CN106883955A - A kind of handmade soap containing seaweed extracted liquor and preparation method thereof - Google Patents
A kind of handmade soap containing seaweed extracted liquor and preparation method thereof Download PDFInfo
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- CN106883955A CN106883955A CN201710181927.3A CN201710181927A CN106883955A CN 106883955 A CN106883955 A CN 106883955A CN 201710181927 A CN201710181927 A CN 201710181927A CN 106883955 A CN106883955 A CN 106883955A
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- added
- extracted liquor
- seaweed extracted
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/225—Polymers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention provides a kind of handmade soap containing seaweed extracted liquor and preparation method thereof.The method is prepared from the following raw materials in parts by weight：5~10 parts of olive oil, 5~15 parts of coconut oil, 1~5 part of tea oil, 2~5 parts of NaOH, 1 part of calcium hydroxide, 50~100 parts of seaweed extracted liquor, 5~10 parts of spermaceti, 1~3 part of shitosan.Olive oil, coconut oil, tea oil are added in heating kettle, add NaOH to be incubated 3 hours in 80 DEG C, after adding spermaceti, seaweed extracted liquor well mixed, be preferably added shitosan, calcium hydroxide, 60 DEG C are incubated 2 hours, and cooling obtains final product handmade soap finished product after injection molding, the demoulding.Various active ingredients of the invention be it is natural there is no toxic and side effect to human body, the effects such as with good cleaning, skin care, repair cell, whitening, moisturizing, its preparation method is simple, it is easy to process, and industrialized production is easy.
Description
Technical field
The present invention relates to household chemicals technical field, specially a kind of handmade soap containing seaweed extracted liquor and its making
Method.
Background technology
With the development of science and technology, there is the every aspect in life in chemical substance, particularly wash protector for collar domain daily,
It is even more so, pregnant woman, infant for skin fragility, chemistry washes shield commodity easily stimulates skin, causes allergic etc.
Reaction.
In order to reduce stimulation of the chemical composition to skin, should try one's best prepare daily washing product using pure natural raw material,
Avoid using artificial synthesized chemical raw material, surfactant and alkalinity soap base high etc..
" marine alga " is the general name of the marine algaes such as sea-tangle, seaweed, undaria pinnitafida, agar, is submarine algae, is
The cryptogam of plant kingdom.Marine alga contains multiple proteins, wherein special protein is referred to as close glycoprotein having in marine alga
The material of strengthen immunity and active anticancer, belongs to special polysaccharide, protein, lipid, pigment and lower-molecular substance.Traditional
In Chinese medicine, several brown algas can be used to prevent and treating cancer afterwards through boiling, and this hot water extract's main component is polysaccharide.
Marine alga can contain more kinds of and volume natural inorganic element than land based vegetation simultaneously, can provide needed by human body.So if
Can be applied in daily chemical products, with wide market prospects.
The content of the invention
Task of the invention is to provide does not have prejudicial natural raw material to health with a kind of, to each stratum at age
People all without any toxic and side effect, with handmade soaps of multiple efficacies such as cleaning moisturizing whitening and preparation method thereof.
A kind of handmade soap containing seaweed extracted liquor and preparation method thereof, it is by following raw material parts by weights proportions
Form：
5~10 parts of olive oil
5~15 parts of coconut oil
1~5 part of tea oil
2~5 parts of NaOH
1 part of calcium hydroxide
50~100 parts of seaweed extracted liquor
5~10 parts of spermaceti
1~3 part of shitosan；
By formula rate by olive oil, coconut oil, tea oil addition heating kettle, after stirring, NaOH is added, by temperature
It is increased to 80 DEG C, insulation reaction 3 hours；Spermaceti, seaweed extracted liquor are added, continues to maintain the temperature at 80 DEG C, be sufficiently mixed uniform
Afterwards, shitosan, calcium hydroxide are added, 60 DEG C are incubated 2 hours, cooling obtains final product handmade soap finished product after injection molding, the demoulding.
The preparation method of wherein described seaweed extracted liquor is as follows：
（1）100 weight portion marine algas are cleaned, is crushed, be dispersed in water, make raw material be 1 with the weight part ratio of water:3, stirring makes it
It is thoroughly mixed to form suspension；
（2）0.5 weight portion hemicellulase is added under the conditions of 60 DEG C in suspension, is stirred, fully react 1h；
（3）1 part by weight of cellulose enzyme is added, is stirred, fully react 1h；
（4）1 weight portion protease is added to stir in suspension, 2h after reaction fully, filtering removes filter residue；
（5）150 weight portions are concentrated the filtrate to, seaweed extracted liquor is obtained final product.
