CN106946623A - The method that residue prepares edible fungus culturing base manure auxiliary material is extracted using purple sweet potato anthocyanin - Google Patents

The method that residue prepares edible fungus culturing base manure auxiliary material is extracted using purple sweet potato anthocyanin Download PDF

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CN106946623A
CN106946623A CN201710148518.3A CN201710148518A CN106946623A CN 106946623 A CN106946623 A CN 106946623A CN 201710148518 A CN201710148518 A CN 201710148518A CN 106946623 A CN106946623 A CN 106946623A
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residue
base manure
edible fungus
auxiliary material
fungus culturing
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米文彪
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ANHUI MILE FOOD Co Ltd
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ANHUI MILE FOOD Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D5/00Fertilisers containing magnesium
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/24Crosslinking, e.g. vulcanising, of macromolecules
    • C08J3/246Intercrosslinking of at least two polymers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/28Treatment by wave energy or particle radiation
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    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L39/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions of derivatives of such polymers
    • C08L39/04Homopolymers or copolymers of monomers containing heterocyclic rings having nitrogen as ring member
    • C08L39/06Homopolymers or copolymers of N-vinyl-pyrrolidones
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2339/00Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Derivatives of such polymers
    • C08J2339/04Homopolymers or copolymers of monomers containing heterocyclic rings having nitrogen as ring member
    • C08J2339/06Homopolymers or copolymers of N-vinyl-pyrrolidones
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2477/00Characterised by the use of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Derivatives of such polymers
    • C08J2477/04Polyamides derived from alpha-amino carboxylic acids
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    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

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Abstract

The method that residue prepares edible fungus culturing base manure auxiliary material is extracted the invention discloses a kind of utilization purple sweet potato anthocyanin, is related to purple potato processing technique field, mainly comprises the following steps:(1) extract residue to dry, (2) extract washing residue, (3) extract residue fermentation, prepared by (4) edible fungus culturing base manure auxiliary material.The present invention effectively removes the acidic materials in extracting residue by the water-washing method on the basis of using water wisely, and clearance rate reaches 99.5%;And by the use of the fertilizer auxiliary agent, strengthen the water holding capacity and diseases and insect pests resistance of made edible fungus culturing base manure auxiliary material, so as to realize that purple sweet potato anthocyanin extracts the reasonable utilization of residue, it is to avoid the wasting of resources, increase economic benefit.

Description

The method that residue prepares edible fungus culturing base manure auxiliary material is extracted using purple sweet potato anthocyanin
Technical field:
The present invention relates to purple potato processing technique field, and in particular to it is edible that one kind extracts residue preparation using purple sweet potato anthocyanin The method of bacteria cultivation base manure auxiliary material.
Background technology:
Purple potato, also known as purple sweetpotato, common perennial dicotyledon, draft, its is climing elongated, and stem is crawled ground.Purple potato Potato meat color be purple, due to rich in the health substance to human nutrition such as anthocyanidin, and be identified as special articles for use in recent years Kind.20-180mg/100 grams of anthocyanidin content, has higher edible and medical value, is a kind of pure natural health food.
At present, commonly using purple sweet potato anthocyanin extracting method mainly includes water extraction and alcohol extracting method, because the ethanol of alcohol extracting method is used Amount is big, although ethanol can be recycled, but removal process power consumption is big, and input cost is high, therefore generally selects water extraction.For The anthocyanidin for improving water extraction extracts yield, inorganic acid or organic acid can be typically added into water as extraction aid, extract solution Macroporous absorbent resin absorption, ethanol elution are recycled after filtering, and eluent is by being concentrated to give final products.As purple potato is spent The extraction of blue or green element can produce a large amount of purple potatos and extract residue, if directly discarded will cause the wasting of resources and environmental pollution.Due to Purple potato extracts residue because being in acid containing acid extraction aid, it is impossible to feed poultry directly as feed.In addition, purple potato is in flower The structure of the material such as its contained protein, starch, pectin, cellulose is destroyed in blue or green element extraction process, and its nutritive value shows Write and decline.For this case, our company develops one kind and prepares edible fungus culturing base manure using purple sweet potato anthocyanin extraction residue The method of auxiliary material, the purple potato for producing anthocyanidin extraction process is extracted residue and rationally recycled, and is provided for edible fungi growth Nutriment.
