CN106821908A - Makeup-removing wet tissue and its compound method with moisture-keeping function - Google Patents
Makeup-removing wet tissue and its compound method with moisture-keeping function Download PDFInfo
- Publication number
- CN106821908A CN106821908A CN201710081883.7A CN201710081883A CN106821908A CN 106821908 A CN106821908 A CN 106821908A CN 201710081883 A CN201710081883 A CN 201710081883A CN 106821908 A CN106821908 A CN 106821908A
- Authority
- CN
- China
- Prior art keywords
- makeup
- wet tissue
- peg
- moisture
- keeping function
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
Abstract
The present invention relates to a kind of makeup-removing wet tissue with moisture-keeping function and preparation method thereof, the present invention is by by the caprylic/capric triglycerides of PEG 6, the iso stearic acid of glycerine ester of PEG 20 and the glyceride of 3 PEG/PPG of polytetramethylene glycol 8/5 etc. are by PEG modified grease, with water soluble humectants, polyalcohol, preservative is engaged, it is especially added with pulullan, dipotassium glycyrrhizinate, aloe barbadensis Miller leaf juice and HERBA DENDROBII stem extraction, the active skull cap components such as Echinacea angustifolia extract, certain grammes per square metre and the spunlace non-woven cloth of weaving ratio is coordinated to be made the makeup-removing wet tissue with moisture-keeping function, with outstanding makeup removing ability, it is simultaneously free of a burden using skin sense, it is salubrious using rear skin moisturizing.Tested and estimation of stability by carrying out makeup removing ability, moisture-retaining capacity to formulation product and commercial like product, as a result show that makeup-removing wet tissue of the present invention has ideal moistening effect, while cleaning capacity is also superior to commercially available makeup removal products.
Description
Technical field
The present invention relates to a kind of makeup-removing wet tissue with moisture-keeping function and its compound method.
Background technology
With the development of cosmetic art, cosmetics play more and more important effect in daily life.
But after face is made up, if removing is not thorough, the cosmetics of residual can cause the pore of skin of face to block, and cause skin oil
Fat water oil dyssecretosis, so as to cause acne, acne and blackhead etc. to make us the skin problem of puzzlement.Meanwhile, the residual of cosmetics
Injury to skin is very big, if can not clean out in time, can form tumour with the breathing of pore, into hair follicle
Problem, is just difficult to clear up away again in long-term existence and skin surface, so, the makeup removing link of skin is particularly significant.Meanwhile, by
While makeup removal products during makeup removing remove face cosmetic, can also have protective effect and water-oil flat skin surface
The sebum that weighing apparatus is acted on is taken away in the lump, therefore often also easily occurs facial dry, tight situation after thorough makeup removing, and this is also right
The performance of keeping humidity of makeup removal products proposes further requirement.
Most of color make-up used in everyday, such as lipstick, lip gloss, eye shadow, rouge, muffin, eyeliner, mascara are all powder
The mixture of body, pigment and grease.Usual color make-up needs to have the maintenance daylong ability of dressing, therefore most of formula can add
Oiling insoluble film former.Oil-soluble film forming agent is water insoluble, such as same layer oiliness diaphragm, and sweat can be avoided to wash color make-up
It is de-, reach and the color make-up of skin surface is kept into more lasting purpose.The common mildy wash based on surfactant is water
Dissolubility system, dry paint cannot be washed away just as common liquid detergent, because water miscible mildy wash cannot dissolve oil soluble
Property film forming agent so that cannot be clean by color make-up cleaning.When thorough removal color make-up is needed, it usually needs produced using special makeup removing
Product, in numerous makeup removal products, makeup remover is most common makeup removal products, can by " oil-oily compatibility principle " easily with face
On the fusion of color make-up greasy dirt, then by way of water emulsification, dirt on the face can completely be taken away during flushing, to reach makeup removing mesh
's.
But makeup remover is due to its characteristic trait, often there is also it is inconvenient to carry, must arrange in pairs or groups makeup removing cotton use, skin sense oil
Greasy the shortcomings of, meanwhile, if face has moisture before makeup removing, the makeup removing effect to makeup remover can also have a great impact.Consumption
Person outside cleaning capacity, also has in terms of the selection of makeup removal products to aspects such as portability, moistening effect and wet water makeup removings
It is required.Makeup-removing wet tissue can thoroughly remove ornaments and formal dress as a portable, convenient product in the state of facial wet water, in makeup removing
Product market share one seat.Makeup-removing wet tissue on the market is mostly using oil-water emulsification by the way of at present, or directly use is unloaded
Adornment oil immersion profit non-woven fabrics is made, and skin sense is more greasy when using, it is limited in one's ability to remove ornaments and formal dress, and excitant is also larger, and product stability is poor, this
Outward, consumer is also more paid close attention to the moistening effect of skin cleaning type product in recent years, and makeup removal products are used as based on grease
Medium is removed in adornment face, and skin surface sebum forfeiture is easily caused during makeup removing, dry skin is caused, so as to cause skin
The consequences such as natural cover for defense destruction, skin water-oil balance destruction, therefore, the moistening effect of makeup removal products is particularly natural to skin
The protection of barrier and the holding of the rear moisture of skin of use are also particularly important for a makeup removal products.
