CN106880057A - The preparation method and leaf mustard diet fiber product of a kind of leaf mustard dietary fiber - Google Patents
The preparation method and leaf mustard diet fiber product of a kind of leaf mustard dietary fiber Download PDFInfo
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- CN106880057A CN106880057A CN201710283066.XA CN201710283066A CN106880057A CN 106880057 A CN106880057 A CN 106880057A CN 201710283066 A CN201710283066 A CN 201710283066A CN 106880057 A CN106880057 A CN 106880057A
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- Prior art keywords
- leaf mustard
- dietary fiber
- preparation
- mustard
- leaf
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- 235000005855 Brassica juncea var. subintegrifolia Nutrition 0.000 title claims abstract description 108
- 235000013325 dietary fiber Nutrition 0.000 title claims abstract description 60
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Seasonings (AREA)
Abstract
The invention belongs to field of health care food, and in particular to a kind of leaf mustard dietary fiber preparation method and leaf mustard diet fiber product.The leaf mustard dietary fiber preparation method includes：Leaf mustard and feed liquid are carried out into blanching, then the leaf mustard after blanching is placed in ethanol is beaten, post-processed after obtaining slurries, obtain leaf mustard dietary fiber.The leaf mustard dietary fiber preparation method yield is high, and can remove the fishy smell in leaf mustard, improves the color of leaf mustard dietary fiber.The color and local flavor of the leaf mustard diet fiber product are preferable, it is easy to allow consumer to receive.The present invention can improve the agriculture added value of leaf mustard, the soluble dietary fiber product of high-quality be provided for market, with obvious economic benefit and social benefit.
Description
Technical field
The invention belongs to field of health care food, and in particular to the preparation method and leaf mustard meals of a kind of leaf mustard dietary fiber are fine
Dimension product, more particularly to a kind of leaf mustard dietary fiber microcapsules.
Background technology
Dietary fiber is a class polysaccharide, and it can neither be absorbed by pipe intestinal digesting, can not produce energy, once once be recognized
Cannot get enough attention for a long time to be a kind of " without nutriment ".However, as meals constitute increasingly finer, meals fibre
Dimension has become the material of academia and ordinary people concern, and regards as the 7th class nutrient by nutrition educational circles supplement, and passes
Six class nutrients of system are that protein, fat, carbohydrate, vitamin, mineral matter and water are arranged side by side.Dietary fiber is to human body
Physiological function has various adjustment effects, and such as anti-CaM antibody, prevention intestinal cancer, treatment constipation, removing toxic substances, prevention and treatment enteron aisle is had a rest
Room disease, treatment cholelithiasis, the blood sugar and control body weight that reduce blood cholesterol levels and triglycerides, reduce maturity-onset diabetes patient.
For the research of dietary fiber sources, mainly there are wheat, soybean, sugarcane, jerusalem artichoke, guar gum etc. in current source, removes
China also has considerable cereal crops not obtain sufficient development and application outside this, targetedly strengthens dietary fiber sources
Research, very important facilitation will be played to the development of China's food industry.
Leaf mustard (Brassica juncea L.) is for cruciate flower (Cruciferae) Brassica genus are annual or biennial herb
Section plant, is one of special vegetable of Chinese Famous, and leaf mustard likes the wetting that cools, and avoids hot, arid, and slightly resistance to frost, general leaf is used
Leaf mustard is less stringent to temperature requirement, with wide adaptability, growing way is strong, management is simple, pest and disease damage is few many advantages, such as, the whole nation
There is cultivation various regions, are distributed in each province on the south the Changjiang river more, and there are the provinces and regions such as Guangdong, Guangxi, Fujian and Taiwan main producing region.In Guangdong,
Leaf mustard distribution is wide, yield is high, price is low, there is good value of exploiting and utilizing.Li Shizhen (1518-1593 A.D.) writes《Compendium of Materia Medica》Describe medical mustard
The medical value of dish, leaf mustard nature and flavor are pungent, temperature, there is facilitaing lung slit phlegm, and the effect of middle benefit gas profit gas is controlled and contained in cold drink, and cough phlegm is stagnant, chest diaphragm
It is full vexed.