The content of the invention:
The technical problems to be solved by the invention are to provide one kind to realize that leftover bits and pieces rationally utilizes, maximizes purple potato utilization The utilization purple sweet potato anthocyanin of value extracts the method that residue prepares edible fungus culturing base manure auxiliary material.
The technical problems to be solved by the invention are realized using following technical scheme:
The method that residue prepares edible fungus culturing base manure auxiliary material is extracted using purple sweet potato anthocyanin, is mainly comprised the following steps:
(1) residue is extracted to dry:Purple sweet potato anthocyanin is extracted into residue through the contained free moisture of filter press press filtration removing, then sent Enter in freeze drier, gained solid residue is ground into fineness 2-3mm meal after fully drying using pulverizer;
(2) washing residue is extracted:In the 35-40 DEG C of water that above-mentioned gained meal is added etc. to weight, and it is small to add pre-gelatinized Wheat starch and hydroxyethyl cellulose, 0.5-1h is stood after being sufficiently mixed, then at insulated and stirred 1-2h at 35-40 DEG C, then through pressure Filter press filtration removes contained free moisture, will naturally cool to room temperature after filter residue water proof boiling 15-30min, produces fermentation residue;
(3) residue fermentation is extracted:By the water content control of above-mentioned made fermentation residue in 65-70%, and use plastic sheeting bag Wrap up in, then be transferred to stacking fermentation 7 days in 35-40 DEG C of environment, produce fermentation material;
(4) prepared by edible fungus culturing base manure auxiliary material:Compare 15-20 according to weight:0.5-1 ratio is to above-mentioned made fermentation material Middle addition fertilizer auxiliary agent, is sufficiently mixed uniformly, produces edible fungus culturing base manure auxiliary material.
The weight ratio of meal, pre-gelatinized wheaten starch and hydroxyethyl cellulose is 30-40 in the step (2):1-2: 0.5-1。
Fertilizer auxiliary agent is made up of the raw material of following parts by weight in the step (4):3-5 parts of grape skin freeze-dried powder, work Property 1-2 parts of carclazyte, Radix Isatidis extract 1-2 part of residue freeze-dried powder, 0.5-1 parts of polyglutamic acid PVPP, pellet Skin extracts 0.5-1 parts of residue freeze-dried powder, 0.1-0.3 parts of tea seed powder, 0.05-0.1 parts of sepiolite fibre powder, molecular screen primary powder 0.05-0.1 parts, its preparation method is:Sepiolite fibre powder and molecular screen primary powder are added into atlapulgite, with 5 DEG C/min's Programming rate is warming up to 110-115 DEG C of insulation mixing 5-10min, adds polyglutamic acid PVPP and tea Seed powder, continues in 110-115 DEG C of insulation mixing 5-10min, then natural cooling cools, and grape is added after temperature is down to room temperature Skin slag freeze-dried powder, Radix Isatidis extract residue freeze-dried powder and the root bark of tree peony extracts residue freeze-dried powder, are sufficiently mixed, gained mixed powder feeding It is polished to cross 60-100 mesh sieves in ball mill, produce fertilizer auxiliary agent.
The polyglutamic acid PVPP by polyglutamic acid and polyvinylpyrrolidone it is crosslinked after Association is made with modification, and its preparation method is:Polyglutamic acid and polyvinylpyrrolidone are dissolved in the water, 10-15min Triphenylphosphine and Organo-Titanate Chelates are added afterwards, microwave treater microwave treatment 5-10min are utilized after being sufficiently mixed, again fully Continue microwave treatment 3-5min after mixing, add poloxamer, ceramic and DAAM, after being well mixed again Secondary microwave treatment 5-10min, gained mixture is cooled to 0-5 DEG C of sealing thermal insulation with 5 DEG C/min cooling rate and stands 1-2h, most Micro mist is made by micronizer, polyglutamic acid PVPP is produced.