The marine alga is the mixture of the arbitrary proportion of one or two or more kinds in undaria pinnitafida, sea lettuce and agar.
The positive effect of the present invention is：Present invention offer is a kind of to contain the handmade soap of seaweed extracted liquor and its making side
Method, using the method for biological enzymolysis, has carried out abundant extraction to the active ingredient of marine alga, and combine various nutrition such as camellia oil into
Point, easy to operate, it is adaptable to industrialized production with raw material is cheap, preparation method process is simple, the handmade soap of preparation has clear
The effects such as clean, whitening, moisturizing, repair cell.
Specific embodiment
Below with reference to embodiment, the present invention will be further described.
Embodiment 1
Olive oil 7kg, coconut oil 10kg, tea oil 3kg are added in heating kettle, after stirring, NaOH 4kg is added, will
Temperature is increased to 80 DEG C, insulation reaction 3 hours；Spermaceti 7kg, seaweed extracted liquor 60kg are added, continues to maintain the temperature at 80 DEG C, filled
Divide after being well mixed, add shitosan 1.5kg, calcium hydroxide 1kg, 60 DEG C are incubated 2 hours, cooling, are to go smoothly after injection molding, the demoulding
Work soap finished product.
The preparation method of wherein seaweed extracted liquor is as follows：
（1）50kg marine algas are cleaned, is crushed, be dispersed in water, make raw material: the mass ratio of solvent is 1:3, stirring is sufficiently mixed；
（2）0.25kg hemicellulases are added under the conditions of 60 DEG C in suspension, 1h is fully reacted in stirring；
（3）0.5kg cellulases are added, 1h is fully reacted in stirring；
（4）The stirring of 0.5kg protease, 2h after reaction fully, filtering is added to remove filter residue in suspension；
（5）75kg is concentrated the filtrate to, seaweed extracted liquor is obtained final product.
Embodiment 2
Olive oil 7.5kg, coconut oil 12kg, tea oil 3kg are added in heating kettle, after stirring, NaOH is added
4.5kg, 80 DEG C, insulation reaction 3 hours are increased to by temperature；Spermaceti 7kg, seaweed extracted liquor 75kg are added, continues keeping temperature
At 80 DEG C, be sufficiently mixed it is uniform after, add shitosan 1.5kg, calcium hydroxide 1kg, 60 DEG C are incubated 2 hours, cooling, injection molding, de-
Handmade soap finished product is obtained final product after mould.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 3
Olive oil 8kg, coconut oil 10kg, tea oil 3.5kg are added in heating kettle, after stirring, NaOH 4kg is added,
Temperature is increased to 80 DEG C, insulation reaction 3 hours；Spermaceti 7.5kg, seaweed extracted liquor 75kg are added, continues to maintain the temperature at 80
DEG C, after being sufficiently mixed uniformly, shitosan 1.5kg, calcium hydroxide 1kg are added, 60 DEG C are incubated 2 hours, cooling, after injection molding, the demoulding
Obtain final product handmade soap finished product.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 4
Olive oil 7.5kg, coconut oil 10kg, tea oil 3.5kg are added in heating kettle, after stirring, NaOH is added
4kg, 80 DEG C, insulation reaction 3 hours are increased to by temperature；Spermaceti 8kg, seaweed extracted liquor 75kg are added, continues to maintain the temperature at
80 DEG C, after being sufficiently mixed uniformly, shitosan 1.2kg, calcium hydroxide 1kg are added, 60 DEG C are incubated 2 hours, cooling, injection molding, the demoulding
After obtain final product handmade soap finished product.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 5
Olive oil 7.5kg, coconut oil 10kg, tea oil 3.5kg are added in heating kettle, after stirring, NaOH is added
4.5kg, 80 DEG C, insulation reaction 3 hours are increased to by temperature；Spermaceti 7kg, seaweed extracted liquor 90kg are added, continues keeping temperature
At 80 DEG C, be sufficiently mixed it is uniform after, add shitosan 1.2kg, calcium hydroxide 1kg, 60 DEG C are incubated 2 hours, cooling, injection molding, de-
Handmade soap finished product is obtained final product after mould.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 6
Olive oil 8.5kg, coconut oil 10kg, tea oil 3kg are added in heating kettle, after stirring, NaOH is added
4.5kg, 80 DEG C, insulation reaction 3 hours are increased to by temperature；Spermaceti 7kg, seaweed extracted liquor 70kg are added, continues keeping temperature
At 80 DEG C, be sufficiently mixed it is uniform after, add shitosan 1.5kg, calcium hydroxide 1kg, 60 DEG C are incubated 2 hours, cooling, injection molding, de-
