CN108308269A - A kind of honey peach antisepsis antistaling agent and preparation method - Google Patents
A kind of honey peach antisepsis antistaling agent and preparation method Download PDFInfo
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- 235000006040 Prunus persica var persica Nutrition 0.000 title claims abstract description 58
- 235000012907 honey Nutrition 0.000 title claims abstract description 58
- 230000003260 anti-sepsis Effects 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 240000006413 Prunus persica var. persica Species 0.000 title 1
- 244000144730 Amygdalus persica Species 0.000 claims abstract description 57
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 42
- 239000004927 clay Substances 0.000 claims abstract description 41
- 229960000892 attapulgite Drugs 0.000 claims abstract description 37
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- 241000894006 Bacteria Species 0.000 claims abstract description 33
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- 239000011347 resin Substances 0.000 claims abstract description 20
- 229920005989 resin Polymers 0.000 claims abstract description 20
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229920002472 Starch Polymers 0.000 claims abstract description 13
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 13
- 235000019698 starch Nutrition 0.000 claims abstract description 13
- 239000008107 starch Substances 0.000 claims abstract description 13
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 13
- 239000011718 vitamin C Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 52
- 239000000203 mixture Substances 0.000 claims description 25
- 239000000706 filtrate Substances 0.000 claims description 20
- 240000002234 Allium sativum Species 0.000 claims description 17
- 235000004611 garlic Nutrition 0.000 claims description 17
- 238000003756 stirring Methods 0.000 claims description 15
- 239000012065 filter cake Substances 0.000 claims description 14
- 241000205585 Aquilegia canadensis Species 0.000 claims description 12
- 241000723353 Chrysanthemum Species 0.000 claims description 12
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 12
- 241000675108 Citrus tangerina Species 0.000 claims description 12
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims description 12
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- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims description 12
- 235000009486 Crataegus bullatus Nutrition 0.000 claims description 12
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims description 12
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- 235000002313 Crataegus paludosa Nutrition 0.000 claims description 12
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- 241000522190 Desmodium Species 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 239000000725 suspension Substances 0.000 claims description 11
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 238000001802 infusion Methods 0.000 claims description 10
- 238000002604 ultrasonography Methods 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 8
- 230000002745 absorbent Effects 0.000 claims description 7
- 239000002250 absorbent Substances 0.000 claims description 7
- 238000003828 vacuum filtration Methods 0.000 claims description 7
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- 239000001814 pectin Substances 0.000 claims description 3
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- 238000012356 Product development Methods 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 238000004320 controlled atmosphere Methods 0.000 description 1
- 238000005138 cryopreservation Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
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- 241000411851 herbal medicine Species 0.000 description 1
- 230000009545 invasion Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/16—Coating with a protective layer; Compositions or apparatus therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Jellies, Jams, And Syrups (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of honey peach antisepsis antistaling agent and preparation method, the antistaling agent includes following component：Starch, high hydroscopic resin, diatomite, shale diatom ooze, modified attapulgite clay, natural bacteria remover, vitamin C.The preparation method includes：Natural bacteria remover is subjected to processing purification first, is then again uniformly mixed each component to get the antistaling agent in batches.Honey peach antisepsis antistaling agent of the present invention, can not only effectively improve the corrosion-resistanting fresh-keeping effect of honey peach, be also greatly reduced the medicament residue on honey peach surface, substantially increase the safety in utilization of honey peach, have preferable application value.
Description
Technical field
The present invention relates to agricultural and sideline product development technique fields, and in particular, to a kind of honey peach antisepsis antistaling agent and preparation
Method.