The polyglutamic acid, polyvinylpyrrolidone, triphenylphosphine, Organo-Titanate Chelates, poloxamer, ceramic Weight ratio with DAAM is 10-15:25-30:0.3-0.5:0.05-0.1:3-5:0.5-1:0.05-0.1.
The condition of work of the microwave treater is:Rated frequency 2450MHz, input power 1300W, power output 700W。
Above-mentioned made polyglutamic acid PVPP has excellent water-retaining property, is reducing the same of water consumption When play fertility controlled-release effect.
The beneficial effects of the invention are as follows:The present invention is effectively removed by the water-washing method on the basis of using water wisely The acidic materials in residue are extracted, clearance rate reaches 99.5%;And by the use of the fertilizer auxiliary agent, strengthen made edible mushroom The water holding capacity and diseases and insect pests resistance of base manure auxiliary material are cultivated, so as to realize that purple sweet potato anthocyanin extracts the reasonable utilization of residue, is kept away Exempt from the wasting of resources, increase economic benefit.
Embodiment:
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, tie below Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
(1) residue is extracted to dry:Purple sweet potato anthocyanin is extracted into residue through the contained free moisture of filter press press filtration removing, then sent Enter in freeze drier, gained solid residue is ground into fineness 2-3mm meal after fully drying using pulverizer;
(2) washing residue is extracted:In the 35-40 DEG C of water that 30 parts of meal of above-mentioned gained are added etc. to weight, and add 1 part it is pre- Wheaten starch and 0.5 part of hydroxyethyl cellulose are gelatinized, 0.5h is stood after being sufficiently mixed, then at insulated and stirred 1h at 35-40 DEG C, so Contained free moisture is removed by filter press press filtration, room temperature will be naturally cooled to after filter residue water proof boiling 15min, fermentation is produced Slag;
(3) residue fermentation is extracted:By the water content control of above-mentioned made fermentation residue in 65-70%, and use plastic sheeting bag Wrap up in, then be transferred to stacking fermentation 7 days in 35-40 DEG C of environment, produce fermentation material;
(4) prepared by edible fungus culturing base manure auxiliary material:Compare 20 according to weight:0.5 ratio adds into above-mentioned made fermentation material Enter fertilizer auxiliary agent, be sufficiently mixed uniformly, produce edible fungus culturing base manure auxiliary material.
The preparation of fertilizer auxiliary agent:0.05 part of sepiolite fibre powder and 0.05 part of molecular screen primary are added into 2 parts of atlapulgites Powder, is warming up to 110-115 DEG C of insulation mixing 10min with 5 DEG C/min programming rate, adds 1 part of polyglutamic acid crosslinking poly- Vinylpyrrolidone and 0.1 part of tea seed powder, continue in 110-115 DEG C of insulation mixing 10min, then natural cooling cools, and treats temperature Degree, which is down to after room temperature, adds 3 parts of grape skin freeze-dried powders, 1 part of Radix Isatidis extraction residue freeze-dried powder and 0.5 part of root bark of tree peony extraction residue Freeze-dried powder, is sufficiently mixed, and in gained mixed powder feeding ball mill, the polished mesh sieve of mistake 60 produces fertilizer auxiliary agent.
The preparation of polyglutamic acid PVPP:By 10 parts of polyglutamic acids and 25 parts of polyvinylpyrrolidines Ketone is dissolved in the water, and 0.5 part of triphenylphosphine and 0.05 part of Organo-Titanate Chelates are added after 15min, and microwave is utilized after being sufficiently mixed Processor microwave treatment 10min, continues microwave treatment 3min after being sufficiently mixed again, add 3 parts of poloxamers, 0.5 part of pottery Porcelain micro mist and 0.05 part of DAAM, microwave treatment 10min again after being well mixed, gained mixture is with 5 DEG C/min Cooling rate be cooled to 0-5 DEG C of sealing thermal insulation and stand 2h, micro mist most is made through micronizer afterwards, polyglutamic acid friendship is produced Join polyvinylpyrrolidone.
