CN106924074A - A kind of colorful washing product and preparation method thereof - Google Patents
A kind of colorful washing product and preparation method thereof Download PDFInfo
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- CN106924074A CN106924074A CN201710317584.9A CN201710317584A CN106924074A CN 106924074 A CN106924074 A CN 106924074A CN 201710317584 A CN201710317584 A CN 201710317584A CN 106924074 A CN106924074 A CN 106924074A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
Abstract
The invention discloses a kind of colorful washing product and preparation method thereof.Colorful washing product of the invention according to weight than each group be divided into：400 600 parts of cleaning solution of toning, 100 200 parts of protecting colloid, 300 400 parts of continuous phase cleaning solution.Colorful washing product color of the present invention appears, pleasing, gives the enjoyment of U.S.；The washing product using the raw material of environmental protection, will not have a negative impact to human body and environment；The washing product technical indicator meets national standard；The mature preparation process of the washing product, adapts to industrialized production.
Description
Technical field
The invention belongs to field of fine chemical, and in particular to a kind of colorful washing product and preparation method thereof.
Background technology
Washing product is family's essential product, usually including shampoo, shower cream, hand cleanser etc..As health of people is anticipated
The continuous enhancing known, the washing product of all kinds of brands is a feast for the eyes on the market.In order to win the market, manufacturers try one's best and beat
Make product miscellaneous.They are formulated health environment-friendly, and effect different properties, Packaging Color appears, handsome in appearance generous.Compare
Under, the content that consumer more takes notice of state in itself but has no characteristic can be sayed.Now, on the market washing product it is basic with
Based on transparent or monochromatic fluid, only only a few product has pearl effect due to adding pearling agent in monochromatic fluid.Product
Homogeneity allow consumer have no way of selection.
The content of the invention
The purpose of the present invention is to solve the shortcomings of the prior art, there is provided a kind of colorful washing product and preparation method thereof.
The made colorful washing product color of the present invention appears, pleasing, the enjoyment of U.S. is given, using the original of environmental protection
Material, will not have a negative impact to human body and environment, and technical indicator meets national standard, and mature preparation process adapts to industrialization
Big production.
To achieve the above object, the present invention is adopted the following technical scheme that：
A kind of colorful washing product, is made up of the raw material of following weight portion：400-600 parts of cleaning solution of toning, protecting colloid 100-
200 parts and 300-400 parts of continuous phase cleaning solution；Described protecting colloid is made up of the raw material of following weight portion：Deionized water
850-950 parts, preservative 1-3 parts, protect 50-150 parts of rubber powder；Described continuous phase cleaning solution by following weight portion raw material group
Into：Deionized water 650-800 parts, anion surfactant 80-200 parts, zwitterionic surfactant 30-80 parts, it is non-from
Sub- surfactant 30-80 parts, thickener 5-20 parts, pH adjusting agent 0-5 parts, water softener 1-3 parts, preservative 1-3 parts, dyestuff 0-
5 parts；The protection rubber powder is lithium magnesium silicate, aluminium-magnesium silicate, sodium carboxymethylcellulose, hydroxyethyl cellulose and hydroxypropyl cellulose
In one or more.
In described continuous phase cleaning solution, anion surfactant is laureth sodium sulfovinate, coceth
One or more in sodium sulfovinate, stereth sodium sulfovinate and neopelex, amphion surface-active
Agent is Cocoamidopropyl betaine, palmitamide CAB, empgen BB, myristyl betaine, cocounut oil
One kind or several in amido propyl amine-oxides, palmitamide propyl group amine-oxides, dodecyl amine-oxides and myristyl amine-oxides
Kind, nonionic surfactant is cocamide, lauryl acid amides, palmityl acid amides, coconut oleyl fatty acid diethanol acyl
Amine, octanol base glucosides, decyl alcohol base glucosides, bay alcohol radical glucosides, palm alcohol radical glucosides, octanol base APEO, bay alcohol radical
One or more in APEO and palm alcohol radical APEO, thickener is guar gum, Carbomer, carboxymethyl cellulose
One or more in plain sodium, hydroxyethyl cellulose, hydroxypropyl cellulose, pH adjusting agent is citric acid, sodium dihydrogen phosphate, hydrogen-oxygen
Change one or more in sodium, potassium hydroxide, ammoniacal liquor, diethanol amine and triethanolamine, water softener is disodium ethylene diamine tetraacetate
Or the one kind in the sodium of diethylene triamine pentacetic acid (DTPA) five, preservative is the one kind in Kathon CG and Phenoxyethanol.