Background technology
Honey peach belongs to spherical edible fruits, there is the functions such as skin makeup, clearing stomach, moistening lung, eliminating the phlegm.Its protein contains
Amount doubles than apple, grape, seven times more than pear；The content of iron is three times more than apple, five times more than pear, is rich in a variety of dimensions
Raw element.But honey peach is how ripe in hot summer, and belong to climacteric type fruit, no matter soften rapidly after picking
It is often to cause larger economic loss, also limit there is a phenomenon where rotten all very universal after mechanical injuries or germ invasion
The extent of supply of honey peach is made.Therefore, it is necessary to carry out the preservation and freshness work of honey peach, effectively extend the storage of fresh fruit
The Tibetan phase ensures that the busy season is not rotten, and dull season is continuous, makes the stable market supply of market anniversary.Currently, the preservation method of honey peach includes mainly changing
Learn the methods of fresh-keeping, cryopreservation, air conditioned storage, radiation treatment, low temperature controlled atmosphere and tin foil.But when fresh chemically
The chemical preservative used is edible to be excessively detrimental to health to human body toxic side effect.
Therefore, research and development one kind can either honey peach corrosion-resistanting fresh-keeping effect, and can effectively reduce honey peach performance medicine
The remaining antistaling agent of object has preferable practical significance, also complies with the demand of existing market.
Invention content
For the defects in the prior art, the object of the present invention is to provide a kind of honey peach antisepsis antistaling agent and preparation sides
Method, the antistaling agent can not only effectively improve the corrosion-resistanting fresh-keeping effect of honey peach, be also greatly reduced the medicine on honey peach surface
Object remains, and substantially increases the safety in utilization of honey peach, has preferable application value.
The present invention solves technical problem and adopts the following technical scheme that：
The present invention relates to a kind of honey peach antisepsis antistaling agents, include each component of following parts by weight：8 ~ 12 parts of starch, super absorbent resin
10 ~ 17 parts of fat, 2 ~ 5 parts of diatomite, 0.5 ~ 3 part of shale diatom ooze, 3 ~ 6 parts of modified attapulgite clay, natural bacteria remover 13 ~ 19
Part, 2 ~ 6 parts of vitamin C, further include suitable water；
The natural bacteria remover includes each component of following parts by weight：
12 ~ 20 parts of Radix Glycyrrhizae, 8 ~ 15 parts of folium isatidis, 3 ~ 8 parts of heterocarpous tickclover herb, 5 ~ 13 parts of honeysuckle, 5 ~ 10 parts of Dalmatian chrysanthemum, tangerine peel 7 ~ 15
Part, 2 ~ 7 parts of hawthorn, 6 ~ 12 parts of garlic.
Preferably, the antisepsis antistaling agent includes each component of following parts by weight：9 parts of starch, 15 parts of high hydroscopic resin, silicon
1.5 parts of diatomaceous earth, 5 parts of shale diatom ooze, 5 parts of modified attapulgite clay, 17 parts of natural bacteria remover, 4 parts of vitamin C further include
Suitable water.
Preferably, the natural bacteria remover includes each component of following parts by weight：18 parts of Radix Glycyrrhizae, 12 parts of folium isatidis, dog tail
Spend 5 parts, 8 parts of honeysuckle, 6 parts of Dalmatian chrysanthemum, 12 parts of tangerine peel, 5 parts of hawthorn, 9 parts of garlic.
Preferably, the super absorbent resin is one or more mixing in polyacrylamide, chitosan, pectin.
Preferably, the modified attapulgite clay is that natural attapulgite clay is purified, is acidified, then through thermal activation
Product later.
The invention further relates to a kind of methods preparing honey peach antisepsis antistaling agent, include the following steps：
（1）Weigh each component Radix Glycyrrhizae, folium isatidis, heterocarpous tickclover herb, honeysuckle, Dalmatian chrysanthemum, the tangerine of natural bacteria remover respectively according to proportioning
Skin, hawthorn crush, and are placed in infusion tank in water mixing, 30 ~ 50min of infusion under the conditions of 80 ~ 100 DEG C, and filtering obtains filtrate
A1, it is spare；
（2）Garlic is weighed according to proportioning, is smashed to pieces, 1 ~ 2h of soak at room temperature in water is subsequently placed in, filters, obtains filtrate a2；
（3）Filtrate a1 and filtrate a2 are uniformly mixed, the vitamin C of proportional quantity is then added, stirs to being completely dissolved, is mixed
Close object a3；
（4）The starch and high hydroscopic resin of proportional quantity are added into mixture a3, is stirred 1 ~ 2h, obtains mixture a4；
（5）The diatomite, shale diatom ooze and modified attapulgite clay of proportional quantity will be separately added into mixture a4, it is fully mixed
It closes uniformly, suitable water is added, then mixture is placed under Ultrasonic Conditions and stirs 20 ~ 40min of ultrasound to get the anti-corrosion
Antistaling agent.
