CN106929134A - One kind machining special plant oil-based coolant and preparation method thereof - Google Patents

One kind machining special plant oil-based coolant and preparation method thereof Download PDF

Info

Publication number
CN106929134A
CN106929134A CN201710206110.7A CN201710206110A CN106929134A CN 106929134 A CN106929134 A CN 106929134A CN 201710206110 A CN201710206110 A CN 201710206110A CN 106929134 A CN106929134 A CN 106929134A
Authority
CN
China
Prior art keywords
parts
plant oil
special plant
based coolant
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710206110.7A
Other languages
Chinese (zh)
Inventor
马峻
孙建明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Yasike Precision Numerical Control Co Ltd
Original Assignee
Suzhou Yasike Precision Numerical Control Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Yasike Precision Numerical Control Co Ltd filed Critical Suzhou Yasike Precision Numerical Control Co Ltd
Priority to CN201710206110.7A priority Critical patent/CN106929134A/en
Publication of CN106929134A publication Critical patent/CN106929134A/en
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/05—Metals; Alloys
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
    • C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08—Inorganic acids or salts thereof
    • C10M2201/084—Inorganic acids or salts thereof containing sulfur, selenium or tellurium
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/087—Boron oxides, acids or salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/022—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
    • C10M2207/124—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms containing hydroxy groups; Ethers thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/14—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/141—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/02—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2217/024—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to an amido or imido group
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/16—Antiseptic; (micro) biocidal or bactericidal
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/24—Emulsion properties
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/40—Low content or no content compositions
    • C10N2030/42—Phosphor free or low phosphor content compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)
  • Dental Preparations (AREA)

Abstract

The invention discloses one kind machining special plant oil-based coolant and preparation method thereof.The cooling agent includes peanut oil, glycerine, silver nano-grain, citric acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, borneol, menthol, polyethylene glycol, benzoic acid and galam butter.Preparation method：Component is weighed, citric acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, polyethylene glycol, benzoic acid are mixed into obtain composition A；Peanut oil, glycerine, borneol, galam butter are mixed into obtain composition B；40 60 DEG C will be heated in composition A input emulsification pots, add composition B, emulsion will be obtained after emulsion reaction；Mixed 5 18 minutes to silver nano-grain ultrasound is added in emulsion.Cooling agent lubricating ability of the present invention is strong, sterilized good and not phosphorous and nitrite, and long-term use will not produce influence to the body of operator.