The content of the invention
It is an object of the invention to provide a kind of makeup-removing wet tissue with moisture-keeping function and preparation method thereof, the present invention is provided
Makeup-removing wet tissue the characteristics of there is strong, easy to use makeup removing ability, low irritant, skin sense salubrious non-greasy, and with certain
Moisture-keeping function, after use skin there is more preferable water holding capacity.To achieve the above objectives, the technical solution adopted by the present invention
It is：
A kind of makeup-removing wet tissue with moisture-keeping function, it is characterised in that wet tissue liquid by weight percentage, including such as the following group
The raw material for dividing is made：Water 20-80%, PEG-6 caprylic/capric triglyceride 1-10%, PEG-20 iso stearic acid of glycerine ester 0.1-
7%th, polytetramethylene glycol -3PEG/PPG-8/5 glyceride 1-10%, pulullan polysaccharide 0.1-10%, aloe barbadensis Miller leaf juice 1-
60%th, polyalcohol 2-25%, NMF 0.5-15%, dipotassium glycyrrhizinate 0.01-2.0%, plant extracts 0.01-10%, anti-
Rotten agent 0.05-2%, above each component percentage composition sum is 100%.
Preferably, the makeup-removing wet tissue with moisture-keeping function, wet tissue liquid by weight percentage, including following component
Raw material is made：It is water 20-80%, PEG-6 caprylic/capric triglyceride 1-8%, PEG-20 iso stearic acid of glycerine ester 0.2-5%, poly-
Butanediol -3PEG/PPG-8/5 glyceride 1-8%, pulullan polysaccharide 0.1-8%, aloe barbadensis Miller leaf juice 1-40%, polyalcohol
2-20%, NMF 0.5-15%, dipotassium glycyrrhizinate 0.01-2.0%, plant extracts 0.01-10%, preservative 0.05-
2%, above each component percentage composition sum is 100%.
Preferably, the makeup-removing wet tissue with moisture-keeping function, wet tissue liquid by weight percentage, including following component
Raw material is made：It is water 20-80%, PEG-6 caprylic/capric triglyceride 1-5%, PEG-20 iso stearic acid of glycerine ester 0.3-4%, poly-
Butanediol -3PEG/PPG-8/5 glyceride 1-5%, pulullan polysaccharide 0.1-5%, aloe barbadensis Miller leaf juice 1-20%, polyalcohol
2-15%, NMF 0.5-15%, dipotassium glycyrrhizinate 0.01-2.0%, plant extracts 0.01-10%, preservative 0.05-
2%, above each component percentage composition sum is 100%.
Preferably, the polyalcohol is that one or more cooperation in the polyalcohol such as glycerine, propane diols, butanediol is formed.
Preferably, the NMF is glycine betaine, trehalose, allantoin, hyaluronic acid, hydrogenated starch hydrolysate, pyrroles
One or more cooperation in the NMFs such as alkanone carboxylic acid sodium, ethoxy urea is formed.
Preferably, the plant extracts is extracted by HERBA DENDROBII stem extraction, aloe barbadensis Miller leaf extract, radix sophorae
One or more cooperation in thing, lycium barbarum berry extract, Echinacea angustifolia extract, flores sambuci extract is formed.
Preferably, the preservative is in Phenoxyethanol, Sensiva SC50, potassium sorbate or parabens preservative
One or more cooperation form.
Preferably, the makeup-removing wet tissue material is spunlace non-woven cloth, wherein gluing fibre ratio for 30-60%, terylene ratio are
30-60% , Mei ㎡ cloth weight 40-55g.
The present invention additionally provides a kind of preparation method of the makeup-removing wet tissue with moisture-keeping function simultaneously, comprises the following steps：
(1) parabens is dissolved in the water at 70 DEG C.
(2) trehalose, allantoin, hyaluronic acid in pulullan polysaccharide and NMF etc. is weighed by weight percentage to have
There is the raw material of swelling property, with disperse polyol, be added to the water afterwards.
(3) raw material in step (1) is mixed at 20-45 DEG C and is sufficiently stirred for, until the liquid of stable homogeneous is formed, then
The soluble solid constituents in dipotassium glycyrrhizinate, NMF and plant extracts are added, with the stirring of 400r/min speed up to it
It is completely dissolved.
(4) PEG-6 caprylic/capric triglycerides, PEG-20 iso stearic acid of glycerine ester, polytetramethylene glycol -3PEG/ are separately added into
PPG-8/5 glyceride, aloe barbadensis Miller leaf juice, remaining NMF, remaining vegetable extract, preservative, each raw material have been added
5-10min is stirred after finishing, until system is homogeneous, is all added and is continued to stir 30min after finishing, then stand 3-8h, crossed and filter
Remove bottom precipitation.