Preferably, the step（1）The middle quality that water is added is 8 ~ 12 times of bacteria remover each component gross mass.
Preferably, the step（2）The quality that water is added is 3 ~ 8 times of garlic quality.
Preferably, the step（5）The preparation method of modified attapulgite clay includes the following steps：
Natural attapulgite clay is crushed to and crossed 150 mesh sieve, adds water, stirring forms mud in suspension, then passes through ultrasonic wave
Under the conditions of 10 ~ 20min of ultrasound, take upper suspension 5 ~ 10min of centrifugal treating in the centrifuge of 3000 turns/min, be filtered by vacuum
Obtain filter cake；
Filter cake is placed in flask, the dilute hydrochloric acid of 2mol/L is added, wherein volume and the concave convex rod quality that dilute hydrochloric acid is added it
Than for 1mL：3g ~ 8g is stirred at reflux 20 ~ 30min in 60 ~ 80 DEG C, vacuum filtration, and wash with distilled water, obtains filter cake；
It is subsequently placed in filtration cakes torrefaction in Muffle furnace, is warming up to 800 DEG C with the heating rate of 20 DEG C/min, then constant temperature calcining
4h is to get the modified attapulgite clay.
Preferably, the step（5）The middle amount that water is added so that the water content of mixture is 70% ~ 85%.
Compared with prior art, the present invention has following advantageous effect：
（1）Honey peach antisepsis antistaling agent of the present invention, can not only effectively improve the corrosion-resistanting fresh-keeping effect of honey peach, also big
The big medicament residue for reducing honey peach surface, substantially increases the safety in utilization of honey peach, has preferable application value.
（2）The bacteria remover used in honey peach antisepsis antistaling agent of the present invention is pure natural Chinese herbal medicine ingredient, can
It is effectively prevent the growth of mould, bacterium, prevents honey peach from rotting, extends the fresh keeping time of honey peach, and the bacteria remover
Human body will not be damaged, improve safety in utilization.
（3）It is added with high hydroscopic resin in honey peach antisepsis antistaling agent of the present invention, on the one hand enables to extract
Bacteria remover ingredient can be adsorbed on super absorbent resin surface, when antistaling agent being on the other hand sprayed on honey peach surface, meeting
Form layer protecting film, one layer of protective film for being uniform-distribution with bacteria remover on the surface of honey peach so that bacteria remover can it is more preferable,
It more uniformly plays a role, condition is provided for the anti-corrosive fresh-keeping of honey peach.
（4）Modified attapulgite clay is also added in honey peach antisepsis antistaling agent of the present invention, due to concave convex rod
The unique chain layer structure of stone clay and larger specific surface area, make it have preferable absorption property, enable to bacteria remover
Ingredient uniform adsorption and the surface for being dispersed in Concave-convex clay rod, improve dispersing uniformity, along with Concave-convex clay rod has
There are preferable suspension, levelability, it is thus possible to improve the mixing uniformity between each component, avoids the precipitation of precipitation.
（5）The preparation method of honey peach antisepsis antistaling agent of the present invention is simple and convenient to operate, and process conditions are mild,
It is suitble to promote and apply.
Specific implementation mode
Present invention will be further explained below with reference to specific examples.These embodiments are merely to illustrate the present invention and do not have to
In limiting the scope of the invention.In the following examples, the experimental methods for specific conditions are not specified, usually according to normal condition, such as
Sambrook equimoleculars are cloned：Laboratory manual（New York:Cold Spring Harbor Laboratory Press,
1989）Described in condition, or according to the normal condition proposed by manufacturer.
