material is dissolved in 70 ~ 90 DEG C of distilled water and dissolved, saturated aqueous solution is made；
（2）Then shearing tank is squeezed into after 0.5 ~ 10 part of oil-in-water emulsifiers and the wall material aqueous solution being mixed, stirred；
（3）By step（One）The core of preparation squeezes into shearing tank mixing shearing and obtains stable emulsion in 10 minutes or so；
（4）Then by emulsion homogeneous twice；
（5）It is dry that emulsion after homogeneous enters the spray drying tower progress spraying that EAT is 160 DEG C, leaving air temp is 80 DEG C
It is dry；
（6）Anticaking agent stirring is added after the screening of 40 mesh classifying screens again and obtains finished product.
Described Pinolenic acid monoglyceride is comprised the following steps：
（1）It is 1 according to molar ratio：1 ~ 4 weighs Pinolenic acid and glycerine；
（2）According to mass ratio 1：0.01 ~ 0.05 to step（1）Middle addition specific lipase；
（3）2 ~ 24h is catalyzed under conditions of 30 ~ 60 DEG C；
（4）It is washed to after neutrality and enters molecular distillation；
（5）Molecular distillation heavy constituent is taken to obtain Pinolenic acid monoglyceride.
It is an advantage of the invention that pine nut polypeptide is carried out into secondary embedding by microcapsule technology, once embedding is by Pinolenic acid
With or pine-seed oil composition oil-soluble wall material, secondary embedding is embedded by water-soluble wall material, finally gives oil-in-water bag
The microcapsule powder of water.The absorption of pine nut polypeptide is so effectively promoted, secondary embedding had not only protected pine nut polypeptide but also played pine nut
Peculiar effect of two kinds of materials of polypeptide and Pinolenic acid, present invention uses Pinolenic acid monoglyceride emulsifying agent, the emulsification in addition
Agent increases the content of Pinolenic acid while good emulsifying effectiveness is played, and had not only played emulsification but also had played Pinolenic acid
Efficacy effect.The stability of product of the present invention is good, not degradable, life span extension, is dissolved in after water without floating oil, precipitation, viscous bottle etc.
Phenomenon.
Embodiment
The Pinolenic acid monoglyceride of use can be obtained by method of the prior art, e.g. be comprised the following steps：
（1）It is 1 according to molar ratio：1 ~ 4 weighs Pinolenic acid and glycerine；
（2）According to mass ratio 1：0.01 ~ 0.05 to step（1）Middle addition specific lipase, including Novi's letter biotechnology have
The Novozym of limit company（lipozyme）435、lipozyme TLIM、lipozyme RMIM；
（3）2 ~ 24h is catalyzed under conditions of 30 ~ 60 DEG C；
（4）It is washed to after neutrality and enters molecular distillation；
（5）Molecular distillation heavy constituent is taken to obtain Pinolenic acid monoglyceride.
Embodiment 1
Comprise the following steps：
（One）Prepare core：
（1）The pine nut polypeptide of 5 parts by weight is configured to saturated aqueous solution；
（2）In the Pinolenic acid that pine nut polypeptide solution is added to 5 parts；
（3）The Pinolenic acid monoglyceride of 2 parts of addition into Pinolenic acid, in disperseing 5 minutes at a high speed under 10000r/min, is made oil
Water-in type emulsion；
（Two）The preparation of microcapsule powder：
（1）50 portions of maltodextrins are dissolved in 70 DEG C of distilled water and dissolved, saturated aqueous solution is made；
（2）Then shearing tank is squeezed into after 0.5 part of casein sodium and the maltodextrin aqueous solution being mixed, stirred；
（3）By step（One）The core of preparation squeezes into shearing tank mixing shearing and obtains stable emulsion in 10 minutes or so；
（4）Then by emulsion homogeneous twice；
（5）It is dry that emulsion after homogeneous enters the spray drying tower progress spraying that EAT is 160 DEG C, leaving air temp is 80 DEG C
It is dry；
（6）Anticaking agent 0.01 part of stirring of silica is added after the screening of 40 mesh classifying screens obtain finished product again.
