CN106966364B - 一种氘化铝锂的合成工艺 - Google Patents
一种氘化铝锂的合成工艺 Download PDFInfo
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- CN106966364B CN106966364B CN201710242771.5A CN201710242771A CN106966364B CN 106966364 B CN106966364 B CN 106966364B CN 201710242771 A CN201710242771 A CN 201710242771A CN 106966364 B CN106966364 B CN 106966364B
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- lithium
- diethyl ether
- tetrahydrofuran
- deuteride
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
- C01B6/24—Hydrides containing at least two metals; Addition complexes thereof
- C01B6/243—Hydrides containing at least two metals; Addition complexes thereof containing only hydrogen, aluminium and alkali metals, e.g. Li(AlH4)
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
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- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
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CN201710242771.5A CN106966364B (zh) | 2017-04-14 | 2017-04-14 | 一种氘化铝锂的合成工艺 |
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CN201710242771.5A CN106966364B (zh) | 2017-04-14 | 2017-04-14 | 一种氘化铝锂的合成工艺 |
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CN106966364A CN106966364A (zh) | 2017-07-21 |
CN106966364B true CN106966364B (zh) | 2020-02-18 |
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Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108358167A (zh) * | 2018-02-11 | 2018-08-03 | 庄英俊 | 一种氘化铝锂的制备及检测方法 |
RU2700522C1 (ru) * | 2018-12-26 | 2019-09-17 | Акционерное общество "Государственный Ордена Трудового Красного Знамени научно-исследовательский институт химии и технологии элементоорганических соединений" (АО "ГНИИХТЭОС") | Способ получения кристаллического литийалюминийдейтерида |
CN114890442B (zh) * | 2022-06-29 | 2023-06-23 | 理道新材(北京)科技有限公司 | 一种氘化铝锂生产过程中氯化锂的回收利用方法 |
CN115215295B (zh) * | 2022-06-29 | 2023-08-22 | 理道新材(北京)科技有限公司 | α-LiAlD4及其制备方法 |
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US4529580A (en) * | 1982-12-15 | 1985-07-16 | Ethyl Corporation | Alkali metal aluminum hydride production |
CN102659080A (zh) * | 2012-05-21 | 2012-09-12 | 天津市北斗星精细化工有限公司 | 一种新型氢化铝锂的制备方法 |
CN104176749B (zh) * | 2014-07-02 | 2015-11-25 | 北京理工大学 | 一种高温直接法制备氘化锂的方法 |
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Effective date of registration: 20171225 Address after: 300071 room 53, Room 204, Southwest Village, Nankai University, Nankai District, Tianjin Applicant after: Che Yingzhao Address before: 300071 room 53, Room 204, Southwest Village, Nankai University, Nankai District, Tianjin Applicant before: Che Rongrui |
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Effective date of registration: 20200107 Address after: 061108 team 18, Zoje farm, Huanghua City, Cangzhou City, Hebei Province Applicant after: Cangzhou Lingang Star Chemical Co., Ltd. Address before: 300071, room 53, building 204, Southwest Village, Nankai University, Tianjin, Nankai District Applicant before: Che Yingzhao |
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