Description

One kind machining special plant oil-based coolant and preparation method thereof
Technical field
The invention belongs to machine cooling field, and in particular to one kind machining special plant oil-based coolant and its preparation Method.
Background technology
Coolant is indispensable articles for use in mechanical processing process.In mechanical processing process, it is often necessary to change cold But liquid, after about 30% coolant is through use, will disappear or evaporates, therefore the composition of cooling agent is most important.It is existing Coolant is divided into oil base coolant and water base coolant.Both cut both ways, due to the addition of coolant, the production of machining Rate can at least improve 2 times.In view of the healthy and mechanical operating of user, urgent need wants a kind of high comprehensive performance, and The coolant that human body will not be caused serious injury.
The patent of publication number CN104673469A discloses a kind of machining and uses multi-functional cooling agent, the system of the cooling agent Preparation Method is comprised the following steps：（1）Waste oil purifies waste cooking oil or waste oil by after precipitation and filtering, taking clean oily 100 weight Amount part, is heated to 125 DEG C, standby after dehydration；（2）Ester exchange reaction takes the weight portion of triethanolamine 25, the weight of potassium hydroxide 8.5 Amount part, while a time heating of stirring, dissolves rear dewater treatment, obtains dry triethanolamine potassium；By the cleansing oil of 100 weight portions with Triethanolamine potassium mixes, and under conditions of heating stirring, carries out one hour of ester exchange reaction；After the completion of ester exchange reaction, after Continuous heating carries out etherificate dehydration, and when being warming up to 180 DEG C of anhydrous abjections, etherificate dehydration terminates.（3）Emulsification adds suitable Amount water, hydrolyzes completely at 100 DEG C, adds water stirring system breast, 0.0003 weight portion defoamer is added, when the emulsion of sampling Stop the emulsification that adds water when being dissolved in water, got product after cooling.Coolant cleaning rust cleaning effect of the present invention is substantially, with low cost, Energy-conserving and environment-protective.But unobvious, the sterilized dynamics of the cooling agent lubricant effect is not enough, and difficult degradation after discharge easily causes pollution.
The content of the invention
In view of the shortcomings of the prior art, it is an object of the invention to provide one kind machining special plant oil-based coolant, should Cooling agent lubricating ability is strong, sterilized good and not phosphorous and nitrite, and long-term use will not produce shadow to the body of operator Ring.
Another object of the present invention is to provide a kind of preparation method for machining special plant oil-based coolant, the party Method is simple and easy to apply, and emulsion that is low for equipment requirements, being formed is difficult layering.
One kind machining special plant oil-based coolant, including following weight portion meter component：Peanut oil 14-22 parts, it is sweet It is oily 14-20 parts, silver nano-grain 2-7 parts, citric acid 10-20 parts, boric acid 2-8 parts, 33-40 parts of polyacrylamide fat, deionization Water 40-50 parts, potassium carbonate 18-20 parts, sodium sulphate 28-34 parts, borneol 4-9 parts, menthol 12-19 parts, polyethylene glycol 2-9 parts, Benzoic acid 3-9 parts, galam butter 1-7 parts.
It is as improved, a diameter of 30-50 μm of the silver nano-grain.
It is as improved, also including lauric acid/dodecanoic acid 3-9 parts.
The preparation method of above-mentioned machining special plant oil-based coolant, comprises the following steps：Step 1, weighs component, will Citric acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, polyethylene glycol, benzoic acid is mixed must combine Thing A；Step 2, composition B is mixed to obtain by peanut oil, glycerine, borneol, galam butter；Step 3, breast is put into by composition A Change and 40-60 DEG C is heated in pot, emulsion is obtained after adding composition B, 120-140rpm emulsion reaction 40-60min；Step 4, to Silver nano-grain ultrasound is added to mix in emulsion 5-18 minutes.
Further improved to be, mixing speed is 150-180rpm in step 1, is stirred 2-5 minutes.
Further improved to be, mixing speed is 100-140rpm in step 2.
Further improved to be, the frequency that ultrasound is mixed in step 4 is 1300-1500Hz.
Compared with existing water base coolant and oil base coolant, cooling agent of the present invention is effectively by vegetable oil and deionization Water is mixed, and forms oil-in-water emulsion, and lubricity is good, anti-corrosion capability is strong, and productivity ratio can be improved to 45%, cutter Service life can improve more than 58%, the addition of silver nano-grain improves the thermal conductivity and bactericidal properties of cooling agent.In addition, this The preparation method of invention is simple, mixes abundant between component, low for equipment requirements, with good industrial prospect.
Specific embodiment
Embodiment 1
One kind machining special plant oil-based coolant, including following weight portion meter component：14 parts of peanut oil, 14 parts of glycerine, 2 parts of silver nano-grain, 10 parts of citric acid, 2 parts of boric acid, 33 parts of polyacrylamide fat, 40 parts of deionized water, 18 parts of potassium carbonate, sulphur 28 parts of sour sodium, 4 parts of borneol, 12 parts of menthol, 2 parts of polyethylene glycol, 3 parts of benzoic acid, 1 part of galam butter.
A diameter of 30 μm of the silver nano-grain.
The preparation method of above-mentioned machining special plant oil-based coolant, comprises the following steps：Step 1, weighs component, will Citric acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, polyethylene glycol, benzoic acid is mixed must combine Thing A；Step 2, composition B is mixed to obtain by peanut oil, glycerine, borneol, galam butter；Step 3, breast is put into by composition A Change and 40 DEG C are heated in pot, emulsion is obtained after adding composition B, 120rpm emulsion reaction 40min；Step 4, adds in emulsion Enter silver nano-grain ultrasound to mix 5 minutes.