Embodiment 1：
The present embodiment is related to a kind of honey peach antisepsis antistaling agent and preparation method；
The honey peach antisepsis antistaling agent is prepared by following component：
It is 9 parts of starch, 15 parts of high hydroscopic resin, 1.5 parts of diatomite, 5 parts of shale diatom ooze, 5 parts of modified attapulgite clay, natural
17 parts of bacteria remover, 4 parts of vitamin C, further include suitable water.
Wherein, the natural bacteria remover includes each component of following parts by weight：18 parts of Radix Glycyrrhizae, 12 parts of folium isatidis, heterocarpous tickclover herb 5
Part, 8 parts of honeysuckle, 6 parts of Dalmatian chrysanthemum, 12 parts of tangerine peel, 5 parts of hawthorn, 9 parts of garlic.
Wherein, the super absorbent resin is polyacrylamide.
Wherein, the modified attapulgite clay be natural attapulgite clay it is purified, acidification, then through thermal activation it
Product afterwards.
The method that the present invention prepares honey peach antisepsis antistaling agent, includes the following steps：
（1）Weigh each component Radix Glycyrrhizae, folium isatidis, heterocarpous tickclover herb, honeysuckle, Dalmatian chrysanthemum, the tangerine of natural bacteria remover respectively according to proportioning
Skin, hawthorn crush, and are placed in infusion tank in water mixing, the infusion 40min under the conditions of 90 ~ 100 DEG C, and filtering obtains filtrate a1,
It is spare；
（2）Garlic is weighed according to proportioning, is smashed to pieces, soak at room temperature 2h in water is subsequently placed in, filters, obtains filtrate a2；
（3）Filtrate a1 and filtrate a2 are uniformly mixed, the vitamin C of proportional quantity is then added, stirs to being completely dissolved, is mixed
Close object a3；
（4）The starch and high hydroscopic resin of proportional quantity are added into mixture a3, is stirred 2h, obtains mixture a4；
（5）The diatomite, shale diatom ooze and modified attapulgite clay of proportional quantity will be separately added into mixture a4, it is fully mixed
It closes uniformly, suitable water is added, mixture is then placed in stirring ultrasound 30min under Ultrasonic Conditions protects to get the anti-corrosion
Fresh dose.
Wherein, the step（1）The middle quality that water is added is 10 times of bacteria remover each component gross mass.
Wherein, the step（2）The quality that water is added is 6 times of garlic quality.
Wherein, the step（5）The preparation method of modified attapulgite clay includes the following steps：
Natural attapulgite clay is crushed to and crossed 150 mesh sieve, adds water, stirring forms mud in suspension, then passes through ultrasonic wave
Under the conditions of ultrasound 15min, take upper suspension centrifugal treating 10min, vacuum filtration in the centrifuge of 3000 turns/min to obtain
Filter cake；
Filter cake is placed in flask, the dilute hydrochloric acid of 2mol/L is added, wherein volume and the concave convex rod quality that dilute hydrochloric acid is added it
Than for 1mL：6g is stirred at reflux 30min in 70 DEG C, vacuum filtration, and wash with distilled water, obtains filter cake；
It is subsequently placed in filtration cakes torrefaction in Muffle furnace, is warming up to 800 DEG C with the heating rate of 20 DEG C/min, then constant temperature calcining
4h is to get the modified attapulgite clay.
Wherein, the step（5）The middle amount that water is added so that the water content of mixture is 80%.
Embodiment 2：
The present embodiment is related to a kind of honey peach antisepsis antistaling agent and preparation method；
The honey peach antisepsis antistaling agent is prepared by following component：
It is 8 parts of starch, 10 parts of high hydroscopic resin, 2 parts of diatomite, 0.5 part of shale diatom ooze, 3 parts of modified attapulgite clay, natural
13 parts of bacteria remover, 2 parts of vitamin C, further include suitable water；
The natural bacteria remover includes each component of following parts by weight：
12 parts of Radix Glycyrrhizae, 8 parts of folium isatidis, 3 parts of heterocarpous tickclover herb, 5 parts of honeysuckle, 5 parts of Dalmatian chrysanthemum, 7 parts of tangerine peel, 2 parts of hawthorn, 6 parts of garlic.