Embodiment 2
（One）Prepare core：
（1）The pine nut polypeptide of 10 parts by weight is configured to saturated aqueous solution；
（2）In the Pinolenic acid that pine nut polypeptide solution is added to 22.5 parts；
（3）The Pinolenic acid monoglyceride of 11 parts of addition into Pinolenic acid, in disperseing 5 minutes at a high speed under 10000r/min, is made
Water-in-oil emulsion；
（Two）The preparation of microcapsule powder：
（1）70 portions of maltodextrins are dissolved in 80 DEG C of distilled water and dissolved, saturated aqueous solution is made；
（2）Then shearing tank is squeezed into after 5 parts of casein sodiums and the maltodextrin aqueous solution being mixed, stirred；
（3）By step（One）The core of preparation squeezes into shearing tank mixing shearing and obtains stable emulsion in 10 minutes or so；
（4）Then by emulsion homogeneous twice；
（5）It is dry that emulsion after homogeneous enters the spray drying tower progress spraying that EAT is 160 DEG C, leaving air temp is 80 DEG C
It is dry；
（6）Anticaking agent 0.5 part of stirring of silica is added after the screening of 40 mesh classifying screens obtain finished product again.
Embodiment 3
（One）Prepare core：
（1）The pine nut polypeptide of 15 parts by weight is configured to saturated aqueous solution；
（2）In the Pinolenic acid that pine nut polypeptide solution is added to 40 parts；
（3）The Pinolenic acid monoglyceride of 20 parts of addition into Pinolenic acid, in disperseing 5 minutes at a high speed under 10000r/min, is made
Water-in-oil emulsion；
（Two）The preparation of microcapsule powder：
（1）90 portions of maltodextrins are dissolved in 90 DEG C of distilled water and dissolved, saturated aqueous solution is made；
（2）Then shearing tank is squeezed into after 10 parts of casein sodiums and the maltodextrin aqueous solution being mixed, stirred；
（3）By step（One）The core of preparation squeezes into shearing tank mixing shearing and obtains stable emulsion in 10 minutes or so；
（4）Then by emulsion homogeneous twice；
（5）It is dry that emulsion after homogeneous enters the spray drying tower progress spraying that EAT is 160 DEG C, leaving air temp is 80 DEG C
It is dry；
（6）Anticaking agent silica 1 part stirring is added after the screening of 40 mesh classifying screens again and obtains finished product.
Embodiment 4
Comprise the following steps：
（One）Prepare core：
（1）The pine nut polypeptide of 5 parts by weight is configured to saturated aqueous solution；
（2）Pine nut polypeptide solution is added in 2.5 parts of Pinolenic acids and 2.5 parts of pine-seed oils；
（3）The Pinolenic acid monoglyceride of 2 parts of addition into Pinolenic acid and pine-seed oil, in scattered 5 points at a high speed under 10000r/min
Clock, is made water-in-oil emulsion；
（Two）The preparation of microcapsule powder：
（1）25 portions of maltodextrins, 25 portions of converted starches are dissolved in 70 DEG C of distilled water and dissolved, saturated aqueous solution is made；
（2）Then by 0.25 part of casein sodium, 0.25 part of single diglycerine fatty acid ester and maltodextrin, the converted starch aqueous solution
Mix, stir after squeeze into shearing tank；
（3）By step（One）The core of preparation squeezes into shearing tank mixing shearing and obtains stable emulsion in 10 minutes or so；
（4）Then by emulsion homogeneous twice；
（5）It is dry that emulsion after homogeneous enters the spray drying tower progress spraying that EAT is 160 DEG C, leaving air temp is 80 DEG C
It is dry；
（6）Anticaking agent 0.01 part of stirring of silica is added after the screening of 40 mesh classifying screens obtain finished product again.
Embodiment 5
（One）Prepare core：
（1）The pine nut polypeptide of 10 parts by weight is configured to saturated aqueous solution；
（2）Pine nut polypeptide solution is added in 5 parts of Pinolenic acid and 23 parts of pine-seed oils；
（3）The Pinolenic acid monoglyceride of 11 parts of addition into Pinolenic acid and pine-seed oil, in scattered 5 points at a high speed under 10000r/min
Clock, is made water-in-oil emulsion；
（Two）The preparation of microcapsule powder：
（1）30 parts of sodium carboxymethylcelluloses, 40 parts of gelatin are dissolved in 80 DEG C of distilled water and dissolved, saturated aqueous solution is made；
（2）Then by 1 part of stearoyl lactate, 4 parts of diacetyl tartarate list double glycerides and sodium carboxymethylcellulose, gelatin water
Solution mixing, stir after squeeze into shearing tank；
（3）By step（One）The core of preparation squeezes into shearing tank mixing shearing and obtains stable emulsion in 10 minutes or so；
（4）Then by emulsion homogeneous twice；
（5）It is dry that emulsion after homogeneous enters the spray drying tower progress spraying that EAT is 160 DEG C, leaving air temp is 80 DEG C
It is dry；
（6）Anticaking agent 0.5 part of stirring of silica is added after the screening of 40 mesh classifying screens obtain finished product again.
