CN106973941A - A kind of attapulgite modified efficient mosquito lures agent and preparation method thereof of going out - Google Patents
A kind of attapulgite modified efficient mosquito lures agent and preparation method thereof of going out Download PDFInfo
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- CN106973941A CN106973941A CN201710305218.1A CN201710305218A CN106973941A CN 106973941 A CN106973941 A CN 106973941A CN 201710305218 A CN201710305218 A CN 201710305218A CN 106973941 A CN106973941 A CN 106973941A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
- A01N37/04—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof polybasic
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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Abstract
Agent of going out is lured the invention discloses the attapulgite modified efficient mosquito of one kind, includes the raw material of following parts by weight：Attapulgite modified 50 70 parts, 0.05 3 parts of nimbin, 0.1 2 parts of pyrethrins, 0.1 1.5 parts of tetramethrin, 13 parts of sodium carboxymethylcellulose, 0.3 0.7 parts of sodium citrate, 5 10 parts of livestock and poultry blood, 0.1 1 parts of kushenin, 0.05 0.7 parts of malathion, 10 20 parts of ancillary additions, 5 10 parts of cementitious additives, 10 20 parts of deionized water.The attapulgite modified efficient mosquito of the present invention lures agent of going out to have very strong attraction to mosquito fly, on the one hand its viscosity is higher, certain humidity can be kept, adhesion is produced to mosquito fly, to making it not escape, until dead, on the other hand lure the insecticidal constituent for agent addition of going out also has preferable insecticidal effect after mosquito sucks, the preparation method material cost of the invention provided is relatively low simultaneously, raw material is easy to get, technique concise, with higher use value and good application prospect.
Description
Technical field
The present invention relates to mosquito control technical field, and in particular to a kind of attapulgite modified efficient mosquito lure go out agent and its
Preparation method.
Background technology
Summer is mosquito, fly most rampant movable season, and skin can be risen " red born of the same parents " after mosquito bite, not only ugly but also strange
Itch incomparable, therefore itching allergy is common phenomenon to skin, more it is a risk that with a large amount of poisonous germs with mosquito, giving human body band
Carry out some fearful infectious diseases, mosquito has had a strong impact on the normal life and sleep of people, has been detrimental to health；And fly is because taking
Band multiple pathogenic microorganisms are propagated and endanger the mankind, the body surface crinosity of fly, and foot, which grabs pad, can secrete mucus, like in people or poultry
Fecaluria, phlegm, vomitus and corpse etc. creep and look for food, easily adhere to substantial amounts of pathogen, such as comma bacillus, typhoid fever bar
Bacterium, shigella dysenteriae, hepatitis bacillus, polio germ, hepatitis A germ, hepatitis B germ, and roundworm egg etc.；Again often in people
Body, food, stop on Dining tool, have the habit for rubbing foot and brush body with the hands when stopping falling, be attached to the pathogen with it and pollute soon
It is to ensure human health that food and Dining tool, which eliminate mosquito, it is to avoid the key of transmission.
Chrysanthemum ester type compound can be used for mosquito control, and with higher insecticidal activity, to be widely known by the people.But current city
The existing various liquid that wipe out the flies and mosquitoes on field, are sprayed in interior, drug volatilization is fast, can effectively kill insect, but be due to medicine when using
Thing discharges rapidly, and duration of efficacy is very short, it is necessary to constantly spray, and is made troubles to user.
Another aspect nimbin is a kind of more perfect plant source biopesticide, and it has been reached as required by insecticide
Whole standards：To the broad-spectrum action of insect, the interference to natural enemy is few, does not have toxicity to vertebrate, is easy to drop in the environment
Solution, aboundresources etc., and can be as insect growth regulator, IGR, and the Pest Species that can be prevented and treated are more, there is wider insecticidal spectrum
With the environmental protection feature of efficient noresidue.But because nimbin raw medicine is liquid, it is necessary to special carrier, otherwise its too fast volatilization, nothing
Method reaches the effect of lasting desinsection.
