CN106904930A - A kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material and preparation method thereof - Google Patents
A kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material and preparation method thereof Download PDFInfo
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- CN106904930A CN106904930A CN201710177193.1A CN201710177193A CN106904930A CN 106904930 A CN106904930 A CN 106904930A CN 201710177193 A CN201710177193 A CN 201710177193A CN 106904930 A CN106904930 A CN 106904930A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
- C04B28/26—Silicates of the alkali metals
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/76—Use at unusual temperatures, e.g. sub-zero
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Building Environments (AREA)
Abstract
The invention discloses a kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material, each material comprising following composition by weight：36 parts of shepardite, 5 10 parts of sepiolite, 6 11 parts of perlite, 37 parts of sodium metasilicate, 48 parts of KP1,8 12 parts of montmorillonite, 37 parts of powdered whiting, 25 parts of colliery powder, 10 15 parts of gallicin, 15 20 parts of triisopropanolamine ring borate, 59 parts of hydroxypropyl cellulose, 15 20 parts of 2 fluoroanisole.The present invention makes it be provided simultaneously with good heat insulation effect and fire-retardant, stability by the original formula of inorganic energy-saving and heat-insulating material, adding inorganic filler and organic principle.
Description
Technical field
The invention belongs to energy-saving and heat-insulating material field, more particularly to a kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material and its preparation side
Method.
Background technology
The fast development of social industry, causes the whole world increasingly to increase the demand of the energy.According to incompletely statistics, architectural energy consumption
The 15-25% of global total energy consumption is accounted for, to alleviate the energy problem of growing tension, building energy conservation is particularly important.Particularly with
The fast development of China's urbanization, the building of various regions vigorously emerges in large numbers like the mushrooms after rain, carries out building energy conservation and is undoubtedly section
About energy consumption, the effective means increased operation rate.Building energy conservation refers to just reasonable employment and effective use of energy sources under construction, constantly
Efficiency of energy utilization is improved, building energy consumption is reduced.On the other hand, building energy conservation will also produce direct or indirect to environmental protection
Influence, the discharge of the carbon dioxide that can reduce 50% is amplified using appropriate heat insulating energy saving material and building energy conservation.
Therefore, energy-saving and heat-insulating material is increasingly becoming the focus of people's concern and research, and over nearly 30 years, various countries are in architectural design
Recognize with construction, the development and application of new building insulation material, the formulation of Regulation of building energy-saving and implementation, building energy conservation product
The aspect such as card and management has done many work, not only saves the substantial amounts of energy, considerable economic benefit is achieved, while changing
It has been apt to environment, has reduced the destruction to atmospheric ozone layer.
Inorganic heat insulation material is a kind of novel heat-preserving energy-saving insulation material painted for building inner-outer wall, with inorganic
Light thermal-insulation particle as lightweight aggregate, plus the dry powder and mortar being made up of Binder Materials, anticrack additive and other inserts etc..
Inorganic heat insulation material has the spies such as energy-conserving profit waste, insulation, the excellent properties for preventing fires antifreeze, ageing-resistant and cheap price
Point, there is the extensive market demand.Such as hollow glass bead, expanded perlite, closed perlite, rock wool etc..Inorganic heat preservation material
Material possesses that fireproof flame-retardant effect is good, deformation coefficient is small, anti-aging, good stability, long service life etc., but because its unit weight is omited
Greatly, cause that its heat preservation hot efficiency comparison is poor, energy-saving effect is not obvious.Organic heat-insulating class material is smaller due to thermal conductivity factor, possesses
, however, traditional organic architecture insulation material is in use, can there is serious disaster hidden-trouble in good heat insulation effect.
In recent years, the building fire for being caused due to the use of this kind of combustable organic insulation material is of common occurrence, has resulted in
Hundreds of millions of heavy economic losses and most personal injuries, the living safety of serious threat people.
The content of the invention
For drawbacks described above, it is an object of the invention to provide a kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material and preparation method thereof,
By in the original formula of inorganic energy-saving and heat-insulating material, adding inorganic filler and organic principle, it is set to be provided simultaneously with good guarantor
Temp effect and fire-retardant, stability.