Mixing speed is 150rpm in step 1, is stirred 2 minutes.
Mixing speed is 100rpm in step 2.
The frequency that ultrasound is mixed in step 4 is 1300Hz.
Embodiment 2
One kind machining special plant oil-based coolant, including following weight portion meter component：20 parts of peanut oil, 16 parts of glycerine, 5 parts of silver nano-grain, 15 parts of citric acid, 5 parts of boric acid, 36 parts of polyacrylamide fat, 44 parts of deionized water, 19 parts of potassium carbonate, sulphur 32 parts of sour sodium, 6 parts of borneol, 15 parts of menthol, 6 parts of polyethylene glycol, 6 parts of benzoic acid, 5 parts of galam butter.
A diameter of 40 μm of the silver nano-grain.
The preparation method of above-mentioned machining special plant oil-based coolant, comprises the following steps：Step 1, weighs component, will Citric acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, polyethylene glycol, benzoic acid is mixed must combine Thing A；Step 2, composition B is mixed to obtain by peanut oil, glycerine, borneol, galam butter；Step 3, breast is put into by composition A Change and 55 DEG C are heated in pot, emulsion is obtained after adding composition B, 120-140rpm emulsion reaction 58min；Step 4, to emulsion Middle addition silver nano-grain ultrasound is mixed 12 minutes.
Mixing speed is 170rpm in step 1, is stirred 2-5 minutes.
Mixing speed is 120rpm in step 2.
The frequency that ultrasound is mixed in step 4 is 1400Hz.
Embodiment 3
One kind machining special plant oil-based coolant, including following weight portion meter component：22 parts of peanut oil, 20 parts of glycerine, 7 parts of silver nano-grain, 20 parts of citric acid, 8 parts of boric acid, 40 parts of polyacrylamide fat, 50 parts of deionized water, 20 parts of potassium carbonate, sulphur 34 parts of sour sodium, 9 parts of borneol, 19 parts of menthol, 9 parts of polyethylene glycol, 9 parts of benzoic acid, 7 parts of galam butter.
A diameter of 50 μm of the silver nano-grain.
The preparation method of above-mentioned machining special plant oil-based coolant, comprises the following steps：Step 1, weighs component, will Citric acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, polyethylene glycol, benzoic acid is mixed must combine Thing A；Step 2, composition B is mixed to obtain by peanut oil, glycerine, borneol, galam butter；Step 3, breast is put into by composition A Change and 60 DEG C are heated in pot, emulsion is obtained after adding composition B, 140rpm emulsion reaction 60min；Step 4, adds in emulsion Enter silver nano-grain ultrasound to mix 18 minutes.
Mixing speed is 180rpm in step 1, is stirred 5 minutes.
Mixing speed is 140rpm in step 2.
The frequency that ultrasound is mixed in step 4 is 1500Hz.
Embodiment 4
One kind machining special plant oil-based coolant, including following weight portion meter component：20 parts of peanut oil, 16 parts of glycerine, 5 parts of silver nano-grain, 15 parts of citric acid, 5 parts of boric acid, 36 parts of polyacrylamide fat, 44 parts of deionized water, 19 parts of potassium carbonate, sulphur 32 parts of sour sodium, 6 parts of borneol, 15 parts of menthol, 6 parts of polyethylene glycol, 6 parts of benzoic acid, 5 parts of galam butter, lauric acid/dodecanoic acid 3-9 parts.
A diameter of 40 μm of the silver nano-grain.
The preparation method of above-mentioned machining special plant oil-based coolant, comprises the following steps：Step 1, weighs component, will Citric acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, polyethylene glycol, benzoic acid, lauric acid/dodecanoic acid mixing are stirred Mix to obtain composition A；Step 2, composition B is mixed to obtain by peanut oil, glycerine, borneol, galam butter；Step 3, by composition 55 DEG C are heated in A input emulsification pots, emulsion is obtained after adding composition B, 120-140rpm emulsion reaction 58min；Step 4, Mixed 12 minutes to silver nano-grain ultrasound is added in emulsion.
Mixing speed is 170rpm in step 1, is stirred 2-5 minutes.
Mixing speed is 120rpm in step 2.
The frequency that ultrasound is mixed in step 4 is 1400Hz.
Comparative example 1
One kind machining special plant oil-based coolant, including following weight portion meter component：20 parts of peanut oil, 16 parts of glycerine, 5 parts of silver nano-grain, 15 parts of citric acid, 5 parts of boric acid, 36 parts of polyacrylamide fat, 44 parts of deionized water, 19 parts of potassium carbonate, sulphur 32 parts of sour sodium, 6 parts of borneol, 15 parts of menthol, 6 parts of polyethylene glycol, 6 parts of benzoic acid, 5 parts of galam butter.
A diameter of 40 μm of the silver nano-grain.
The preparation method of above-mentioned machining special plant oil-based coolant, comprises the following steps：Component is weighed, by lemon Acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, polyethylene glycol, benzoic acid, peanut oil, glycerine, borneol, Galam butter is mixed, and is added silver nano-grain ultrasound and is mixed 12 minutes.
Wherein, mixing speed is 170rpm, is stirred 2-5 minutes, and the frequency that ultrasound is mixed is 1400HZ.
Cooling agent to embodiment 1-4 and comparative example 1 carries out performance test, and the data obtained is as shown in table 1 below.
It is seen from the above data that cooling agent antirust ability of the present invention is strong, sterilizing rate is high, lubricity good, substantially increases life Yield, extends cutting-tool's used life, and composition is natural, and environmental pollution is small, with good market prospects.
General principle of the invention and principal character and advantages of the present invention has been shown and described above.The technology of the industry Personnel simply illustrate this hair it will be appreciated that the present invention is not limited to the above embodiments described in above-described embodiment and specification Bright principle, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Be all fall within the protetion scope of the claimed invention with improvement, its is equivalent by appending claims for the claimed scope of the invention Thing is defined.