The content of the invention
For the defect of prior art, agent of going out is lured it is an object of the invention to provide the attapulgite modified efficient mosquito of one kind,
The mosquito lures agent of going out to have very strong attraction to mosquito fly, and on the one hand its viscosity is higher, certain humidity can be kept, to mosquito
Worm fly produces adhesion, and to making it not escape, until dead, the insecticidal constituent on the other hand luring agent of going out to add is sucked in mosquito
Also there is preferable insecticidal effect afterwards, while the preparation method material cost that the present invention is provided is relatively low, raw material is easy to get, technique letter
It is bright, with higher use value and good application prospect.
The present invention solves technical problem and adopted the following technical scheme that：
Agent of going out is lured the invention provides the attapulgite modified efficient mosquito of one kind, includes the raw material of following parts by weight：
Attapulgite modified 50-70 parts, 0.05-3 parts of nimbin, 0.1-2 parts of pyrethrins, 0.1-1.5 parts of tetramethrin, carboxymethyl
1-3 parts of sodium cellulosate, 0.3-0.7 parts of sodium citrate, 5-10 parts of livestock and poultry blood, 0.1-1 parts of kushenin, malathion 0.05-0.7
Part, 10-20 parts of ancillary additions, 5-10 parts of cementitious additives, 10-20 parts of deionized water.
Preferably, the attapulgite modified efficient mosquito lures agent of going out to include the raw material of following parts by weight：
Attapulgite modified 60 parts, 1.45 parts of nimbin, 1.25 parts of pyrethrins, 0.8 part of tetramethrin, sodium carboxymethylcellulose 2
It is part, 0.5 part of sodium citrate, 7.5 parts of livestock and poultry blood, 0.55 part of kushenin, 0.35 part of malathion, 15 parts of ancillary additions, viscous
Tie 8 parts of additive, 15 parts of deionized water.
Preferably, the ancillary additions are that vermiculite power, zeolite powder, calper calcium peroxide compare 1 according to weight:0.5:2, it is size-reduced
Cross the mixture of 100 mesh sieves composition.
Preferably, the cementitious additives are that starch, bentonite, sodium hydroxide compare 3 according to weight:7:The mixing of 1 composition
Thing.
Present invention also offers the preparation method that a kind of attapulgite modified efficient mosquito lures agent of going out, comprise the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 100 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, kushenin, malathion, ancillary additions, cementitious additives, stir 15-25 minutes, speed of agitator
For 850-950r/min, mixture A is obtained；
Step 3, by mixture A made from step 2, sodium citrate, livestock and poultry blood, nimbin, pyrethrins, tetramethrin, goes
Ionized water is added in Multifunction colloid grinder, and grinding rotating speed is in 3000-4000r/min, and milling time is 30-60 minutes,
Paste mixture is obtained, paste mixture grain fineness is less than 0.045 millimeter, paste mixture vacuum packaging is modified
The efficient mosquito of attapulgite lures agent of going out.
Preferably, the attapulgite modified efficient mosquito lures the preparation process for agent of going out to be：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 100 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, kushenin, malathion, ancillary additions, cementitious additives, stir 20 minutes, speed of agitator is
900r/min, obtains mixture A；
Step 3, by mixture A made from step 2, sodium citrate, livestock and poultry blood, nimbin, pyrethrins, tetramethrin, goes
Ionized water is added in Multifunction colloid grinder, and grinding rotating speed is 45 minutes in 3500 r/min, milling time, obtains paste
Mixture, paste mixture grain fineness is less than 0.045 millimeter, and paste mixture vacuum packaging is obtained into attapulgite modified
Efficient mosquito lures agent of going out.
Preferably, the attapulgite modified preparation method is as follows：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 65-75 DEG C, with 500-
1000r/min speed of agitator stirring 1-2h, filtering, filter residue is washed with deionized to neutrality, drying；C, by gains in b
Matter is mixed with calgon, Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate, and heating water bath is extremely
85-95 DEG C, with 500-1000r/min speed of agitator, stir 40-70 minutes, centrifuge, sediment is washed with deionized
To neutral, drying, it is subsequently placed in Muffle furnace at 420-480 DEG C and calcines 1-2h, cooling produces attapulgite modified.