Embodiment 6
（One）Prepare core：
（1）The pine nut polypeptide of 15 parts by weight is configured to saturated aqueous solution；
（2）Pine nut polypeptide solution is added in 10 parts of Pinolenic acid and 30 parts of pine-seed oils；
（3）The Pinolenic acid monoglyceride of 20 parts of addition into Pinolenic acid and pine-seed oil, in scattered 5 points at a high speed under 10000r/min
Clock, is made water-in-oil emulsion；
（Two）The preparation of microcapsule powder：
（1）80 portions of sucrose, 10 parts of Arabic gums are dissolved in 90 DEG C of distilled water and dissolved, saturated aqueous solution is made；
（2）Then 2 parts of sucrose fatty esters, 8 parts of modified soy bean lipoids and sucrose, the Arabic gum aqueous solution mixed, stir equal
Shearing tank is squeezed into after even；
（3）By step（One）The core of preparation squeezes into shearing tank mixing shearing and obtains stable emulsion in 10 minutes or so；
（4）Then by emulsion homogeneous twice；
（5）It is dry that emulsion after homogeneous enters the spray drying tower progress spraying that EAT is 160 DEG C, leaving air temp is 80 DEG C
It is dry；
（6）Anticaking agent silica 1 part stirring is added after the screening of 40 mesh classifying screens again and obtains finished product.
Claims (5)
1. a kind of Pinolenic acid and or pine-seed oil pine nut polypeptide microcapsule powder, it is characterised in that be by the raw material system of following parts by weight
Into：Water-soluble 5 ~ 15 parts of core, 5 ~ 40 parts of mixing oiliness core, 2 ~ 20 parts of emulsifying agent, 50 ~ 90 parts of wall material, oil-in-water type breast
0.5 ~ 10 part of agent, 0.01 ~ 1 part of anticaking agent.
2. Pinolenic acid according to claim 1 and or pine-seed oil pine nut polypeptide microcapsule powder, it is characterised in that：
The water-soluble core is pine nut polypeptide；
The mixing oiliness core is one or both of Pinolenic acid and pine-seed oil；
The emulsifying agent is Pinolenic acid monoglyceride；
The wall material is one kind or two in maltodextrin, converted starch, gelatin, Arabic gum, sodium carboxymethylcellulose, sucrose
Plant the mixture of any of the above ratio composition；
The oil-in-water emulsifiers are casein sodium, single diglycerine fatty acid ester, stearoyl lactate, diacetyl tartarate
One or both of single double glyceride, sucrose fatty ester, modified soy bean lipoid, starch Sodium Octenyl Succinate any of the above
The mixture of ratio composition；
The anticaking agent is silica.
3. Pinolenic acid as claimed in claim 1 and or pine-seed oil pine nut polypeptide microcapsule powder preparation method, its feature exists
In comprising the following steps：
（One）Prepare core：
（1）The water-soluble core of 5 ~ 15 parts by weight is configured to saturated aqueous solution；
（2）Water-soluble core material solution is added in 5 ~ 40 parts of mixing oiliness core；
（3）The emulsifying agent of 2 ~ 20 parts of addition into mixing oiliness core, in disperseing 5 minutes at a high speed under 10000r/min, is made oil
Water-in type emulsion；
（Two）The preparation of microcapsule powder：
（1）Wall material is dissolved in 70 ~ 90 DEG C of distilled water and dissolved, saturated aqueous solution is made；
（2）Then shearing tank is squeezed into after 0.5 ~ 10 part of oil-in-water emulsifiers and the wall material aqueous solution being mixed, stirred；
（3）By step（One）The core of preparation squeezes into shearing tank mixing shearing and obtains stable emulsion in 10 minutes or so；
（4）Then by emulsion homogeneous twice；
（5）It is dry that emulsion after homogeneous enters the spray drying tower progress spraying that EAT is 160 DEG C, leaving air temp is 80 DEG C
It is dry；
（6）Anticaking agent stirring is added after the screening of 40 mesh classifying screens again and obtains finished product.