(5) the wet tissue liquid for adding above-mentioned steps to prepare in wet tissue filling apparatus are automated, it is filling using automation wet tissue
Uniformly be sprayed on spunlace non-woven cloth wet tissue liquid by equipment, then is made wet tissue by operations such as cutting, folding, encapsulation.
In above-mentioned technical proposal of the invention, PEG-6 caprylic/capric triglycerides, PEG-20 iso stearic acid of glycerine ester
And polytetramethylene glycol -3PEG/PPG-8/5 glyceride is that, by PEG modified grease, above-mentioned grease is modified by PEG, tool
Have hydrophilic radical, as can in water phase stable existence grease, have the effect of surfactant concurrently.Added in water phase
PEG-6 caprylic/capric triglycerides, PEG-20 iso stearic acid of glycerine ester and polytetramethylene glycol -3PEG/PPG-8/5 glyceride, can be with
Make makeup removal products water miscible simultaneously in guarantee, adornment face that also can be well with oil/silicone oil system is combined, and it is together dissolved in
In water phase, the purpose of makeup removing is reached.Simultaneously as by modified, containing PEG-6 caprylic/capric triglycerides, PEG-20 glycerine
The aqueous makeup removal products of isostearate and polytetramethylene glycol -3PEG/PPG-8/5 glyceride and O/W, W/O emulsifying makeup removal products
Compare, makeup removing ability is stronger, more gentle, and does not have the greasy skin sense of emulsifying makeup removal products.Additionally, water-soluble grease
Addition, the emulsifying makeup removal products for also making product more traditional in terms of performance of keeping humidity and stability are even better.
Pulullan polysaccharide is called pullulan, because its straight-chain polysaccharide structure in cosmetics by as film forming agent, protect
Humectant is added, and pulullan polysaccharide is added in makeup-removing wet tissue liquid of the invention, can while makeup removing skin surface it is rapid into
Film, other moisturizing ingredients in attachment system, makes NMF stay in skin surface after makeup removing, reaches the effect of long-acting moisturizing, together
When, itself also there is certain performance of keeping humidity, and system can be helped to improve stability.
Aloe barbadensis Miller (AloeBarbadensis) is nowadays widely used in cosmetic material, traditional Curacao
Aloe extract be mostly by aloe barbadensis Miller leaf juice carry out it is lyophilized form, being added in cosmetics has the work(such as moisturizing, anti-inflammatory
Effect, but due to freeze-drying process some trace elements and active component in aloe barbadensis Miller leaf juice can lose, and it is of the invention
Aloe barbadensis Miller (AloeBarbadensis) leaf juice is then that the method by naturally squeezing obtains sterling Aloe Barbadensis Miller
Juice, then by purify method labile element therein is removed, the aloe barbadensis Miller leaf juice for finally giving had concurrently moisturizing,
The effects such as anti-inflammatory and reparation, releive, reduce excitant etc. effect.
Dipotassium glycyrrhizinate is the material extracted with natural radix glycyrrhizae taste raw material, there is the effects such as anti-inflammatory, antiallergy, moisturizing.Changing
It is widely used as agent of releiving in cosmetic, can effectively reduces the excitant of cosmetics.
The present invention is with PEG-6 caprylic/capric triglycerides, PEG-20 iso stearic acid of glycerine ester and polytetramethylene glycol -3PEG/
The water-soluble grease of PPG-8/5 glyceride be system, coordinate pulullan, aloe barbadensis Miller (AloeBarbadensis) leaf juice,
Dipotassium glycyrrhizinate, polyalcohol, NMF, plant extracts, the use of preservative, are carrier, makeup removing effect by spunlace non-woven cloth
It is really excellent, while having low irritant, good skin sense, stability higher and excellent moistening effect, nutrition concurrently moistens flesh
The features such as skin.
In the inventive solutions, polyalcohol is glycerine, propane diols, butanediol, be mainly used to aid in dissolving adornment face,
Auxiliary moisturizing and the dispersion indissoluble raw material in preparation process.
In the inventive solutions, NMF is glycine betaine, trehalose, allantoin, hyaluronic acid, hydrogenated starch water
Solution thing, pyrrolidone sodium carboxylate, ethoxy urea, its adding method respectively according to its property, by the way that polyalcohol is swelling, direct addition
Method addition system in.
In some embodiments of the invention, plant extracts is extracted by HERBA DENDROBII (Dendrobium Nobile) stem
Thing, aloe barbadensis Miller (Aloe Barbadensis) leaf extract, kuh-seng (Sophora Flavescens) root extract, Ningxia
Matrimony vine (Lycium Barbarum) berry extract, purple coneflower (Echinacea Purpurea) extract, flores sambuci are extracted
Coordinate in thing and form.