The purpose of the present invention can be achieved through the following technical solutions：
A kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material, each material comprising following composition by weight：Shepardite 3-6 parts, sepiolite 5-10
Part, perlite 6-11 parts, sodium metasilicate 3-7 parts, KP1 4-8 parts, montmorillonite 8-12 parts, powdered whiting 3-7 parts, bastard coal
Stone flour 2-5 parts, gallicin 10-15 parts, 15-20 parts of triisopropanolamine ring borate, hydroxypropyl cellulose 5-9 parts, 2-
Fluoroanisole 15-20 parts.
Preferably, described shepardite 4-6 parts, sepiolite 6-9 parts, perlite 7-10 parts, sodium metasilicate 4-6 parts, potassium water glass
Glass 5-7 parts, montmorillonite 9-11 parts, powdered whiting 4-7 parts, colliery powder 2-4 parts, gallicin 12-14 parts, three isopropyls
16-18 parts of hydramine ring borate, hydroxypropyl cellulose 6-9 parts, 16-19 parts of 2- fluoroanisoles.
Preferably, 5 parts of the shepardite, 8 parts of sepiolite, 9 parts of perlite, 5 parts of sodium metasilicate, 6 parts of KP1, illiteracy are de-
10 parts of soil, 5 parts of powdered whiting, 3 parts of colliery powder, 13 parts of gallicin, 17 parts of triisopropanolamine ring borate, hydroxypropyl
8 parts of base cellulose, 17 parts of 2- fluoroanisoles.
A kind of preparation method of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material, comprises the following steps：
S1：By shepardite 3-6 parts, sepiolite 5-10 parts, perlite 6-11 parts, KP1 4-8 parts, montmorillonite 8-12 parts, weight
It is crushed in 3-7 parts, colliery powder 2-5 parts addition pulverizer of matter calcium carbonate powdered；
S2：In step S1 3-7 parts of sodium metasilicate, gallicin 10-15 parts, 2- fluoroanisoles will be added in gained powder
15-20 parts, rise high-temperature to 100-120 DEG C, stirring reaction 30-35min；
S3：It is subsequently added 15-20 parts of triisopropanolamine ring borate, hydroxypropyl cellulose 5-9 parts, continuation liter high-temperature to 140-
160 DEG C, stirring reaction 15-25min；
S4：Products therefrom in step S3 carries out high temperature is compressing, pressing pressure is 40-80Mpa, and press temperature is 80-100
DEG C, it is compressing to can obtain the compound energy-saving heat-preservation material afterwards.
Preferably, it is crushed to 200-400 mesh in step S1.
Preferably, temperature described in step S2 is 115 DEG C, with speed 400-600r/min stirring reactions 33min.
Preferably, temperature described in step S3 is 150 DEG C, with speed 500-600r/min stirring reactions 20min.
Preferably, pressing pressure described in step S4 is 65Mpa, and press temperature is 90 DEG C.
Compared with prior art, its advantage is the present invention：
A kind of preparation method of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material of the present invention, in inorganic heat insulation material formula, adds and covers
De- soil is used as supplement inorganic filler, while adding gallicin, triisopropanolamine ring borate, hydroxypropyl cellulose, 2-
The organic principles such as fluoroanisole, the fireproof flame-retardant effect that possesses of inorganic material is good, deformation coefficient is small keeping, anti-aging, steady
It is qualitative good, while the advantages of long service life, its heat insulation effect is greatly improved, increase its range of application.The insulation
The limited oxygen index of material is 90-95%, and compression strength is 2-5MPa, and thermal conductivity factor is 0.03-0.06W/ (mK).
Specific embodiment
The present invention is further illustrated with reference to embodiments.