Wherein, the condition of work of microwave treater is:Rated frequency 2450MHz, input power 1300W, power output 700W。
Embodiment 2
(1) residue is extracted to dry:Purple sweet potato anthocyanin is extracted into residue through the contained free moisture of filter press press filtration removing, then sent Enter in freeze drier, gained solid residue is ground into fineness 2-3mm meal after fully drying using pulverizer;
(2) washing residue is extracted:In the 35-40 DEG C of water that 40 parts of meal of above-mentioned gained are added etc. to weight, and add 1 part it is pre- Wheaten starch and 0.5 part of hydroxyethyl cellulose are gelatinized, 0.5h is stood after being sufficiently mixed, then at insulated and stirred 1h at 35-40 DEG C, so Contained free moisture is removed by filter press press filtration, room temperature will be naturally cooled to after filter residue water proof boiling 15min, fermentation is produced Slag;
(3) residue fermentation is extracted:By the water content control of above-mentioned made fermentation residue in 65-70%, and use plastic sheeting bag Wrap up in, then be transferred to stacking fermentation 7 days in 35-40 DEG C of environment, produce fermentation material;
(4) prepared by edible fungus culturing base manure auxiliary material:Compare 20 according to weight:0.5 ratio adds into above-mentioned made fermentation material Enter fertilizer auxiliary agent, be sufficiently mixed uniformly, produce edible fungus culturing base manure auxiliary material.
The preparation of fertilizer auxiliary agent:0.05 part of sepiolite fibre powder and 0.05 part of molecular screen primary are added into 1 part of atlapulgite Powder, is warming up to 110-115 DEG C of insulation mixing 10min with 5 DEG C/min programming rate, adds 1 part of polyglutamic acid crosslinking poly- Vinylpyrrolidone and 0.15 part of tea seed powder, continue in 110-115 DEG C of insulation mixing 10min, then natural cooling cools, and treats temperature Degree, which is down to after room temperature, adds 5 parts of grape skin freeze-dried powders, 1 part of Radix Isatidis extraction residue freeze-dried powder and 0.5 part of root bark of tree peony extraction residue Freeze-dried powder, is sufficiently mixed, and in gained mixed powder feeding ball mill, the polished mesh sieve of mistake 60 produces fertilizer auxiliary agent.
The preparation of polyglutamic acid PVPP:By 15 parts of polyglutamic acids and 30 parts of polyvinylpyrrolidines Ketone is dissolved in the water, and 0.3 part of triphenylphosphine and 0.1 part of Organo-Titanate Chelates are added after 15min, using at microwave after being sufficiently mixed Device microwave treatment 10min is managed, continues microwave treatment 3min after being sufficiently mixed again, adds 5 parts of poloxamers, 0.5 part of ceramics Micro mist and 0.05 part of DAAM, microwave treatment 10min again after being well mixed, gained mixture is with 5 DEG C/min's Cooling rate is cooled to 0-5 DEG C of sealing thermal insulation and stands 2h, and micro mist most is made through micronizer afterwards, produces polyglutamic acid crosslinking Polyvinylpyrrolidone.