Handmade soap finished product is obtained final product after mould.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 7
Olive oil 8.5kg, coconut oil 11kg, tea oil 3kg are added in heating kettle, after stirring, NaOH is added
4.5kg, 80 DEG C, insulation reaction 3 hours are increased to by temperature；Spermaceti 7kg, seaweed extracted liquor 60kg are added, continues keeping temperature
At 80 DEG C, be sufficiently mixed it is uniform after, add shitosan 1.5kg, calcium hydroxide 1kg, 60 DEG C are incubated 2 hours, cooling, injection molding, de-
Handmade soap finished product is obtained final product after mould.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 8
Olive oil 9kg, coconut oil 10kg, tea oil 43kg are added in heating kettle, after stirring, NaOH 4.5kg is added,
Temperature is increased to 80 DEG C, insulation reaction 3 hours；Spermaceti 9kg, seaweed extracted liquor 65kg are added, continue to maintain the temperature at 80 DEG C,
After being sufficiently mixed uniformly, shitosan 1.5kg, calcium hydroxide 1kg are added, 60 DEG C are incubated 2 hours, and cooling is obtained final product after injection molding, the demoulding
Handmade soap finished product.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 9
Olive oil 9kg, coconut oil 10kg, tea oil 34kg are added in heating kettle, after stirring, NaOH 3kg is added, will
Temperature is increased to 80 DEG C, insulation reaction 3 hours；Spermaceti 8.5kg, seaweed extracted liquor 60kg are added, continue to maintain the temperature at 80 DEG C,
After being sufficiently mixed uniformly, shitosan 1.5kg, calcium hydroxide 1kg are added, 60 DEG C are incubated 2 hours, and cooling is obtained final product after injection molding, the demoulding
Handmade soap finished product.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 10
Olive oil 6.5kg, coconut oil 12.5kg, tea oil 3.5kg are added in heating kettle, after stirring, NaOH is added
4.2kg, 80 DEG C, insulation reaction 3 hours are increased to by temperature；Spermaceti 8kg, seaweed extracted liquor 85kg are added, continues keeping temperature
At 80 DEG C, be sufficiently mixed it is uniform after, add shitosan 1.5kg, calcium hydroxide 1kg, 60 DEG C are incubated 2 hours, cooling, injection molding, de-
Handmade soap finished product is obtained final product after mould.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 11
Olive oil 9.5kg, coconut oil 12.5kg, tea oil 3.5kg are added in heating kettle, after stirring, NaOH is added
4.8kg, 80 DEG C, insulation reaction 3 hours are increased to by temperature；Spermaceti 6kg, seaweed extracted liquor 80kg are added, continues keeping temperature
At 80 DEG C, after being sufficiently mixed uniformly, shitosan 2kg, calcium hydroxide 1kg are added, 60 DEG C are incubated 2 hours, cooling, injection molding, the demoulding
After obtain final product handmade soap finished product.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiment 12
Olive oil 7.8kg, coconut oil 11.5kg, tea oil 4.5kg are added in heating kettle, after stirring, NaOH is added
3.5kg, 80 DEG C, insulation reaction 3 hours are increased to by temperature；Spermaceti 7.5kg, seaweed extracted liquor 95kg are added, continues to keep temperature
Degree at 80 DEG C, be sufficiently mixed it is uniform after, add shitosan 2kg, calcium hydroxide 1kg, 60 DEG C are incubated 2 hours, cooling, injection molding, de-
Handmade soap finished product is obtained final product after mould.
The preparation method of wherein seaweed extracted liquor is same as Example 1.
Embodiments of the invention are the foregoing is only, the scope of the claims of the invention is not thereby limited, it is every to utilize this hair
Equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks
Domain, is included within the scope of the present invention.
Claims (3)
1. a kind of handmade soap containing seaweed extracted liquor and preparation method thereof, it is characterised in that：
1）Formula is by weight：
5~10 parts of olive oil
5~15 parts of coconut oil
1~5 part of tea oil
2~5 parts of NaOH
1 part of calcium hydroxide
50~100 parts of seaweed extracted liquor
5~10 parts of spermaceti
1~3 part of shitosan；
2）Prepare：
By formula rate by olive oil, coconut oil, tea oil addition heating kettle, after stirring, NaOH is added, by temperature
It is increased to 80 DEG C, insulation reaction 3 hours；Spermaceti, seaweed extracted liquor are added, continues to maintain the temperature at 80 DEG C, be sufficiently mixed uniform
Afterwards, shitosan, calcium hydroxide are added, 60 DEG C are incubated 2 hours, cooling obtains final product handmade soap finished product after injection molding, the demoulding.
