CN106879577A - A kind of store method of walnut green husk pigment - Google Patents
A kind of store method of walnut green husk pigment Download PDFInfo
- Publication number
- CN106879577A CN106879577A CN201710112618.0A CN201710112618A CN106879577A CN 106879577 A CN106879577 A CN 106879577A CN 201710112618 A CN201710112618 A CN 201710112618A CN 106879577 A CN106879577 A CN 106879577A
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- Prior art keywords
- walnut
- pigment
- green
- rascal
- store method
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N3/00—Preservation of plants or parts thereof, e.g. inhibiting evaporation, improvement of the appearance of leaves or protection against physical influences such as UV radiation using chemical compositions; Grafting wax
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
- A61K2800/4324—Direct dyes in preparations for permanently dyeing the hair
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Birds (AREA)
- Dentistry (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Toxicology (AREA)
- Epidemiology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of store method of walnut green husk pigment, comprise the following steps：（1）Fresh green rind walnut is freezed, is taken out after a period of time and melted；（2）The rascal of outer layer is peeled with plastic spatula in depositing in hermetic bag；（3）The hermetic bag of rascal will be contained with it is put into freeze-drying in freeze drier and taken out after more than 72 hours, rascal is broken into powder with pulverizer, it is stand-by to preserve.Through the above way, green peel of walnut can be made hair keep preferably upper dye in 72 hours by the store method of walnut green husk pigment of the present invention by the pigment dye liquor that extraction is obtained again afterwards by freeze-drying, colouring works well, pigment still can be used to have hair dyed after being deposited through long-time, there is extensive market prospects in the popularization of the store method of walnut green husk pigment.
Description
Technical field
Preservation and extraction field the present invention relates to natural pigment, more particularly to a kind of preservation side of walnut green husk pigment
Method.
Background technology
Walnut is a kind of nut with healthy intelligence function, and walnut husk raw material sources are extensive, safety non-toxic, cost
It is cheap, reasonable development is carried out, huge economic benefit will be brought to the walnut place of production.Therefore research extracts color from green peel of walnut
Element has practical significance.But the pigment in green peel of walnut is easily aoxidized in atmosphere, the rascal pigment after oxidation cannot go up dye
Textile fabric, therefore, the store method of pigment has particularly important meaning in research green peel of walnut.
The juice of green peel of walnut splash on staff skin will blackening, even with rubber gloves, what infiltration was entered lacks
Skin on hand can also be contaminated black by amount rascal juice, and permanent colour-fast.In Europe, still useful green peel of walnut among the people dyes hair
The custom of brown, illustrates that walnut green husk pigment has coloring potential well.With stepping up and beautiful for people's health consciousness
The continuous progress of appearance science, people are no longer simply satisfied with dyeing of the hair dyeing product to hair, similarly pursue the health of body
And influence of the nutriment to hair metabolism in hair dyeing product.Under the trend of back to nature, people are in the urgent need to peace
Atoxic, allergic natural botanical hair dye will not be caused.Therefore, finding safety, natural organic pigment has turned into mesh
The study hotspot in the preceding field.
The content of the invention
The present invention solves the technical problem of a kind of store method of walnut green husk pigment is provided, by freeze-drying
Hair can be made to keep preferably upper dye, effect of painting by the pigment dye liquor that extraction is obtained green peel of walnut again afterwards within 72 hours
Well, pigment still can be used to have hair dyed after being deposited through long-time, have in the popularization of the store method of walnut green husk pigment
Extensive market prospects.
In order to solve the above technical problems, the present invention provides a kind of store method of walnut green husk pigment, comprise the following steps：
（1）Fresh green rind walnut is freezed, is taken out after a period of time and melted；
（2）The rascal of outer layer is peeled with plastic spatula in depositing in hermetic bag；
（3）The hermetic bag of rascal will be contained with it is put into freeze-drying in freeze drier and taken out after more than 72 hours, uses pulverizer
Rascal is broken into powder, it is stand-by to preserve.
In a preferred embodiment of the present invention, step（1）In thawing method include be soaked in water acceleration melt or put
Put and melt naturally in atmosphere.