The makeup-removing wet tissue that the present invention is provided brings salubrious skin different with existing product sense while makeup removing, wipes
Being rinsed with clear water afterwards can thoroughly clean face, and makeup removing rear face skin refreshing moistens, and noresidue is non-stimulated, easy to use, and
And can remove adornment face in the case where skin surface has moisture, it is adapted to various skin quality particularly dryness, oily skin and unloads
Adornment.
Brief description of the drawings
Fig. 1 is four kinds of score value criterion legends in subject's makeup removing effect contrast test, wherein " 10 " are divided into adornment face base
This removing, noresidue or only remains a small amount of adornment face；" 7 " are divided into adornment face and distinguish and remove, it is seen that pattern is substantially thin out；" 4 " are divided into
Adornment face only has part removing, and pattern is slightly thin out；" 0 " is divided into adornment face and does not remove, and pattern remains unchanged clearly.
Fig. 2 is the result of subject's makeup removing effect contrast test, and its center pillar 1 shows with the makeup-removing wet tissue of formula 3 in embodiment 1
It is sample detection result (24 groups of average value of numerical value) that post 2 shows (24 groups of the testing result with commercially available control makeup-removing wet tissue as sample
The average value of numerical value).
Fig. 3 is the result of subject's moistening effect contrast test, wherein, group 1 is shown wet with the makeup removing of formula 3 in embodiment 1
Towel increases ratio average (24 groups of average value of numerical value) using the percutaneous water loss speed of rear 10min, 30min, organizes 2 Shi Yi cities
Sell control sample and use percutaneous water loss speed increase ratio average (24 groups of average value of numerical value) of rear 10min, 30min.
Fig. 4 is makeup-removing wet tissue aqueous solution pH result of variations under different storage requirements, is displayed in during study on the stability and matches somebody with somebody
The makeup-removing wet tissue sample pH value change of side 3.
Specific embodiment
The following examples can make those skilled in the art that the present invention is more completely understood, but limit never in any form
The present invention.
The instrument that the present invention is used is all common commercially available product, can all be bought in market.
With reference to embodiment, the present invention is expanded on further：
Embodiment 1：The preparation of makeup-removing wet tissue
Formula such as table 1：
The makeup-removing wet tissue formula of table 1
| Formula 1 | Formula 2 | Formula 3 | Formula 4 | |
| Water | 40 | 52 | 71 | 68 |
| PEG-6 caprylic/capric triglycerides | 4 | 1 | 3 | 2 |
| PEG-20 iso stearic acid of glycerine ester | 0.5 | 3 | 0.2 | 2 |
| Polytetramethylene glycol -3PEG/PPG-8/5 glyceride | 9 | 6 | 3 | 1 |
| Glycerine | 2 | 1 | 2 | 4 |
| 1,3 propane diols | 10 | 7.5 | 5 | 9 |
| Pulullan polysaccharide | 1 | 0.1 | 0.4 | 2 |
| Aloe barbadensis Miller (AloeBarbadensis) leaf juice | 22 | 26 | 4 | 5 |
| Dipotassium glycyrrhizinate | 0.02 | 0.02 | 0.05 | 0.02 |
| Glycine betaine | 1 | 1 | 4 | 0.2 |
| Trehalose | 3 | 0 | 1 | 0 |
| Allantoin | 2 | 0 | 0.5 | 1 |
| Ethoxy urea | 3 | 0.5 | 2 | 2 |
| Glycosyl trehalose, hydrogenated starch hydrolysate | 1 | 0 | 1 | 1 |
| Pyrrolidone sodium carboxylate | 0.5 | 0.5 | 0.5 | 0.5 |
| HERBA DENDROBII (Dendrobium Nobile) stem extraction | 0.1 | 0.1 | 0.1 | 0.1 |
| Aloe barbadensis Miller (Aloe Barbadensis) leaf extract | 0 | 0.1 | 0.3 | 0.4 |
| Kuh-seng (Sophora Flavescens) root extract | 0.2 | 0 | 0.2 | 0.2 |
| Lycium barbarum (Lycium Barbarum) berry extract | 0.08 | 0.23 | 0.3 | 0.4 |
| Purple coneflower (Echinacea Purpurea) extract | 0 | 0.1 | 0.5 | 0.2 |
| Flores sambuci extract | 0.15 | 0.4 | 0.5 | 0.53 |
| Methyl hydroxybenzoate | 0.1 | 0.1 | 0.1 | 0.1 |
| Phenoxyethanol | 0.3 | 0.3 | 0.3 | 0.3 |
| Sensiva SC50 | 0.5 | 0.5 | 0.5 | 0.5 |
Operating procedure is as follows：
(1) parabens is dissolved in the water at 70 DEG C.
(2) trehalose, allantoin, hyaluronic acid in pulullan polysaccharide and NMF etc. is weighed by weight percentage to have
There is the raw material of swelling property, with disperse polyol, be added to the water afterwards.