2. a kind of handmade soap containing seaweed extracted liquor according to claim 1 and preparation method thereof, it is characterised in that institute
The preparation method of the seaweed extracted liquor stated is as follows：
（1）100 weight portion marine algas are cleaned, is crushed, be dispersed in water, make raw material be 1 with the weight part ratio of water:3, stirring makes it
It is thoroughly mixed to form suspension；
（2）0.5 weight portion hemicellulase is added under the conditions of 60 DEG C in suspension, is stirred, fully react 1h；
（3）1 part by weight of cellulose enzyme is added, is stirred, fully react 1h；
（4）1 weight portion protease is added to stir in suspension, 2h after reaction fully, filtering removes filter residue；
（5）150 weight portions are concentrated the filtrate to, seaweed extracted liquor is obtained final product.
3. a kind of handmade soap containing seaweed extracted liquor according to claim 1 and preparation method thereof, it is characterised in that institute
The marine alga stated is the mixture of the arbitrary proportion of one or two or more kinds in undaria pinnitafida, sea lettuce and agar.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710181927.3A CN106883955A (en) | 2017-03-24 | 2017-03-24 | A kind of handmade soap containing seaweed extracted liquor and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710181927.3A CN106883955A (en) | 2017-03-24 | 2017-03-24 | A kind of handmade soap containing seaweed extracted liquor and preparation method thereof |
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| CN106883955A true CN106883955A (en) | 2017-06-23 |
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| CN201710181927.3A Pending CN106883955A (en) | 2017-03-24 | 2017-03-24 | A kind of handmade soap containing seaweed extracted liquor and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108085198A (en) * | 2017-12-31 | 2018-05-29 | 跨越生物科技（滁州）有限公司 | A kind of preparation method with high-efficiency antimicrobial effect perfumed soap |
| WO2020012136A1 (en) | 2018-07-13 | 2020-01-16 | Gifrer Barbezat | Alkaline oleo-liniment |
| CN111454794A (en) * | 2020-04-02 | 2020-07-28 | 济南芙本生物技术有限公司 | Handmade soap for makeup removal, cleaning and moisturizing and preparation method thereof |
| CN115418283A (en) * | 2022-07-05 | 2022-12-02 | 济宁医学院 | Skin-care liquid soap and preparation method thereof |
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| CN1252954A (en) * | 1998-11-06 | 2000-05-17 | 荣成市神通海洋生物公司 | Process for preparing liquid extract of kelp |
| CN102643726A (en) * | 2011-02-21 | 2012-08-22 | 上海成增科技发展有限公司 | Tea soap capable of cleaning and caring skin |
| CN104371861A (en) * | 2013-08-15 | 2015-02-25 | 青岛鹏远康华天然产物有限公司 | Seaweed health soap and making method thereof |
| CN105950323A (en) * | 2016-05-11 | 2016-09-21 | 德施普科技发展温州有限公司 | Kelp soap and preparation method thereof |
| CN106479765A (en) * | 2015-08-31 | 2017-03-08 | 台山市金昊贸易有限公司 | A kind of algae clay facial soap |
-
2017
- 2017-03-24 CN CN201710181927.3A patent/CN106883955A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1252954A (en) * | 1998-11-06 | 2000-05-17 | 荣成市神通海洋生物公司 | Process for preparing liquid extract of kelp |
| CN102643726A (en) * | 2011-02-21 | 2012-08-22 | 上海成增科技发展有限公司 | Tea soap capable of cleaning and caring skin |
| CN104371861A (en) * | 2013-08-15 | 2015-02-25 | 青岛鹏远康华天然产物有限公司 | Seaweed health soap and making method thereof |
| CN106479765A (en) * | 2015-08-31 | 2017-03-08 | 台山市金昊贸易有限公司 | A kind of algae clay facial soap |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108085198A (en) * | 2017-12-31 | 2018-05-29 | 跨越生物科技（滁州）有限公司 | A kind of preparation method with high-efficiency antimicrobial effect perfumed soap |
| WO2020012136A1 (en) | 2018-07-13 | 2020-01-16 | Gifrer Barbezat | Alkaline oleo-liniment |
| CN111454794A (en) * | 2020-04-02 | 2020-07-28 | 济南芙本生物技术有限公司 | Handmade soap for makeup removal, cleaning and moisturizing and preparation method thereof |
| CN115418283A (en) * | 2022-07-05 | 2022-12-02 | 济宁医学院 | Skin-care liquid soap and preparation method thereof |
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Application publication date: 20170623 |
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