The preparation method of protecting colloid is：
1）The deionized water of formula ratio is put into reactor, 400-500 revs/min of rotating speed is controlled；
2）The protection rubber powder of 1/2 formula ratio and the preservative of formula ratio are put into in reactor, stirring 30-40 minute to dissolving；
3）Input surplus protects rubber powder in reactor, is stirred 30-40 minutes under same rotational speed, obtains final product protecting colloid.
The preparation method of continuous phase cleaning solution is：
1）By in the deionized water addition reactor of formula ratio, 150-200 revs/min of rotating speed is controlled, sequentially add water softener, the moon
Ionic surface active agent, zwitterionic surfactant and nonionic surfactant, stir 30-40 minutes, until completely molten
Solution；
2）Thickener is slowly added to, is stirred 30-40 minutes；
3）Preservative and dyestuff are added, is stirred 10-15 minutes；
4）The pH of base paint is determined using pH meter, if necessary, addition qs pH adjuster makes system pH=7 or so, is obtained final product continuous
Phase cleaning solution.
The toning cleaning solution is made up of the raw material of following weight portion：980-1000 parts, dyestuff 0-5 parts of basic cleaning liquid；
Described dyestuff is assorted cosmetics-stage transparency dye.
The basic cleaning liquid is made up of the raw material of following weight portion：Deionized water 550-650 parts, protecting colloid 100-
150 parts, anion surfactant 80-200 parts, zwitterionic surfactant 30-80 parts, nonionic surfactant 30-
80 parts, thickener 5-20 parts, pH adjusting agent 0-5 parts, water softener 1-3 parts, preservative 1-3 parts.
In basic cleaning liquid, described anion surfactant is laureth sodium sulfovinate, coceth sulphur
One or more in acid esters sodium, stereth sodium sulfovinate and neopelex；Described amphion surface
Activating agent be Cocoamidopropyl betaine, palmitamide CAB, empgen BB, myristyl betaine,
One kind in cocamidopropyl propyl amide amine-oxides, palmitamide propyl group amine-oxides, dodecyl amine-oxides and myristyl amine-oxides
Or it is several；Described nonionic surfactant is cocamide, lauryl acid amides, palmityl acid amides, octanol base glucosides, the last of the ten Heavenly stems
One or more in alcohol radical glucosides, bay alcohol radical glucosides, palm alcohol radical glucosides and coconut oil base fatty diglycollic amide；Institute
The thickener stated be guar gum, Carbomer, sodium carboxymethylcellulose, hydroxyethyl cellulose and hydroxypropyl cellulose in one kind or
It is several；The pH adjusting agent is citric acid, sodium dihydrogen phosphate, NaOH, potassium hydroxide, ammoniacal liquor, diethanol amine and three ethanol
One or more in amine；Described water softener is in disodium ethylene diamine tetraacetate and the sodium of diethylene triamine pentacetic acid (DTPA) five
Kind；Described preservative is the one kind in Kathon CG and Phenoxyethanol；The described protecting colloid is lithium magnesium silicate, magnesium silicate
One or more in aluminium, sodium carboxymethylcellulose, hydroxyethyl cellulose and hydroxypropyl cellulose.
Mix colours cleaning solution preparation process be：
1）By in the deionized water addition reactor of formula ratio, 150-200 revs/min of rotating speed is controlled, sequentially add anion table
Face activating agent, zwitterionic surfactant, nonionic surfactant is stirred 30-40 minutes, until being completely dissolved；
2）Thickener is slowly added to, is stirred 30-40 minutes；
3）Protecting colloid is added, is stirred 30-40 minutes；
4）Preservative is added, is stirred 10-15 minutes；
5）Adding qs pH adjuster makes system pH=7, obtains final product basic cleaning liquid；
6）By in the basic cleaning liquid addition reactor of formula ratio, stirred with 200-300 revs/min of speed；
7）The required dyestuff of formula ratio is separately added into, is stirred 20-30 minutes, obtain final product toning cleaning solution.
A kind of method for preparing colorful washing product as described above, including step as described below：
1）Stirred during the protecting colloid of formula ratio is added into reactor, control mixing speed is at 100-150 revs/min；
2）By the toning cleaning solution of formula ratio by comminutor, gained particle is directly added into protecting colloid, and granulation terminates follow-up
Continuous stirring 10-15 minutes；
3）Continuous phase cleaning solution is slowly added to reactor, 20-30 minutes is stirred with 100-150 revs/min of speed, i.e., much
Color washing product.
