CN106822598A - A kind of preparation containing Tea Polyphenols - Google Patents
A kind of preparation containing Tea Polyphenols Download PDFInfo
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- A61K2236/30—Extraction of the material
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- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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Abstract
The invention discloses a kind of preparation containing Tea Polyphenols, said preparation is by the Tea Polyphenols, dendrobium candidum extract, wolfberry fruit extract, anthocyanidin, Abelmoschus Esculentus Linn extract, glidant and the sweetener that necessarily match for raw material is prepared from.Said preparation can anti-aging, strengthen male's sexual, and its preparation method is simple, raw material sources extensively, be easy to get, low cost.
Description
Technical field
The invention belongs to health medicine technical field, and in particular to a kind of preparation containing Tea Polyphenols.
Background technology
Tea (Camellia sinensis (L.) O.Ktze) drinks a kind of traditional health plant of more than 2,000 years for the mankind
Beverage raw material, with anti-aging, refresh the mind, prevent and treat three it is high the effects such as.There is the tealeaves base of large-scale plantation all parts of the country
Ground, and produce all kinds of well-known teas with region feature various in style.However, with the progress of society and science and technology, dietotherapeutic
Teas resource be developed, and traditional tea deep processed product is received due to starting with stronger health-care efficacy
To the welcome of people.
The main active of Tea Industry deep processed product is Tea Polyphenols, with work(such as anti-oxidant, anti-aging, bacteriostasis, preservations
Effect.With Tea Polyphenols as major ingredient, scientific formula is carried out, the medicine that production has more health value is the direction of Tea Industry deep processing development.
The content of the invention
Based on above-mentioned prior art, the invention provides a kind of preparation containing Tea Polyphenols, said preparation being capable of anti-aging, enhancing
Male's sexual.
Realize technical scheme that above-mentioned purpose of the present invention used for:
A kind of preparation containing Tea Polyphenols, is prepared from by the raw material of following mass parts:
Further, described dendrobium candidum extract is Dendrobium officinale polysaccharide or dendrobine, and described wolfberry fruit extract is
Matrimony vine isoflavones or matrimony vine Thick many candies, when dendrobium candidum extract is Dendrobium officinale polysaccharide, wolfberry fruit extract is that matrimony vine is slightly more
Sugar, when dendrobium candidum extract is dendrobine, wolfberry fruit extract is matrimony vine isoflavones.
Further, described Tea Polyphenols is prepared from by following methods:
By fresh tea leaf drying, crush, obtain tea-leaf power, by the tea-leaf power 3-5 times of boiling water of quality of addition, insulation is soaked
Bubble 30 minutes, filtering adds filter residue in the 3-5 times of boiling water of quality again, so operates 2-3 times repeatedly, collects and combines every time
Filtrate obtained by filtering, obtains aqueous extract, adds chloroform to be extracted after aqueous extract is concentrated, and water phase is separated to obtain, by water phase
Concentration, drying, crush, and obtain powdered Tea Polyphenols.
Further, when described dendrobium candidum extract is Dendrobium officinale polysaccharide, Dendrobium officinale polysaccharide is by following methods system
It is standby to form:
By dendrobium candidum dries pulverizing, dendrobium candidum powder is obtained, entered during dendrobium candidum powder is added into the 3-5 times of water of quality
Row is decocted, and is filtered after the completion of decoction, and filtrate is evaporated, and obtains dendrobium candidum aqueous extract, and dendrobium candidum aqueous extract is crushed, and is obtained
The Dendrobium officinale polysaccharide of meal shape.
Further, when described dendrobium candidum extract is dendrobine, dendrobine is prepared from by following methods:
By dendrobium candidum dries pulverizing, dendrobium candidum powder is obtained, entered during dendrobium candidum powder is added into the 3-5 times of water of quality
Row is decocted, and is filtered after the completion of decoction, is boiled boiling is carried out in the filter residue 3-5 times of ethanol solution of more than the 95wt% of quality of addition, is boiled
Filtered after the completion of boiling, filtrate is evaporated, obtain dendrobium candidum ethanol extract, dendrobium candidum ethanol extract is really concentrated into drying, powder
It is broken, obtain the dendrobine of meal shape.