In a preferred embodiment of the present invention, step（3）The Green Tangerine Peel of middle acquisition, is 1.2g/50mL in material ratio
Water, pH be 3~4, temperature be 50 DEG C in the environment of pigment extraction is carried out to green peel of walnut using extraction.
The beneficial effects of the invention are as follows：The store method of walnut green husk pigment of the present invention passes through freeze-drying 72 hours afterwards
Hair can be made to keep preferably upper dye by the pigment dye liquor that extraction is obtained green peel of walnut again, colouring works well, pigment
Still can be used to have hair dyed after being deposited through long-time, there is extensive market in the popularization of the store method of walnut green husk pigment
Prospect.
Specific embodiment
The technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, this area is common
All other embodiment that technical staff is obtained under the premise of creative work is not made, belongs to the model of present invention protection
Enclose.
The embodiment of the present invention includes：
A kind of store method of walnut green husk pigment, comprises the following steps：
（1）Fresh green rind walnut is freezed, is taken out after a period of time and melted；
（2）The rascal of outer layer is peeled with plastic spatula in depositing in hermetic bag；
（3）The hermetic bag of rascal will be contained with it is put into freeze-drying in freeze drier and taken out after more than 72 hours, uses pulverizer
Rascal is broken into powder, it is stand-by to preserve.
Preferably, step（1）In thawing method include be soaked in water acceleration melt or place in atmosphere naturally thawing.
Preferably, step（3）The Green Tangerine Peel of middle acquisition, is 1.2g/50mL water in material ratio, and pH is 3~4, and temperature is
Pigment extraction is carried out to green peel of walnut using extraction in the environment of 50 DEG C, pigment extraction effect now is optimal.
The present invention has not only investigated store method, while also studied material using the orthogonal test of the level of four factor three
Than, pH, the factor such as temperature is in extraction process to the influence of pigment.Due to extracting the pigment in green peel of walnut primarily to dye
Hair, therefore by extracting the pigment in green peel of walnut and hair being dyeed, the color depth of hair after dyeing is characterized
The content of pigment.
Colouring method：By the dye liquor suction filtration after extraction, weigh 1g hair samples and be put into dye liquor, the heating water bath at 60 DEG C
1h, the K/S values of hair after to dyeing, electron microscopic section and reflectivity come characterize dye after hair color depth；
| Tested number | Material ratio/g/50mL | pH | Store method | Temperature/DEG C | K/S |
| 1 | 0.8 | 3~4 | It is lyophilized | 50 | 16.1266 |
| 2 | 0.8 | 4~5 | Drying | 60 | 4.292 |
| 3 | 0.8 | 5~6 | Freezing | 70 | 7.9336 |
| 4 | 1 | 3~4 | Drying | 70 | 4.4034 |
| 5 | 1 | 4~5 | Freezing | 50 | 10.4064 |
| 6 | 1 | 5~6 | It is lyophilized | 60 | 11.1988 |
| 7 | 1.2 | 3~4 | Freezing | 60 | 11.6496 |
| 8 | 1.2 | 4~5 | It is lyophilized | 70 | 14.1818 |
| 9 | 1.2 | 5~6 | Drying | 50 | 2.9778 |
| K1 | 9.451 | 10.727 | 13.836 | 9.837 | |
| K2 | 8.670 | 9.627 | 3.891 | 9.047 | |
| K3 | 9.603 | 7.370 | 9.997 | 8.840 | |
| R | 0.933 | 3.357 | 9.945 | 0.997 |
By experimental result as can be seen that by freeze-drying preserve green peel of walnut compared with other two kinds of preserving type Colors most
It is good, and extracting effect is 1.2g/50mL water in material ratio, pH is 3~4, and temperature is preferable when being 50 DEG C.
The beneficial effect of the store method of walnut green husk pigment of the present invention is：
First, by the way that green peel of walnut dried and powder is broken into, is easy to the preservation of green peel of walnut；
2nd, exposed under the pigment normal temperature in green peel of walnut and easily aoxidized in atmosphere, the common methods such as drying of drying can cause
The oxidation of rascal pigment, the moisture in rascal is removed using the method for freeze-drying, under low temperature, it is ensured that its when moisture removal is removed not
Aoxidize, hair can be made to keep preferably upper dye, colouring works well, pigment still can be used to after being deposited through long-time
Hair dyeing.