(3) raw material in step (1) is mixed at 25 DEG C and is sufficiently stirred for, until forming the liquid of stable homogeneous, Ran Houjia
Enter the soluble solid constituents in dipotassium glycyrrhizinate, NMF and plant extracts, with the stirring of 400r/min speed until its is complete
CL.
(4) PEG-6 caprylic/capric triglycerides, PEG-20 iso stearic acid of glycerine ester, polytetramethylene glycol -3PEG/ are separately added into
PPG-8/5 glyceride, aloe barbadensis Miller (AloeBarbadensis) leaf juice, remaining NMF, remaining vegetable extract, anti-corrosion
Agent, each raw material is added after finishing and stirs 5-10min, until system is homogeneous, is all added and is continued to stir 30min after finishing, so
After stand 4.5h, be filtered to remove bottom precipitation.
(5) the wet tissue liquid for adding above-mentioned steps to prepare in wet tissue filling apparatus are automated, it is filling using automation wet tissue
Uniformly be sprayed on spunlace non-woven cloth wet tissue liquid by equipment, then is made wet tissue by operations such as cutting, folding, encapsulation.
Embodiment 2：Makeup removing effect contrast test
1. test principle：First using color make-up (eyeliner) in skin surface picture case, afterwards respectively using of the present invention
Makeup-removing wet tissue and control makeup-removing wet tissue remove pattern, and makeup removing effect is evaluated according to the situation of removing.
2. testing program：Human test's scheme, 24 volunteers select 20 × 20mm regions picture frame in forearm, and in frame
With waterproof informer's stroke smiling face's pattern, wait 5min adornment face is fully merged with skin, use makeup removing of the present invention respectively afterwards
Wet tissue and control makeup-removing wet tissue wipe smiling face's pattern 15 times in respective frame respectively with identical dynamics, then with warm water washing, clap afterwards
According to and record adornment face remove situation, elimination effect is evaluated with following standard (Fig. 1 is four kinds of evaluation result legends)：
“10”：Adornment face is removed substantially, noresidue or only remains a small amount of adornment face；
“7”：Adornment face is distinguished and removed, it is seen that pattern is substantially thin out；
“4”：Adornment face only has part removing, and pattern is slightly thin out；
“0”：Adornment face is not removed, and pattern remains unchanged clearly.
3. result of the test：Test result is analyzed, as a result as shown in table 2, Fig. 2.Wherein, post 1 shows and unloaded with being formulated 3
Adornment wet tissue is sample detection result (24 groups of average value of numerical value), and post 2 shows the detection knot with commercially available control makeup-removing wet tissue as sample
Really (24 groups of average value of numerical value)
The makeup removing effect comparative test result of table 2
4. result shows that makeup-removing wet tissue of the present invention is compared with makeup-removing wet tissue is compareed, and the cleaning effect to adornment face is stronger,
Cleaning to adornment face is more thorough.
5. this experiment, using waterproof eyeliner as cleaning object, is because black waterproof eyeliner is various color make-up products
The maximum product of middle cleaning difficulty, in case water eyeliner is cleaning object, can contrast unloading for different product with more obvious
Adornment capacity variance.
Embodiment 3：Moistening effect contrast test
1. test principle：Skin surface moisture situation first is detected using mp-580 skin detections instrument, afterwards respectively using this
Invent the makeup-removing wet tissue and compare commercially available makeup-removing wet tissue cleaning skin, and respectively at detecting skin after 10min, 30min again
Surface moisture situation.
2. testing program：Human test's scheme, 24 volunteers select 20 × 20mm regions picture frame in forearm, use mp-
580 skin detection instrument detect skin surface moisture situation, (are formulated in embodiment 1 with makeup-removing wet tissue of the present invention respectively afterwards
3) with the commercially available cosmetic wet tissue of reference substance, region 15 times in respective frame are wiped with identical dynamics respectively, then with warm water washing, Zhi Houfen
Not in detecting skin surface moisture situation after 10min, 30min again.
3. result of the test：Test result is analyzed, as a result as shown in table 3, Fig. 3.Wherein, group 1 is shown with embodiment 1
The makeup-removing wet tissue of formula 3 for the percutaneous water loss speed of sample 10min, 30min increase ratio average (24 groups of numerical value it is average
Value), group 2 is shown to compare commercially available makeup-removing wet tissue increases ratio average (24 as the percutaneous water loss speed of sample 10min, 30min
The average value of group numerical value), calculated according to below equation：
The moistening effect comparative test result of table 3 (percutaneous water loss speed)
4. result shows that after being removed ornaments and formal dress using makeup-removing wet tissue, due to the forfeiture of skin surface sebum, skin surface is through the severe edema due to hypofunction of the spleen
Dividing bleed rate can increased, but contrast commercially available prod makeup-removing wet tissue, and makeup-removing wet tissue of the present invention after use, can be effective
The incrementss of the percutaneous water loss speed of skin surface are reduced, shows that there is makeup-removing wet tissue of the present invention good moisturizing to imitate
Really.
