CN106852953A - A kind of Chinese medical extract of nti-freckle and preparation method thereof - Google Patents
A kind of Chinese medical extract of nti-freckle and preparation method thereof Download PDFInfo
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- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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Abstract
The invention belongs to the field of Chinese medicines, a kind of Chinese medical extract of nti-freckle and preparation method thereof is disclosed, the Chinese medical extract of described nti-freckle includes the extract of following weight parts：Waxgourd peel water extract is 12 25 parts, semen astragali complanati supercritical extract is 24 parts, meadow pine ethanol extract is 39 parts.The techniques such as preparation method to different traditional Chinese medicine ingredients including being dried, crushing, solvent extraction, supercritical extract, mixing, prepare the Chinese medical extract with spot-removing function.Chinese medical extract of the invention has preferable curative effect in treatment freckle and chloasma field.
Description
Technical field
The invention belongs to tcm field, it is related to a kind of Chinese medical extract and preparation method thereof, more particularly to a kind of Chinese medical extract of nti-freckle and preparation method thereof.
Background technology
Freckle is the yellowish-brown point-like pigmentation spots on skin of face, is autosomal dominant inheritance.Sun direct irradiation can induce and aggravate freckle.Freckle is more in women, and its numbers with age increases and gradually increases.Face, particularly nose and two cheeks are apt to occur in, the exposure portions such as neck, shoulder, the back of the hand can be involved.It is shallow brown or crineous syringe needle size to the big macula of mung bean to damage, circular, oval or irregular.Summer fash color burn, number after Exposure to Sunlight increase, and winter then mitigates or disappears.Often there is family history.Chloasma is also referred to as chloasma hepaticum, is the yellowish-brown pigmentation of face.Many symmetrical butterflies are distributed in cheek.Women is more common in, estrogen level height is main cause in blood, its morbidity is relevant with gestation, Long-term Oral contraceptive, paramenia.
The Chinese medicine for the treatment of freckle and chloasma is less, and patent authorization number is a kind of Chinese medicine composition of beauty treatment and eliminating spot of disclosure of the invention of CN1207038A, including Radix Angelicae Sinensis, safflower, pearl powder, vitamin E.The Chinese medicine composition of the invention improves also unobvious on nti-freckle.In addition, most Chinese medicine does not have preferable curative effect in treatment freckle and chloasma, it is impossible to avoid freckle and chloasma in the deposition of face.Therefore need to extract the active ingredient in Chinese medicine obtaining treatment freckle and chloasma and there is the Chinese medical extract of remarkable effect.
The content of the invention
The technical problem to be solved：Face seriously annoyings people's life due to the chloasma of sunlight irradiation or other reasonses generation with freckle, the chloasma of generation is simultaneously few with the method for freckle removing, treatment by Chinese herbs place to go chloasma is also poor with the method effect of freckle, the chloasma and freckle of people's face can not preferably be dispelled, it is therefore desirable to a kind of Chinese medical extract of nti-freckle and preparation method thereof.
Technical scheme：Regarding to the issue above, the invention discloses a kind of Chinese medical extract of nti-freckle, the Chinese medical extract of described nti-freckle includes the extract of following weight parts：Waxgourd peel water extract is 12 25 parts, semen astragali complanati supercritical extract is 24 parts, meadow pine ethanol extract is 39 parts.
Preferably, a kind of extract of the Chinese medical extract of described nti-freckle, including following weight parts：Waxgourd peel water extract is 12 25 parts, semen astragali complanati supercritical extract is 24 parts, meadow pine ethanol extract is 39 parts, rice sprout water extract is 27 parts, Aloe Vera Gel is 37 parts.
It is further preferred that a kind of Chinese medical extract of described nti-freckle, including following weight parts extract：Waxgourd peel water extract is 18 parts, semen astragali complanati supercritical extract is 3 parts, meadow pine ethanol extract is 6 parts, rice sprout water extract is 5 parts, Aloe Vera Gel is 6 parts.Described waxgourd peel is dry waxgourd peel.