Preferably, the attapulgite modified preparation method is as follows：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 70 DEG C, with stirring for 700r/min
Mix rotating speed stirs 1.5h, filtering, and filter residue is washed with deionized to neutrality, drying；C, by gained material and hexa metaphosphoric acid in b
Sodium, Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 90 DEG C, with 750r/
Min speed of agitator, is stirred 55 minutes, is centrifuged, and sediment is washed with deionized to neutrality, drying, is subsequently placed in horse
1.5h is not calcined in stove at 450 DEG C, cooling produces attapulgite modified.
Compared with prior art, the present invention has following beneficial effect：
（1）A kind of attapulgite modified efficient mosquito of the present invention lures agent of going out to employ attapulgite as major ingredient carrier, due to
Attapulgite has higher specific surface area, can effectively extend nimbin, pyrethrins, tetramethrin desinsection effective time.
（2）A kind of attapulgite modified efficient mosquito of the present invention lures the nimbin for agent use of going out to have wide spectrum work to insect
With, there is no toxicity to vertebrate, be easy to degraded in the environment, aboundresources etc., and can be as insect growth regulator, IGR, and can
The Pest Species of preventing and treating are more, there is wider insecticidal spectrum and the environmental protection feature of efficient noresidue；The pyrethrins of use, amine chrysanthemum
Ester, kushenin, malathion have stronger killing effect to mosquito fly, and the competence exertion toxicity only in insect bodies is entered
It can be fallen after entering in warm-blooded animal body by hydrolysis quickly and lose toxicity so that be obtained to lure the agent safety and environmental protection that goes out.
（3）A kind of attapulgite modified efficient mosquito of the present invention lures the livestock and poultry blood for agent addition of going out, and has to mosquito, fly
Stronger allure, after mosquito, fly smell smell, can directly fly to lure and be ingested in agent of going out, reach the purpose of trapping and killing flies.
（4）A kind of attapulgite modified efficient mosquito of the present invention lures agent of going out to be a kind of paste object, and its viscosity is higher,
Certain humidity can be kept, adhesion is produced to mosquito fly, to making it not escape, until death, effectively increases and lure agent of going out
Insecticidal effect.
（5）A kind of attapulgite modified efficient mosquito of the present invention lures the auxiliary additive and cementitious additives for agent addition of going out
And sodium carboxymethylcellulose, it can increase the viscosity for luring agent of going out, improve the adhesion performance of lotion, prevent from luring agent aging of going out hard
Change.
（6）A kind of attapulgite modified efficient mosquito of the present invention lures the attapulgite for agent use of going out after modified prepare
The needle bar shape group accumulated in a jumble can be caused to become loose porous, add void content and specific surface area, strengthen its adsorption capacity,
Substantially increase the properties for luring agent of going out.
Embodiment
With reference to specific embodiment, the technical scheme in the embodiment of the present invention is clearly and completely described, shown
So, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based on the reality in the present invention
Example is applied, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made all belongs to
In the scope of protection of the invention.
Embodiment 1.
A kind of attapulgite modified efficient mosquito of the present embodiment lures agent of going out, and includes the raw material of following parts by weight：
Attapulgite modified 50 parts, 0.05 part of nimbin, 0.1 part of pyrethrins, 0.1 part of tetramethrin, sodium carboxymethylcellulose 1
Part, 0.3 part of sodium citrate, 5 parts of livestock and poultry blood, 0.1 part of kushenin, 0.05 part of malathion, 10 parts of ancillary additions, bonding add
Plus 5 parts of agent, 10 parts of deionized water.
Ancillary additions are that vermiculite power, zeolite powder, calper calcium peroxide compare 1 according to weight in the present embodiment:0.5:2, it is size-reduced
Cross the mixture of 100 mesh sieves composition.
Cementitious additives are that starch, bentonite, sodium hydroxide compare 3 according to weight in the present embodiment:7:The mixing of 1 composition
Thing.