Embodiment 4：Sample Storage stability test
1. test principle
In aqueous phase solution, whether pH changes in main reflection system irreversible metamorphic reaction, by periodic detection
Under different condition place makeup-removing wet tissue solution ph, add to outward appearance, color, smell evaluation, can embody sample storage
Quality comparison during Tibetan, thus judges its storage-stable.
2. test method
Outward appearance, the evaluation method of color check whether sample the feelings such as layering, muddy, precipitation, discoloration occurs directly to estimate
Condition；The evaluation method of smell checks whether sample spoiled situation occurs directly to smell survey；The measure of pH is complete by electronics pH meter
Into.Determine before first with standard liquid calibrate, afterwards in beaker add 60ml deionized waters, be put into a makeup-removing wet tissue, with do
Net haemostatic clamp is rinsed 15 times, squeezes the water out discard afterwards, is put into second makeup-removing wet tissue, repeats step, afterwards electricity consumption before this
Sub- pH meter determines solution ph, and each sample carries out 2 replications.Study on the stability condition be 45 DEG C, 40 DEG C, 5 DEG C, -16
DEG C, circulating temperature (40, -10 DEG C), normal temperature, 7 conditions of illumination, probation is respectively：45 DEG C, -16 DEG C is 1 month, is surveyed weekly
Once；40 DEG C, 5 DEG C, normal temperature, illumination be 3 months, first month to survey weekly once, latter two moon for survey in two weeks once；Follow
(40, -10 DEG C) of ring temperature is 12 circulations, and each condition circulation phase is 2 days (48h).
3. experimental result
As shown in table 4, Fig. 4, after probation terminates, formula 3 is under each storage requirement, and its outward appearance, smell, color are equal
There is not ANOMALOUS VARIATIONS, each group of pH value is stable between 6.2-7.2, each condition group pH also stablizes under long-term storage
Between 6.2-6.8, change of pH does not interfere with product quality in the range of this, shows within the shelf-life, of the present invention to unload
Adornment wet tissue stability is preferable.
The makeup-removing wet tissue of table 4 is formulated 3 study on the stability results
The above is only concrete application example of the invention, protection scope of the present invention is not limited in any way.All uses
Equivalents or equivalence replacement and the technical scheme that is formed, all fall within rights protection scope of the present invention.
Claims (9)
1. a kind of makeup-removing wet tissue with moisture-keeping function, it is characterised in that wet tissue liquid by weight percentage, including following component
Raw material be made：Water 20-80%, PEG-6 caprylic/capric triglyceride 1-10%, PEG-20 iso stearic acid of glycerine ester 0.1-7%,
It is the PEG/PPG-8/5 glyceride of polytetramethylene glycol -3 1-10%, pulullan polysaccharide 0.1-10%, aloe barbadensis Miller leaf juice 1-60%, polynary
Alcohol 2-25%, NMF 0.5-15%, dipotassium glycyrrhizinate 0.01-2.0%, plant extracts 0.01-10% and preservative 0.05-2%,
Above each component percentage composition sum is 100%.
2. there is the makeup-removing wet tissue of moisture-keeping function according to claim 1, it is characterised in that wet tissue liquid is by weight percentage
Meter, including the raw material of following component is made：Water 20-80%, PEG-6 caprylic/capric triglyceride 1-8%, PEG-20 glycerine is different hard
Resin acid ester 0.2-5%, the PEG/PPG-8/5 glyceride of polytetramethylene glycol -3 1-8%, pulullan polysaccharide 0.1-8%, aloe barbadensis Miller leaf juice
1-40%, polyalcohol 2-20%, NMF 0.5-15%, dipotassium glycyrrhizinate 0.01-2.0%, plant extracts 0.01-10% and anti-corrosion
Agent 0.05-2%, above each component percentage composition sum is 100%.
3. there is the makeup-removing wet tissue of moisture-keeping function according to claim 1, it is characterised in that wet tissue liquid is by weight percentage
Meter, including the raw material of following component is made：Water 20-80%, PEG-6 caprylic/capric triglyceride 1-5%, PEG-20 glycerine is different hard
Resin acid ester 0.3-4%, the PEG/PPG-8/5 glyceride of polytetramethylene glycol -3 1-5%, pulullan polysaccharide 0.1-5%, aloe barbadensis Miller leaf juice
1-20%, polyalcohol 2-15%, NMF 0.5-15%, dipotassium glycyrrhizinate 0.01-2.0%, plant extracts 0.01-10% and anti-corrosion
Agent 0.05-2%, above each component percentage composition sum is 100%.
4. the makeup-removing wet tissue with moisture-keeping function according to any in claim 1-3, it is characterised in that the polyalcohol is
One or more cooperation in the polyalcohols such as glycerine, propane diols or butanediol is formed.