The beneficial effects of the present invention are：
1）The made novel colorful washing product color of the present invention appears, pleasing, gives the enjoyment of U.S.；
2）Made washing product using the raw material of environmental protection, will not have a negative impact to human body and environment；
3）Made washing product technical indicator meets national standard；
4）The mature preparation process of made washing product, adapts to industrialized production.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described.
Obviously, described embodiment is only a part of the invention, and based on the embodiment in the present invention, those skilled in the art exist
The every other embodiment obtained under the premise of creative work is not made, the scope of protection of the invention is belonged to.
Embodiment 1
A kind of colorful shampoo, is made up of the raw material of following weight portion：550 parts of cleaning solution of toning, 100 parts of protecting colloid and continuous
350 parts of phase cleaning solution.
1st, the preparation of protecting colloid：
Protecting colloid is made up of the raw material of following weight portion：917 parts of deionized water, 3 parts of Kathon CG, 80 parts of lithium magnesium silicate.
The preparation process of protecting colloid is：
1）The deionized water of formula ratio is put into reactor, 500 revs/min of rotating speed is controlled；
2）The Preservative Kathon CG(Methylchloroisothiazolinone/Methylisothiazolinone combination) of the lithium magnesium silicate and formula ratio that put into 1/2 formula ratio is added in reactor, and stirring 40 minutes is to molten
Solution；
3）Input surplus lithium magnesium silicate is stirred 40 minutes in reactor under same rotational speed, obtains final product protecting colloid.
2nd, the preparation of continuous phase cleaning solution：
Continuous phase cleaning solution is made up of the raw material of following weight portion：687 parts of deionized water, 150 parts of laureth sodium sulfovinate,
70 parts of Cocoamidopropyl betaine, 60 parts of octanol base APEO, 10 parts of Carbomer, 10 parts of hydroxyethyl cellulose, hydrogen-oxygen
Change 4 parts of sodium, 3 parts of disodium ethylene diamine tetraacetate, 3 parts of Kathon CG, 3 parts of blue dyes.
The preparation process of continuous phase is：
1）By in the deionized water addition reactor of formula ratio, 200 revs/min of rotating speed is controlled, sequentially add ethylenediamine tetra-acetic acid
Disodium, laureth sodium sulfovinate, Cocoamidopropyl betaine and octanol base APEO, stir 30 minutes, until
It is completely dissolved；
2）It is slow to sequentially add Carbomer and hydroxyethyl cellulose, stir 40 minutes；
3）Kathon CG and blue dyes are added, is stirred 10 minutes；
4）Adding NaOH makes system pH=7, obtains final product continuous phase cleaning solution.
3rd, the preparation of toning cleaning solution：
Toning cleaning solution is made up of the raw material of following weight portion：995 parts of basic cleaning liquid, 5 parts of dyestuff.
Basic cleaning liquid is made up of the raw material of following weight portion：600 parts of deionized water, 100 parts of protecting colloid, bay alcohol radical
150 parts of polyethers sodium sulfovinate, 70 parts of Cocoamidopropyl betaine, 60 parts of octanol base APEO, 10 parts of guar gum, hydrogen-oxygen
Change 4 parts of sodium, 3 parts of disodium ethylene diamine tetraacetate, 3 parts of Kathon CG.
Mix colours cleaning solution preparation process be：
1）By in the deionized water addition reactor of formula ratio, 200 revs/min of rotating speed is controlled, sequentially add laureth sulphur
Acid esters sodium, Cocoamidopropyl betaine and octanol base APEO, stir 30 minutes, until being completely dissolved；
2）Guar gum is slowly added to, is stirred 30 minutes；
3）Disodium ethylene diamine tetraacetate is added, is stirred 30 minutes；
4）Preservative Kathon CG(Methylchloroisothiazolinone/Methylisothiazolinone combination) is added, is stirred 10 minutes；
5）Adding NaOH makes system pH=7 or so, obtains final product basic cleaning liquid；
6）By in the basic cleaning liquid addition reactor of formula ratio, stirred with 300 revs/min of speed；
7）The green colouring material of formula ratio is separately added into, is stirred 20 minutes, obtain final product green cleaning solution.
Red and white cleaning solution preparation process is identical with green cleaning solution.