Wherein, the super absorbent resin is chitosan.
Wherein, the modified attapulgite clay be natural attapulgite clay it is purified, acidification, then through thermal activation it
Product afterwards.
The method that the present invention prepares honey peach antisepsis antistaling agent, includes the following steps：
（1）Weigh each component Radix Glycyrrhizae, folium isatidis, heterocarpous tickclover herb, honeysuckle, Dalmatian chrysanthemum, the tangerine of natural bacteria remover respectively according to proportioning
Skin, hawthorn crush, and are placed in infusion tank in water mixing, the infusion 50min under the conditions of 80 ~ 90 DEG C, and filtering obtains filtrate a1, standby
With；
（2）Garlic is weighed according to proportioning, is smashed to pieces, soak at room temperature 1h in water is subsequently placed in, filters, obtains filtrate a2；
（3）Filtrate a1 and filtrate a2 are uniformly mixed, the vitamin C of proportional quantity is then added, stirs to being completely dissolved, is mixed
Close object a3；
（4）The starch and high hydroscopic resin of proportional quantity are added into mixture a3, is stirred 1h, obtains mixture a4；
（5）The diatomite, shale diatom ooze and modified attapulgite clay of proportional quantity will be separately added into mixture a4, it is fully mixed
It closes uniformly, suitable water is added, mixture is then placed in stirring ultrasound 20min under Ultrasonic Conditions protects to get the anti-corrosion
Fresh dose.
Wherein, the step（1）The middle quality that water is added is 8 times of bacteria remover each component gross mass.
Wherein, the step（2）The quality that water is added is 3 times of garlic quality.
Wherein, the step（5）The preparation method of modified attapulgite clay includes the following steps：
Natural attapulgite clay is crushed to and crossed 150 mesh sieve, adds water, stirring forms mud in suspension, then passes through ultrasonic wave
Under the conditions of ultrasound 10min, take upper suspension centrifugal treating 5min in the centrifuge of 3000 turns/min, filtered
Cake；
Filter cake is placed in flask, the dilute hydrochloric acid of 2mol/L is added, wherein volume and the concave convex rod quality that dilute hydrochloric acid is added it
Than for 1mL：3g is stirred at reflux 30min in 60 DEG C, vacuum filtration, and wash with distilled water, obtains filter cake；
It is subsequently placed in filtration cakes torrefaction in Muffle furnace, is warming up to 800 DEG C with the heating rate of 20 DEG C/min, then constant temperature calcining
4h is to get the modified attapulgite clay.
Wherein, the step（5）The middle amount that water is added so that the water content of mixture is 70%.
Embodiment 3：
The present embodiment is related to a kind of honey peach antisepsis antistaling agent and preparation method；
The honey peach antisepsis antistaling agent is prepared by following component：
It is 12 parts of starch, 17 parts of high hydroscopic resin, 5 parts of diatomite, 3 parts of shale diatom ooze, 6 parts of modified attapulgite clay, natural
19 parts of bacteria remover, 6 parts of vitamin C, further include suitable water；
The natural bacteria remover includes each component of following parts by weight：
20 parts of Radix Glycyrrhizae, 15 parts of folium isatidis, 8 parts of heterocarpous tickclover herb, 13 parts of honeysuckle, 10 parts of Dalmatian chrysanthemum, 15 parts of tangerine peel, 7 parts of hawthorn, garlic
12 parts.
Wherein, the super absorbent resin is pectin.
Wherein, the modified attapulgite clay be natural attapulgite clay it is purified, acidification, then through thermal activation it
Product afterwards.