Embodiment 1
S1：By 3 parts of shepardite, 5 parts of sepiolite, 6 parts of perlite, 4 parts of KP1,8 parts of montmorillonite, 3 parts of powdered whiting, coal
Powdered 200-300 mesh is crushed in 2 parts of addition pulverizers of spoil powder；
S2：3 parts of sodium metasilicate, 10 parts of gallicin, 15 parts of 2- fluoroanisoles will be added in gained powder in step S1, risen
High-temperature to 100 DEG C, with speed 400r/min stirring reactions 30min；
S3：15 parts of triisopropanolamine ring borate, 5 parts of hydroxypropyl cellulose are subsequently added, continue to rise high-temperature to 140 DEG C, with
Speed 500r/min stirring reactions 15min；
S4：Products therefrom in step S3 is carried out into high temperature compressing, pressing pressure is 40Mpa, press temperature is 80 DEG C, compacting
The compound energy-saving heat-preservation material is can obtain after shaping.
Above-mentioned energy-saving and heat-insulating material is carried out into performance test, is as a result shown：The limited oxygen index of the insulation material is 90%, is resisted
Compressive Strength is 2MPa, and thermal conductivity factor is 0.06W/ (mK).
Comparative example 1
S1：By 3 parts of shepardite, 5 parts of sepiolite, 6 parts of perlite, 4 parts of KP1,3 parts of powdered whiting, 2 parts of colliery powder
Powdered 200-300 mesh is crushed in addition pulverizer；
S2：3 parts of sodium metasilicate will be added in gained powder in step S1, rise high-temperature to 100 DEG C, stirred with speed 400r/min
Reaction 30min；
S3：To carry out high temperature compressing for products therefrom in later step S2, and pressing pressure is 40Mpa, and press temperature is 80 DEG C, pressure
The compound energy-saving heat-preservation material is can obtain after being made type.
Above-mentioned energy-saving and heat-insulating material is carried out into performance test, is as a result shown：The limited oxygen index of the insulation material is 92%, is resisted
Compressive Strength is 3MPa, and thermal conductivity factor is 0.18W/ (mK).
Embodiment 2
S1：By 6 parts of shepardite, 10 parts of sepiolite, 11 parts of perlite, 8 parts of KP1,12 parts of montmorillonite, powdered whiting 7
Powdered 300-400 mesh is crushed in part, 5 parts of addition pulverizers of colliery powder；
S2：7 parts of sodium metasilicate, 15 parts of gallicin, 20 parts of 2- fluoroanisoles will be added in gained powder in step S1, risen
High-temperature to 120 DEG C, with speed 600r/min stirring reactions 35min；
S3：20 parts of triisopropanolamine ring borate, 9 parts of hydroxypropyl cellulose are subsequently added, continue to rise high-temperature to 160 DEG C, with
Speed 600r/min stirring reactions 25min；
S4：Products therefrom in step S3 is carried out into high temperature compressing, pressing pressure is 80Mpa, press temperature is 100 DEG C, pressure
The compound energy-saving heat-preservation material is can obtain after being made type.
Above-mentioned energy-saving and heat-insulating material is carried out into performance test, is as a result shown：The limited oxygen index of the insulation material is 92%, is resisted
Compressive Strength is 3MPa, and thermal conductivity factor is 0.05W/ (mK).
Comparative example 2
S1：By 6 parts of shepardite, 10 parts of sepiolite, 11 parts of perlite, 8 parts of KP1,7 parts of powdered whiting, colliery powder 5
Powdered 300-400 mesh is crushed in part addition pulverizer；
S2：7 parts of sodium metasilicate will be added in gained powder in step S1, rise high-temperature to 120 DEG C, stirred with speed 600r/min
Reaction 35min；
S3：Products therefrom in step S2 then carries out high temperature is compressing, pressing pressure is 80Mpa, and press temperature is 100
DEG C, it is compressing to can obtain the compound energy-saving heat-preservation material afterwards.
Above-mentioned energy-saving and heat-insulating material is carried out into performance test, is as a result shown：The limited oxygen index of the insulation material is 92.5%,
Compression strength is 3.6MPa, and thermal conductivity factor is 0.15W/ (mK).
