CN108641796A - Intermetallic composite coating fully synthetic cutting fluid and preparation method thereof - Google Patents

Intermetallic composite coating fully synthetic cutting fluid and preparation method thereof Download PDF

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Publication number
CN108641796A
CN108641796A CN201810263217.XA CN201810263217A CN108641796A CN 108641796 A CN108641796 A CN 108641796A CN 201810263217 A CN201810263217 A CN 201810263217A CN 108641796 A CN108641796 A CN 108641796A
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acid
deionized water
composite coating
transparent
fully synthetic
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CN201810263217.XA
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Chinese (zh)
Inventor
熊志
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Wuhu Zhi Dao Information Technology Co Ltd
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Wuhu Zhi Dao Information Technology Co Ltd
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Priority to CN201810263217.XA priority Critical patent/CN108641796A/en
Publication of CN108641796A publication Critical patent/CN108641796A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/087—Boron oxides, acids or salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/028—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers containing aliphatic monomers having more than four carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/127—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids polycarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/22—Acids obtained from polymerised unsaturated acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C10M2207/402—Castor oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/044—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms having cycloaliphatic groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/223—Five-membered rings containing nitrogen and carbon only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/04—Detergent property or dispersant property
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention belongs to metal cutting process technical fields.The technical scheme is that：Intermetallic composite coating fully synthetic cutting fluid is made of the raw material of following mass parts：First deionized water 10~35, straight chain dodecanedicarboxylic acid 1~5, boric acid 1~6, benzotriazole 0.1~0.5, monoethanolamine 2~8, diethanol amine 5~20, D1550 aliphatic acid 3~6, ricinoleic acid 1~3, four poly- ricinoleic acids 2~7, isononanoic acid 1.6~5.2, pungent capric acid 1.2~4.3, dicyclohexyl amine 2~2.5, fatty alcohol 2~4.3, polyolefin (16 carbon) 1~2.6, isomery octadecanol 1~2, second deionized water 10~70, fungicide 1~3 and antifoaming agent 0.1~1.The invention has the advantages that the intermetallic composite coating is low with fully synthetic cutting use cost, dilution is not easy corruption and generates peculiar smell, and greasy property is good, and the usage time period is long.