The method that the present invention prepares honey peach antisepsis antistaling agent, includes the following steps：
（1）Weigh each component Radix Glycyrrhizae, folium isatidis, heterocarpous tickclover herb, honeysuckle, Dalmatian chrysanthemum, the tangerine of natural bacteria remover respectively according to proportioning
Skin, hawthorn crush, and are placed in infusion tank in water mixing, the infusion 30min under the conditions of 90 ~ 100 DEG C, and filtering obtains filtrate a1,
It is spare；
（2）Garlic is weighed according to proportioning, is smashed to pieces, soak at room temperature 2h in water is subsequently placed in, filters, obtains filtrate a2；
（3）Filtrate a1 and filtrate a2 are uniformly mixed, the vitamin C of proportional quantity is then added, stirs to being completely dissolved, is mixed
Close object a3；
（4）The starch and high hydroscopic resin of proportional quantity are added into mixture a3, is stirred 2h, obtains mixture a4；
（5）The diatomite, shale diatom ooze and modified attapulgite clay of proportional quantity will be separately added into mixture a4, it is fully mixed
It closes uniformly, suitable water is added, mixture is then placed in stirring ultrasound 40min under Ultrasonic Conditions protects to get the anti-corrosion
Fresh dose.
Wherein, the step（1）The middle quality that water is added is 12 times of bacteria remover each component gross mass.
Wherein, the step（2）The quality that water is added is 8 times of garlic quality.
Wherein, the step（5）The preparation method of modified attapulgite clay includes the following steps：
Natural attapulgite clay is crushed to and crossed 150 mesh sieve, adds water, stirring forms mud in suspension, then passes through ultrasonic wave
Under the conditions of ultrasound 20min, take upper suspension centrifugal treating 10min, vacuum filtration in the centrifuge of 3000 turns/min to obtain
Filter cake；
Filter cake is placed in flask, the dilute hydrochloric acid of 2mol/L is added, wherein volume and the concave convex rod quality that dilute hydrochloric acid is added it
Than for 1mL：8g is stirred at reflux 20min in 80 DEG C, vacuum filtration, and wash with distilled water, obtains filter cake；
It is subsequently placed in filtration cakes torrefaction in Muffle furnace, is warming up to 800 DEG C with the heating rate of 20 DEG C/min, then constant temperature calcining
4h is to get the modified attapulgite clay.
Wherein, the step（5）The middle amount that water is added so that the water content of mixture is 85%.
In conclusion honey peach antisepsis antistaling agent of the present invention, the anti-corrosion that can not only effectively improve honey peach is protected
Fresh effect is also greatly reduced the medicament residue on honey peach surface, substantially increases the safety in utilization of honey peach, has preferable
Application value.In addition, the preparation method of the honey peach antisepsis antistaling agent is simple and convenient to operate, process conditions are mild, fit
Close industrialization promotion production.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (10)
1. a kind of honey peach antisepsis antistaling agent, which is characterized in that include each component of following parts by weight：8 ~ 12 parts of starch, high suction
10 ~ 17 parts of water-resin, 2 ~ 5 parts of diatomite, 0.5 ~ 3 part of shale diatom ooze, 3 ~ 6 parts of modified attapulgite clay, natural bacteria remover
13 ~ 19 parts, 2 ~ 6 parts of vitamin C, further include suitable water；
The natural bacteria remover includes each component of following parts by weight：
12 ~ 20 parts of Radix Glycyrrhizae, 8 ~ 15 parts of folium isatidis, 3 ~ 8 parts of heterocarpous tickclover herb, 5 ~ 13 parts of honeysuckle, 5 ~ 10 parts of Dalmatian chrysanthemum, tangerine peel 7 ~ 15
Part, 2 ~ 7 parts of hawthorn, 6 ~ 12 parts of garlic.
2. honey peach antisepsis antistaling agent according to claim 1, which is characterized in that the antisepsis antistaling agent includes following weight
Measure each component of part：9 parts of starch, 15 parts of high hydroscopic resin, 1.5 parts of diatomite, 5 parts of shale diatom ooze, modified attapulgite are viscous
5 parts of soil, 17 parts of natural bacteria remover, 4 parts of vitamin C, further include suitable water.