Embodiments of the invention are the foregoing is only, the scope of the claims of the invention is not thereby limited, it is every to utilize this hair
Equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks
Domain, is included within the scope of the present invention.
Claims (3)
1. a kind of store method of walnut green husk pigment, it is characterised in that comprise the following steps：
（1）Fresh green rind walnut is freezed, is taken out after a period of time and melted；
（2）The rascal of outer layer is peeled with plastic spatula in depositing in hermetic bag；
（3）The hermetic bag of rascal will be contained with it is put into freeze-drying in freeze drier and taken out after more than 72 hours, uses pulverizer
Rascal is broken into powder, it is stand-by to preserve.
2. the store method of walnut green husk pigment according to claim 1, it is characterised in that step（1）In thawing side
Method includes being soaked in water acceleration thawing or places thawing naturally in atmosphere.
3. the store method of walnut green husk pigment according to claim 1, it is characterised in that step（3）The green grass or young crops of middle acquisition
Skin powder, material ratio be 1.2g/50mL water, pH be 3~4, temperature be 50 DEG C in the environment of using extraction to green peel of walnut
Carry out pigment extraction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710112618.0A CN106879577A (en) | 2017-02-28 | 2017-02-28 | A kind of store method of walnut green husk pigment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710112618.0A CN106879577A (en) | 2017-02-28 | 2017-02-28 | A kind of store method of walnut green husk pigment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106879577A true CN106879577A (en) | 2017-06-23 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710112618.0A Pending CN106879577A (en) | 2017-02-28 | 2017-02-28 | A kind of store method of walnut green husk pigment |
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| Country | Link |
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| CN (1) | CN106879577A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109431933A (en) * | 2018-11-28 | 2019-03-08 | 山东师范大学 | A kind of sun-proof color protection hair-cream and its preparation method and application |
| CN115433474A (en) * | 2022-09-21 | 2022-12-06 | 阿克苏市韩妮克时尚科技有限公司 | Preparation method of walnut green husk plant color-dyed fabric |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103073911A (en) * | 2012-12-28 | 2013-05-01 | 宁波广源纺织品有限公司 | Extraction method of walnut shell dye |
| CN105133380A (en) * | 2015-10-19 | 2015-12-09 | 新疆大学 | Method for extracting pigment from walnut green hulls through subcritical water and using pigment for dyeing |
| CN105331141A (en) * | 2014-08-16 | 2016-02-17 | 天水龙飞纺织有限公司 | Walnut green husk pigment extracting and dyeing method |
-
2017
- 2017-02-28 CN CN201710112618.0A patent/CN106879577A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103073911A (en) * | 2012-12-28 | 2013-05-01 | 宁波广源纺织品有限公司 | Extraction method of walnut shell dye |
| CN105331141A (en) * | 2014-08-16 | 2016-02-17 | 天水龙飞纺织有限公司 | Walnut green husk pigment extracting and dyeing method |
| CN105133380A (en) * | 2015-10-19 | 2015-12-09 | 新疆大学 | Method for extracting pigment from walnut green hulls through subcritical water and using pigment for dyeing |
Non-Patent Citations (3)
| Title |
|---|
| 史宏艺 等: "核桃青皮中色素的染色性能及成分分析", 《天然产物研究与开发》 * |
| 易建华: "提取方法对核桃青皮色素理化性质的影响", 《食品与机械》 * |
| 赵国建 等: "螯合剂辅助提取核桃青皮原花色素研究", 《农产品加工（学刊）》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109431933A (en) * | 2018-11-28 | 2019-03-08 | 山东师范大学 | A kind of sun-proof color protection hair-cream and its preparation method and application |
| CN109431933B (en) * | 2018-11-28 | 2021-11-09 | 山东师范大学 | Sunscreen and color-care hair cream and preparation method and application thereof |
| CN115433474A (en) * | 2022-09-21 | 2022-12-06 | 阿克苏市韩妮克时尚科技有限公司 | Preparation method of walnut green husk plant color-dyed fabric |
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Application publication date: 20170623 |
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