The preparation method of the Chinese medical extract of-kind of nti-freckle, the preparation method of described Chinese medical extract is comprised the following steps：（1) waxgourd peel is extracted with water, separate vacuum concentration after extraction, is waxgourd peel water extract after concentration；（2) supercritical carbon dioxide extracting will be carried out after semen astragali complanati freeze-drying, crushing, liquid in separating still is collected after extraction, liquid is semen astragali complanati supercritical extract；（3) crushed after meadow pine is dried, solvent extraction is carried out with absolute ethyl alcohol, filtered after extraction, be concentrated to give meadow pine ethanol extract；（4) extracted with pure water after rice sprout is crushed, filtered after extraction, vacuum concentration, is rice sprout water extract；
(5) fresh aloe is beaten, glue is separated with aloe slag, is prepared into Aloe Vera Gel；（6) take by weight waxgourd peel water extract for 12 25 parts, semen astragali complanati supercritical extract be 24 parts, meadow pine ethanol extract be 39 parts, rice sprout water extract be 27 parts, Aloe Vera Gel be 37 parts, above-mentioned extract is well mixed, is the Chinese medical extract with spot-removing function.
Preferably, a kind of preparation method of the Chinese medical extract of described nti-freckle, the preparation method of described Chinese medical extract is comprised the following steps：1) fresh waxgourd peel is cut, fresh waxgourd peel is beaten, waxgourd peel is soaked in 2h in water after mashing, extracted with water after h, Extracting temperature is 45.C, extraction time is 3h, and solid-liquid ratio is 1:5, supernatant is passed through into centrifugation with precipitation after extraction, supernatant is concentrated in vacuo after separation, temperature concentrated in vacuo is 50C, is waxgourd peel water extract after concentration；（2) semen astragali complanati is carried out into freeze-drying first, semen astragali complanati is crushed after freeze-drying, supercritical carbon dioxide extracting is carried out after crushing, supercritical carbon dioxide extracting pressure is 25MPa, one-level separating still and the second-order separation kettle pressure are 7MPa, and extraction temperature is 55C, and extraction time is 3h, liquid in separating still is collected after extraction, liquid is semen astragali complanati supercritical extract；（3) crushed again after meadow pine high temperature is dried, carry out solvent extraction after crushing with absolute ethyl alcohol, Extracting temperature is 60C, and extraction time is 2h, and solid-liquid ratio is 1:8, filtered after extraction, supernatant vacuum concentration is obtained into meadow pine ethanol extract after filtering；（4) rice sprout is taken, rice sprout is crushed with disintegrating machine, extracted with pure water after crushing, Extracting temperature is 55C, and extraction time is 2h, and solid-liquid ratio is 1:7, filtered after extraction, filtrate is concentrated in vacuo, concentrate is rice sprout water extract；（5) fresh aloe is beaten, glue is separated with aloe slag after mashing, be prepared into Aloe Vera Gel；（6) take by weight waxgourd peel water extract for 12 25 parts, semen astragali complanati supercritical extract be 24 parts, meadow pine ethanol extract be 39 parts, rice sprout water extract be 27 parts, Aloe Vera Gel be 37 parts, above-mentioned extract is well mixed, is the Chinese medical extract with spot-removing function.
In to Chinese medicine on the basis of natural component research, the present invention is extracted to the composition with specific spot-removing function in the traditional Chinese medicine ingredients of different properties, mixed after extraction, the extract of the different properties combined has played corresponding synergy, has preferable curative effect to nti-freckle.
Beneficial effect：Chinese traditional medicine composition extract of the invention has extraordinary effect in terms for the treatment of freckle and chloasma, after Chinese medical extract of the invention is diluted into 3 times, is coated in face, and the freckle and chloasma of patient facial region have obtained effective and comprehensively healing.Embodiment measurement result shows that the effective cure rate of freckle and chloasma of patient is very high, has reached 86% to 94%.
Specific embodiment
Embodiment 1
(1) fresh waxgourd peel is cut, fresh waxgourd peel is beaten, waxgourd peel is soaked in 2h in water after mashing, extracted with water after 2h, Extracting temperature is 45C, and extraction time is 3h, and solid-liquid ratio is 1:5, supernatant is passed through into centrifugation with precipitation after extraction, supernatant is concentrated in vacuo after separation, temperature concentrated in vacuo is 50C, is waxgourd peel water extract after concentration；(2) semen astragali complanati is carried out into freeze-drying first, semen astragali complanati is crushed after freeze-drying, supercritical carbon dioxide extracting is carried out after crushing, supercritical carbon dioxide extracting pressure is 25MPa, one-level separating still and the second-order separation kettle pressure are 7MPa, and extraction temperature is 55C, and extraction time is 3h, liquid in separating still is collected after extraction, liquid is semen astragali complanati supercritical extract；（3) crushed again after meadow pine high temperature is dried, carry out solvent extraction after crushing with absolute ethyl alcohol, Extracting temperature is 60C, and extraction time is 2h, and solid-liquid ratio is 1:8, filtered after extraction, supernatant vacuum concentration is obtained into meadow pine ethanol extract after filtering；（4) rice sprout is taken, rice sprout is crushed with disintegrating machine, extracted with pure water after crushing, Extracting temperature is 55C, and extraction time is 2h, and solid-liquid ratio is 1:7, filtered after extraction, filtrate is concentrated in vacuo, concentrate is rice sprout water extract；（5) fresh aloe is beaten, glue is separated with aloe slag after mashing, be prepared into Aloe Vera Gel；（6) take by weight waxgourd peel water extract for 18 parts, semen astragali complanati supercritical extract be 3 parts, meadow pine ethanol extract be 6 parts, rice sprout water extract be 5 parts, Aloe Vera Gel be 6 parts, above-mentioned extract is well mixed, is the Chinese medical extract with spot-removing function.