Wherein, the condition of work of microwave treater is:Rated frequency 2450MHz, input power 1300W, power output 700W。
Reference examples 1
(1) residue is extracted to dry:Purple sweet potato anthocyanin is extracted into residue through the contained free moisture of filter press press filtration removing, then sent Enter in freeze drier, gained solid residue is ground into fineness 2-3mm meal after fully drying using pulverizer;
(2) washing residue is extracted:In the 35-40 DEG C of water that 40 parts of meal of above-mentioned gained are added etc. to weight, after being sufficiently mixed 0.5h is stood, then at insulated and stirred 1h at 35-40 DEG C, then contained free moisture is removed through filter press press filtration, by filter residue water proof Room temperature is naturally cooled to after boiling 15min, fermentation residue is produced;
(3) residue fermentation is extracted:By the water content control of above-mentioned made fermentation residue in 65-70%, and use plastic sheeting bag Wrap up in, then be transferred to stacking fermentation 7 days in 35-40 DEG C of environment, produce fermentation material;
(4) prepared by edible fungus culturing base manure auxiliary material:Compare 20 according to weight:0.5 ratio adds into above-mentioned made fermentation material Enter fertilizer auxiliary agent, be sufficiently mixed uniformly, produce edible fungus culturing base manure auxiliary material.
The preparation of fertilizer auxiliary agent:0.05 part of sepiolite fibre powder and 0.05 part of molecular screen primary are added into 1 part of atlapulgite Powder, is warming up to 110-115 DEG C of insulation mixing 10min with 5 DEG C/min programming rate, adds 1 part of polyglutamic acid crosslinking poly- Vinylpyrrolidone and 0.15 part of tea seed powder, continue in 110-115 DEG C of insulation mixing 10min, then natural cooling cools, and treats temperature Degree, which is down to after room temperature, adds 5 parts of grape skin freeze-dried powders, 1 part of Radix Isatidis extraction residue freeze-dried powder and 0.5 part of root bark of tree peony extraction residue Freeze-dried powder, is sufficiently mixed, and in gained mixed powder feeding ball mill, the polished mesh sieve of mistake 60 produces fertilizer auxiliary agent.
The preparation of polyglutamic acid PVPP:By 15 parts of polyglutamic acids and 30 parts of polyvinylpyrrolidines Ketone is dissolved in the water, and 0.3 part of triphenylphosphine and 0.1 part of Organo-Titanate Chelates are added after 15min, using at microwave after being sufficiently mixed Device microwave treatment 10min is managed, continues microwave treatment 3min after being sufficiently mixed again, adds 5 parts of poloxamers, 0.5 part of ceramics Micro mist and 0.05 part of DAAM, microwave treatment 10min again after being well mixed, gained mixture is with 5 DEG C/min's Cooling rate is cooled to 0-5 DEG C of sealing thermal insulation and stands 2h, and micro mist most is made through micronizer afterwards, produces polyglutamic acid crosslinking Polyvinylpyrrolidone.
Wherein, the condition of work of microwave treater is:Rated frequency 2450MHz, input power 1300W, power output 700W。
Reference examples 2
(1) residue is extracted to dry:Purple sweet potato anthocyanin is extracted into residue through the contained free moisture of filter press press filtration removing, then sent Enter in freeze drier, gained solid residue is ground into fineness 2-3mm meal after fully drying using pulverizer;
(2) washing residue is extracted:In the 35-40 DEG C of water that 40 parts of meal of above-mentioned gained are added etc. to weight, and add 1 part it is pre- Wheaten starch and 0.5 part of hydroxyethyl cellulose are gelatinized, 0.5h is stood after being sufficiently mixed, then at insulated and stirred 1h at 35-40 DEG C, so Contained free moisture is removed by filter press press filtration, room temperature will be naturally cooled to after filter residue water proof boiling 15min, fermentation is produced Slag;
(3) residue fermentation is extracted:By the water content control of above-mentioned made fermentation residue in 65-70%, and use plastic sheeting bag Wrap up in, then be transferred to stacking fermentation 7 days in 35-40 DEG C of environment, produce fermentation material;
(4) prepared by edible fungus culturing base manure auxiliary material:Compare 20 according to weight:0.5 ratio adds into above-mentioned made fermentation material Enter fertilizer auxiliary agent, be sufficiently mixed uniformly, produce edible fungus culturing base manure auxiliary material.