Embodiment 3
S1：By 4 parts of shepardite, 6 parts of sepiolite, 7 parts of perlite, 5 parts of KP1,9 parts of montmorillonite, 4 parts of powdered whiting, coal
Powdered 300-400 mesh is crushed in 2 parts of addition pulverizers of spoil powder；
S2：4 parts of sodium metasilicate, 12 parts of gallicin, 16 parts of 2- fluoroanisoles will be added in gained powder in step S1, risen
High-temperature to 100 DEG C, with speed 400r/min stirring reactions 35min；
S3：16 parts of triisopropanolamine ring borate, 6 parts of hydroxypropyl cellulose are subsequently added, continue to rise high-temperature to 160 DEG C, with
Speed 500r/min stirring reactions 25min；
S4：Products therefrom in step S3 is carried out into high temperature compressing, pressing pressure is 50Mpa, press temperature is 80 DEG C, compacting
The compound energy-saving heat-preservation material is can obtain after shaping.
Above-mentioned energy-saving and heat-insulating material is carried out into performance test, is as a result shown：The limited oxygen index of the insulation material is 92.6%,
Compression strength is 3.8MPa, and thermal conductivity factor is 0.052W/ (mK).
Embodiment 4
S1：By 6 parts of shepardite, 9 parts of sepiolite, 10 parts of perlite, 7 parts of KP1,11 parts of montmorillonite, 7 parts of powdered whiting,
Powdered 200-300 mesh is crushed in 4 parts of addition pulverizers of colliery powder；
S2：6 parts of sodium metasilicate, 14 parts of gallicin, 19 parts of 2- fluoroanisoles will be added in gained powder in step S1, risen
High-temperature to 120 DEG C, with speed 600r/min stirring reactions 30min；
S3：18 parts of triisopropanolamine ring borate, 9 parts of hydroxypropyl cellulose are subsequently added, continue to rise high-temperature to 150 DEG C, with
Speed 600r/min stirring reactions 15min；
S4：Products therefrom in step S3 is carried out into high temperature compressing, pressing pressure is 60Mpa, press temperature is 100 DEG C, pressure
The compound energy-saving heat-preservation material is can obtain after being made type.
Above-mentioned energy-saving and heat-insulating material is carried out into performance test, is as a result shown：The limited oxygen index of the insulation material is 93.8%,
Compression strength is 4.5MPa, and thermal conductivity factor is 0.038W/ (mK).
Embodiment 5
S1：By 5 parts of shepardite, 8 parts of sepiolite, 9 parts of perlite, 6 parts of KP1,10 parts of montmorillonite, 5 parts of powdered whiting,
Powdered 200-300 mesh is crushed in 3 parts of addition pulverizers of colliery powder；
S2：5 parts of sodium metasilicate, 13 parts of gallicin, 17 parts of 2- fluoroanisoles will be added in gained powder in step S1, risen
High-temperature to 115 DEG C, with speed 500r/min stirring reactions 33min；
S3：17 parts of triisopropanolamine ring borate, 8 parts of hydroxypropyl cellulose are subsequently added, continue to rise high-temperature to 150 DEG C, with
Speed 550r/min stirring reactions 20min；
S4：Products therefrom in step S3 is carried out into high temperature compressing, pressing pressure is 65Mpa, press temperature is 90 DEG C, compacting
The compound energy-saving heat-preservation material is can obtain after shaping.
Above-mentioned energy-saving and heat-insulating material is carried out into performance test, is as a result shown：The limited oxygen index of the insulation material is 95%, is resisted
Compressive Strength is 5MPa, and thermal conductivity factor is 0.03W/ (mK).
The invention is not restricted to embodiment here, those skilled in the art's announcement of the invention does not depart from the present invention
The improvement and modification that category is made all should be within protection scope of the present invention.
Claims (8)
1. a kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material, it is characterised in that each material comprising following composition by weight：Shepardite 3-6
Part, sepiolite 5-10 parts, perlite 6-11 parts, sodium metasilicate 3-7 parts, KP1 4-8 parts, montmorillonite 8-12 parts, heavy carbon
Sour calcium 3-7 parts, colliery powder 2-5 parts, gallicin 10-15 parts, 15-20 parts of triisopropanolamine ring borate, hydroxypropyl
Cellulose 5-9 parts, 15-20 parts of 2- fluoroanisoles.