Description

Intermetallic composite coating fully synthetic cutting fluid and preparation method thereof
Technical field
The invention belongs to metal cutting process technical fields, more particularly to intermetallic composite coating fully synthetic cutting fluid and its preparation Method.
Background technology
When metal cutting process, generally use cutting fluid cools down and lubricates cutter.Tradition cutting liquid product use cost The shortcomings of height, the easy corruption generation peculiar smell of dilution, lack of lubrication, the usage time period is short.
Invention content
Present invention aims at provide a kind of intermetallic composite coating fully synthetic cutting fluid, the intermetallic composite coating fully synthetic cutting fluid Use cost is low, and dilution is not easy corruption and generates peculiar smell, and greasy property is good, and the usage time period is long.
To achieve the above object, the present invention adopts the following technical scheme that：
Intermetallic composite coating fully synthetic cutting fluid of the present invention, is made of the raw material of following mass parts：First deionized water 10~ 35, straight chain dodecanedicarboxylic acid 1~5, boric acid 1~6, benzotriazole 0.1~0.5, monoethanolamine 2~8, diethanol amine 5~ 20, D1550 aliphatic acid 3~6, ricinoleic acid 1~3, four poly- ricinoleic acids 2~7, isononanoic acid 1.6~5.2, pungent capric acid 1.2~ 4.3, dicyclohexyl amine 2~2.5, fatty alcohol 2~4.3, polyolefin (16 carbon) 1~2.6, isomery octadecanol 1~2, second goes Ionized water 10~70, fungicide 1~3 and antifoaming agent 0.1~1.
In this product, deionized water, which plays, helps solubility property, and straight chain dodecanedicarboxylic acid is mainly anti-rust action, D1550 fat Fat acid primarily serves lubrication and anti-rust action, and (aliphatic acid of Long carbon chain has absorption anti-rust action well to metal, and can improve Lubricity), polyolefin (16 carbon) and fatty alcohol play lubricating action, and amine and other fatty acid responses generate esters and play profit Sliding, antirust and cleaning action, isononanoic acid mainly play dissolution assistant effect and so that product is more stable.This product solve traditional product use at This height, dilution is easy corruption and generates peculiar smell, the shortcomings of lack of lubrication, the usage time period is short, also have outstanding cooling and Cleaning rust-proof performance makes metal working lubricant product obtain certain progress in terms of machining lubrication, the maximum spy of the product Point is exactly the lubricity requirement for the heavy processing method that can ensure the difficult Material Processing of some in machining, meanwhile, product is free of There are base oil component, usage time that can greatly extend.
Present invention simultaneously provides a kind of production technologies of intermetallic composite coating fully synthetic cutting fluid：Include the following steps：
Step 1: by the first deionized water, straight chain dodecanedicarboxylic acid, boric acid and benzotriazole are put into reaction kettle, (40 ± 5) DEG C are then heated to, and open stirring, mixing time is (10 ± 5) min；
Step 2: input monoethanolamine, and stirring makes solid be completely dissolved to transparent, and the control of whipping process temperature exists (40 ± 5) DEG C, mixing time are (30 ± 5) min；
Step 3: D1550 aliphatic acid, ricinoleic acid, four poly- ricinoleic acids, isononanoic acid and pungent capric acid are put into successively, stirring To homogeneous transparent, for the control of whipping process temperature in (40 ± 5) DEG C, mixing time is (10 ± 5) min；
Step 4: input dicyclohexyl amine, be stirred until homogeneous it is transparent, whipping process temperature control at (40 ± 5) DEG C, stirring Between be (10 ± 5) min；
Step 5: input fatty alcohol, polyolefin (16 carbon) and isomery octadecanol, stirring to transparent, whipping process temperature In (40 ± 5) DEG C, mixing time is (30 ± 5) min. for degree control；
Step 6: stopping heating, the second deionized water is put into, then detection chemical examination, qualification confirms；
Step 7: input fungicide, and stir to transparent, then sample detection, qualification confirm；
Step 8: input antifoaming agent, and packed after stirring evenly.
The invention has the advantages that the intermetallic composite coating is low with fully synthetic cutting use cost, dilution is not easy corrupt production Raw peculiar smell, greasy property is good, and the usage time period is long.
Specific implementation mode
Embodiment 1, intermetallic composite coating fully synthetic cutting fluid of the present invention, is made of the raw material of following mass parts：First go from Sub- water 10~35, straight chain dodecanedicarboxylic acid 1~5, boric acid 1~6, benzotriazole 0.1~0.5, monoethanolamine 2~8, diethyl Hydramine 5~20, D1550 aliphatic acid 3~6, ricinoleic acid 1~3, four poly- ricinoleic acids 2~7, isononanoic acid 1.6~5.2, pungent capric acid 1.2~4.3, dicyclohexyl amine 2~2.5, fatty alcohol 2~4.3, polyolefin (16 carbon) 1~2.6, isomery octadecanol 1~2, the Two deionized waters 10~70, fungicide 1~3 and antifoaming agent 0.1~1.
Present invention simultaneously provides a kind of production technologies of intermetallic composite coating fully synthetic cutting fluid：Include the following steps：
Step 1: by the first deionized water, straight chain dodecanedicarboxylic acid, boric acid and benzotriazole are put into reaction kettle, (40 ± 5) DEG C are then heated to, and open stirring, mixing time is (10 ± 5) min；
Step 2: input monoethanolamine, and stirring makes solid be completely dissolved to transparent, and the control of whipping process temperature exists (40 ± 5) DEG C, mixing time are (30 ± 5) min；
Step 3: D1550 aliphatic acid, ricinoleic acid, four poly- ricinoleic acids, isononanoic acid and pungent capric acid are put into successively, stirring To homogeneous transparent, for the control of whipping process temperature in (40 ± 5) DEG C, mixing time is (10 ± 5) min；
Step 4: input dicyclohexyl amine, be stirred until homogeneous it is transparent, whipping process temperature control at (40 ± 5) DEG C, stirring Between be (10 ± 5) min；
Step 5: input fatty alcohol, polyolefin (16 carbon) and isomery octadecanol, stirring to transparent, whipping process temperature In (40 ± 5) DEG C, mixing time is (30 ± 5) min. for degree control；
Step 6: stopping heating, the second deionized water is put into, then detection chemical examination, qualification confirms；
Step 7: input fungicide, and stir to transparent, then sample detection, qualification confirm；
Step 8: input antifoaming agent, and packed after stirring evenly.
Embodiment described above is only that the preferred embodiment of the present invention is described, not to the model of the present invention It encloses and is defined, under the premise of not departing from design spirit of the present invention, technical side of the those of ordinary skill in the art to the present invention The various modifications and improvement that case is made should all be fallen into the protection domain of claims of the present invention determination.