A kind of attapulgite modified efficient mosquito of the present embodiment lures the preparation method for agent of going out, and comprises the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 100 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, kushenin, malathion, ancillary additions, cementitious additives, stir 15-25 minutes, speed of agitator
For 850r/min, mixture A is obtained；
Step 3, by mixture A made from step 2, sodium citrate, livestock and poultry blood, nimbin, pyrethrins, tetramethrin, goes
Ionized water is added in Multifunction colloid grinder, and grinding rotating speed is 60 minutes in 3000r/min, milling time, obtains paste
Mixture, paste mixture grain fineness is less than 0.045 millimeter, and paste mixture vacuum packaging is obtained into attapulgite modified
Efficient mosquito lures agent of going out.
Attapulgite modified preparation method is as follows in the present embodiment：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 65 DEG C, with stirring for 500r/min
Mix rotating speed stirs 2h, filtering, and filter residue is washed with deionized to neutrality, drying；C, by b gained material and calgon,
Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 85 DEG C, with 500r/min
Speed of agitator, stir 70 minutes, centrifuge, sediment is washed with deionized to neutrality, drying is subsequently placed in Muffle furnace
In calcine 2h at 420 DEG C, cooling produces attapulgite modified.
Embodiment 2.
A kind of attapulgite modified efficient mosquito of the present embodiment lures agent of going out, and includes the raw material of following parts by weight：
Attapulgite modified 70 parts, 3 parts of nimbin, 2 parts of pyrethrins, 1.5 parts of tetramethrin, 3 parts of sodium carboxymethylcellulose, lemon
Sour 0.7 part of sodium, 10 parts of livestock and poultry blood, 1 part of kushenin, 0.7 part of malathion, 20 parts of ancillary additions, 10 parts of cementitious additives,
20 parts of deionized water.
Ancillary additions are that vermiculite power, zeolite powder, calper calcium peroxide compare 1 according to weight in the present embodiment:0.5:2, it is size-reduced
Cross the mixture of 100 mesh sieves composition.
Cementitious additives are that starch, bentonite, sodium hydroxide compare 3 according to weight in the present embodiment:7:The mixing of 1 composition
Thing.
A kind of attapulgite modified efficient mosquito of the present embodiment lures the preparation method for agent of going out, and comprises the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 100 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, kushenin, malathion, ancillary additions, cementitious additives, stir 25 minutes, speed of agitator is
950r/min, obtains mixture A；
Step 3, by mixture A made from step 2, sodium citrate, livestock and poultry blood, nimbin, pyrethrins, tetramethrin, goes
Ionized water is added in Multifunction colloid grinder, and grinding rotating speed is 30 minutes in 4000r/min, milling time, obtains paste
Mixture, paste mixture grain fineness is less than 0.045 millimeter, and paste mixture vacuum packaging is obtained into attapulgite modified
Efficient mosquito lures agent of going out.
Attapulgite modified preparation method is as follows in the present embodiment：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 75 DEG C, with 1000r/min's
Speed of agitator stirs 2h, filtering, and filter residue is washed with deionized to neutrality, drying；C, by gained material and hexa metaphosphoric acid in b
Sodium, Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 95 DEG C, with
1000r/min speed of agitator, is stirred 40 minutes, is centrifuged, and sediment is washed with deionized to neutrality, is dried, then
It is placed in Muffle furnace at 480 DEG C and calcines 1h, cooling produces attapulgite modified.
Embodiment 3.
A kind of attapulgite modified efficient mosquito of the present embodiment lures agent of going out, and includes the raw material of following parts by weight：
Attapulgite modified 60 parts, 1.45 parts of nimbin, 1.25 parts of pyrethrins, 0.8 part of tetramethrin, sodium carboxymethylcellulose 2
It is part, 0.5 part of sodium citrate, 7.5 parts of livestock and poultry blood, 0.55 part of kushenin, 0.35 part of malathion, 15 parts of ancillary additions, viscous
Tie 8 parts of additive, 15 parts of deionized water.
Ancillary additions are that vermiculite power, zeolite powder, calper calcium peroxide compare 1 according to weight in the present embodiment:0.5:2, it is size-reduced
Cross the mixture of 100 mesh sieves composition.
Cementitious additives are that starch, bentonite, sodium hydroxide compare 3 according to weight in the present embodiment:7:The mixing of 1 composition
Thing.