Claims (7)

1. it is a kind of to machine special plant oil-based coolant, it is characterised in that the component including following weight portion meter：Peanut oil 14-22 parts, glycerine 14-20 parts, silver nano-grain 2-7 parts, citric acid 10-20 parts, boric acid 2-8 parts, polyacrylamide fat 33-40 Part, deionized water 40-50 parts, potassium carbonate 18-20 parts, sodium sulphate 28-34 parts, borneol 4-9 parts, menthol 12-19 parts, poly- second two Alcohol 2-9 parts, benzoic acid 3-9 parts, galam butter 1-7 parts.
2. one kind according to claim 1 machines special plant oil-based coolant, it is characterised in that the silver nanoparticle The diameter of grain is 30-50 μm.
3. one kind according to claim 1 machines special plant oil-based coolant, it is characterised in that also including lauric acid/dodecanoic acid 3-9 parts.
4. a kind of preparation method of the machining special plant oil-based coolant being based on described in claim 1, it is characterised in that bag Include following steps：Step 1, weighs component, by citric acid, boric acid, polyacrylamide fat, deionized water, potassium carbonate, sodium sulphate, Polyethylene glycol, benzoic acid mix to obtain composition A；Step 2, peanut oil, glycerine, borneol, galam butter are mixed Composition B；Step 3, will be heated to 40-60 DEG C in composition A input emulsification pots, add composition B, 120-140rpm emulsification anti- Emulsion is obtained after answering 40-60min；Step 4, mixes 5-18 minutes to silver nano-grain ultrasound is added in emulsion.
5. it is according to claim 4 it is a kind of machine special plant oil-based coolant preparation method, it is characterised in that step Mixing speed is 150-180rpm in rapid 1, is stirred 2-5 minutes.
6. it is according to claim 4 it is a kind of machine special plant oil-based coolant preparation method, it is characterised in that step Mixing speed is 100-140rpm in rapid 2.
7. it is according to claim 4 it is a kind of machine special plant oil-based coolant preparation method, it is characterised in that step The frequency that ultrasound is mixed in rapid 4 is 1300-1500HZ.
CN201710206110.7A 2017-03-31 2017-03-31 One kind machining special plant oil-based coolant and preparation method thereof Pending CN106929134A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710206110.7A CN106929134A (en) 2017-03-31 2017-03-31 One kind machining special plant oil-based coolant and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710206110.7A CN106929134A (en) 2017-03-31 2017-03-31 One kind machining special plant oil-based coolant and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106929134A true CN106929134A (en) 2017-07-07