The preparation process of wherein described basic cleaning liquid is：
4th, the preparation of colorful shampoo, comprises the following steps：
1）Stirred during the protecting colloid of formula ratio is added into reactor, control mixing speed is at 150 revs/min；
2）By the toning cleaning solution of formula ratio by comminutor, gained particle is directly added into protecting colloid, and granulation terminates follow-up
Continuous stirring 10 minutes；
3）Continuous phase cleaning solution is slowly added to reactor, is stirred 20 minutes with 150 revs/min of speed.Obtain final product colorful hair washing
Dew A.
Embodiment 2
A kind of colorful shampoo, is made up of the raw material of following weight portion：550 parts of cleaning solution of toning, 150 parts of protecting colloid, continuously
300 parts of phase cleaning solution.
1st, the preparation of protecting colloid：
Protecting colloid is made up of the raw material of following weight portion：917 parts of deionized water, 3 parts of Phenoxyethanol, 80 parts of aluminium-magnesium silicate.
The preparation process of protecting colloid is：
1）The deionized water of formula ratio is put into reactor, 500 revs/min of rotating speed is controlled；
2）The preservative Phenoxyethanol of the aluminium-magnesium silicate and formula ratio that put into 1/2 formula ratio is added in reactor, is stirred 40 minutes
To dissolving；
3）Input surplus aluminium-magnesium silicate is stirred 40 minutes in reactor under same rotational speed, obtains final product protecting colloid.
2nd, the preparation of continuous phase cleaning solution：
Continuous phase cleaning solution is made up of the raw material of following weight portion：687 parts of deionized water, 120 parts of octanol base polyethers sodium sulfovinate,
80 parts of cocamidopropyl propyl amide amine-oxides, 80 parts of bay alcohol radical APEO, 10 parts of Carbomer, 10 parts of hydroxyethyl cellulose, hydrogen
4 parts of sodium oxide molybdena, 3 parts of disodium ethylene diamine tetraacetate, 3 parts of Phenoxyethanol, 3 parts of white dye.
The preparation process of continuous phase is：
1）By in the deionized water addition reactor of formula ratio, 200 revs/min of rotating speed is controlled, sequentially add ethylenediamine tetra-acetic acid
Disodium, laureth sodium sulfovinate, Cocoamidopropyl betaine and octanol base APEO, stir 30 minutes, until
It is completely dissolved；
2）It is slow to sequentially add Carbomer and hydroxyethyl cellulose, stir 40 minutes；
3）Phenoxyethanol and white dye are added, is stirred 10 minutes；
4）Adding NaOH makes system pH=7, obtains final product continuous phase cleaning solution.
3rd, the preparation of toning cleaning solution：
Toning cleaning solution is made up of the raw material of following weight portion：995 parts of basic cleaning liquid, 5 parts of blue dyes.
Basic cleaning liquid is made up of the raw material of following weight portion：600 parts of deionized water, 100 parts of protecting colloid, octanol base gathers
120 parts of ether sodium sulfovinate, 80 parts of cocamidopropyl propyl amide amine-oxides, 80 parts of octanol base APEO, 10 parts of guar gum, hydroxide
4 parts of sodium, 3 parts of disodium ethylene diamine tetraacetate, 3 parts of Phenoxyethanol.
Mix colours cleaning solution preparation process be：
1）By in the deionized water addition reactor of formula ratio, 200 revs/min of rotating speed is controlled, sequentially add octanol base polyether thiourea
Acid esters sodium, cocamidopropyl propyl amide amine-oxides, laureth is stirred 30 minutes, until being completely dissolved；
2）Guar gum is slowly added to, is stirred 30 minutes；
3）Disodium ethylene diamine tetraacetate is added, is stirred 30 minutes；
4）Phenoxyethanol is added, is stirred 10 minutes；
5）Adding NaOH makes system pH=7, obtains final product basic cleaning liquid；
6）By in the basic cleaning liquid addition reactor of formula ratio, stirred with 300 revs/min of speed；
7）The blue dyes of formula ratio is separately added into, is stirred 20 minutes, obtain final product blue cleaning solution.
The preparation method of colorful shampoo, comprises the following steps：
1）Stirred during the protecting colloid of formula ratio is added into reactor, control mixing speed is at 150 revs/min；
2）By the toning cleaning solution of formula ratio by comminutor, gained particle is directly added into protecting colloid, and granulation terminates follow-up
Continuous stirring 10 minutes；
3）Continuous phase cleaning solution is slowly added to reactor, is stirred 20 minutes with 150 revs/min of speed.Obtain final product novel colorful
Washing product B.