Further, when described wolfberry fruit extract is matrimony vine isoflavones, matrimony vine isoflavones is prepared from by following methods:
By fresh fruit of Chinese wolfberry dries pulverizing, fruit of Chinese wolfberry powder is obtained, entered during fruit of Chinese wolfberry powder is added into the 3-10 times of water of quality
Row is decocted, and is filtered after the completion of decoction, is concentrated the filtrate in pulpous state, adds ethyl acetate extraction, separates to obtain organic phase, will be had
Machine phase concentration and recovery ethyl acetate, obtains Fructus Lycii extractum, and Fructus Lycii extractum is dried, and crushes, and obtains powdered matrimony vine different
Flavones.
Further, when described wolfberry fruit extract is matrimony vine different Thick many candies, the different Thick many candies of Qi are prepared from by following methods:
By fresh fruit of Chinese wolfberry dries pulverizing, fruit of Chinese wolfberry powder is obtained, entered during fruit of Chinese wolfberry powder is added into the 3-10 times of water of quality
Row is decocted, and is filtered after the completion of decoction, by the final concentration of of the ethanol solution of filter residue addition 95wt%-100wt%- to ethanol
75wt%-85wt%, is stood to precipitating completely, and collection is precipitated and dried, and obtains matrimony vine Thick many candies.
Further, described anthocyanidin is prepared from by following methods:
By the mashing of fresh purple potato, purple potato slurry is obtained, the 5-10 times of ethanol of more than the 95wt% of volume is added in being starched to purple potato
Solution, stirs, and stands, collection supernatant complete to precipitating, and is concentrated to dryness, and crushes, and obtains the cyanine of meal shape
Element.
Further, described Abelmoschus Esculentus Linn extract is prepared from by following methods:
By the drying of fresh okra fruit, crush, obtain okra fruit powder, okra fruit powder is added into 3-5
The water of times quality carries out boiling and boils, and boiling is filtered after the completion of boiling, and filter residue is added again and carry out boiling in the 3-5 times of water of volume and boil, so
Operate 2-3 times repeatedly, collect and combine the filtrate every time obtained by filtering, concentrate and dry, obtain Abelmoschus Esculentus Linn extract.
Compared with prior art, the advantages of the present invention are:
1st, the present invention is extracted from Tea Polyphenols, dendrobium candidum extract, Fructus lycii P.E, anthocyanidin and okra first
Thing is compounded, and develops the health medicine acted on significant anti-aging and enhancing sexual function.
2nd, said preparation centering old age sexual deterioration is evident in efficacy and stable.
3rd, each raw material can be extracted from plant in said preparation, and extracting method is simple, just can be direct without refined and purifying
Use, the cost needed for considerably reducing raw material.
4th, the simple production process of said preparation, easy to operate, with low cost needed for preparing.
Specific embodiment
With reference to specific embodiment, the present invention is described in detail.
Embodiment 1
A kind of preparation containing Tea Polyphenols, is prepared from by the raw material of following mass parts:
The preparation method of the above-mentioned preparation containing Tea Polyphenols, its step is:
1st, the preparation of Tea Polyphenols:
By fresh tea leaf drying, crush, obtain tea-leaf power, by tea-leaf power add 4 times of boiling water of quality in, heat-insulation soaking
30min, filtering adds filter residue in 4 times of boiling water of quality again, so operates 3 times repeatedly, collects the filter obtained by 3 filterings
Liquid, obtains aqueous extract, and aqueous extract is concentrated in vacuo into 1/3rd volumes at 60 DEG C, obtains concentrate, and concentrate is added
The chloroform of the volume of one half is extracted, and separates to obtain water phase, water is mutually concentrated, is dried, and is crushed, and obtains powdered Tea Polyphenols.