5. the makeup-removing wet tissue with moisture-keeping function according to any in claim 1-3, it is characterised in that the NMF is
In glycine betaine, trehalose, allantoin, hyaluronic acid, hydrogenated starch hydrolysate, pyrrolidone sodium carboxylate or ethoxy urea NMF
One or more cooperation form.
6. there is the makeup-removing wet tissue of moisture-keeping function according to any in claim 1-3, it is characterised in that the plant extract
Thing is by HERBA DENDROBII stem extraction, aloe barbadensis Miller leaf extract, kuh-seng root extract, lycium barbarum berry extract, purple pine nut
One or more cooperation in chrysanthemum extract or flores sambuci extract is formed.
7. the makeup-removing wet tissue with moisture-keeping function according to any in claim 1-3, it is characterised in that the preservative is
One or more cooperation in Phenoxyethanol, Sensiva SC50, potassium sorbate or parabens preservative is formed.
8. there is the makeup-removing wet tissue of moisture-keeping function according to any in claim 1-3, it is characterised in that the makeup-removing wet tissue
Material is spunlace non-woven cloth, wherein gluing fibre ratio for 30-60%, terylene ratio are 30-60% , Mei ㎡ cloth weight 40-55g.
9. there is the preparation method of the makeup-removing wet tissue of moisture-keeping function as described in any in a kind of 1-3 such as claim, it is characterised in that
Comprise the following steps：
（1）Parabens is dissolved in the water at 70 DEG C；
（2）Weigh by weight percentage trehalose, allantoin, hyaluronic acid in pulullan polysaccharide and NMF etc. have it is molten
The raw material of swollen property, with disperse polyol, is added to the water afterwards；
（3）By step at 20-45 DEG C（1）Middle raw material mixing is sufficiently stirred for, until forming the liquid of stable homogeneous, is subsequently adding
Soluble solid constituents in dipotassium glycyrrhizinate, NMF and plant extracts, with the stirring of 400r/min speed until its is complete
Dissolving；
（4）It is separately added into PEG-6 caprylic/capric triglycerides, PEG-20 iso stearic acid of glycerine ester, the PEG/ of polytetramethylene glycol -3
PPG-8/5 glyceride, aloe barbadensis Miller leaf juice, remaining NMF, remaining vegetable extract, preservative, each raw material have been added
5-10min is stirred after finishing, until system is homogeneous, is all added and is continued to stir 30min after finishing, then stand 3-8h, crossed and filter
Remove bottom precipitation；
（5）The wet tissue liquid for adding above-mentioned steps to prepare in wet tissue filling apparatus are automated, uses automation wet tissue filling apparatus
Wet tissue liquid is uniformly sprayed on spunlace non-woven cloth, then wet tissue is made by operations such as cutting, folding, encapsulation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710081883.7A CN106821908A (en) | 2017-02-15 | 2017-02-15 | Makeup-removing wet tissue and its compound method with moisture-keeping function |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710081883.7A CN106821908A (en) | 2017-02-15 | 2017-02-15 | Makeup-removing wet tissue and its compound method with moisture-keeping function |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106821908A true CN106821908A (en) | 2017-06-13 |
Family
ID=59128745
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710081883.7A Pending CN106821908A (en) | 2017-02-15 | 2017-02-15 | Makeup-removing wet tissue and its compound method with moisture-keeping function |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106821908A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107049834A (en) * | 2017-02-16 | 2017-08-18 | 武汉创新欧派科技有限公司 | A kind of moisturizing paper handkerchief and preparation method thereof |
| CN107569435A (en) * | 2017-09-08 | 2018-01-12 | 武汉芘芘薇莎生物科技有限公司 | A kind of makeup-removing wet tissue and preparation method thereof |
| CN109010105A (en) * | 2018-08-17 | 2018-12-18 | 广州艾蓓生物科技有限公司 | A kind of composition and its preparation method and application of multiple-effect unification |
| CN110184853A (en) * | 2019-05-17 | 2019-08-30 | 华南理工大学 | A kind of oil-Absorbing Sheets and preparation method thereof |
| CN110448510A (en) * | 2019-09-06 | 2019-11-15 | 广州留今科学研究有限公司 | A kind of skin condition type plant extract composition, makeup remover, makeup removing film and preparation method thereof |
| CN112336675A (en) * | 2020-11-18 | 2021-02-09 | 广州莱倩化妆品有限公司 | Skin-nourishing makeup-removing wet tissue without surfactant and preparation method thereof |
| CN117530898A (en) * | 2023-10-28 | 2024-02-09 | 珠海市健朗生活用品有限公司 | Wet tissue for cleansing and preparation method thereof |