The physical and chemical index of the colorful shampoo A and B obtained by embodiment 1 and embodiment 2 is as shown in table 1.
The physical and chemical index of the colorful shampoo A and B obtained by the embodiment 1 of table 1. and embodiment 2
The foregoing is only presently preferred embodiments of the present invention, all impartial changes done according to scope of the present invention patent with repair
Decorations, should all belong to covering scope of the invention.
Claims (10)
1. a kind of colorful washing product, it is characterised in that：It is made up of the raw material of following weight portion：400-600 parts of cleaning solution of toning,
Protecting colloid 100-200 parts and 300-400 parts of continuous phase cleaning solution；Described protecting colloid by following weight portion raw material group
Into：Deionized water 850-950 parts, preservative 1-3 parts, protect 50-150 parts of rubber powder；Described continuous phase cleaning solution is by following heavy
Measure the raw material composition of part：Deionized water 650-800 parts, anion surfactant 80-200 parts, zwitterionic surfactant
30-80 parts, nonionic surfactant 30-80 parts, thickener 5-20 parts, pH adjusting agent 0-5 parts, water softener 1-3 parts, preservative
1-3 parts, dyestuff 0-5 parts.
2. colorful washing product according to claim 1, it is characterised in that：The protection rubber powder is lithium magnesium silicate, silicic acid
One or more in magnalium, sodium carboxymethylcellulose, hydroxyethyl cellulose and hydroxypropyl cellulose.
3. colorful washing product according to claim 1, it is characterised in that：In described continuous phase cleaning solution, anion
Surfactant is laureth sodium sulfovinate, coceth sodium sulfovinate, stereth sodium sulfovinate and dodecane
One or more in base benzene sulfonic acid sodium salt, zwitterionic surfactant is Cocoamidopropyl betaine, palmitamide propyl group
Glycine betaine, empgen BB, myristyl betaine, cocamidopropyl propyl amide amine-oxides, palmitamide propyl group amine-oxides, ten
One or more in dialkyl group amine-oxides and myristyl amine-oxides, nonionic surfactant is cocamide, bay
Base acid amides, palmityl acid amides, coconut oil base fatty diglycollic amide, octanol base glucosides, decyl alcohol base glucosides, bay alcohol radical sugar
In glycosides, palm alcohol radical glucosides, octanol base APEO, bay alcohol radical APEO and palm alcohol radical APEO one
Plant or several, thickener is in guar gum, Carbomer, sodium carboxymethylcellulose, hydroxyethyl cellulose, hydroxypropyl cellulose
Plant or several, pH adjusting agent is citric acid, sodium dihydrogen phosphate, NaOH, potassium hydroxide, ammoniacal liquor, diethanol amine and three ethanol
One or more in amine, water softener is the one kind in disodium ethylene diamine tetraacetate or the sodium of diethylene triamine pentacetic acid (DTPA) five, anti-corrosion
Agent is the one kind in Kathon CG and Phenoxyethanol.
4. the colorful washing product according to claim any one of 1-3, it is characterised in that：The preparation method of protecting colloid
For：
1）The deionized water of formula ratio is put into reactor, 400-500 revs/min of rotating speed is controlled；
2）The protection rubber powder of 1/2 formula ratio and the preservative of formula ratio are put into in reactor, stirring 30-40 minute to dissolving；
3）Input surplus protects rubber powder in reactor, is stirred 30-40 minutes under same rotational speed, obtains final product protecting colloid.
5. the colorful washing product according to claim any one of 1-3, it is characterised in that：The preparation side of continuous phase cleaning solution
Method is：
1）By in the deionized water addition reactor of formula ratio, 150-200 revs/min of rotating speed is controlled, sequentially add water softener, the moon
Ionic surface active agent, zwitterionic surfactant and nonionic surfactant, stir 30-40 minutes, until completely molten
Solution；
B：Thickener is slowly added to, is stirred 30-40 minutes；
C：Preservative and dyestuff are added, is stirred 10-15 minutes；
D：The pH of base paint is determined using pH meter, if necessary, addition qs pH adjuster makes system pH=7 or so, is obtained final product continuous
Phase cleaning solution.