2nd, the preparation of Dendrobium officinale polysaccharide
By dendrobium candidum dries pulverizing, dendrobium candidum powder is obtained, decocted during dendrobium candidum powder is added into 4 times of water of quality
30min, filtering, filtrate is evaporated, and obtains dendrobium candidum aqueous extract, and the content of dendrobium polysaccharide is in dendrobium candidum aqueous extract
25.8wt%, dendrobium candidum aqueous extract is crushed, and obtains the Dendrobium officinale polysaccharide of meal shape.
3rd, the preparation of matrimony vine Thick many candies:
By the sub- dries pulverizing of fresh lycium barbarum, fruit of Chinese wolfberry powder is obtained, decocted during fruit of Chinese wolfberry powder is added into 6 times of water of quality
30min is boiled, is filtered, add the ethanol solution of 95wt% to the final concentration of 80wt% of ethanol filter residue, staticly settled 5 hours,
Collection is precipitated and dried, and obtains matrimony vine Thick many candies, and with glucose meter, the content of polysaccharide is 30.5wt% in matrimony vine Thick many candies.
4th, the preparation of anthocyanidin:
By the mashing of fresh purple potato, purple potato slurry is obtained, 8 times of ethanol solutions of the 95wt% of volume are added in being starched to purple potato, filled
Divide and stir, stand to precipitating completely, collection supernatant, concentration is evaporated, and crushes, and obtains the anthocyanidin of meal shape.
5th, the preparation of Abelmoschus Esculentus Linn extract:
By the drying of fresh okra fruit, crush, obtain okra fruit powder, okra fruit powder is added 4 times
30min is boiled in the water boiling of quality, is filtered, and filter residue is added again and carry out boiling in 4 times of water of volume and boil, and is so operated 3 times repeatedly, is received
Collection merges the filtrate obtained by 3 filterings, is concentrated in vacuo and dries at 60 DEG C, obtains Abelmoschus Esculentus Linn extract.
6th, weigh each raw material by said ratio, by each raw material be well mixed it is laggard expect carry out compressing tablet in tablet press machine, produce
Chewable tablet, every 1.5 grams of Single seed weight;Or crushed after each raw material is well mixed, reproduction is filled into capsule in each capsule
Fill 0.8 gram of powder.
The anti-aging effects experiment of the experiment one, preparation containing Tea Polyphenols of the invention
Experimental technique:
Preparation (being control with gavage physiological saline) prepared by 24 monthly age aged mouse gavage embodiment 1 is used, dosage is
0.1 gram/day/only, the gavage time be 15 days, after gavage terminates, test mouse in serum reduction-state level (DPPH methods) and its resist
Fatigue capability (using swimming time as criterion).
Experimental result:
Experiment 5 times is repeated, is averaged, as a result as shown in table 1:
The anti-reduction-state level of serum and anti-fatigue ability (test number (TN) N=5) of the mouse of table 1
Free radical scavenging activity (%) in serum | Swimming time (min) | |
Control group | 35.5±5.1 | 31±8 |
Administration group | 48.5±5.5 | 44±11 |
From table 1 it follows that after mouse takes said preparation, free radical scavenging activity substantially becomes big in mice serum, shows
The serum reduction-state level of mouse is improved, and mouse swimming time is substantially elongated, shows the anti-fatigue ability enhancing of mouse, can
See, the general health of mouse is significantly improved.It is indicated above that said preparation energy anti-aging, anti-aging.
Experiment two, the enhancing sexual function effect test of the preparation containing Tea Polyphenols of the invention
Use preparation (being control with gavage physiological saline) prepared by 24 monthly ages old-age group's male mice gavage embodiment 1, agent
It is 0.1 gram/day/to measure, and the gavage time is 15 days, and after gavage terminates, test male mice is with female mice in 12 hours
Number of copulations.
Experimental result:
Experiment 20 times is repeated, is averaged, as a result as shown in table 2:
The number of copulations (experiment repeats N=20) of the male mouse of table 2
Ride total degree | |
Control group | 18 |
Administration group | 31 |
Find out as known from Table 2, after male mouse takes said preparation, the number of copulations pole of mouse dramatically increases, it is indicated above that should
Preparation can significantly increase male sexuality.