4. Pinolenic acid according to claim 3 and or pine-seed oil pine nut polypeptide microcapsule powder preparation method, its feature exists
In：
The water-soluble core is pine nut polypeptide；
The mixing oiliness core is one or both of Pinolenic acid and pine-seed oil；
The emulsifying agent is Pinolenic acid monoglyceride；
The wall material is one kind or two in maltodextrin, converted starch, gelatin, Arabic gum, sodium carboxymethylcellulose, sucrose
Plant the mixture of any of the above ratio composition；
The oil-in-water emulsifiers are casein sodium, single diglycerine fatty acid ester, stearoyl lactate, diacetyl tartarate
One or both of single double glyceride, sucrose fatty ester, modified soy bean lipoid, starch Sodium Octenyl Succinate any of the above
The mixture of ratio composition.
5. Pinolenic acid according to claim 4 and or pine-seed oil pine nut polypeptide microcapsule powder preparation method, its feature exists
In：Described Pinolenic acid monoglyceride is comprised the following steps：
（1）It is 1 according to molar ratio：1 ~ 4 weighs Pinolenic acid and glycerine；
（2）According to mass ratio 1：0.01 ~ 0.05 to step（1）Middle addition specific lipase；
（3）2 ~ 24h is catalyzed under conditions of 30 ~ 60 DEG C；
（4）It is washed to after neutrality and enters molecular distillation；
（5）Molecular distillation heavy constituent is taken to obtain Pinolenic acid monoglyceride.
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Cited By (3)
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| CN108118074A (en) * | 2017-12-29 | 2018-06-05 | 吉林派诺生物技术股份有限公司 | A kind of pine-seed oil rich in Pinolenic acid lutein ester and preparation method thereof |
| CN111358004A (en) * | 2019-09-10 | 2020-07-03 | 吉林农业大学 | Low-temperature airflow suspension pinocembrin seed oil pinolenic acid nanoemulsion composition microcapsule |
| CN111961116A (en) * | 2020-08-17 | 2020-11-20 | 安徽农业大学 | Bird embryo allantoic fluid bioactive peptide and preparation method and application thereof |
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| CN101559041A (en) * | 2009-05-19 | 2009-10-21 | 中国科学院过程工程研究所 | Polypeptide medicament sustained release microsphere or microcapsule preparation with uniform grain size and preparation method thereof |
| CN103263401A (en) * | 2013-05-23 | 2013-08-28 | 吉林大学 | Pinenut oil pinolenic acid microcapsule and preparation method thereof |
| CN105192841A (en) * | 2015-08-17 | 2015-12-30 | 吉林大学 | Multifunctional Korean pine seed peptide microcapsule effervescent tablets and preparation method thereof |
| CN105331648A (en) * | 2015-10-08 | 2016-02-17 | 中科田园(北京)农业科技有限公司 | High-purity alpha-linolenic acid monoglyceride and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101559041A (en) * | 2009-05-19 | 2009-10-21 | 中国科学院过程工程研究所 | Polypeptide medicament sustained release microsphere or microcapsule preparation with uniform grain size and preparation method thereof |
| CN103263401A (en) * | 2013-05-23 | 2013-08-28 | 吉林大学 | Pinenut oil pinolenic acid microcapsule and preparation method thereof |
| CN105192841A (en) * | 2015-08-17 | 2015-12-30 | 吉林大学 | Multifunctional Korean pine seed peptide microcapsule effervescent tablets and preparation method thereof |
| CN105331648A (en) * | 2015-10-08 | 2016-02-17 | 中科田园(北京)农业科技有限公司 | High-purity alpha-linolenic acid monoglyceride and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108118074A (en) * | 2017-12-29 | 2018-06-05 | 吉林派诺生物技术股份有限公司 | A kind of pine-seed oil rich in Pinolenic acid lutein ester and preparation method thereof |
| CN111358004A (en) * | 2019-09-10 | 2020-07-03 | 吉林农业大学 | Low-temperature airflow suspension pinocembrin seed oil pinolenic acid nanoemulsion composition microcapsule |
| CN111961116A (en) * | 2020-08-17 | 2020-11-20 | 安徽农业大学 | Bird embryo allantoic fluid bioactive peptide and preparation method and application thereof |
| CN111961116B (en) * | 2020-08-17 | 2023-03-10 | 安徽农业大学 | Bird embryo allantoic fluid bioactive peptide and preparation method and application thereof |
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