Leaf mustard contains vitamin A, vitamin B complex, vitamin C and vitamin D, is of high nutritive value, and data analysis shows, often
Moisture 91%, protein 1.9g, fat 0.4g, carbohydrate 6.5g, ash content 0.8g in 100g leaf mustard, also containing various
Free amino acid.Leaf mustard tissue is more thick and stiff, containing carrotene and a large amount of edible celluloses, lead to improving eyesight profit diaphragm, intestines wide
Just, orectic effect, treats constipation to anti-, is suitable for the elderly and habitual constipation person edible especially, more can be used as ophthalmic patient
Diet good food.Therefore, leaf mustard is processed into dietary fiber, its agriculture added value can be greatly improved, for market provides one kind
The soluble dietary fiber product of high-quality.
Mainly there is enzymatic isolation method currently used for the method for preparing dietary fiber, with various enzymes (such as AMS, protease, sugar
Change enzyme and cellulase etc.) other impurities that contain in degraded dietary fiber, purity dietary fiber higher is obtained, but use enzyme
The dietary fiber yield that solution prepares leaf mustard is not high.Additionally, containing fishy smell material in leaf mustard, make the color of its diet fiber product
Consumer is not easy to local flavor to receive.Also, contain glucide, mainly glucose and fructose in leaf mustard, in process
In, being heated can occur Maillard reaction (browning reaction), produce brown color substance, do not only result in finished color deepen, local flavor hair
Changing, also results in final product quality decline.It is therefore desirable to find a kind of method suitable for preparing leaf mustard dietary fiber, it is used for
Solve preparation leaf mustard dietary fiber yield not high, the color of leaf mustard diet fiber product and local flavor and be not easy to asking for consumer's receiving
Topic.
The content of the invention
In view of this, the invention provides a kind of leaf mustard dietary fiber preparation method and leaf mustard diet fiber product, it is used for
Solve preparation leaf mustard dietary fiber yield not high, the color of leaf mustard diet fiber product and local flavor and be not easy to asking for consumer's receiving
Topic.
Concrete technical scheme of the invention is as follows：
A kind of leaf mustard dietary fiber preparation method, including：Leaf mustard is placed in ethanol water after being scalded through hydro-thermal and is beaten, and takes slurry
Liquid is post-processed, and obtains leaf mustard dietary fiber.
Preferably, the leaf mustard and the mass ratio of water are 1：10~1：25；
Concentration of alcohol in the ethanol water is 60%~80%；
Based on g/ml, leaf mustard and the mass volume ratio of ethanol water after the blanching are 1:6~1：12.
Preferably, the temperature of the blanching is 60~100 DEG C；
The time of the blanching is 3~5min；
The rotating speed of the mashing is 15000~20000rpm；
The time of the mashing is 1~5min.
Preferably, the post processing includes：
Suction filtration after slurries are stood, collects filter residue and is crushed, dried.
Preferably, the temperature of the standing is 10~40 DEG C；
The time of the standing is 10~30min；
The suction filtration is decompression suction filtration；
The dry temperature is 60~90 DEG C；
The dry time is 8~12h.
The present invention also provides a kind of leaf mustard diet fiber product, including can on prepared leaf mustard dietary fiber and health products
The auxiliary material of receiving.
Preferably, the leaf mustard diet fiber product is leaf mustard dietary fiber microcapsules, leaf mustard food fibre powder or leaf mustard
Meal fiber tablet.
The auxiliary material is wall material and emulsifying agent.
The present invention also provides a kind of preparation method of leaf mustard dietary fiber microcapsules, including：
Prepared leaf mustard dietary fiber is placed in the wall material solution that wall material is made into water, is wrapped after adding emulsifier
Bury, then be spray-dried and compressing tablet.
Preferably, the wall material is beta-schardinger dextrin or carragheen.
The concentration of wall material is 1wt%~3wt% in the wall material solution.
The emulsifying agent is octenyl succinic acid starch fat.
The addition of the emulsifying agent is the 1wt%~5wt% of the wall material solution.
The leaf mustard dietary fiber is 1 with the mass ratio of water:50.
Preferably, the temperature of the emulsification is 40~70 DEG C.
The homogenization pressure of the embedding is 20-50MPa.
The EAT of the spray drying is 150~180 DEG C；The leaving air temp of the spray drying is 55~85 DEG C；
The charging rate of the spray drying is 0.2~0.8ml/s；The stream pressure of the spray drying is 0.1~0.3MPa.