Claims (2)

1. a kind of intermetallic composite coating fully synthetic cutting fluid, it is characterized in that：It is made of the raw material of following mass parts：First deionized water 10~35, straight chain dodecanedicarboxylic acid 1~5, boric acid 1~6, benzotriazole 0.1~0.5, monoethanolamine 2~8, diethanol amine 5~20, D1550 aliphatic acid 3~6, ricinoleic acid 1~3, four poly- ricinoleic acids 2~7, isononanoic acid 1.6~5.2, pungent capric acid 1.2 ~4.3, dicyclohexyl amine 2~2.5, fatty alcohol 2~4.3, polyolefin (16 carbon) 1~2.6, isomery octadecanol 1~2, second Deionized water 10~70, fungicide 1~3 and antifoaming agent 0.1~1.
2. a kind of method preparing intermetallic composite coating fully synthetic cutting fluid as described in claim 1, characterized in that including walking as follows Suddenly：
Step 1: by the first deionized water, straight chain dodecanedicarboxylic acid, boric acid and benzotriazole are put into reaction kettle, then (40 ± 5) DEG C are warming up to, and open stirring, mixing time is (10 ± 5) min；
Step 2: input monoethanolamine, and stirring makes solid be completely dissolved to transparent, the control of whipping process temperature (40 ± 5) DEG C, mixing time is (30 ± 5) min；
Step 3: putting into D1550 aliphatic acid, ricinoleic acid, four poly- ricinoleic acids, isononanoic acid and pungent capric acid successively, stir to equal Even transparent, for the control of whipping process temperature in (40 ± 5) DEG C, mixing time is (10 ± 5) min；
Step 4: input dicyclohexyl amine, be stirred until homogeneous it is transparent, whipping process temperature control in (40 ± 5) DEG C, mixing time is (10±5)min；
Step 5: input fatty alcohol, polyolefin (16 carbon) and isomery octadecanol, stirring to transparent, whipping process temperature control For system in (40 ± 5) DEG C, mixing time is (30 ± 5) min.；
Step 6: stopping heating, the second deionized water is put into, then detection chemical examination, qualification confirms；
Step 7: input fungicide, and stir to transparent, then sample detection, qualification confirm；
Step 8: input antifoaming agent, and packed after stirring evenly.
CN201810263217.XA 2018-03-28 2018-03-28 Intermetallic composite coating fully synthetic cutting fluid and preparation method thereof Withdrawn CN108641796A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113249163A (en) * 2021-05-25 2021-08-13 烟台诺贝国际贸易有限公司 Microemulsion and preparation method thereof
CN113999717A (en) * 2021-06-23 2022-02-01 盐城杰润科技有限公司 Stable water-based stamping forging liquid and production process thereof
CN115521825A (en) * 2022-11-07 2022-12-27 季华实验室 Water-based punching liquid and preparation method and application thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113249163A (en) * 2021-05-25 2021-08-13 烟台诺贝国际贸易有限公司 Microemulsion and preparation method thereof
CN113999717A (en) * 2021-06-23 2022-02-01 盐城杰润科技有限公司 Stable water-based stamping forging liquid and production process thereof
CN115521825A (en) * 2022-11-07 2022-12-27 季华实验室 Water-based punching liquid and preparation method and application thereof
CN115521825B (en) * 2022-11-07 2023-11-21 季华实验室 Water-based stamping liquid and preparation method and application thereof

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Application publication date: 20181012