3. honey peach antisepsis antistaling agent according to claim 1, which is characterized in that the natural bacteria remover includes following weight
Measure each component of part：18 parts of Radix Glycyrrhizae, 12 parts of folium isatidis, 5 parts of heterocarpous tickclover herb, 8 parts of honeysuckle, 6 parts of Dalmatian chrysanthemum, 12 parts of tangerine peel, hawthorn 5
Part, 9 parts of garlic.
4. honey peach antisepsis antistaling agent according to claim 1, which is characterized in that the super absorbent resin is polypropylene
One or more mixing in amide, chitosan, pectin.
5. honey peach antisepsis antistaling agent according to claim 1, which is characterized in that the modified attapulgite clay is day
Right Concave-convex clay rod is purified, is acidified, then the product after thermal activation.
6. a kind of preparing the method such as claim 1 ~ 5 any one of them honey peach antisepsis antistaling agent, which is characterized in that including
Following steps：
（1）Weigh each component Radix Glycyrrhizae, folium isatidis, heterocarpous tickclover herb, honeysuckle, Dalmatian chrysanthemum, the tangerine of natural bacteria remover respectively according to proportioning
Skin, hawthorn crush, and are placed in infusion tank in water mixing, 30 ~ 50min of infusion under the conditions of 80 ~ 100 DEG C, and filtering obtains filtrate
A1, it is spare；
（2）Garlic is weighed according to proportioning, is smashed to pieces, 1 ~ 2h of soak at room temperature in water is subsequently placed in, filters, obtains filtrate a2；
（3）Filtrate a1 and filtrate a2 are uniformly mixed, the vitamin C of proportional quantity is then added, stirs to being completely dissolved, is mixed
Close object a3；
（4）The starch and high hydroscopic resin of proportional quantity are added into mixture a3, is stirred 1 ~ 2h, obtains mixture a4；
（5）The diatomite, shale diatom ooze and modified attapulgite clay of proportional quantity will be separately added into mixture a4, it is fully mixed
It closes uniformly, suitable water is added, then mixture is placed under Ultrasonic Conditions and stirs 20 ~ 40min of ultrasound to get the anti-corrosion
Antistaling agent.
7. the preparation method of honey peach antisepsis antistaling agent according to claim 6, which is characterized in that the step（1）In
The quality that water is added is 8 ~ 12 times of bacteria remover each component gross mass.
8. the preparation method of honey peach antisepsis antistaling agent according to claim 6, which is characterized in that the step（2）Add
The quality for entering water is 3 ~ 8 times of garlic quality.
9. the preparation method of honey peach antisepsis antistaling agent according to claim 6, which is characterized in that the step（5）Change
The preparation method of property Concave-convex clay rod includes the following steps：
Natural attapulgite clay is crushed to and crossed 150 mesh sieve, adds water, stirring forms mud in suspension, then passes through ultrasonic wave
Under the conditions of 10 ~ 20min of ultrasound, take upper suspension 5 ~ 10min of centrifugal treating in the centrifuge of 3000 turns/min, be filtered by vacuum
Obtain filter cake；
Filter cake is placed in flask, the dilute hydrochloric acid of 2mol/L is added, wherein volume and the concave convex rod quality that dilute hydrochloric acid is added it
Than for 1mL：3g ~ 8g is stirred at reflux 20 ~ 30min in 60 ~ 80 DEG C, vacuum filtration, and wash with distilled water, obtains filter cake；
It is subsequently placed in filtration cakes torrefaction in Muffle furnace, is warming up to 800 DEG C with the heating rate of 20 DEG C/min, then constant temperature calcining
4h is to get the modified attapulgite clay.
10. the preparation method of honey peach antisepsis antistaling agent according to claim 6, which is characterized in that the step（5）In
The amount that water is added so that the water content of mixture is 70% ~ 85%.
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| CN114097561A (en) * | 2021-12-14 | 2022-03-01 | 黑龙江新标志生物工程有限公司 | Production method of green Chinese onions with long-acting freshness preservation |
| CN118452275A (en) * | 2024-07-09 | 2024-08-09 | 西南林业大学 | Walnut preservative and preservation method |
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Application publication date: 20180724 |