Embodiment 2
(1) fresh waxgourd peel is cut, fresh waxgourd peel is beaten, waxgourd peel is soaked in 2h in water after mashing, extracted with water after 2h, Extracting temperature is 45.C, extraction time is 3h, and solid-liquid ratio is 1:5, supernatant is passed through into centrifugation with precipitation after extraction, supernatant is concentrated in vacuo after separation, temperature concentrated in vacuo is 50C, is waxgourd peel water extract after concentration；(2) semen astragali complanati is carried out into freeze-drying first, semen astragali complanati is crushed after freeze-drying, supercritical carbon dioxide extracting is carried out after crushing, supercritical carbon dioxide extracting pressure is 25MPa, one-level separating still and the second-order separation kettle pressure are 7MPa, and extraction temperature is 55C, and extraction time is 3h, liquid in separating still is collected after extraction, liquid is semen astragali complanati supercritical extract；（3) crushed again after meadow pine high temperature is dried, carry out solvent extraction after crushing with absolute ethyl alcohol, Extracting temperature is 60C, and extraction time is 2h, and solid-liquid ratio is 1:8, filtered after extraction, supernatant vacuum concentration is obtained into meadow pine ethanol extract after filtering；（4) rice sprout is taken, rice sprout is crushed with disintegrating machine, extracted with pure water after crushing, Extracting temperature is 55C, and extraction time is 2h, and solid-liquid ratio is 1:7, filtered after extraction, filtrate is concentrated in vacuo, concentrate is rice sprout water extract；（5) fresh aloe is beaten, glue is separated with aloe slag after mashing, be prepared into Aloe Vera Gel；(6) take by weight waxgourd peel water extract for 25 parts, semen astragali complanati supercritical extract be 4 parts, meadow pine ethanol extract be 9 parts, rice sprout water extract be 2 parts, Aloe Vera Gel be 7 parts, above-mentioned extract is well mixed, is the Chinese medical extract with spot-removing function.
Embodiment 3
(1) fresh waxgourd peel is cut, fresh waxgourd peel is beaten, waxgourd peel is soaked in 2h in water after mashing, extracted with water after 2h, Extracting temperature is 45C, and extraction time is 3h, and solid-liquid ratio is 1:5, supernatant is passed through into centrifugation with precipitation after extraction, supernatant is concentrated in vacuo after separation, temperature concentrated in vacuo is 50C, is waxgourd peel water extract after concentration；(2) semen astragali complanati is carried out into freeze-drying first, semen astragali complanati is crushed after freeze-drying, supercritical carbon dioxide extracting is carried out after crushing, supercritical carbon dioxide extracting pressure is 25MPa, one-level separating still and the second-order separation kettle pressure are 7MPa, and extraction temperature is 55C, and extraction time is 3h, liquid in separating still is collected after extraction, liquid is semen astragali complanati supercritical extract；（3) crushed again after meadow pine high temperature is dried, carry out solvent extraction after crushing with absolute ethyl alcohol, Extracting temperature is 60C, and extraction time is 2h, and solid-liquid ratio is 1:8, filtered after extraction, supernatant vacuum concentration is obtained into meadow pine ethanol extract after filtering；（4) rice sprout is taken, rice sprout is crushed with disintegrating machine, extracted with pure water after crushing, Extracting temperature is 55C, and extraction time is 2h, and solid-liquid ratio is 1:7, filtered after extraction, filtrate is concentrated in vacuo, concentrate is rice sprout water extract；（5) fresh aloe is beaten, glue is separated with aloe slag after mashing, be prepared into Aloe Vera Gel；（6) take by weight waxgourd peel water extract for 12 parts, semen astragali complanati supercritical extract be 2 parts, meadow pine ethanol extract be 3 parts, rice sprout water extract be 7 parts, Aloe Vera Gel be 3 parts, above-mentioned extract is well mixed, is the Chinese medical extract with spot-removing function.