Embodiment 2
A kind of preparation containing Tea Polyphenols, is prepared from by the raw material of following mass parts:
The preparation method of the above-mentioned preparation containing Tea Polyphenols, its step is:
1st, the preparation of Tea Polyphenols:
By fresh tea leaf drying, crush, obtain tea-leaf power, by tea-leaf power add 3 times of boiling water of quality in, heat-insulation soaking
30min, filtering adds filter residue in 3 times of boiling water of quality again, so operates 3 times repeatedly, collects the filter obtained by 3 filterings
Liquid, obtains aqueous extract, and aqueous extract is concentrated in vacuo into 1/3rd volumes at 60 DEG C, obtains concentrate, and concentrate is added
The chloroform of the volume of one half is extracted, and separates to obtain water phase, water is mutually concentrated, is dried, and is crushed, and obtains powdered Tea Polyphenols.
2nd, the preparation of dendrobine
By dendrobium candidum dries pulverizing, dendrobium candidum powder is obtained, decocted during dendrobium candidum powder is added into 5 times of water of quality
30min, filtering, 20min is boiled in boiling during filter residue is added into 4 times of ethanol solutions of the 95wt% of quality, is filtered, and filtrate is evaporated, and is obtained
To dendrobium candidum ethanol extract, the content of dendrobine is 8.55t% in dendrobium candidum ethanol extract, by dendrobium candidum ethanol extract
True concentration drying, crushes, and obtains the dendrobine of meal shape.
3rd, the preparation of matrimony vine isoflavones:
By the sub- dries pulverizing of fresh lycium barbarum, fruit of Chinese wolfberry powder is obtained, by fruit of Chinese wolfberry powder 10 times of water of quality of addition
30min is decocted, filtering is concentrated the filtrate in pulpous state, adds ethyl acetate extraction, separates to obtain organic phase, and organic phase is dense
Retract and receive ethyl acetate, obtain Fructus Lycii extractum, Fructus Lycii extractum is dried, crush, obtain powdered matrimony vine isoflavones, its
The content of isoflavones is 50.6t%.
4th, the preparation of anthocyanidin:
By the mashing of fresh purple potato, purple potato slurry is obtained, 5 times of ethanol solutions of the 95wt% of volume are added in being starched to purple potato, filled
Divide and stir, stand to precipitating completely, collection supernatant, concentration is evaporated, and crushes, and obtains the anthocyanidin of meal shape.
5th, the preparation of Abelmoschus Esculentus Linn extract:
By the drying of fresh okra fruit, crush, obtain okra fruit powder, okra fruit powder is added 5 times
30min is boiled in the water boiling of quality, is filtered, and filter residue is added again and carry out boiling in 5 times of water of volume and boil, and is so operated 3 times repeatedly, is received
Collection merges the filtrate obtained by 3 filterings, is concentrated in vacuo and dries at 60 DEG C, obtains Abelmoschus Esculentus Linn extract.
6th, weigh each raw material by said ratio, by each raw material be well mixed it is laggard expect carry out compressing tablet in tablet press machine, produce
Chewable tablet, every 1.5 grams of Single seed weight;Or crushed after each raw material is well mixed, reproduction is filled into capsule in each capsule
Fill 0.8 gram of powder.
The anti-aging effects experiment of the experiment three, preparation containing Tea Polyphenols of the invention
Experimental technique:
Preparation (being control with gavage physiological saline) prepared by 24 monthly age aged mouse gavage embodiment 2 is used, dosage is
0.1 gram/day/only, the gavage time be 15 days, after gavage terminates, test mouse in serum reduction-state level (DPPH methods) and its resist
Fatigue capability (using swimming time as criterion).