Family

ID=59425480

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710206110.7A Pending CN106929134A (en) 2017-03-31 2017-03-31 One kind machining special plant oil-based coolant and preparation method thereof

Country Status (1)

Country Link
CN (1) CN106929134A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1222563A (en) * 1997-06-06 1999-07-14 南宁钟氏实业发展公司 Cooling lubricat for stone cutting
CN101979482A (en) * 2010-11-15 2011-02-23 大连金泉科技发展有限公司 Environmentally-friendly lubricating coolant and preparation method
CN102942984A (en) * 2012-12-07 2013-02-27 沈阳洪达信息科技有限公司 Novel metal cooling liquid
CN104004579A (en) * 2014-05-27 2014-08-27 安徽蓝德集团股份有限公司 Rust-proof cooling solution of processing center
CN105368547A (en) * 2015-11-11 2016-03-02 安徽孟凌精密电子有限公司 Cooling solution for machining

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1222563A (en) * 1997-06-06 1999-07-14 南宁钟氏实业发展公司 Cooling lubricat for stone cutting
CN101979482A (en) * 2010-11-15 2011-02-23 大连金泉科技发展有限公司 Environmentally-friendly lubricating coolant and preparation method
CN102942984A (en) * 2012-12-07 2013-02-27 沈阳洪达信息科技有限公司 Novel metal cooling liquid
CN104004579A (en) * 2014-05-27 2014-08-27 安徽蓝德集团股份有限公司 Rust-proof cooling solution of processing center
CN105368547A (en) * 2015-11-11 2016-03-02 安徽孟凌精密电子有限公司 Cooling solution for machining

Similar Documents

Publication Publication Date Title
CN102433207B (en) A kind of cutting fluid
CN104232283B (en) Metal is fully synthetic cutting fluid and preparation method thereof for processing
CN106011877B (en) A kind of non-phosphate environment-friendly type metal surface degreasing agent and preparation method thereof
CN103305325A (en) Release agent and preparation method thereof
CN105001967A (en) Emulsified cooling liquid for processing automobile parts
CN103966011A (en) Environmental-friendly antirust cutting fluid and preparation method thereof
CN106929134A (en) One kind machining special plant oil-based coolant and preparation method thereof
CN101985577A (en) Linear cutting emulsified oil
CN105950268A (en) Metal processing multifunctional lubricating agent containing graphene additive and preparation method of metal processing multifunctional lubricating agent
CN101092727A (en) Chemic spent meal in use for processing surfaces of ferrous metal, and preparation method
CN108641796A (en) Intermetallic composite coating fully synthetic cutting fluid and preparation method thereof
CN101647760B (en) Massage emulsion
CN106190520B (en) A kind of machine cut coolant liquid
CN105296232A (en) Arnebia root handmade soap and production method thereof
CN102766515B (en) Microemulsion-type cutting fluid with good defoaming performance
CN102634421B (en) laundry detergent and preparation method thereof
CN104140876B (en) Metalworking lubricant
CN103937621A (en) Tea saponin-containing pesticide removal detergent and preparation method thereof
CN110613651A (en) Oil-removing and anti-acne facial cleanser containing hemp extract and preparation method thereof
CN102703189A (en) Preparation method of micro-emulsion cutting fluid with good antifoaming performance
CN108949331A (en) A kind of water base lathe rust preventive cutting fluid and preparation method thereof
CN104775130B (en) A kind of environment-friendly metal skimmed milk and preparation method thereof
CN111700824B (en) Alcohol-free sweet wormwood wax oil washing-free antibacterial hand sanitizer and preparation method thereof
CN109762645A (en) A kind of high-lubricity polysilicon slice water base cutting liquid and preparation method thereof
CN106883915A (en) A kind of wire drawing oil of electric wire copper wire processing and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20170707