The preparation of fertilizer auxiliary agent:0.05 part of sepiolite fibre powder and 0.05 part of molecular screen primary are added into 1 part of atlapulgite Powder, is warming up to 110-115 DEG C of insulation mixing 10min with 5 DEG C/min programming rate, adds 0.15 part of tea seed powder, continue 110-115 DEG C of insulation mixing 10min, then natural cooling cooling adds 5 parts of grape skins lyophilized after temperature is down to room temperature Powder, 1 part of Radix Isatidis extract residue freeze-dried powder and 0.5 part of root bark of tree peony extracts residue freeze-dried powder, are sufficiently mixed, gained mixed powder feeding In ball mill, the polished mesh sieve of mistake 60 produces fertilizer auxiliary agent.
Reference examples 3
(1) residue is extracted to dry:Purple sweet potato anthocyanin is extracted into residue through the contained free moisture of filter press press filtration removing, then sent Enter in freeze drier, gained solid residue is ground into fineness 2-3mm meal after fully drying using pulverizer;
(2) washing residue is extracted:In the 35-40 DEG C of water that 40 parts of meal of above-mentioned gained are added etc. to weight, and add 1 part it is pre- Wheaten starch and 0.5 part of hydroxyethyl cellulose are gelatinized, 0.5h is stood after being sufficiently mixed, then at insulated and stirred 1h at 35-40 DEG C, so Contained free moisture is removed by filter press press filtration, room temperature will be naturally cooled to after filter residue water proof boiling 15min, fermentation is produced Slag;
(3) residue fermentation is extracted:By the water content control of above-mentioned made fermentation residue in 65-70%, and use plastic sheeting bag Wrap up in, then be transferred to stacking fermentation 7 days in 35-40 DEG C of environment, produce fermentation material;
(4) prepared by edible fungus culturing base manure auxiliary material:Above-mentioned made fermentation material is sufficiently mixed uniformly, edible fungus culturing is produced Base manure auxiliary material.
Embodiment 3
Being utilized respectively embodiment 1, embodiment 2, reference examples 1, reference examples 2 and the methods described of reference examples 3 will be purple with batch equivalent Potato anthocyanidin extracts residue and is made edible fungus culturing base manure auxiliary material, and by made base manure auxiliary material by matched table 1 Suo Shi be made it is aqueous 65-70% edible fungus culturing base manure is measured, the cultivation with batch pleurotus eryngii is then used it for, cultural method is identical, is determined The application effect of embodiment of the present invention methods described, as a result as shown in table 2.
The edible fungus culturing base manure raw material proportioning of table 1
Project Embodiment 1 Embodiment 2 Reference examples 1 Reference examples 2 Reference examples 3
Dry sheep manure/kg 100 100 100 100 100
Cultivate base manure auxiliary material/kg 50 50 50 50 50
Wheat Straw powder/kg 20 20 20 20 20
Bagasse/kg 10 10 10 10 10
The application effect of the embodiment of the present invention methods described of table 2
Wherein, it with reference examples 3 is reference that water conservation cycle stretch-out percentage, which is,.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appending claims and its Equivalent thereof.

Claims (6)

1. extract the method that residue prepares edible fungus culturing base manure auxiliary material using purple sweet potato anthocyanin, it is characterised in that mainly include Following steps:
(1) residue is extracted to dry:Purple sweet potato anthocyanin is extracted into residue through the contained free moisture of filter press press filtration removing, is re-fed into cold In lyophilizer, gained solid residue is ground into fineness 2-3mm meal after fully drying using pulverizer;
(2) washing residue is extracted:By above-mentioned gained meal add etc. weight 35-40 DEG C of water in, and add pre-gelatinized wheat shallow lake Powder and hydroxyethyl cellulose, 0.5-1h is stood after being sufficiently mixed, then at insulated and stirred 1-2h at 35-40 DEG C, then through filter press Press filtration removes contained free moisture, will naturally cool to room temperature after filter residue water proof boiling 15-30min, produces fermentation residue;
(3) residue fermentation is extracted:The water content control of above-mentioned made fermentation residue is wrapped up in 65-70%, and with plastic sheeting, then It is transferred in 35-40 DEG C of environment and stacks fermentation 7 days, produces fermentation material;
(4) prepared by edible fungus culturing base manure auxiliary material:Compare 15-20 according to weight:0.5-1 ratio adds into above-mentioned made fermentation material Enter fertilizer auxiliary agent, be sufficiently mixed uniformly, produce edible fungus culturing base manure auxiliary material.