Experimental result:
Experiment 5 times is repeated, is averaged, as a result as shown in table 3:
The anti-reduction-state level of serum and anti-fatigue ability (test number (TN) N=5) of the mouse of table 3
Free radical scavenging activity (%) in serum | Swimming time (min) | |
Control group | 36.5±8.3 | 31±5 |
Administration group | 47.5±3.5 | 46±7 |
From table 3 it is observed that after mouse takes said preparation, free radical scavenging activity substantially becomes big in mice serum, shows
The serum reduction-state level of mouse is improved, and mouse swimming time is substantially elongated, shows the anti-fatigue ability enhancing of mouse, can
See, the general health of mouse is significantly improved.It is indicated above that said preparation energy anti-aging, anti-aging.
Experiment four, the enhancing sexual function effect test of the preparation containing Tea Polyphenols of the invention
Use preparation (being control with gavage physiological saline) prepared by 24 monthly ages old-age group's male mice gavage embodiment 2, agent
Measure is 0.1 gram/day/only, gavage 15 days, after gavage terminates, test male mice with female mice in 12 hours mate it is secondary
Number.
Experimental result:
Experiment 20 times is repeated, is averaged, as a result as shown in table 4:
The number of copulations (experiment repeats N=20) of the male mouse of table 4
Ride total degree | |
Control group | 21 |
Administration group | 37 |
Find out as known from Table 4, after male mouse takes said preparation, the number of copulations pole of mouse dramatically increases, it is indicated above that should
Preparation can significantly increase male sexuality.
Embodiment 3
A kind of preparation containing Tea Polyphenols, is prepared from by the raw material of following mass parts:
The preparation method of the above-mentioned preparation containing Tea Polyphenols, its step is:
1st, the preparation of Tea Polyphenols:
By fresh tea leaf drying, crush, obtain tea-leaf power, by tea-leaf power 5 times of boiling water of quality of addition, insulation is soaked
Bubble 30min, filtering adds filter residue in 5 times of boiling water of quality again, so operates 3 times repeatedly, collects obtained by 3 filterings
Filtrate, obtains aqueous extract, and aqueous extract is concentrated in vacuo into 1/3rd volumes at 60 DEG C, obtains concentrate, by concentrate plus
The chloroform for entering the volume of one half is extracted, and separates to obtain water phase, water is mutually concentrated, is dried, and is crushed, and obtains powdered Tea Polyphenols.
2nd, the preparation of Dendrobium officinale polysaccharide
By dendrobium candidum dries pulverizing, dendrobium candidum powder is obtained, decocted during dendrobium candidum powder is added into 3 times of water of quality
30min, filtering, filtrate is evaporated, and obtains dendrobium candidum aqueous extract, and the content of dendrobium polysaccharide is in dendrobium candidum aqueous extract
20.15wt%, dendrobium candidum aqueous extract is crushed, and obtains the Dendrobium officinale polysaccharide of meal shape.
3rd, the preparation of matrimony vine Thick many candies:
By the sub- dries pulverizing of fresh lycium barbarum, fruit of Chinese wolfberry powder is obtained, decocted during fruit of Chinese wolfberry powder is added into 3 times of water of quality
30min is boiled, is filtered, add the ethanol solution of 95wt% to the final concentration of 80wt% of ethanol filter residue, staticly settled 3 hours,
Collection is precipitated and dried, and obtains matrimony vine Thick many candies, and with glucose meter, the content of polysaccharide is 35.5wt% in matrimony vine Thick many candies.
4th, the preparation of anthocyanidin:
By the mashing of fresh purple potato, purple potato slurry is obtained, 10 times of ethanol solutions of the 95wt% of volume are added in being starched to purple potato, filled
Divide and stir, stand to precipitating completely, collection supernatant, concentration is evaporated, and crushes, and obtains the anthocyanidin of meal shape.
5th, the preparation of Abelmoschus Esculentus Linn extract:
By the drying of fresh okra fruit, crush, obtain okra fruit powder, okra fruit powder is added 3 times
30min is boiled in the water boiling of quality, is filtered, and filter residue is added again and carry out boiling in 3 times of water of volume and boil, and is so operated 3 times repeatedly, is received
Collection merges the filtrate obtained by 3 filterings, is concentrated in vacuo and dries at 60 DEG C, obtains Abelmoschus Esculentus Linn extract.