6. the colorful washing product according to claim any one of 1-3, it is characterised in that：The toning cleaning solution is by following
The raw material composition of weight portion：980-1000 parts, dyestuff 0-5 parts of basic cleaning liquid.
7. colorful washing product according to claim 6, it is characterised in that：The basic cleaning liquid is by following weight portion
Raw material is constituted：Deionized water 550-650 parts, protecting colloid 100-150 parts, anion surfactant 80-200 parts, both sexes from
Sub- surfactant 30-80 parts, nonionic surfactant 30-80 parts, thickener 5-20 parts, pH adjusting agent 0-5 parts, water softener
1-3 parts, preservative 1-3 parts.
8. colorful washing product according to claim 7, it is characterised in that：In basic cleaning liquid, described anion table
Face activating agent is laureth sodium sulfovinate, coceth sodium sulfovinate, stereth sodium sulfovinate and dodecyl
One or more in benzene sulfonic acid sodium salt；Described zwitterionic surfactant is Cocoamidopropyl betaine, palmitamide
CAB, empgen BB, myristyl betaine, cocamidopropyl propyl amide amine-oxides, the oxidation of palmitamide propyl group
One or more in ammonium, dodecyl amine-oxides and myristyl amine-oxides；Described nonionic surfactant is cocounut oil
Base acid amides, lauryl acid amides, palmityl acid amides, octanol base glucosides, decyl alcohol base glucosides, bay alcohol radical glucosides, palm alcohol radical glucosides
With one or more in coconut oil base fatty diglycollic amide；Described thickener is guar gum, Carbomer, carboxymethyl fibre
One or more in the plain sodium of dimension, hydroxyethyl cellulose and hydroxypropyl cellulose；The pH adjusting agent is citric acid, biphosphate
One or more in sodium, NaOH, potassium hydroxide, ammoniacal liquor, diethanol amine and triethanolamine；Described water softener is second two
One kind in amine tetraacethyl disodium and the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is in Kathon CG and Phenoxyethanol
Kind.
9. colorful washing product according to claim 7, it is characterised in that：Mix colours cleaning solution preparation process be：
1）By in the deionized water addition reactor of formula ratio, 150-200 revs/min of rotating speed is controlled, sequentially add anion table
Face activating agent, zwitterionic surfactant, nonionic surfactant is stirred 30-40 minutes, until being completely dissolved；
2）Thickener is slowly added to, is stirred 30-40 minutes；
3）Protecting colloid is added, is stirred 30-40 minutes；
4）Preservative is added, is stirred 10-15 minutes；
5）Adding qs pH adjuster makes system pH=7, obtains final product basic cleaning liquid；
6）By in the basic cleaning liquid addition reactor of formula ratio, stirred with 200-300 revs/min of speed；
7）The required dyestuff of formula ratio is separately added into, is stirred 20-30 minutes, obtain final product toning cleaning solution.
10. a kind of method for preparing the colorful washing product as described in claim any one of 1-3, it is characterised in that：Including such as
Under the step：
1）Stirred during the protecting colloid of formula ratio is added into reactor, control mixing speed is at 100-150 revs/min；
2）By the toning cleaning solution of formula ratio by comminutor, gained particle is directly added into protecting colloid, and granulation terminates follow-up
Continuous stirring 10-15 minutes；
3）Continuous phase cleaning solution is slowly added to reactor, 20-30 minutes is stirred with 100-150 revs/min of speed, i.e., much
Color washing product.
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| US20020182161A1 (en) * | 2001-04-06 | 2002-12-05 | Unilever Home & Personal Care Usa, Division Of Conopco, Inc. | Hair treatment compositions |
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| CN106109275A (en) * | 2016-07-20 | 2016-11-16 | 珠海伊斯佳科技股份有限公司 | A kind of foaming bath oil rich in vegetable oil and preparation method thereof |
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2017
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20020182161A1 (en) * | 2001-04-06 | 2002-12-05 | Unilever Home & Personal Care Usa, Division Of Conopco, Inc. | Hair treatment compositions |
| CN1870973A (en) * | 2003-10-27 | 2006-11-29 | 荷兰联合利华有限公司 | Antidandruff shampoo composition |
| CN102065834A (en) * | 2008-06-19 | 2011-05-18 | 帝斯曼知识产权资产管理有限公司 | Shampoo preparations |
| CN104688621A (en) * | 2015-03-02 | 2015-06-10 | 上海卡卡化妆品有限公司 | Self-foaming cosmetic composition and preparation method thereof |
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