A kind of attapulgite modified efficient mosquito of the present embodiment lures the preparation method for agent of going out, and comprises the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 100 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, kushenin, malathion, ancillary additions, cementitious additives, stir 20 minutes, speed of agitator is
900r/min, obtains mixture A；
Step 3, by mixture A made from step 2, sodium citrate, livestock and poultry blood, nimbin, pyrethrins, tetramethrin, goes
Ionized water is added in Multifunction colloid grinder, and grinding rotating speed is 45 minutes in 3500 r/min, milling time, obtains paste
Mixture, paste mixture grain fineness is less than 0.045 millimeter, and paste mixture vacuum packaging is obtained into attapulgite modified
Efficient mosquito lures agent of going out.
Attapulgite modified preparation method is as follows in the present embodiment：A, following component raw material is weighed by weight：It is concavo-convex
100 parts of rod soil, 2 parts of calgon, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, dodecyl sulphate
2 parts of sodium；B, attapulgite is put into the hydrochloric acid solution that concentration is 1mol/L, heating water bath is to 70 DEG C, with stirring for 700r/min
Mix rotating speed stirs 1.5h, filtering, and filter residue is washed with deionized to neutrality, drying；C, by gained material and hexa metaphosphoric acid in b
Sodium, Sodium Polyacrylate, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 90 DEG C, with 750r/
Min speed of agitator, is stirred 55 minutes, is centrifuged, and sediment is washed with deionized to neutrality, drying, is subsequently placed in horse
1.5h is not calcined in stove at 450 DEG C, cooling produces attapulgite modified.
Attapulgite modified efficient mosquito lures agent the performance test results of going out as follows made from various embodiments above：
| Experimental project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example |
| Lower 24 hours capture insect numbers of identical environment | 45 | 51 | 52 | 12 |
| Capture the insect death rate | 100% | 100% | 100% | 80% |
| Firm time | 40h | 37h | 37h | 12h |
A kind of attapulgite modified efficient mosquito of the present invention lures agent of going out to mosquito fly very strong attraction, and on the one hand its is sticky
Degree is higher, can keep certain humidity, and adhesion is produced to mosquito fly, to making it not escape, until death, is on the other hand lured
The insecticidal constituent of agent of going out addition also has preferable insecticidal effect after mosquito sucks, while the preparation method material that the present invention is provided
Expect that cost is relatively low, raw material is easy to get, technique is concise, with higher use value and good application prospect.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It may be appreciated other embodiment.
Claims (8)
1. a kind of attapulgite modified efficient mosquito lures agent of going out, it is characterised in that include the raw material of following parts by weight：
Attapulgite modified 50-70 parts, 0.05-3 parts of nimbin, 0.1-2 parts of pyrethrins, 0.1-1.5 parts of tetramethrin, carboxymethyl
1-3 parts of sodium cellulosate, 0.3-0.7 parts of sodium citrate, 5-10 parts of livestock and poultry blood, 0.1-1 parts of kushenin, malathion 0.05-0.7
Part, 10-20 parts of ancillary additions, 5-10 parts of cementitious additives, 10-20 parts of deionized water.
2. the attapulgite modified efficient mosquito of one kind according to claim 1 lures agent of going out, it is characterised in that the modification is recessed
Efficiently mosquito lures agent of going out to include the raw material of following parts by weight to convex rod soil：
Attapulgite modified 60 parts, 1.45 parts of nimbin, 1.25 parts of pyrethrins, 0.8 part of tetramethrin, sodium carboxymethylcellulose 2
It is part, 0.5 part of sodium citrate, 7.5 parts of livestock and poultry blood, 0.55 part of kushenin, 0.35 part of malathion, 15 parts of ancillary additions, viscous
Tie 8 parts of additive, 15 parts of deionized water.
3. the attapulgite modified efficient mosquito of one kind according to claim 1 or 2 lures agent of going out, it is characterised in that described auxiliary
Additive is helped to compare 1 according to weight for vermiculite power, zeolite powder, calper calcium peroxide:0.5:2, the mixing of the size-reduced mesh sieve of mistake 100 composition
Thing.