2. utilization purple sweet potato anthocyanin according to claim 1 extracts the method that residue prepares edible fungus culturing base manure auxiliary material, It is characterized in that:The weight ratio of meal, pre-gelatinized wheaten starch and hydroxyethyl cellulose is 30-40 in the step (2):1-2: 0.5-1。
3. utilization purple sweet potato anthocyanin according to claim 1 extracts the method that residue prepares edible fungus culturing base manure auxiliary material, Characterized in that, fertilizer auxiliary agent is made up of the raw material of following parts by weight in the step (4):3-5 parts of grape skin freeze-dried powder, 1-2 parts of atlapulgite, Radix Isatidis extract 1-2 parts of residue freeze-dried powder, 0.5-1 parts of polyglutamic acid PVPP, The root bark of tree peony extracts 0.5-1 parts of residue freeze-dried powder, 0.1-0.3 parts of tea seed powder, 0.05-0.1 parts of sepiolite fibre powder, molecular screen primary powder 0.05-0.1 parts, its preparation method is:Sepiolite fibre powder and molecular screen primary powder are added into atlapulgite, with 5 DEG C/min's Programming rate is warming up to 110-115 DEG C of insulation mixing 5-10min, adds polyglutamic acid PVPP and tea Seed powder, continues in 110-115 DEG C of insulation mixing 5-10min, then natural cooling cools, and grape is added after temperature is down to room temperature Skin slag freeze-dried powder, Radix Isatidis extract residue freeze-dried powder and the root bark of tree peony extracts residue freeze-dried powder, are sufficiently mixed, gained mixed powder feeding It is polished to cross 60-100 mesh sieves in ball mill, produce fertilizer auxiliary agent.
4. utilization purple sweet potato anthocyanin according to claim 3 extracts the method that residue prepares edible fungus culturing base manure auxiliary material, It is characterized in that:The polyglutamic acid PVPP is crosslinked with polyvinylpyrrolidone by polyglutamic acid After assist and be made with modification, its preparation method is:Polyglutamic acid and polyvinylpyrrolidone are dissolved in the water, 10- Triphenylphosphine and Organo-Titanate Chelates are added after 15min, microwave treater microwave treatment 5-10min is utilized after being sufficiently mixed, then It is secondary be sufficiently mixed after continue microwave treatment 3-5min, add poloxamer, ceramic and DAAM, mixing is equal Microwave treatment 5-10min again after even, gained mixture is cooled to 0-5 DEG C of sealing thermal insulation standing with 5 DEG C/min cooling rate 1-2h, is most made micro mist through micronizer afterwards, produces polyglutamic acid PVPP.
5. utilization purple sweet potato anthocyanin according to claim 4 extracts the method that residue prepares edible fungus culturing base manure auxiliary material, It is characterized in that:The polyglutamic acid, polyvinylpyrrolidone, triphenylphosphine, Organo-Titanate Chelates, poloxamer, ceramics The weight ratio of micro mist and DAAM is 10-15:25-30:0.3-0.5:0.05-0.1:3-5:0.5-1:0.05- 0.1。
6. utilization purple sweet potato anthocyanin according to claim 4 extracts the method that residue prepares edible fungus culturing base manure auxiliary material, It is characterized in that:The condition of work of the microwave treater is:Rated frequency 2450MHz, input power 1300W, power output 700W。
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Application publication date: 20170714