6th, weigh each raw material by said ratio, by each raw material be well mixed it is laggard expect carry out compressing tablet in tablet press machine, produce
Chewable tablet, every 1.5 grams of Single seed weight;Or crushed after each raw material is well mixed, reproduction is filled into capsule in each capsule
Fill 0.8 gram of powder.
The anti-aging effects experiment of the experiment five, preparation containing Tea Polyphenols of the invention
Experimental technique:
Preparation (being control with gavage physiological saline) prepared by 24 monthly age aged mouse gavage embodiment 3 is used, dosage is
0.1 gram/day/only, the gavage time be 15 days, after gavage terminates, test mouse in serum reduction-state level (DPPH methods) and its resist
Fatigue capability (using swimming time as criterion).
Experimental result:
Experiment 5 times is repeated, is averaged, as a result as shown in table 5:
The anti-reduction-state level of serum and anti-fatigue ability (test number (TN) N=5) of the mouse of table 5
Free radical scavenging activity (%) in serum | Swimming time (min) | |
Control group | 35.5±5.1 | 31±8 |
Administration group | 48.5±5.5 | 44±11 |
As can be seen from Table 5, after mouse takes said preparation, free radical scavenging activity substantially becomes big in mice serum, shows
The serum reduction-state level of mouse is improved, and mouse swimming time is substantially elongated, shows the anti-fatigue ability enhancing of mouse, can
See, the general health of mouse is significantly improved.It is indicated above that said preparation energy anti-aging, anti-aging.
Experiment six, the enhancing sexual function effect test of the preparation containing Tea Polyphenols of the invention
Use preparation (being control with gavage physiological saline) prepared by 24 monthly ages old-age group's male mice gavage embodiment 3, agent
Measure is 0.1 gram/day/only, gavage 15 days, after gavage terminates, test male mice with female mice in 12 hours mate it is secondary
Number.
Experimental result:
Experiment 20 times is repeated, is averaged, as a result as shown in table 6:
The number of copulations (experiment repeats N=20) of the male mouse of table 6
Ride total degree | |
Control group | 18 |
Administration group | 31 |
Find out as known from Table 6, after male mouse takes said preparation, the number of copulations pole of mouse dramatically increases, it is indicated above that should
Preparation can significantly increase male sexuality.
Claims (10)
1. a kind of preparation containing tea polyphenol preparation, it is characterised in that be prepared from by the raw material of following mass parts:
2. the preparation containing Tea Polyphenols according to claim 1, it is characterised in that:Described dendrobium candidum extract is iron sheet
Dendrobium polysaccharide or dendrobine, described wolfberry fruit extract is matrimony vine isoflavones or matrimony vine Thick many candies, when dendrobium candidum extract is
During Dendrobium officinale polysaccharide, wolfberry fruit extract is matrimony vine Thick many candies, and when dendrobium candidum extract is dendrobine, wolfberry fruit extract is
Matrimony vine isoflavones.
3. the preparation containing Tea Polyphenols according to claim 2, it is characterised in that described Tea Polyphenols is prepared by following methods
Form:
By fresh tea leaf drying, crush, obtain tea-leaf power, by tea-leaf power add the 3-5 times of boiling water of quality in, heat-insulation soaking
20-40 minutes, filtering added filter residue in the 3-5 times of boiling water of quality again, so operates 2-3 times repeatedly, collects and combines every time
Filtrate obtained by filtering, obtains aqueous extract, adds chloroform to be extracted after aqueous extract is concentrated, and water phase is separated to obtain, by water phase
Concentration, drying, crush, and obtain powdered Tea Polyphenols.