In sum, the invention provides a kind of leaf mustard dietary fiber preparation method and leaf mustard diet fiber product.The mustard
Dish dietary fiber preparation method includes：Leaf mustard and feed liquid are carried out into blanching, then the leaf mustard after blanching is placed in ethanol is beaten
Slurry, is post-processed after obtaining slurries, obtains leaf mustard dietary fiber.The leaf mustard dietary fiber preparation method yield is high, and energy
Fishy smell enough in removal leaf mustard, improves the color of leaf mustard dietary fiber.The color and local flavor of the leaf mustard diet fiber product are preferable,
It is easy to allow consumer to receive.The present invention can improve the agriculture added value of leaf mustard, for the soluble dietary that market provides high-quality is fine
Dimension product, with obvious economic benefit and social benefit.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing
The accompanying drawing to be used needed for having technology description is briefly described.
Fig. 1 is leaf mustard meals microcapsules obtained in embodiment 2；
Fig. 2 is leaf mustard dietary fiber obtained in comparative example 1.
Specific embodiment
The invention discloses the preparation method and leaf mustard diet fiber product of a kind of leaf mustard dietary fiber.People in the art
Member can use for reference present disclosure, be suitably modified technological parameter realization.In particular, all similar replacements and change
Apparent to those skilled in the art, they are considered as being included in the present invention.The method of the present invention and product
Be described by preferred embodiment, related personnel substantially can not depart from it is right in present invention, spirit and scope
Method described herein is modified or suitably change is realized and apply the technology of the present invention with combining.
The invention provides a kind of leaf mustard dietary fiber preparation method, including：It is water-soluble that leaf mustard is placed in ethanol after being scalded through hydro-thermal
It is beaten in liquid, takes slurries and post-processed, obtains leaf mustard dietary fiber.
In the present invention, the leaf mustard is 1 with the mass ratio of water：10~1：25；
Concentration of alcohol in the ethanol water is 60%~80%；
Based on g/ml, leaf mustard and the mass volume ratio of ethanol water after the blanching are 1:6~1：12.
In the present invention, the leaf mustard is preferably fresh leaf mustard, it is to avoid to the excessive pretreatment of raw material.
Phytochrome class (Phytochromes) mainly has fat-soluble pigment and the class of water colo(u)r two.Fat-soluble pigment master
To be chlorophyll, lutein and carrotene, three often coexists；In addition still there are crocin, capsorubin etc..In addition to chlorophyll,
Mostly four triterpene derivatives.This kind of pigment is water insoluble, is insoluble in methyl alcohol, and being soluble in high concentration ethanol, ether, chloroform, benzene etc. has
Machine solvent.Chlorophyll etc. extracts other active ingredients often must be as Impurity removal, so that finished product is purified, plant (particularly leaf
Class, whole grass) ethanol extract in containing volume chlorophyll, can be added water in concentrate is allowed to settle out, also can by oxidation
The adsorbents such as aluminium, calcium carbonate and remove.Water colo(u)r is mainly pattern glucoside, also known as anthocyanidin, is prevalent in spending.It is molten
In water and ethanol, insoluble in organic solvents such as ether, chloroforms, anthocyanin in preparation of preparation or effective component extracting, frequently as
Impurity removal.
Mainly there are glucose and fructose containing glucide in leaf mustard, also (meals are fine for other alcohol insoluble matter polysaccharides
Dimension).Monose in process, can occur Maillard reaction (browning reaction) due to being heated, and produce brown color substance old.Not only
Cause finished color to deepen, local flavor changes, also result in final product quality decline.The fishy smell material predominantly fat contained in leaf mustard
Class, can occur exchange reaction with ethanol, so as to reduce the smell of leaf mustard in finished product.So, using ethanol as master in the present invention
Reagent treatment is wanted, ethanol is volatile so that the chemical agent residue amount of finished product is substantially reduced.High concentration ethanol can dissolve pigment,
Sugar, fishy smell material, and retain dietary fiber.Mashing operation can destroy eucaryotic cell structure, while increasing the contact surface of ethanol and raw material
Product, operation raw material finished product is low and operating process is simple and quick, is adapted to industrialized production.
The temperature of the blanching is 60~100 DEG C；
The time of the blanching is 3~5min；
The rotating speed of the mashing is 15000~20000rpm；
The time of the mashing is 1~5min.