Embodiment 4
(1) fresh waxgourd peel is cut, fresh waxgourd peel is beaten, waxgourd peel is soaked in 2h in water after mashing, extracted with water after 2h, Extracting temperature is 45C, and extraction time is 3h, and solid-liquid ratio is 1:5, supernatant is passed through into centrifugation with precipitation after extraction, supernatant is concentrated in vacuo after separation, temperature concentrated in vacuo is 50C, is waxgourd peel water extract after concentration；(2) semen astragali complanati is carried out into freeze-drying first, semen astragali complanati is crushed after freeze-drying, supercritical carbon dioxide extracting is carried out after crushing, supercritical carbon dioxide extracting pressure is 25MPa,-level separating still and the second-order separation kettle pressure are 7MPa, and extraction temperature is 55C, and extraction time is 3h, liquid in separating still is collected after extraction, liquid is semen astragali complanati supercritical extract；（3) crushed again after meadow pine high temperature is dried, carry out solvent extraction after crushing with absolute ethyl alcohol, Extracting temperature is 60C, and extraction time is 2h,
Solid-liquid ratio is 1:8, filtered after extraction, supernatant vacuum concentration is obtained into meadow pine ethanol extract after filtering；（4) take by weight waxgourd peel water extract for 25 parts, semen astragali complanati supercritical extract be 4 parts, meadow pine ethanol extract be 9 parts, above-mentioned extract is well mixed, be the Chinese medical extract with spot-removing function.
Comparative example：
Take by weight when be classified as 10 parts, safflower be 3 parts, pearl powder be 3 parts, vitamin E be 4 parts.Patient facial region is coated in after extract solution is concentrated after decocting, patient is 10,30min is applied daily, the cycle is 10 days, and the effective cure rate of patient's part spot point is 55% after 10 days, less than the Cure of Chinese medical extract of the invention.
Claims (4)
1. a kind of Chinese medical extract of nti-freckle, it is characterised in that the Chinese medical extract of described nti-freckle includes carrying for following weight parts
Take thing：Waxgourd peel water extract is 12 25 parts, semen astragali complanati supercritical extract is 24 parts, meadow pine ethanol extract is 3
9 parts.
2. a kind of Chinese medical extract of nti-freckle according to claim 1, it is characterised in that the traditional Chinese medicine extraction of described nti-freckle
Thing includes the extract of following weight parts：Waxgourd peel water extract is 12 25 parts, semen astragali complanati supercritical extract is 24 parts,
Meadow pine ethanol extract is 39 parts, rice sprout water extract is 27 parts, Aloe Vera Gel is 37 parts.
3. a kind of Chinese medical extract of nti-freckle according to claim 2, it is characterised in that the traditional Chinese medicine extraction of described nti-freckle
Waxgourd peel water extract weight is 18 parts in thing.
4. a kind of preparation method of the Chinese medical extract of nti-freckle according to claim 2, it is characterised in that described Chinese medicine
The preparation method of extract is comprised the following steps：（1) waxgourd peel is extracted with water, separate vacuum concentration after extraction, concentration
It is afterwards waxgourd peel water extract；（2) supercritical carbon dioxide extracting will be carried out after semen astragali complanati freeze-drying, crushing, is collected after extraction
Liquid in separating still, liquid is semen astragali complanati supercritical extract；（3) crushed after meadow pine is dried, solvent is carried out with absolute ethyl alcohol
Extract, filtered after extraction, be concentrated to give meadow pine ethanol extract；（4) extracted with pure water after rice sprout is crushed, after extraction
Filtering, vacuum concentration, is rice sprout water extract；（5) fresh aloe is beaten, glue is separated with aloe slag, is prepared into aloe
Glue；（6) waxgourd peel water extract is taken by weight for 12 25 parts, semen astragali complanati supercritical extract are 24 parts, meadow pine ethanol
Extract is 39 parts, rice sprout water extract is 27 parts, Aloe Vera Gel is 37 parts, and above-mentioned extract is well mixed,
It is the Chinese medical extract with spot-removing function.
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| CN110101666A (en) * | 2019-05-22 | 2019-08-09 | 湖南华康生物科技股份有限公司 | The production method that a kind of low ash divides Horsetail P.E |
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| CN110101666A (en) * | 2019-05-22 | 2019-08-09 | 湖南华康生物科技股份有限公司 | The production method that a kind of low ash divides Horsetail P.E |
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