4. the attapulgite modified efficient mosquito of one kind according to claim 1 or 2 lures agent of going out, it is characterised in that described viscous
Knot additive is starch, bentonite, sodium hydroxide compare 3 according to weight:7:The mixture of 1 composition.
5. a kind of prepare the method that attapulgite modified efficient mosquito as claimed in claim 1 or 2 lures agent of going out, its feature exists
In comprising the following steps：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 100 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, kushenin, malathion, ancillary additions, cementitious additives, stir 15-25 minutes, speed of agitator
For 850-950r/min, mixture A is obtained；
Step 3, by mixture A made from step 2, sodium citrate, livestock and poultry blood, nimbin, pyrethrins, tetramethrin, goes
Ionized water is added in Multifunction colloid grinder, and grinding rotating speed is in 3000-4000r/min, and milling time is 30-60 minutes,
Paste mixture is obtained, paste mixture grain fineness is less than 0.045 millimeter, paste mixture vacuum packaging is modified
The efficient mosquito of attapulgite lures agent of going out.
6. a kind of attapulgite modified efficient mosquito according to claim 5 lures the preparation method for agent of going out, it is characterised in that
The preparation process is：
Step one, each component raw material is weighed on request；
Step 2, will grind in attapulgite modified addition grinder, is added to after crossing 100 mesh sieves in homogenizer, then add
Enter sodium carboxymethylcellulose, kushenin, malathion, ancillary additions, cementitious additives, stir 20 minutes, speed of agitator is
900r/min, obtains mixture A；
Step 3, by mixture A made from step 2, sodium citrate, livestock and poultry blood, nimbin, pyrethrins, tetramethrin, goes
Ionized water is added in Multifunction colloid grinder, and grinding rotating speed is 45 minutes in 3500 r/min, milling time, obtains paste
Mixture, paste mixture grain fineness is less than 0.045 millimeter, and paste mixture vacuum packaging is obtained into attapulgite modified
Efficient mosquito lures agent of going out.
7. a kind of attapulgite modified efficient mosquito according to claim 5 or 6 lures the preparation method for agent of going out, its feature exists
In the attapulgite modified preparation method is as follows：A, following component raw material is weighed by weight：100 parts of attapulgite, six
2 parts of sodium metaphosphate, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, 2 parts of lauryl sodium sulfate；B, will be recessed
Convex rod soil is put into the hydrochloric acid solution that concentration is 1mol/L, and heating water bath is turned to 65-75 DEG C with 500-1000r/min stirring
Speed stirring 1-2h, filtering, filter residue is washed with deionized to neutrality, drying；C, by gained material and calgon in b, gather
PAA, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 85-95 DEG C, with 500-
1000r/min speed of agitator, is stirred 40-70 minutes, is centrifuged, and sediment is washed with deionized to neutrality, is dried, so
After be placed in Muffle furnace at 420-480 DEG C and calcine 1-2h, cooling produces attapulgite modified.
8. a kind of attapulgite modified efficient mosquito according to claim 5 or 6 lures the preparation method for agent of going out, its feature exists
In the attapulgite modified preparation method is as follows：A, following component raw material is weighed by weight：100 parts of attapulgite, six
2 parts of sodium metaphosphate, 2 parts of Sodium Polyacrylate, 1 part of polyvinyl alcohol, 4 parts of silane coupler, 2 parts of lauryl sodium sulfate；B, will be recessed
Convex rod soil is put into the hydrochloric acid solution that concentration is 1mol/L, and heating water bath is stirred to 70 DEG C with 700r/min speed of agitator
1.5h, filtering, filter residue is washed with deionized to neutrality, drying；C, by gained material and calgon, polyacrylic acid in b
Sodium, polyvinyl alcohol, silane coupler, lauryl sodium sulfate mixing, and heating water bath is to 90 DEG C, is turned with 750r/min stirring
Speed, is stirred 55 minutes, is centrifuged, and sediment is washed with deionized to neutrality, drying, is subsequently placed in Muffle furnace 450
1.5h is calcined at DEG C, cooling produces attapulgite modified.
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