In the present invention, the post processing includes：
Suction filtration after slurries are stood, collects filter residue and is crushed, dried.
In the present invention, the temperature of the standing is 10~40 DEG C；
The time of the standing is 10~30min；
The suction filtration is decompression suction filtration；
The dry temperature is 60~90 DEG C；
The dry time is 8~12h.
The present invention also provides a kind of leaf mustard diet fiber product, including can on prepared leaf mustard dietary fiber and health products
The auxiliary material of receiving.
In the present invention, the leaf mustard diet fiber product is leaf mustard dietary fiber microcapsules, leaf mustard food fibre powder or mustard
Dish meal fiber tablet.
The auxiliary material is wall material and/or emulsifying agent.
The present invention also provides a kind of preparation method of leaf mustard dietary fiber microcapsules, including：By prepared leaf mustard meals
Fiber is placed in the wall material solution that wall material is made into water, is embedded after adding emulsifier, then be spray-dried and compressing tablet.
Microcapsules refer to a kind of miniature vessel or packing material with polymer wall.Microcapsules granulating technique is exactly will be solid
Body, liquid or gas entrapment, seal up for safekeeping in a kind of microencapsulation turn into a kind of technology of solia particle product.Its major function
Have：Powdered, dry powder is become by liquid, gas etc.；Volatility is reduced, the material for making some readily volatilized becomes difficult to
Volatilization；Improve the stability (oxidizable, to be clear to light decomposition, the material for easily being influenceed by temperature or moisture) of material；Taste masking；Isolation is lived
Property composition；Control release.The dried vegetable taste of product can be further covered using microcapsules technology and improve the color of product.
In the present invention, the wall material is beta-schardinger dextrin or carragheen.
The concentration of wall material is 1wt%~3wt% in the wall material solution.
The emulsifying agent is octenyl succinic acid starch matter.
The addition of the emulsifying agent is the 1wt%~5wt% of the wall material solution.
The leaf mustard dietary fiber is 1 with the mass ratio of water:50.
Preferably, the temperature of the emulsification is 40~70 DEG C.
The homogenization pressure of the embedding is 20-50MPa.
The EAT of the spray drying is 150~180 DEG C；The leaving air temp of the spray drying is 55~85 DEG C；
The charging rate of the spray drying is 0.2~0.8ml/s；The stream pressure of the spray drying is 0.1~0.3MPa.
For a further understanding of the present invention, below in conjunction with the embodiment of the present invention, to the technical side in the embodiment of the present invention
Case is clearly and completely described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole
Embodiment.Based on the embodiment in the present invention, those of ordinary skill in the art institute under the premise of creative work is not made
The every other embodiment for obtaining, belongs to the scope of protection of the invention.
Unless otherwise specified, reagent involved in the embodiment of the present invention is commercially available prod, can be by business canal
Road purchase is obtained.
Embodiment 1
Fresh leaf mustard 2000g clear water cleans vegetables, drains, be 12.5 with solid-liquid ratio：1 ratio adds water carries out heat
Scald, heat iron temperature is 80 DEG C, and blanching treatment time 5min is drained, and is 1 with solid-liquid ratio：8 add 80% ethanol water to be beaten
Slurry, mashing rotating speed is 20000rpm, beating time 5min.Slurries carry out decompression suction filtration after standing 30min at normal temperatures, retain filter
Slag.Filter residue is placed in blowing-type drying box and is dried 10h with 90 DEG C, obtain drying filter residue, then crushing shape is carried out with pulverizer
Into dry powder, leaf mustard dietary fiber is obtained.Dietary fiber yield is more than 77.5%.
Embodiment 2
The leaf mustard dietary fiber that embodiment 1 is obtained with water as solvent, 3% beta-schardinger dextrin as wall material, 5% octenyl amber
Amber acid-starch matter is emulsifying agent, and solid-liquid ratio is 3：7, emulsifying temperature is 70 DEG C, and homogenization pressure is carried out at embedding for the condition of 50MPa
Reason.Afterwards, with 180 DEG C of EAT, 85 DEG C of leaving air temp feeds 0.8ml/s, and stream pressure 0.3MPa is sprayed for condition
Dry.Dried powder carries out compressing tablet, and formation is with leaf mustard as raw material, smell disappears substantially, color is chlorine leaf mustard
Dietary fiber microcapsules (Fig. 1).