2. a kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material according to claim 1, it is characterised in that described shepardite 4-6 parts,
Sepiolite 6-9 parts, perlite 7-10 parts, sodium metasilicate 4-6 parts, KP1 5-7 parts, montmorillonite 9-11 parts, powdered whiting
4-7 parts, colliery powder 2-4 parts, gallicin 12-14 parts, 16-18 parts of triisopropanolamine ring borate, hydroxy propyl cellulose
Plain 6-9 parts, 16-19 parts of 2- fluoroanisoles.
3. a kind of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material according to claim 2, it is characterised in that 5 parts of the shepardite, sea
8 parts of afrodite, 9 parts of perlite, 5 parts of sodium metasilicate, 6 parts of KP1,10 parts of montmorillonite, 5 parts of powdered whiting, colliery powder 3
Part, 13 parts of gallicin, 17 parts of triisopropanolamine ring borate, 8 parts of hydroxypropyl cellulose, 17 parts of 2- fluoroanisoles.
4. a kind of preparation method of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material, it is characterised in that comprise the following steps：
S1：By shepardite 3-6 parts, sepiolite 5-10 parts, perlite 6-11 parts, KP1 4-8 parts, montmorillonite 8-12 parts, weight
It is crushed in 3-7 parts, colliery powder 2-5 parts addition pulverizer of matter calcium carbonate powdered；
S2：In step S1 3-7 parts of sodium metasilicate, gallicin 10-15 parts, 2- fluoroanisoles will be added in gained powder
15-20 parts, rise high-temperature to 100-120 DEG C, stirring reaction 30-35min；
S3：It is subsequently added 15-20 parts of triisopropanolamine ring borate, hydroxypropyl cellulose 5-9 parts, continuation liter high-temperature to 140-
160 DEG C, stirring reaction 15-25min；
S4：Products therefrom in step S3 carries out high temperature is compressing, pressing pressure is 40-80Mpa, and press temperature is 80-100
DEG C, it is compressing to can obtain the compound energy-saving heat-preservation material afterwards.
5. a kind of preparation method of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material according to claim 4, it is characterised in that step S1
In be crushed to 200-400 mesh.
6. a kind of preparation method of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material according to claim 4, it is characterised in that step S2
Described in temperature be 115 DEG C, with speed 400-600r/min stirring reactions 33min.
7. a kind of preparation method of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material according to claim 4, it is characterised in that step S3
Described in temperature be 150 DEG C, with speed 500-600r/min stirring reactions 20min.
8. a kind of preparation method of NEW TYPE OF COMPOSITE energy-saving and heat-insulating material according to claim 4, it is characterised in that step S4
Described in pressing pressure be 65Mpa, press temperature be 90 DEG C.
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Cited By (3)
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| CN107603034A (en) * | 2017-09-25 | 2018-01-19 | 佛山市飞时达新材料科技有限公司 | A kind of light rubber plastic foaming thermal-insulating and preparation method thereof |
| CN110423088A (en) * | 2019-08-02 | 2019-11-08 | 上海嗣高新材料科技有限公司 | A kind of high-performance fire-resistant clay and preparation method thereof |
| CN110451826A (en) * | 2019-09-18 | 2019-11-15 | 王紫娴 | A kind of villages and towns in rural areas and cracking resistance concrete 32.5 mixed Portland cements and preparation method thereof |
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| CN101913836A (en) * | 2010-07-23 | 2010-12-15 | 朱光皓 | Inorganic heat insulation material with low water absorption ratio and low heat conduction coefficient |
| CN104230264A (en) * | 2014-09-02 | 2014-12-24 | 德清扬泰建筑材料有限公司 | Cement-based waterproof material and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107603034A (en) * | 2017-09-25 | 2018-01-19 | 佛山市飞时达新材料科技有限公司 | A kind of light rubber plastic foaming thermal-insulating and preparation method thereof |
| CN110423088A (en) * | 2019-08-02 | 2019-11-08 | 上海嗣高新材料科技有限公司 | A kind of high-performance fire-resistant clay and preparation method thereof |
| CN110451826A (en) * | 2019-09-18 | 2019-11-15 | 王紫娴 | A kind of villages and towns in rural areas and cracking resistance concrete 32.5 mixed Portland cements and preparation method thereof |
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Application publication date: 20170630 |