4. the preparation containing Tea Polyphenols according to claim 2, it is characterised in that described dendrobium candidum extract is iron sheet
During dendrobium polysaccharide, Dendrobium officinale polysaccharide is prepared from by following methods:
By dendrobium candidum dries pulverizing, dendrobium candidum powder is obtained, decocted during dendrobium candidum powder is added into the 3-5 times of water of quality
Boil, filtered after the completion of decoction, filtrate is evaporated, obtain dendrobium candidum aqueous extract, dendrobium candidum aqueous extract is crushed, obtain meal
The Dendrobium officinale polysaccharide of shape.
5. the preparation containing Tea Polyphenols according to claim 2, it is characterised in that described dendrobium candidum extract is the stem of noble dendrobium
During alkali, dendrobine is prepared from by following methods:
By dendrobium candidum dries pulverizing, dendrobium candidum powder is obtained, decocted during dendrobium candidum powder is added into the 3-5 times of water of quality
Boil, filtered after the completion of decoction, boiled boiling is carried out in the filter residue 3-5 times of ethanol solution of more than the 95wt% of quality of addition, boiling has been boiled
Into rear filtering, filtrate is evaporated, obtains dendrobium candidum ethanol extract, dendrobium candidum ethanol extract is really concentrated into drying, crushed, obtained
To the dendrobine of meal shape.
6. the preparation containing Tea Polyphenols according to claim 2, it is characterised in that described wolfberry fruit extract is the different Huang of matrimony vine
During ketone, matrimony vine isoflavones is prepared from by following methods:
By fresh fruit of Chinese wolfberry dries pulverizing, fruit of Chinese wolfberry powder is obtained, decocted during fruit of Chinese wolfberry powder is added into the 3-10 times of water of quality
Boil, filtered after the completion of decoction, concentrate the filtrate in pulpous state, add ethyl acetate extraction, organic phase is separated to obtain, by organic phase
Concentration and recovery ethyl acetate, obtains Fructus Lycii extractum, and Fructus Lycii extractum is dried, and crushes, and obtains powdered matrimony vine isoflavones.
7. the preparation containing Tea Polyphenols according to claim 2, it is characterised in that described wolfberry fruit extract is different thick matrimony vine
During polysaccharide, the different Thick many candies of Qi are prepared from by following methods:
By fresh fruit of Chinese wolfberry dries pulverizing, fruit of Chinese wolfberry powder is obtained, decocted during fruit of Chinese wolfberry powder is added into the 3-10 times of water of quality
Boil, filtered after the completion of decoction, filter residue is added into the ethanol solution of 95wt%-100wt%- to the final concentration of 75wt%- of ethanol
85wt%, is stood to precipitating completely, and collection is precipitated and dried, and obtains matrimony vine Thick many candies.
8. the preparation containing Tea Polyphenols according to claim 2, it is characterised in that described anthocyanidin is prepared by following methods
Form:
By the mashing of fresh purple potato, purple potato slurry is obtained, the 5-10 times of ethanol solution of more than the 95wt% of volume is added in being starched to purple potato,
Stir, stand, collection supernatant complete to precipitating, be concentrated to dryness, crush, obtain the anthocyanidin of meal shape.
9. the preparation containing Tea Polyphenols according to claim 2, it is characterised in that described Abelmoschus Esculentus Linn extract is by with lower section
Method is prepared from:
By the drying of fresh okra fruit, crush, obtain okra fruit powder, okra fruit powder is added into 3-5 times of matter
The water of amount carries out boiling and boils, and boiling is filtered after the completion of boiling, and filter residue is added again and carry out boiling in the 3-5 times of water of volume and boil, so repeatedly
Operation 2-3 times, collects and combines the filtrate every time obtained by filtering, concentrates and dries, and obtains Abelmoschus Esculentus Linn extract.
10. the preparation containing Tea Polyphenols according to claim 2, it is characterised in that:The described preparation containing Tea Polyphenols is piece
Agent or capsule, described glidant is magnesium stearate, and sweetener is stevioside.
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Cited By (1)
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CN108524921A (en) * | 2018-03-30 | 2018-09-14 | 广西中医药大学 | A kind of antiradiation injury protective agent and its preparation method and application |
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