Comparative example 1
Fresh leaf mustard 2000g clear water cleans vegetables, drains, be 12.5 with solid-liquid ratio：1 ratio adds water mashing,
Mashing rotating speed is 20000rpm, beating time 5min.Slurries carry out decompression suction filtration after standing 30min at normal temperatures, retain filter residue.
Filter residue is placed in blowing-type drying box and is dried 10h with 90 DEG C, obtain drying filter residue, then crushing is carried out with pulverizer and form dry
Powder, obtains leaf mustard dietary fiber.Color is soil sepia, and with strong leaf mustard fishy smell (Fig. 2)
Comparative example 2
Fresh leaf mustard dries that to beat powder standby, weighs the pretreated leaf mustard powder of 20.00g, pH value be 4.5 sodium acetate-
Hac buffer presses solid-liquid ratio 1：30 mixing.On the basis of leaf mustard powder content, 3% cellulase solution is added, shaken in constant temperature
Swing and digest 1h in water-bath, gone out enzyme 5min in boiling water bath after enzymolysis, be centrifuged with 4000rpm rotating speeds, take supernatant, add 80% second
Alcohol precipitates 2h, filters to take filter residue, as 105 DEG C of air dry oven drying, surveys dietary fiber content.
Same step is not enzyme-added as blank assay
Computing formula：Yield=precipitate weight/example weight × 100%
As a result：Blank group dietary fiber yield is 24.06%, and experimental group dietary fiber yield is 24.91%.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of leaf mustard dietary fiber preparation method, it is characterised in that including：Leaf mustard is placed in ethanol water after being scalded through hydro-thermal
Mashing, takes slurries and is post-processed, and obtains leaf mustard dietary fiber.
2. preparation method according to claim 1, it is characterised in that the leaf mustard is 1 with the mass ratio of water：10~1：
25；
Concentration of alcohol in the ethanol water is 60%~80%；
Based on g/ml, leaf mustard and the mass volume ratio of ethanol water after the blanching are 1:6~1：12.
3. preparation method according to claim 1, it is characterised in that the temperature of the blanching is 60~100 DEG C；
The time of the blanching is 3~5min；
The rotating speed of the mashing is 15000~20000rpm；
The time of the mashing is 1~5min.
4. preparation method according to claim 1, it is characterised in that the post processing includes：
Suction filtration after slurries are stood, collects filter residue and is crushed, dried.
5. preparation method according to claim 4, it is characterised in that the temperature of the standing is 10~40 DEG C；
The time of the standing is 10~30min；
The suction filtration is decompression suction filtration；
The dry temperature is 60~90 DEG C；
The dry time is 8~12h.
6. a kind of leaf mustard diet fiber product, it is characterised in that including preparation method system described in Claims 1 to 5 any one
Acceptable auxiliary material on the leaf mustard dietary fiber and health products for obtaining.
7. leaf mustard diet fiber product according to claim 6, it is characterised in that the leaf mustard diet fiber product is mustard
Dish dietary fiber microcapsules, leaf mustard food fibre powder or leaf mustard meal fiber tablet；
The auxiliary material is wall material and emulsifying agent.
8. a kind of preparation method of leaf mustard dietary fiber microcapsules, it is characterised in that
Leaf mustard dietary fiber obtained in preparation method described in Claims 1 to 5 any one is placed in the wall that wall material is made into water
In material solution, embedded after adding emulsifier, then be spray-dried and compressing tablet.
9. preparation method according to claim 8, it is characterised in that the wall material is beta-schardinger dextrin or carragheen；
The concentration of wall material is 1wt%~3wt% in the wall material solution；
The emulsifying agent is octenyl succinic acid starch fat；
The addition of the emulsifying agent is the 1wt%~5wt% of the wall material solution；
The leaf mustard dietary fiber is 1 with the mass ratio of water:50.
10. preparation method according to claim 8, it is characterised in that the temperature of the emulsification is 40~70 DEG C；
The homogenization pressure of the embedding is 20-50MPa；
The EAT of the spray drying is 150~180 DEG C；
The leaving air temp of the spray drying is 55~85 DEG C；
The charging rate of the spray drying is 0.2~0.8ml/s；
The stream pressure of the spray drying is 0.1~0.3MPa.
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Application publication date: 20170623 |