| CN117530898B (en) * | 2023-10-28 | 2024-05-10 | 珠海市健朗生活用品有限公司 | Wet tissue for cleansing and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106265155A (en) * | 2016-08-31 | 2017-01-04 | 苏州宝丽洁日化有限公司 | A kind of breast of removing ornaments and formal dress, wet tissue containing this makeup removing breast and preparation method thereof |
-
2017
- 2017-02-15 CN CN201710081883.7A patent/CN106821908A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106265155A (en) * | 2016-08-31 | 2017-01-04 | 苏州宝丽洁日化有限公司 | A kind of breast of removing ornaments and formal dress, wet tissue containing this makeup removing breast and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| ZZ258369: "Bifesta碧菲丝特 抗痘即净卸妆水 2016", 《COSDNA》 * |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107049834A (en) * | 2017-02-16 | 2017-08-18 | 武汉创新欧派科技有限公司 | A kind of moisturizing paper handkerchief and preparation method thereof |
| CN107569435A (en) * | 2017-09-08 | 2018-01-12 | 武汉芘芘薇莎生物科技有限公司 | A kind of makeup-removing wet tissue and preparation method thereof |
| CN109010105A (en) * | 2018-08-17 | 2018-12-18 | 广州艾蓓生物科技有限公司 | A kind of composition and its preparation method and application of multiple-effect unification |
| CN109010105B (en) * | 2018-08-17 | 2021-08-10 | 广州艾蓓生物科技有限公司 | Multi-effect composition and preparation method and application thereof |
| CN110184853A (en) * | 2019-05-17 | 2019-08-30 | 华南理工大学 | A kind of oil-Absorbing Sheets and preparation method thereof |
| CN110184853B (en) * | 2019-05-17 | 2021-10-22 | 华南理工大学 | Oil-absorbing paper and preparation method thereof |
| CN110448510A (en) * | 2019-09-06 | 2019-11-15 | 广州留今科学研究有限公司 | A kind of skin condition type plant extract composition, makeup remover, makeup removing film and preparation method thereof |
| CN110448510B (en) * | 2019-09-06 | 2022-07-19 | 广州一一生物技术有限公司 | Skin conditioning type plant extract composition, makeup remover, makeup removing film and preparation method thereof |
| CN112336675A (en) * | 2020-11-18 | 2021-02-09 | 广州莱倩化妆品有限公司 | Skin-nourishing makeup-removing wet tissue without surfactant and preparation method thereof |
| CN117530898A (en) * | 2023-10-28 | 2024-02-09 | 珠海市健朗生活用品有限公司 | Wet tissue for cleansing and preparation method thereof |
| CN117530898B (en) * | 2023-10-28 | 2024-05-10 | 珠海市健朗生活用品有限公司 | Wet tissue for cleansing and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106821908A (en) | Makeup-removing wet tissue and its compound method with moisture-keeping function | |
| CN107007492B (en) | A kind of makeup remover and preparation method thereof | |
| CN107693433B (en) | Moisturizing essence and preparation method thereof | |
| Kumar et al. | Evaluation of prepared shampoo formulations and to compare formulated shampoo with marketed shampoos | |
| KR100787328B1 (en) | Macro-sized lipid capsule emulsion composition and cosmetic composition containing the same | |
| CN105267085B (en) | Skin makeup mildy wash and preparation method thereof | |
| CN106214515A (en) | A kind of oil-containing moisturizing astringent and preparation method thereof | |
| CN110420152A (en) | A kind of salubrious mild double-deck make up remover and preparation method thereof | |
| CN110339077A (en) | A kind of facial mask and preparation method thereof containing tremella and Herba Dendrobii extract | |
| CN112957302B (en) | Amino acid facial cleanser and preparation method thereof | |
| CN107536773A (en) | The production technology of foaming face cleaning gel afterwards | |
| CN111358730A (en) | Double-layer cleansing lotion and preparation method thereof | |
| CN105832615A (en) | Cleansing and removing two-in-one cleansing oil and preparation method thereof | |
| JP2981975B2 (en) | Cosmetic composition | |
| CN105287277B (en) | A kind of preparation method and skin-beautifying agent of the agent of pure plant antisenescence and skin makeup | |
| CN106606427A (en) | Long-lasting powder essence composition with improved coloring and skin feeling and preparation method thereof | |
| CN110772437A (en) | Wash-free cleaning composition capable of rapidly absorbing oil, preparation method and application thereof in hair wet tissue | |
| CN106726786A (en) | Makeup remover with moisture-keeping function | |
| CN111920711B (en) | Gel composition and preparation method and application thereof | |
| CN103340778A (en) | Lotion composition containing chamomile extracts and ginseng root extracts | |
| CN106511144A (en) | Eye and lip makeup remover and preparation method thereof | |
| JP4871438B2 (en) | Cosmetics | |
| CN107375017B (en) | Cleansing composition and its preparation method and application | |
| CN107260586B (en) | Makeup removing cream gel and preparation method thereof | |
| CN113750002B (en) | Stick-shaped facial mask and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170613 |
|
| WD01 | Invention patent application deemed withdrawn after publication |